#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/01/2100145.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100145_Fobs loop_ _publ_author_name 'Nishi, Koji' 'Hidaka, Akira' 'Yokomori, Yoshinobu' _publ_section_title ; Structure of toluene6.4-ZSM-5 and the toluene disproportionation reaction on ZSM-5 ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 160 _journal_page_last 163 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 20.0990 _cell_length_b 19.8440 _cell_length_c 13.4240 _exptl_crystal_F_000 3280.00 _reflns_d_resolution_high 0.8193 _[local]_cod_data_source_file bs5009sup2.hkl _[local]_cod_data_source_block tol_zsm5 #BEGIN Tags that were not found in dictionaries: _shelx_title ' Tol_ZSM5 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 944.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 125892.69 116935.42 1938.82 o 4 0 0 33959.42 32761.49 437.36 o 6 0 0 86797.74 85330.46 1183.58 o 8 0 0 143617.09 141107.50 1907.25 o 10 0 0 439601.28 412819.09 5052.19 o 12 0 0 127.96 313.37 56.36 o 14 0 0 6685.95 7139.80 245.73 o 16 0 0 160153.11 143449.86 3079.56 o 1 1 0 0.01 2.05 2.24 o 2 1 0 899.16 1569.31 40.58 o 3 1 0 6.13 4.96 10.14 o 4 1 0 10955.47 9420.43 112.17 o 5 1 0 28.53 31.51 6.22 o 6 1 0 7108.25 6830.66 86.08 o 7 1 0 13.52 23.45 5.41 o 8 1 0 61.38 63.20 6.38 o 9 1 0 94.18 76.33 7.89 o 10 1 0 3696.58 4207.66 289.70 o 11 1 0 185.60 182.61 27.05 o 12 1 0 1714.12 1809.45 138.65 o 13 1 0 0.03 2.31 32.65 o 14 1 0 3616.45 4071.51 211.92 o 15 1 0 3.17 85.67 58.62 o 16 1 0 360.37 299.84 128.50 o 17 1 0 7.07 0.37 60.61 o 0 2 0 81713.20 52291.57 497.61 o 1 2 0 33.16 49.60 3.19 o 2 2 0 12678.23 10461.55 100.77 o 3 2 0 38.01 55.44 5.64 o 4 2 0 9001.92 8385.41 81.93 o 5 2 0 849.17 789.14 43.96 o 6 2 0 738.65 682.91 23.20 o 7 2 0 162.17 158.34 20.29 o 8 2 0 29512.91 24147.96 299.85 o 9 2 0 238.09 275.52 22.54 o 10 2 0 18776.12 21518.18 288.87 o 11 2 0 234.45 275.52 58.62 o 12 2 0 574.62 788.33 77.78 o 13 2 0 46.54 40.21 26.96 o 14 2 0 2072.88 2400.98 160.07 o 15 2 0 344.16 295.33 121.74 o 18 2 0 5791.71 6395.84 261.51 o 24 2 0 91.39 151.05 58.62 o 1 3 0 34.67 40.58 4.78 o 2 3 0 3951.88 4681.28 60.87 o 3 3 0 264.64 229.10 7.89 o 4 3 0 37097.20 40912.11 1255.72 o 5 3 0 127.55 152.38 9.56 o 6 3 0 28604.35 27548.08 828.51 o 7 3 0 200.21 192.48 12.46 o 8 3 0 3915.03 3507.74 67.63 o 9 3 0 32.01 40.58 12.75 o 10 3 0 2569.70 2826.21 209.66 o 11 3 0 1066.71 1117.96 39.45 o 12 3 0 61910.22 65234.40 892.76 o 13 3 0 85.93 199.30 32.76 o 14 3 0 22019.94 23910.56 376.49 o 15 3 0 157.91 67.63 105.96 o 21 3 0 23.12 90.18 94.69 o 22 3 0 4976.06 5922.41 356.20 o 24 3 0 434.52 214.17 60.87 o 0 4 0 74589.69 47078.87 487.89 o 1 4 0 18.32 25.55 5.64 o 2 4 0 2450.09 2710.38 38.33 o 3 4 0 41.39 12.24 5.41 o 4 4 0 277.85 303.74 9.17 o 5 4 0 88.67 62.69 10.27 o 6 4 0 30.50 48.27 9.17 o 7 4 0 315.91 395.11 25.93 o 8 4 0 428.32 153.65 15.78 o 9 4 0 7.14 20.29 22.54 o 10 4 0 7563.83 7770.74 184.86 o 11 4 0 276.41 251.36 23.67 o 12 4 0 169.90 97.93 26.00 o 13 4 0 44.46 103.70 37.20 o 14 4 0 5.72 0.00 42.83 o 15 4 0 93.19 137.52 76.65 o 17 4 0 122.91 157.81 58.62 o 19 4 0 2.25 15.78 83.41 o 20 4 0 57.93 99.20 99.20 o 21 4 0 3.78 2.17 61.36 o 22 4 0 21.18 17.79 57.78 o 23 4 0 56.05 51.80 60.89 o 24 4 0 215.33 226.09 42.54 o 1 5 0 85.14 64.58 7.04 o 2 5 0 36537.27 30516.98 378.75 o 3 5 0 121.36 137.52 12.40 o 4 5 0 8004.63 7797.70 126.25 o 5 5 0 49.64 25.30 6.76 o 6 5 0 20401.25 18757.01 175.94 o 7 5 0 406.82 252.02 24.80 o 8 5 0 253.99 136.88 19.16 o 9 5 0 487.21 474.53 21.48 o 10 5 0 485.62 601.09 48.47 o 11 5 0 631.71 704.08 149.92 o 12 5 0 7094.23 7244.56 279.55 o 13 5 0 381.74 403.54 49.60 o 14 5 0 16118.69 16101.19 297.59 o 15 5 0 0.17 -45.09 47.34 o 16 5 0 10539.32 11982.33 261.51 o 17 5 0 359.49 392.27 76.65 o 18 5 0 5682.72 6929.37 223.87 o 19 5 0 169.02 287.66 73.28 o 20 5 0 1860.77 2063.33 123.17 o 21 5 0 0.51 47.46 67.63 o 22 5 0 6.84 51.22 66.51 o 23 5 0 0.45 -35.17 55.52 o 24 5 0 3655.05 3180.96 222.06 o 0 6 0 82980.30 63870.98 638.45 o 1 6 0 1.14 9.02 6.76 o 2 6 0 246.38 205.04 14.65 o 3 6 0 680.15 619.31 16.91 o 4 6 0 579.80 445.60 12.75 o 5 6 0 432.70 439.86 13.53 o 6 6 0 1817.60 1570.94 25.36 o 7 6 0 181.81 215.99 13.48 o 8 6 0 5779.44 4096.42 58.62 o 9 6 0 44.79 40.58 14.35 o 10 6 0 6226.96 7322.94 438.49 o 11 6 0 300.32 359.15 77.78 o 12 6 0 3734.08 4284.19 358.46 o 13 6 0 71.71 56.36 38.33 o 14 6 0 211.30 214.17 63.12 o 15 6 0 372.61 412.56 65.38 o 16 6 0 6511.22 6954.94 189.37 o 17 6 0 60.32 40.58 58.62 o 18 6 0 2143.75 2389.70 126.25 o 19 6 0 0.24 25.23 62.95 o 20 6 0 533.12 885.73 92.42 o 21 6 0 31.33 52.05 68.40 o 22 6 0 19.72 22.96 60.01 o 23 6 0 0.80 89.05 42.54 o 1 7 0 132.58 107.67 9.56 o 2 7 0 2588.54 2422.12 30.81 o 3 7 0 58.25 49.29 8.66 o 4 7 0 29294.20 23665.24 199.34 o 5 7 0 83.58 65.69 7.97 o 6 7 0 114.20 75.79 7.04 o 7 7 0 137.71 96.88 11.88 o 8 7 0 1638.11 1664.14 32.65 o 9 7 0 140.85 129.38 23.67 o 10 7 0 1443.54 1361.70 157.81 o 11 7 0 20.61 63.99 24.72 o 12 7 0 45839.46 45900.35 615.46 o 13 7 0 49.50 72.14 40.58 o 14 7 0 14566.77 15262.54 302.09 o 15 7 0 226.71 216.43 60.87 o 16 7 0 513.45 712.40 74.40 o 17 7 0 259.77 347.18 67.63 o 18 7 0 1825.48 2062.81 112.72 o 19 7 0 11.40 75.59 77.57 o 20 7 0 1473.08 1840.17 126.20 o 21 7 0 0.18 65.38 83.41 o 22 7 0 3357.99 3998.07 178.70 o 23 7 0 4.95 12.89 57.49 o 0 8 0 103437.77 76941.43 856.69 o 1 8 0 72.34 63.91 14.65 o 2 8 0 8447.10 6976.56 66.44 o 3 8 0 1.59 9.02 11.27 o 4 8 0 5201.78 3859.25 85.67 o 5 8 0 13.94 11.77 7.04 o 6 8 0 3219.32 2918.61 82.29 o 7 8 0 859.74 609.09 50.72 o 8 8 0 34355.67 32311.44 453.14 o 9 8 0 94.19 104.48 19.50 o 10 8 0 1306.21 1186.54 71.01 o 11 8 0 33.58 62.48 25.23 o 12 8 0 4429.99 4684.72 146.54 o 13 8 0 151.37 211.92 51.85 o 14 8 0 2.78 -22.54 47.34 o 15 8 0 1672.43 1530.76 94.69 o 16 8 0 1957.46 1657.01 101.45 o 17 8 0 14.52 36.07 67.63 o 18 8 0 2622.38 3208.06 151.05 o 19 8 0 19.02 -6.76 67.63 o 20 8 0 19601.10 22011.06 963.77 o 21 8 0 310.16 352.97 131.88 o 22 8 0 1764.02 1959.36 208.54 o 23 8 0 9.57 92.43 49.60 o 1 9 0 317.77 346.68 14.65 o 2 9 0 120.87 85.16 10.27 o 3 9 0 124.35 89.18 11.16 o 4 9 0 241.64 265.50 11.88 o 5 9 0 25.75 21.42 7.97 o 6 9 0 274.76 329.11 46.22 o 7 9 0 212.91 193.60 17.87 o 8 9 0 299.71 276.37 25.93 o 9 9 0 135.42 300.12 38.33 o 10 9 0 148.45 148.76 25.98 o 11 9 0 11.14 2.25 51.85 o 12 9 0 25.98 60.87 45.09 o 13 9 0 8.45 90.18 67.63 o 14 9 0 170.89 51.85 58.62 o 15 9 0 21.29 139.78 65.38 o 16 9 0 92.30 96.94 74.40 o 17 9 0 74.68 60.87 69.89 o 18 9 0 103.89 211.92 81.16 o 19 9 0 2.65 22.54 58.62 o 20 9 0 168.35 168.10 63.12 o 21 9 0 60.10 47.21 35.09 o 22 9 0 163.49 232.72 49.83 o 0 10 0 610198.50 514548.78 10706.32 o 1 10 0 430.77 573.70 24.80 o 2 10 0 17585.40 17363.24 618.84 o 3 10 0 235.20 221.22 13.48 o 4 10 0 2734.85 2631.95 153.30 o 5 10 0 1975.93 1964.82 71.01 o 6 10 0 7537.80 7025.40 96.94 o 7 10 0 139.38 156.87 17.32 o 8 10 0 3958.46 3728.04 139.78 o 9 10 0 8.72 30.70 20.54 o 10 10 0 40913.02 38687.98 793.56 o 11 10 0 12.33 51.85 51.85 o 12 10 0 91.98 196.14 74.40 o 13 10 0 6.09 -67.63 67.63 o 14 10 0 2131.91 1880.20 155.56 o 15 10 0 325.12 304.35 85.67 o 16 10 0 23718.72 26095.12 640.26 o 17 10 0 26.72 105.96 69.89 o 18 10 0 1909.55 2116.92 126.25 o 19 10 0 9.86 -24.80 58.62 o 20 10 0 3603.11 4316.98 193.56 o 21 10 0 216.33 85.67 38.33 o 22 10 0 28.49 31.46 29.81 o 1 11 0 93.84 87.15 14.35 o 2 11 0 23.12 31.31 14.08 o 3 11 0 1.94 26.79 13.48 o 4 11 0 1441.39 1283.74 26.27 o 5 11 0 30.96 20.29 14.35 o 6 11 0 129.31 100.24 18.28 o 7 11 0 11.34 95.32 41.71 o 8 11 0 1499.06 1334.53 48.72 o 9 11 0 284.62 315.90 37.37 o 10 11 0 731.63 661.07 58.72 o 11 11 0 611.66 976.17 110.47 o 12 11 0 301.46 369.73 87.92 o 13 11 0 604.80 574.88 101.45 o 15 11 0 620.51 766.51 83.41 o 16 11 0 487.88 631.24 92.43 o 17 11 0 75.86 155.56 67.63 o 18 11 0 487.37 595.17 78.91 o 19 11 0 8.02 33.82 56.36 o 20 11 0 550.03 613.66 66.51 o 21 11 0 37.85 26.70 38.33 o 0 12 0 212.55 634.28 40.63 o 1 12 0 6.56 50.10 37.20 o 2 12 0 4574.36 4549.57 190.50 o 3 12 0 789.42 744.93 39.45 o 4 12 0 2659.17 2800.40 82.29 o 5 12 0 386.33 284.51 19.13 o 6 12 0 2813.98 2075.27 42.04 o 7 12 0 0.07 5.76 30.62 o 8 12 0 34068.66 30686.40 563.61 o 9 12 0 47.38 31.36 42.78 o 10 12 0 240.96 276.14 43.20 o 11 12 0 66.25 101.45 56.36 o 12 12 0 4893.83 4878.60 160.07 o 13 12 0 1227.47 1183.58 164.57 o 14 12 0 3158.37 4035.44 241.22 o 15 12 0 288.74 430.60 74.40 o 16 12 0 3500.53 4326.27 169.08 o 17 12 0 68.05 69.89 72.14 o 18 12 0 5001.40 5230.30 200.64 o 19 12 0 6.81 9.02 47.34 o 20 12 0 2269.76 2173.16 119.72 o 21 12 0 0.01 -26.94 38.33 o 1 13 0 196.30 233.58 29.31 o 2 13 0 5419.79 4833.49 373.11 o 3 13 0 882.50 686.37 37.20 o 4 13 0 102169.52 102315.61 1156.53 o 5 13 0 499.21 447.85 30.33 o 6 13 0 18985.52 17450.34 229.26 o 7 13 0 1372.09 1192.23 99.20 o 8 13 0 17661.37 17082.27 473.43 o 9 13 0 1462.00 1563.13 61.11 o 10 13 0 6670.11 6590.10 207.41 o 11 13 0 3753.45 4373.61 153.30 o 12 13 0 157270.81 162556.22 2608.38 o 15 13 0 13.82 0.00 87.92 o 16 13 0 18718.05 19072.54 619.97 o 17 13 0 2555.47 2854.12 191.63 o 18 13 0 207.58 200.64 63.12 o 19 13 0 384.09 417.07 54.11 o 20 13 0 3442.65 3321.87 178.10 o 0 14 0 2466.25 2155.72 64.66 o 1 14 0 18.86 -9.51 18.28 o 2 14 0 18.04 33.58 23.07 o 3 14 0 548.18 608.81 39.76 o 4 14 0 0.93 12.40 60.87 o 5 14 0 3317.10 3192.69 82.29 o 6 14 0 2221.85 2009.29 78.91 o 7 14 0 45.23 84.86 40.45 o 8 14 0 2890.59 3052.27 200.64 o 9 14 0 142.30 93.76 39.45 o 10 14 0 327.10 234.46 69.89 o 11 14 0 344.47 473.43 72.14 o 15 14 0 8.05 200.64 90.18 o 17 14 0 22.24 146.54 51.85 o 18 14 0 32.69 -13.53 42.83 o 19 14 0 9.09 38.33 36.07 o 20 14 0 2743.02 1914.82 335.91 o 1 15 0 100.47 122.59 34.58 o 2 15 0 1000.17 781.97 49.60 o 3 15 0 298.54 347.86 40.63 o 4 15 0 12587.05 14356.17 245.73 o 5 15 0 19.60 47.34 36.69 o 6 15 0 2094.49 2147.20 184.86 o 7 15 0 7.31 16.18 37.89 o 8 15 0 127.58 97.89 59.74 o 9 15 0 374.06 441.75 64.25 o 10 15 0 1108.97 1194.85 128.50 o 11 15 0 26.64 15.78 85.67 o 12 15 0 782.00 798.07 117.23 o 14 15 0 78.81 293.08 99.20 o 16 15 0 1192.97 1400.01 144.28 o 17 15 0 245.22 209.66 78.91 o 18 15 0 932.83 703.38 58.62 o 19 15 0 32.69 36.60 23.75 o 0 16 0 79532.59 86873.61 3868.61 o 1 16 0 1569.78 1677.16 105.96 o 2 16 0 3825.20 3622.77 105.58 o 3 16 0 4962.02 4866.92 98.84 o 4 16 0 2854.75 3400.38 85.91 o 5 16 0 25595.77 27501.57 332.64 o 6 16 0 2755.79 3260.80 87.59 o 7 16 0 1147.24 1073.49 60.87 o 8 16 0 3966.23 3738.35 277.30 o 9 16 0 30.48 123.99 60.87 o 10 16 0 9271.85 9382.97 272.79 o 11 16 0 21.22 -11.27 56.36 o 12 16 0 821.69 874.72 83.41 o 13 16 0 1950.43 1814.82 110.47 o 14 16 0 132.11 119.49 72.14 o 15 16 0 1.42 27.05 85.67 o 17 16 0 105.58 173.59 67.63 o 18 16 0 30.78 65.38 24.80 o 1 17 0 585.39 542.68 55.31 o 2 17 0 1357.66 1576.95 76.65 o 3 17 0 23.37 34.23 46.98 o 4 17 0 3141.63 3475.58 139.78 o 5 17 0 15.79 24.05 40.87 o 6 17 0 1341.33 1513.64 117.23 o 7 17 0 1137.43 1288.80 72.15 o 8 17 0 65.30 18.94 46.56 o 9 17 0 741.98 834.14 90.18 o 10 17 0 255.54 247.99 65.38 o 11 17 0 581.94 768.76 78.91 o 12 17 0 13555.29 13758.83 446.38 o 13 17 0 172.87 130.76 51.85 o 14 17 0 3097.49 3124.65 151.05 o 15 17 0 95.83 112.72 49.60 o 16 17 0 115.22 114.98 69.89 o 0 18 0 34575.12 36904.18 2077.46 o 1 18 0 466.35 484.15 68.76 o 2 18 0 2936.19 3361.99 123.99 o 3 18 0 814.73 723.76 116.10 o 4 18 0 2538.43 2919.80 103.75 o 5 18 0 4647.36 4952.05 182.61 o 6 18 0 1956.49 2133.00 78.84 o 7 18 0 381.67 439.11 52.90 o 8 18 0 4557.14 4869.58 157.81 o 9 18 0 30.51 94.69 78.91 o 10 18 0 1297.93 1235.43 96.94 o 11 18 0 23.97 54.11 60.87 o 12 18 0 116.46 166.83 58.62 o 13 18 0 100.68 38.33 49.60 o 14 18 0 227.51 157.81 49.60 o 15 18 0 503.71 527.54 58.62 o 1 19 0 214.21 269.65 55.31 o 2 19 0 2.98 -21.48 51.03 o 3 19 0 62.79 125.33 75.52 o 4 19 0 608.35 771.19 63.53 o 5 19 0 16.80 28.38 49.74 o 6 19 0 224.71 197.57 46.70 o 7 19 0 1056.16 1235.43 92.43 o 8 19 0 339.53 583.90 83.41 o 9 19 0 510.71 529.79 74.40 o 10 19 0 117.09 123.99 58.62 o 11 19 0 552.09 563.61 67.63 o 12 19 0 4.30 -6.76 47.34 o 13 19 0 517.38 694.37 67.63 o 14 19 0 67.47 133.01 42.83 o 15 19 0 202.23 259.26 40.58 o 0 20 0 28478.79 32224.96 1739.30 o 1 20 0 49.58 32.25 101.45 o 2 20 0 1443.60 1804.13 252.50 o 3 20 0 70.37 98.74 47.01 o 4 20 0 1006.96 1237.52 67.14 o 5 20 0 116.24 144.28 54.11 o 6 20 0 3304.47 4091.80 151.05 o 7 20 0 45.80 63.12 67.63 o 8 20 0 9325.85 9479.91 322.38 o 9 20 0 4.35 -20.29 51.85 o 10 20 0 657.63 757.49 74.40 o 11 20 0 1.07 -36.07 42.83 o 12 20 0 98.05 92.43 42.83 o 13 20 0 103.03 99.20 45.09 o 1 21 0 123.21 64.76 31.93 o 2 21 0 588.10 748.47 112.72 o 3 21 0 550.27 498.23 101.45 o 4 21 0 941.68 904.03 65.38 o 5 21 0 2.40 -11.27 45.09 o 6 21 0 3409.29 3870.87 189.37 o 7 21 0 467.73 435.11 92.43 o 8 21 0 3792.34 3764.91 171.34 o 9 21 0 622.74 647.02 67.63 o 10 21 0 55.82 103.70 49.60 o 11 21 0 1102.39 1345.90 85.67 o 0 22 0 179.88 250.24 139.78 o 1 22 0 0.48 -24.80 81.16 o 2 22 0 230.04 365.22 92.43 o 3 22 0 124.62 85.67 42.83 o 4 22 0 104.56 110.47 45.09 o 5 22 0 2.70 20.29 56.36 o 6 22 0 187.99 144.28 60.87 o 7 22 0 399.25 441.87 60.87 o 8 22 0 498.11 791.31 69.89 o 9 22 0 30.40 60.87 38.33 o 10 22 0 5.84 15.78 33.82 o 3 23 0 288.30 421.58 112.72 o 4 23 0 6424.73 8161.06 378.75 o 5 23 0 18.19 45.09 42.83 o 6 23 0 249.85 225.44 51.85 o 7 23 0 317.05 453.14 47.34 o 2 24 0 178.93 365.22 72.14 o 3 24 0 21.63 4.51 54.11 o 1 0 1 98616.30 87839.01 734.01 o 2 0 1 6.95 41.74 3.19 o 3 0 1 32096.63 32343.59 561.35 o 4 0 1 360.38 263.94 7.97 o 5 0 1 892418.06 724344.69 10002.94 o 6 0 1 7284.14 6632.49 276.17 o 7 0 1 3876.05 3408.89 44.55 o 8 0 1 1541.38 1873.79 31.41 o 9 0 1 1896.15 2247.59 48.47 o 10 0 1 869.34 915.95 29.31 o 11 0 1 5000.14 6509.98 134.14 o 12 0 1 3524.41 3550.87 83.41 o 14 0 1 1510.02 1509.83 110.47 o 16 0 1 21660.63 22707.45 362.02 o 17 0 1 177.60 142.03 137.52 o 18 0 1 2818.59 2078.59 200.64 o -18 1 1 2719.29 2141.72 191.63 o -17 1 1 311.76 191.63 74.40 o -16 1 1 7523.35 8052.85 324.64 o -15 1 1 260.48 520.78 142.03 o -14 1 1 717.16 704.99 103.70 o -13 1 1 354.38 412.85 39.20 o -12 1 1 1752.04 2424.02 87.63 o -11 1 1 1363.45 1562.33 42.83 o -10 1 1 5251.24 5117.26 70.28 o -9 1 1 92.27 72.07 11.27 o -8 1 1 11888.26 9427.91 145.41 o -7 1 1 1959.92 2136.91 55.23 o -6 1 1 495.09 570.72 49.60 o -5 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