#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2100278.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100278_Fobs loop_ _publ_author_name 'Nichol, Gary S.' 'Clegg, William' _publ_section_title ; A variable-temperature study of a phase transition in barbituric acid dihydrate ; _journal_coeditor_code WS5026 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 464 _journal_page_last 472 _journal_volume 61 _journal_year 2005 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2bc 2a' _symmetry_space_group_name_H-M 'P m n b' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1770 _cell_length_b 12.7851 _cell_length_c 8.8984 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.7479 _[local]_cod_data_source_file ws5026217sup10.hkl _[local]_cod_data_source_block 217 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 220 in Pmnb' _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' 'x+1/2, -y, -z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y-1/2, -z-1/2' '-x-1/2, y, z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 978.54 1144.25 66.38 o 1 2 0 2286.40 2143.87 65.01 o 2 2 0 783.16 532.09 34.74 o 3 2 0 482.13 493.53 13.62 o 0 4 0 39.22 41.65 1.68 o 1 4 0 657.76 606.05 21.12 o 2 4 0 4.87 4.25 0.45 o 4 4 0 1.44 1.00 0.69 o 5 4 0 11.72 11.66 2.10 o 6 4 0 2.96 3.01 1.50 o 7 4 0 1.34 0.41 1.58 o 8 4 0 1.06 2.73 1.42 o 0 6 0 40.51 59.11 2.31 o 1 6 0 255.86 230.55 6.16 o 2 6 0 26.96 32.95 1.18 o 3 6 0 68.97 67.37 2.06 o 4 6 0 10.61 12.88 1.11 o 5 6 0 26.86 28.90 1.68 o 6 6 0 3.54 4.80 1.58 o 0 8 0 593.28 663.86 22.31 o 1 8 0 413.49 473.05 12.47 o 2 8 0 295.65 291.19 10.99 o 3 8 0 104.59 101.50 3.30 o 4 8 0 50.56 52.99 2.05 o 5 8 0 3.04 2.66 0.83 o 6 8 0 5.18 4.81 2.06 o 7 8 0 0.39 -1.27 1.58 o 0 10 0 536.28 604.02 24.33 o 1 10 0 162.15 160.60 5.72 o 2 10 0 354.55 360.58 12.24 o 3 10 0 49.81 45.06 1.91 o 4 10 0 140.40 140.06 4.51 o 5 10 0 4.02 7.52 1.87 o 6 10 0 44.43 41.87 3.93 o 0 12 0 132.08 137.00 6.42 o 1 12 0 157.92 169.42 9.82 o 2 12 0 67.33 67.12 3.38 o 3 12 0 96.18 85.93 3.52 o 4 12 0 10.22 14.36 1.89 o 5 12 0 36.03 32.75 2.18 o 0 14 0 47.82 55.84 4.51 o 1 14 0 4.11 5.48 1.99 o 2 14 0 34.40 37.36 2.07 o 3 14 0 0.20 1.05 1.37 o 4 14 0 16.37 16.90 1.49 o 0 16 0 337.21 353.40 20.48 o 1 16 0 9.56 16.32 1.64 o 2 16 0 265.29 274.97 16.09 o 1 0 1 3295.06 2850.25 123.74 o 0 1 1 20.49 19.27 0.57 o 1 1 1 226.36 200.60 5.16 o 2 1 1 19.46 28.39 2.11 o 4 1 1 7.84 14.25 1.52 o 5 1 1 3.56 2.89 0.70 o 6 1 1 1.51 0.27 1.05 o 0 2 1 1320.64 1423.12 55.01 o 1 2 1 269.25 235.46 4.77 o 2 2 1 567.48 494.83 19.25 o 7 2 1 3.21 6.10 2.14 o 0 3 1 5.29 6.32 0.52 o 1 3 1 2068.19 2149.99 46.32 o 2 3 1 0.52 4.99 0.36 o 4 3 1 1.27 0.66 0.42 o 6 3 1 0.00 0.18 0.95 o 8 3 1 0.05 0.27 1.52 o 0 4 1 487.18 567.08 16.85 o 1 4 1 3502.21 3667.64 65.85 o 2 4 1 230.41 214.45 4.68 o 3 4 1 779.83 678.79 13.29 o 4 4 1 16.60 12.44 1.08 o 6 4 1 0.08 0.74 0.67 o 7 4 1 11.92 18.26 1.68 o 8 4 1 0.23 1.39 1.83 o 0 5 1 392.04 502.98 15.48 o 1 5 1 1866.43 2119.04 42.16 o 2 5 1 132.80 137.32 2.91 o 3 5 1 498.93 479.67 9.69 o 4 5 1 8.72 9.39 0.65 o 5 5 1 68.88 67.18 2.19 o 6 5 1 0.18 0.51 0.67 o 0 6 1 423.73 490.63 13.17 o 1 6 1 103.26 123.01 2.39 o 2 6 1 212.73 203.01 4.00 o 3 6 1 66.21 66.55 1.51 o 4 6 1 14.27 12.94 0.71 o 5 6 1 25.38 26.28 0.98 o 6 6 1 1.29 1.29 0.90 o 7 6 1 6.21 11.22 1.79 o 0 7 1 642.71 765.30 20.21 o 1 7 1 462.19 531.99 10.50 o 2 7 1 300.76 299.22 7.67 o 3 7 1 164.63 149.80 3.37 o 4 7 1 61.77 60.01 1.57 o 5 7 1 29.47 27.38 1.16 o 6 7 1 14.39 15.56 0.84 o 7 7 1 3.56 6.11 2.50 o 0 8 1 355.10 372.40 11.74 o 1 8 1 22.65 20.52 0.65 o 2 8 1 179.45 162.42 3.68 o 3 8 1 8.13 10.61 0.78 o 4 8 1 39.28 37.20 1.18 o 5 8 1 2.11 3.63 0.80 o 6 8 1 7.22 11.44 1.09 o 7 8 1 0.40 17.88 2.43 o 0 9 1 23.99 29.95 1.31 o 1 9 1 38.10 39.83 0.97 o 2 9 1 35.43 37.64 1.13 o 3 9 1 31.28 28.70 1.02 o 4 9 1 32.40 30.87 1.04 o 5 9 1 19.96 21.55 0.98 o 6 9 1 13.17 19.54 1.14 o 0 10 1 194.02 221.59 8.09 o 1 10 1 487.85 556.80 14.36 o 2 10 1 97.95 95.06 2.27 o 3 10 1 230.80 232.00 4.93 o 4 10 1 16.24 20.83 0.96 o 5 10 1 74.93 76.81 2.17 o 6 10 1 1.27 10.27 1.69 o 0 11 1 0.48 0.08 0.77 o 1 11 1 907.47 994.30 25.09 o 2 11 1 2.54 2.66 0.73 o 3 11 1 431.14 426.99 9.31 o 4 11 1 4.90 8.94 1.06 o 5 11 1 115.13 120.32 3.45 o 6 11 1 2.63 15.74 1.33 o 0 12 1 229.60 244.67 8.62 o 1 12 1 7.62 12.65 0.85 o 2 12 1 169.01 171.93 4.39 o 3 12 1 0.02 2.25 0.81 o 4 12 1 69.38 66.51 1.78 o 5 12 1 1.18 4.29 1.06 o 0 13 1 18.96 21.28 1.69 o 1 13 1 56.35 59.73 2.07 o 2 13 1 16.49 17.27 0.87 o 3 13 1 26.66 34.10 1.21 o 4 13 1 10.67 14.45 1.33 o 5 13 1 7.67 20.02 3.79 o 0 14 1 34.32 36.20 2.43 o 1 14 1 384.36 379.92 11.15 o 2 14 1 24.26 28.48 1.29 o 3 14 1 163.93 152.49 3.96 o 4 14 1 9.07 15.01 1.61 o 0 15 1 5.77 9.57 1.59 o 1 15 1 92.84 95.13 3.25 o 2 15 1 3.44 6.65 0.94 o 3 15 1 40.68 46.32 1.76 o 0 16 1 26.84 27.93 4.18 o 1 16 1 53.68 60.63 2.40 o 2 16 1 22.67 24.48 2.87 o 0 0 2 982.36 877.41 29.35 o 2 0 2 369.18 342.89 11.01 o 6 0 2 5.25 8.89 3.07 o 0 1 2 152.30 157.65 4.25 o 1 1 2 159.74 170.72 3.60 o 2 1 2 136.58 133.72 2.50 o 3 1 2 62.47 52.26 2.50 o 4 1 2 25.18 13.78 2.70 o 5 1 2 9.75 10.76 0.95 o 6 1 2 0.28 -0.50 1.01 o 0 2 2 1483.42 1656.58 39.17 o 1 2 2 128.36 117.95 2.35 o 2 2 2 656.96 638.66 16.20 o 3 2 2 41.58 30.53 0.86 o 4 2 2 89.27 75.65 9.64 o 5 2 2 6.09 5.41 0.76 o 6 2 2 7.21 8.57 1.80 o 7 2 2 0.56 5.04 2.66 o 0 3 2 316.28 334.15 10.54 o 1 3 2 889.48 902.07 17.67 o 2 3 2 202.74 206.62 4.16 o 4 3 2 38.60 35.31 1.83 o 5 3 2 12.70 14.87 1.70 o 6 3 2 2.64 2.51 1.11 o 7 3 2 1.89 5.58 2.47 o 8 3 2 0.21 0.62 1.52 o 0 4 2 27.04 34.28 1.49 o 1 4 2 2163.48 2196.42 41.17 o 2 4 2 4.42 7.00 0.39 o 3 4 2 533.32 510.70 10.41 o 4 4 2 3.52 2.89 0.46 o 5 4 2 67.39 59.55 4.01 o 6 4 2 5.89 5.96 1.45 o 7 4 2 7.83 8.87 1.58 o 0 5 2 9.74 8.54 0.53 o 1 5 2 674.66 740.38 13.89 o 2 5 2 6.42 9.29 0.45 o 3 5 2 90.47 84.22 1.73 o 4 5 2 0.27 0.99 0.41 o 5 5 2 2.45 2.36 0.63 o 6 5 2 0.24 1.23 1.08 o 7 5 2 0.04 -0.43 1.33 o 0 6 2 1748.04 2120.76 81.39 o 1 6 2 987.02 1103.70 22.33 o 2 6 2 948.34 984.05 18.94 o 3 6 2 322.16 316.68 6.13 o 4 6 2 213.22 197.88 4.45 o 5 6 2 57.73 53.25 1.91 o 6 6 2 34.33 34.89 1.68 o 7 6 2 8.28 10.36 3.38 o 0 7 2 56.89 68.51 2.24 o 1 7 2 284.20 307.80 6.29 o 2 7 2 33.79 36.62 0.96 o 3 7 2 71.47 72.74 1.73 o 4 7 2 8.90 12.05 0.73 o 5 7 2 19.96 21.43 1.32 o 6 7 2 1.57 2.76 0.94 o 7 7 2 6.91 4.43 1.70 o 0 8 2 503.81 533.55 14.07 o 1 8 2 69.00 80.68 1.93 o 2 8 2 289.01 274.72 5.34 o 3 8 2 17.98 17.46 0.74 o 4 8 2 62.69 61.67 1.96 o 5 8 2 1.63 1.26 0.66 o 6 8 2 6.47 10.49 1.13 o 7 8 2 0.07 4.98 2.12 o 0 9 2 121.51 115.65 3.41 o 1 9 2 20.46 24.62 0.78 o 2 9 2 94.95 81.39 2.01 o 3 9 2 38.37 38.84 1.24 o 4 9 2 55.59 49.86 1.54 o 5 9 2 25.81 26.02 1.15 o 6 9 2 24.07 24.63 1.56 o 0 10 2 942.10 1034.83 34.38 o 1 10 2 359.99 353.52 7.32 o 2 10 2 610.64 604.14 12.29 o 3 10 2 130.55 123.95 2.82 o 4 10 2 190.17 178.17 4.71 o 5 10 2 22.65 26.85 1.09 o 6 10 2 35.82 40.01 2.89 o 0 11 2 910.03 933.62 26.70 o 1 11 2 148.44 135.79 2.91 o 2 11 2 635.20 613.43 13.89 o 3 11 2 84.78 76.75 2.05 o 4 11 2 233.62 219.13 5.45 o 5 11 2 26.69 29.57 1.43 o 0 12 2 218.58 225.97 8.01 o 1 12 2 4.22 4.96 0.76 o 2 12 2 137.84 145.73 3.47 o 3 12 2 1.30 3.04 0.70 o 4 12 2 39.47 41.17 2.66 o 5 12 2 0.06 1.82 0.96 o 0 13 2 56.96 55.91 2.61 o 1 13 2 75.06 65.94 2.01 o 2 13 2 33.11 33.88 1.23 o 3 13 2 43.37 38.29 1.44 o 4 13 2 5.48 10.91 1.49 o 5 13 2 16.35 24.59 2.96 o 0 14 2 15.35 18.94 1.39 o 1 14 2 6.31 9.75 1.25 o 2 14 2 6.34 12.54 0.95 o 3 14 2 1.22 1.08 0.81 o 4 14 2 0.09 4.99 1.79 o 0 15 2 76.28 80.64 3.96 o 1 15 2 4.32 9.72 1.52 o 2 15 2 52.39 59.06 2.59 o 3 15 2 2.26 3.48 1.21 o 0 16 2 1.28 1.66 2.58 o 1 16 2 23.37 29.49 2.26 o 2 16 2 1.21 4.43 2.20 o 1 0 3 8266.79 8589.82 222.92 o 3 0 3 1806.99 1815.41 63.40 o 0 1 3 74.88 78.11 1.94 o 1 1 3 925.60 971.67 18.64 o 2 1 3 35.71 33.60 0.90 o 3 1 3 243.80 241.70 6.83 o 4 1 3 8.57 7.66 0.64 o 5 1 3 15.19 16.62 1.21 o 6 1 3 1.97 1.06 1.15 o 7 1 3 0.06 0.44 2.19 o 0 2 3 0.49 0.13 0.26 o 1 2 3 325.16 355.70 7.00 o 2 2 3 0.11 0.41 0.27 o 3 2 3 23.50 24.80 1.05 o 4 2 3 4.17 4.27 0.66 o 5 2 3 0.14 0.22 0.65 o 6 2 3 7.51 6.91 0.80 o 7 2 3 0.82 2.50 2.40 o 0 3 3 24.89 29.58 0.89 o 1 3 3 213.92 227.46 4.20 o 2 3 3 6.75 8.72 0.42 o 3 3 3 41.56 39.02 1.07 o 4 3 3 1.76 2.25 0.55 o 5 3 3 3.90 5.20 0.80 o 6 3 3 1.61 -0.01 0.61 o 7 3 3 0.17 2.25 2.89 o 0 4 3 175.59 186.94 4.56 o 1 4 3 1205.02 1292.16 24.26 o 2 4 3 53.51 46.20 1.14 o 3 4 3 435.05 408.04 8.34 o 4 4 3 0.56 1.76 0.53 o 5 4 3 74.82 69.00 2.66 o 6 4 3 1.17 1.50 0.83 o 7 4 3 9.32 16.16 1.89 o 0 5 3 36.05 39.32 1.48 o 1 5 3 812.21 823.97 14.93 o 2 5 3 36.64 44.47 1.09 o 3 5 3 288.05 268.07 5.01 o 4 5 3 16.17 19.25 0.79 o 5 5 3 48.43 43.85 1.89 o 6 5 3 3.09 3.06 1.51 o 7 5 3 5.50 10.95 3.03 o 0 6 3 209.83 261.86 6.87 o 1 6 3 222.50 277.57 5.43 o 2 6 3 136.08 152.60 2.93 o 3 6 3 100.73 101.16 2.04 o 4 6 3 30.29 29.51 1.06 o 5 6 3 30.54 29.45 1.46 o 6 6 3 2.33 4.19 1.12 o 7 6 3 6.80 9.44 1.24 o 0 7 3 49.75 44.49 1.31 o 1 7 3 462.69 491.55 9.94 o 2 7 3 17.00 19.74 0.67 o 3 7 3 140.93 145.56 3.17 o 4 7 3 1.98 7.44 0.69 o 5 7 3 18.64 21.20 1.52 o 6 7 3 0.76 2.34 1.11 o 7 7 3 1.49 1.74 1.31 o 0 8 3 178.94 178.63 5.84 o 1 8 3 36.28 31.54 0.88 o 2 8 3 96.52 93.41 1.91 o 3 8 3 9.54 11.26 0.83 o 4 8 3 12.65 12.76 0.80 o 5 8 3 1.36 6.26 1.06 o 6 8 3 0.09 0.47 0.83 o 0 9 3 52.49 52.40 1.91 o 1 9 3 6.74 6.25 0.53 o 2 9 3 14.47 14.26 0.72 o 3 9 3 8.75 7.40 0.69 o 4 9 3 0.14 -0.13 0.78 o 5 9 3 8.08 11.45 1.20 o 6 9 3 1.74 2.30 1.14 o 0 10 3 67.78 62.22 2.22 o 1 10 3 59.18 45.59 1.14 o 2 10 3 34.60 31.56 1.02 o 3 10 3 15.13 16.19 0.91 o 4 10 3 3.44 3.97 0.83 o 5 10 3 1.61 3.23 0.90 o 6 10 3 0.01 4.90 2.65 o 0 11 3 24.50 13.81 0.92 o 1 11 3 20.09 16.16 0.81 o 2 11 3 24.73 18.05 0.76 o 3 11 3 17.73 15.19 0.91 o 4 11 3 16.79 15.66 0.99 o 5 11 3 9.25 12.76 1.18 o 0 12 3 78.68 63.69 2.28 o 1 12 3 93.73 83.44 2.20 o 2 12 3 55.79 48.58 1.51 o 3 12 3 35.94 32.65 1.31 o 4 12 3 20.56 20.73 1.02 o 5 12 3 7.39 20.38 2.88 o 0 13 3 8.92 7.39 1.07 o 1 13 3 103.82 94.35 2.47 o 2 13 3 6.41 5.44 0.74 o 3 13 3 49.65 45.55 1.73 o 4 13 3 2.62 6.02 0.98 o 0 14 3 158.75 158.45 5.90 o 1 14 3 18.69 19.41 1.14 o 2 14 3 102.90 101.91 3.14 o 3 14 3 10.92 11.91 1.31 o 4 14 3 30.28 35.86 3.38 o 0 15 3 46.09 47.52 2.89 o 1 15 3 2.05 6.19 1.40 o 2 15 3 29.98 30.18 1.75 o 3 15 3 3.73 6.12 1.58 o 0 16 3 6.81 8.09 1.76 o 1 16 3 2.72 2.98 1.72 o 0 0 4 38.53 46.34 1.77 o 2 0 4 31.24 28.24 1.13 o 4 0 4 0.03 2.18 0.71 o 6 0 4 12.59 12.56 2.31 o 0 1 4 543.15 544.10 13.78 o 1 1 4 1741.27 1828.03 36.89 o 2 1 4 257.75 247.32 4.69 o 3 1 4 528.96 493.08 9.16 o 4 1 4 37.64 41.84 1.27 o 5 1 4 80.13 76.51 2.11 o 6 1 4 3.28 6.01 1.09 o 0 2 4 1031.76 1129.19 26.54 o 1 2 4 316.56 362.87 6.77 o 2 2 4 411.96 393.07 9.24 o 3 2 4 138.32 146.86 3.16 o 4 2 4 44.09 44.71 1.29 o 5 2 4 53.38 56.24 1.82 o 6 2 4 2.41 4.75 1.31 o 0 3 4 1.65 1.32 0.45 o 1 3 4 38.76 40.58 0.92 o 2 3 4 0.33 1.78 0.28 o 3 3 4 13.37 19.05 0.87 o 4 3 4 0.10 1.16 0.52 o 5 3 4 1.79 2.08 0.59 o 6 3 4 0.17 2.15 1.61 o 7 3 4 0.05 4.19 3.49 o 0 4 4 301.36 272.49 7.30 o 1 4 4 509.54 546.51 9.17 o 2 4 4 111.58 89.72 1.92 o 3 4 4 170.11 158.93 3.49 o 4 4 4 9.21 9.66 0.78 o 5 4 4 21.74 18.24 0.96 o 6 4 4 0.49 0.69 0.86 o 7 4 4 2.11 6.29 2.35 o 0 5 4 562.99 622.95 14.76 o 1 5 4 2.28 2.63 0.32 o 2 5 4 328.52 325.45 6.71 o 3 5 4 0.53 1.21 0.48 o 4 5 4 87.85 77.90 1.92 o 5 5 4 0.05 -0.07 0.64 o 6 5 4 17.01 16.87 1.18 o 7 5 4 0.02 2.45 1.92 o 0 6 4 2.58 6.98 0.58 o 1 6 4 286.28 310.41 5.76 o 2 6 4 0.48 1.23 0.37 o 3 6 4 68.60 67.75 1.63 o 4 6 4 0.00 0.81 0.63 o 5 6 4 0.58 2.02 0.76 o 6 6 4 0.01 1.37 1.12 o 7 6 4 1.46 3.25 1.53 o 0 7 4 0.06 0.00 0.43 o 1 7 4 50.55 44.76 1.05 o 2 7 4 0.83 2.71 0.48 o 3 7 4 28.03 26.04 0.85 o 4 7 4 2.00 1.79 0.69 o 5 7 4 11.86 14.84 1.15 o 6 7 4 1.03 6.98 1.04 o 0 8 4 27.10 19.69 0.98 o 1 8 4 31.38 23.44 0.76 o 2 8 4 18.73 15.27 0.67 o 3 8 4 8.62 8.42 0.67 o 4 8 4 8.89 8.98 0.74 o 5 8 4 2.33 3.85 0.99 o 6 8 4 3.49 8.12 1.07 o 0 9 4 4.97 8.30 0.94 o 1 9 4 190.54 179.19 3.45 o 2 9 4 4.73 6.99 0.61 o 3 9 4 51.85 52.66 1.42 o 4 9 4 3.11 4.04 0.96 o 5 9 4 3.53 5.39 1.36 o 6 9 4 1.09 4.94 1.58 o 0 10 4 306.17 269.78 8.55 o 1 10 4 32.01 26.87 0.93 o 2 10 4 184.98 161.10 4.10 o 3 10 4 8.35 9.61 0.65 o 4 10 4 52.47 52.06 1.85 o 5 10 4 1.03 4.23 0.89 o 0 11 4 54.96 56.55 2.13 o 1 11 4 14.42 12.68 0.66 o 2 11 4 39.06 40.61 1.21 o 3 11 4 7.36 9.37 0.84 o 4 11 4 15.31 17.85 1.75 o 5 11 4 2.69 5.85 1.36 o 0 12 4 13.39 10.46 0.92 o 1 12 4 113.02 98.39 2.48 o 2 12 4 4.65 4.74 0.65 o 3 12 4 62.81 54.78 2.17 o 4 12 4 0.07 1.46 0.78 o 0 13 4 77.72 64.87 2.82 o 1 13 4 6.56 10.05 0.62 o 2 13 4 54.54 42.62 1.83 o 3 13 4 5.17 8.44 1.53 o 4 13 4 20.29 19.55 2.64 o 0 14 4 99.65 92.85 3.81 o 1 14 4 0.54 2.86 0.68 o 2 14 4 56.33 50.71 1.88 o 3 14 4 0.45 1.26 1.85 o 0 15 4 108.60 123.82 5.47 o 1 15 4 1.03 3.15 0.80 o 2 15 4 84.25 90.41 5.97 o 1 0 5 1248.64 1296.95 33.82 o 3 0 5 355.85 351.27 9.39 o 5 0 5 68.68 64.33 3.59 o 7 0 5 12.93 17.22 1.56 o 0 1 5 288.06 353.54 8.45 o 1 1 5 5.22 6.47 0.42 o 2 1 5 190.40 199.60 4.08 o 3 1 5 5.89 6.46 0.50 o 4 1 5 60.64 56.10 1.38 o 5 1 5 0.61 0.82 0.81 o 6 1 5 11.80 11.76 0.86 o 7 1 5 0.00 6.92 1.35 o 0 2 5 204.99 205.77 4.98 o 1 2 5 405.19 418.47 8.36 o 2 2 5 114.17 117.20 2.46 o 3 2 5 109.26 95.31 2.16 o 4 2 5 33.79 37.27 1.17 o 5 2 5 18.55 15.63 0.78 o 6 2 5 8.87 10.31 0.94 o 7 2 5 2.68 5.70 2.21 o 0 3 5 1118.30 1115.23 26.23 o 1 3 5 13.61 19.65 0.55 o 2 3 5 550.77 530.11 10.36 o 3 3 5 2.78 10.95 0.62 o 4 3 5 97.01 93.23 2.32 o 5 3 5 0.59 5.56 0.63 o 6 3 5 11.95 12.60 1.33 o 7 3 5 0.06 0.01 0.94 o 0 4 5 41.94 46.43 1.36 o 1 4 5 1.25 3.36 0.39 o 2 4 5 26.00 31.90 1.02 o 3 4 5 0.01 0.04 0.52 o 4 4 5 3.08 8.13 0.70 o 5 4 5 1.43 1.99 0.68 o 6 4 5 0.06 2.50 0.89 o 0 5 5 166.39 173.84 4.31 o 1 5 5 174.65 165.47 3.11 o 2 5 5 51.25 53.48 1.41 o 3 5 5 39.45 38.03 1.20 o 4 5 5 0.08 1.52 0.58 o 5 5 5 0.71 1.38 0.75 o 6 5 5 2.26 2.64 1.00 o 7 5 5 0.47 -0.24 1.19 o 0 6 5 1737.78 1677.94 39.45 o 1 6 5 75.64 77.79 1.64 o 2 6 5 1068.59 975.86 18.77 o 3 6 5 35.83 37.35 1.20 o 4 6 5 325.22 306.13 6.72 o 5 6 5 10.29 12.84 1.45 o 6 6 5 69.47 69.10 3.19 o 0 7 5 711.00 690.22 17.64 o 1 7 5 2.05 6.54 0.56 o 2 7 5 449.28 412.32 8.08 o 3 7 5 1.58 2.76 0.65 o 4 7 5 157.03 146.40 4.07 o 5 7 5 0.66 2.40 0.88 o 6 7 5 43.75 45.87 3.85 o 0 8 5 215.14 218.34 6.55 o 1 8 5 72.77 63.49 1.61 o 2 8 5 133.67 126.09 2.82 o 3 8 5 42.32 37.88 1.18 o 4 8 5 32.04 28.10 1.16 o 5 8 5 17.87 16.29 1.07 o 6 8 5 3.38 3.57 1.28 o 0 9 5 143.43 116.01 3.69 o 1 9 5 69.16 61.43 1.55 o 2 9 5 116.46 93.00 2.19 o 3 9 5 44.48 38.23 1.45 o 4 9 5 56.72 50.67 1.60 o 5 9 5 20.29 21.49 1.68 o 0 10 5 286.34 259.13 7.74 o 1 10 5 148.23 118.53 2.88 o 2 10 5 185.98 163.65 3.66 o 3 10 5 68.82 55.34 1.67 o 4 10 5 53.64 52.20 1.83 o 5 10 5 19.50 17.87 1.10 o 0 11 5 0.44 0.99 0.63 o 1 11 5 154.79 125.41 3.08 o 2 11 5 0.67 0.16 0.66 o 3 11 5 78.77 64.66 2.04 o 4 11 5 1.22 3.73 1.08 o 5 11 5 24.27 20.87 3.24 o 0 12 5 17.78 16.92 1.03 o 1 12 5 29.07 22.22 0.99 o 2 12 5 7.90 9.11 0.86 o 3 12 5 10.50 11.36 1.19 o 4 12 5 0.24 2.50 1.01 o 0 13 5 21.06 20.16 1.28 o 1 13 5 65.27 65.35 2.61 o 2 13 5 15.99 13.50 0.85 o 3 13 5 16.92 21.51 1.79 o 0 14 5 5.08 4.40 1.30 o 1 14 5 24.15 24.12 1.38 o 2 14 5 3.69 5.34 0.76 o 0 15 5 0.09 0.53 2.01 o 1 15 5 14.21 19.58 1.47 o 0 0 6 122.14 119.30 4.26 o 2 0 6 57.71 60.21 2.29 o 4 0 6 6.60 10.18 0.84 o 6 0 6 0.18 -0.33 2.08 o 0 1 6 338.23 321.68 7.73 o 1 1 6 106.20 95.98 1.97 o 2 1 6 183.53 166.92 3.41 o 3 1 6 26.25 25.94 0.84 o 4 1 6 23.26 19.72 0.86 o 5 1 6 1.72 3.02 0.83 o 6 1 6 0.08 1.35 1.10 o 7 1 6 0.00 3.78 2.30 o 0 2 6 18.43 17.44 0.74 o 1 2 6 110.32 106.52 2.31 o 2 2 6 23.89 23.54 0.74 o 3 2 6 33.52 33.91 0.96 o 4 2 6 24.51 22.66 0.90 o 5 2 6 3.68 4.65 0.72 o 6 2 6 12.28 12.98 2.03 o 7 2 6 0.10 0.44 2.10 o 0 3 6 40.39 42.39 1.36 o 1 3 6 28.72 37.52 0.94 o 2 3 6 29.89 31.26 0.90 o 3 3 6 20.44 22.92 0.93 o 4 3 6 8.81 10.31 0.66 o 5 3 6 14.97 14.07 0.70 o 6 3 6 1.24 7.13 1.06 o 0 4 6 386.99 386.95 9.27 o 1 4 6 102.73 100.22 2.32 o 2 4 6 250.00 231.25 5.26 o 3 4 6 69.58 69.11 1.76 o 4 4 6 79.42 71.59 1.83 o 5 4 6 33.13 34.39 1.21 o 6 4 6 16.41 17.84 1.92 o 0 5 6 23.91 21.71 0.91 o 1 5 6 361.28 373.54 7.42 o 2 5 6 9.45 9.45 0.67 o 3 5 6 209.75 196.13 4.34 o 4 5 6 0.82 0.73 0.72 o 5 5 6 67.13 65.13 1.72 o 6 5 6 0.04 0.93 0.78 o 0 6 6 60.82 67.57 2.07 o 1 6 6 283.58 278.33 5.57 o 2 6 6 48.32 48.57 1.39 o 3 6 6 149.35 137.82 3.17 o 4 6 6 25.48 26.77 0.98 o 5 6 6 49.72 49.73 1.59 o 6 6 6 9.15 12.00 0.87 o 0 7 6 89.48 92.85 3.57 o 1 7 6 1234.42 1130.74 24.03 o 2 7 6 53.99 54.31 1.56 o 3 7 6 517.35 455.07 10.13 o 4 7 6 14.81 16.44 0.88 o 5 7 6 132.87 122.74 3.37 o 6 7 6 2.91 5.09 1.00 o 0 8 6 480.94 467.33 15.98 o 1 8 6 20.09 15.43 0.75 o 2 8 6 338.37 309.74 7.00 o 3 8 6 5.40 7.48 0.64 o 4 8 6 128.77 123.15 3.31 o 5 8 6 0.27 1.00 0.87 o 0 9 6 1.12 0.48 0.85 o 1 9 6 92.87 83.33 2.16 o 2 9 6 3.42 0.91 0.47 o 3 9 6 79.67 66.55 1.92 o 4 9 6 8.29 9.40 0.85 o 5 9 6 37.45 40.36 2.24 o 0 10 6 36.47 34.59 1.82 o 1 10 6 7.56 10.26 0.67 o 2 10 6 18.18 20.67 1.02 o 3 10 6 1.15 3.22 0.78 o 4 10 6 1.74 3.73 0.79 o 5 10 6 0.04 0.32 1.28 o 0 11 6 48.55 39.63 2.05 o 1 11 6 290.33 260.88 6.17 o 2 11 6 38.23 31.18 1.33 o 3 11 6 121.77 107.96 3.60 o 4 11 6 17.98 18.76 1.13 o 0 12 6 2.88 6.58 1.00 o 1 12 6 26.88 29.12 1.12 o 2 12 6 3.06 5.80 1.11 o 3 12 6 17.67 18.69 1.03 o 4 12 6 2.49 23.87 3.57 o 0 13 6 5.27 7.11 1.56 o 1 13 6 51.01 45.03 1.69 o 2 13 6 4.08 5.51 1.44 o 0 14 6 0.19 2.75 1.99 o 1 14 6 48.33 44.73 1.69 o 1 0 7 15.38 19.10 0.90 o 3 0 7 2.54 5.82 0.77 o 5 0 7 0.78 2.84 1.57 o 0 1 7 14.09 14.30 0.94 o 1 1 7 256.51 242.23 4.69 o 2 1 7 4.52 5.13 0.57 o 3 1 7 88.19 84.08 1.92 o 4 1 7 0.00 0.55 0.81 o 5 1 7 18.42 20.09 0.97 o 6 1 7 0.51 2.36 1.21 o 0 2 7 332.53 346.41 10.63 o 1 2 7 60.63 62.68 1.52 o 2 2 7 203.70 197.28 4.24 o 3 2 7 65.14 60.29 1.67 o 4 2 7 57.49 58.18 1.66 o 5 2 7 36.55 33.47 1.19 o 6 2 7 10.32 14.79 1.02 o 0 3 7 576.38 576.59 19.55 o 1 3 7 93.11 93.10 2.08 o 2 3 7 367.42 345.98 6.90 o 3 3 7 44.28 41.32 1.28 o 4 3 7 123.79 115.26 2.84 o 5 3 7 9.93 12.48 0.86 o 6 3 7 31.75 34.31 1.54 o 0 4 7 1737.64 1764.03 52.72 o 1 4 7 79.96 74.57 1.74 o 2 4 7 1156.84 1047.84 21.62 o 3 4 7 19.37 18.82 0.83 o 4 4 7 379.59 333.67 7.15 o 5 4 7 1.43 4.97 0.64 o 6 4 7 77.36 63.99 5.76 o 0 5 7 37.64 38.45 1.62 o 1 5 7 118.19 113.47 2.84 o 2 5 7 44.82 44.61 1.32 o 3 5 7 54.12 46.36 1.32 o 4 5 7 37.65 38.67 1.24 o 5 5 7 13.82 15.24 1.17 o 6 5 7 15.74 20.92 2.67 o 0 6 7 62.41 67.90 2.41 o 1 6 7 6.47 10.45 0.97 o 2 6 7 42.73 42.26 1.25 o 3 6 7 5.44 8.66 0.78 o 4 6 7 13.29 13.71 0.75 o 5 6 7 3.69 8.37 0.92 o 6 6 7 2.22 4.80 2.61 o 0 7 7 155.02 175.23 7.90 o 1 7 7 0.01 0.36 0.63 o 2 7 7 103.18 101.95 2.46 o 3 7 7 0.98 1.13 0.63 o 4 7 7 38.03 38.34 1.36 o 5 7 7 2.01 5.57 0.80 o 0 8 7 68.48 66.79 2.91 o 1 8 7 4.42 6.16 0.77 o 2 8 7 44.97 42.21 1.29 o 3 8 7 7.55 7.32 0.70 o 4 8 7 12.21 12.99 0.94 o 5 8 7 6.20 5.26 1.76 o 0 9 7 278.86 266.75 9.44 o 1 9 7 5.59 8.53 1.16 o 2 9 7 190.11 169.81 4.05 o 3 9 7 3.71 5.47 0.75 o 4 9 7 62.93 65.15 1.94 o 5 9 7 2.03 4.13 2.56 o 0 10 7 2.11 4.62 0.92 o 1 10 7 3.89 8.05 1.19 o 2 10 7 1.46 3.95 0.84 o 3 10 7 4.16 8.50 1.35 o 4 10 7 0.35 0.27 0.99 o 0 11 7 14.97 14.26 1.31 o 1 11 7 1.16 0.06 1.02 o 2 11 7 12.33 15.72 1.14 o 3 11 7 0.28 0.95 0.99 o 4 11 7 6.92 12.23 1.81 o 0 12 7 59.65 59.39 2.63 o 1 12 7 13.19 16.39 1.39 o 2 12 7 44.30 40.80 1.86 o 0 13 7 85.02 79.51 3.33 o 1 13 7 12.74 20.29 3.59 o 2 13 7 68.32 64.53 5.51 o 0 0 8 112.12 126.40 6.00 o 2 0 8 57.45 58.92 1.94 o 4 0 8 11.71 12.07 1.29 o 0 1 8 6.70 10.62 1.86 o 1 1 8 416.81 387.18 8.44 o 2 1 8 2.53 3.97 0.65 o 3 1 8 176.85 160.03 3.53 o 4 1 8 0.02 -0.06 0.61 o 5 1 8 39.88 41.03 1.47 o 0 2 8 37.55 28.10 1.32 o 1 2 8 58.90 43.76 1.36 o 2 2 8 42.31 37.49 1.16 o 3 2 8 22.49 19.61 0.92 o 4 2 8 32.17 29.88 1.21 o 5 2 8 3.26 5.79 1.41 o 0 3 8 14.36 7.92 0.94 o 1 3 8 128.91 130.47 3.50 o 2 3 8 8.15 7.16 0.73 o 3 3 8 90.20 79.56 2.00 o 4 3 8 1.68 4.74 1.26 o 5 3 8 39.35 37.57 1.50 o 0 4 8 16.99 15.27 1.25 o 1 4 8 364.75 369.66 8.61 o 2 4 8 11.02 11.12 0.74 o 3 4 8 181.86 172.29 4.10 o 4 4 8 5.09 8.41 0.96 o 5 4 8 49.87 48.44 1.61 o 0 5 8 1.80 4.20 1.26 o 1 5 8 258.04 272.02 7.85 o 2 5 8 3.90 5.31 0.68 o 3 5 8 103.19 105.74 2.56 o 4 5 8 6.63 8.82 0.82 o 5 5 8 20.65 26.46 1.11 o 0 6 8 6.16 6.27 1.56 o 1 6 8 60.81 60.56 1.97 o 2 6 8 3.29 4.19 0.71 o 3 6 8 29.62 28.29 1.03 o 4 6 8 0.63 1.24 0.75 o 5 6 8 9.84 14.40 1.39 o 1 7 8 116.64 122.30 3.36 o 2 7 8 13.88 11.55 0.89 o 3 7 8 50.18 51.60 1.47 o 4 7 8 2.63 5.33 1.05 o 0 8 8 17.60 20.04 1.84 o 1 8 8 113.56 118.20 3.66 o 2 8 8 12.82 15.80 1.26 o 3 8 8 55.90 53.96 1.67 o 4 8 8 4.76 9.37 0.96 o 0 9 8 1.14 4.71 1.67 o 1 9 8 99.10 92.02 3.38 o 2 9 8 1.09 2.60 0.88 o 3 9 8 37.19 36.02 1.33 o 4 9 8 0.79 1.08 2.51 o 0 10 8 10.95 10.85 1.42 o 1 10 8 64.93 68.37 2.42 o 2 10 8 4.92 6.33 1.78 o 3 10 8 31.45 30.65 2.23 o 0 11 8 33.51 31.98 3.16 o 1 11 8 0.95 0.24 0.85 o 2 11 8 22.82 27.20 3.89 o 0 12 8 0.35 6.80 2.60 o 1 12 8 54.09 56.20 3.01 o 1 0 9 58.37 49.08 2.00 o 3 0 9 29.18 27.21 1.32 o 5 0 9 6.59 14.87 2.09 o 0 1 9 195.46 192.53 6.25 o 1 1 9 113.73 120.72 3.11 o 2 1 9 136.59 125.20 3.78 o 3 1 9 35.85 35.89 1.17 o 4 1 9 51.27 48.59 1.61 o 5 1 9 2.96 13.17 2.82 o 0 2 9 23.19 19.52 1.15 o 1 2 9 7.90 12.21 0.72 o 2 2 9 19.64 15.64 0.84 o 3 2 9 1.07 2.84 0.83 o 4 2 9 10.42 9.21 0.70 o 5 2 9 0.01 3.13 2.46 o 0 3 9 44.11 43.96 2.16 o 1 3 9 8.16 7.35 0.79 o 2 3 9 32.14 31.12 1.30 o 3 3 9 4.98 6.18 0.94 o 4 3 9 12.21 12.60 0.87 o 0 4 9 114.52 122.35 4.81 o 1 4 9 101.34 92.67 2.74 o 2 4 9 70.79 74.29 2.36 o 3 4 9 53.96 49.18 1.63 o 4 4 9 19.05 25.39 1.15 o 5 4 9 18.46 16.73 1.75 o 0 5 9 11.53 14.79 1.93 o 1 5 9 22.37 21.66 1.42 o 2 5 9 10.74 10.57 0.80 o 3 5 9 10.62 10.59 0.81 o 4 5 9 6.45 10.62 1.27 o 0 6 9 34.44 34.19 2.40 o 1 6 9 60.37 63.95 2.32 o 2 6 9 19.14 19.74 1.05 o 3 6 9 30.15 33.10 1.56 o 4 6 9 2.24 10.27 1.69 o 0 7 9 158.00 158.56 11.88 o 1 7 9 70.91 82.21 3.20 o 2 7 9 101.83 100.96 3.26 o 3 7 9 35.21 41.07 1.82 o 4 7 9 32.00 35.89 2.38 o 0 8 9 0.42 3.69 1.60 o 1 8 9 45.94 46.85 2.14 o 2 8 9 0.86 4.30 1.93 o 3 8 9 21.67 27.76 3.29 o 0 9 9 104.02 117.10 6.57 o 1 9 9 0.01 0.16 0.87 o 2 9 9 64.76 72.15 2.93 o 3 9 9 0.67 26.45 3.48 o 0 10 9 0.67 2.98 1.32 o 1 10 9 4.58 10.53 3.26 o 0 0 10 0.59 -0.50 0.89 o 2 0 10 0.15 -0.80 1.30 o 0 1 10 48.58 54.38 2.25 o 1 1 10 1.57 2.53 0.66 o 2 1 10 32.63 36.83 1.76 o 3 1 10 0.33 1.38 1.04 o 0 2 10 2.63 0.64 0.82 o 1 2 10 94.17 87.36 2.43 o 2 2 10 0.35 0.40 0.69 o 3 2 10 42.61 40.44 1.62 o 0 3 10 28.07 30.46 1.84 o 1 3 10 139.09 143.67 4.39 o 2 3 10 21.74 21.31 1.03 o 3 3 10 56.90 57.27 2.09 o 4 3 10 9.60 13.06 2.84 o 0 4 10 5.61 9.82 1.06 o 1 4 10 145.07 159.16 5.45 o 2 4 10 2.74 5.98 0.86 o 3 4 10 80.75 80.86 2.76 o 4 4 10 0.20 14.11 3.10 o 0 5 10 80.58 81.28 4.90 o 1 5 10 17.48 20.33 1.12 o 2 5 10 51.79 52.51 2.14 o 3 5 10 1.87 7.72 3.88 o 0 6 10 4.04 5.12 1.54 o 1 6 10 30.41 36.95 1.88 o 2 6 10 1.31 3.09 0.92 o 3 6 10 14.49 26.46 2.12 o 0 7 10 82.45 93.95 7.77 o 1 7 10 0.65 0.92 0.88 o 2 7 10 65.77 76.55 3.50 o 1 0 11 1.02 2.72 1.05 o 0 1 11 1.90 3.12 1.09 o 1 1 11 0.20 1.76 0.69 o 2 1 11 1.20 2.35 0.96 o 0 2 11 230.23 242.31 9.00 o 1 2 11 42.43 61.92 2.48 o 2 2 11 152.56 148.58 5.15 o 0 3 11 10.22 13.42 1.43 o 1 3 11 2.54 7.49 0.94 o 2 3 11 9.10 14.13 2.41 o 0 4 11 68.48 83.85 4.64 o 1 4 11 16.72 24.47 1.64 o 2 4 11 51.98 66.53 5.02 o 0 5 11 13.86 14.84 2.66 o 1 5 11 11.61 15.30 2.36 o 2 5 11 9.38 11.09 1.66 o