#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2100279.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100279_Fobs loop_ _publ_author_name 'Nichol, Gary S.' 'Clegg, William' _publ_section_title ; A variable-temperature study of a phase transition in barbituric acid dihydrate ; _journal_coeditor_code WS5026 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 464 _journal_page_last 472 _journal_volume 61 _journal_year 2005 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2bc 2a' _symmetry_space_group_name_H-M 'P m n b' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1626 _cell_length_b 12.7574 _cell_length_c 8.8756 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.7513 _[local]_cod_data_source_file ws5026218sup11.hkl _[local]_cod_data_source_block 218 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 218 in Pmnb' _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' 'x+1/2, -y, -z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y-1/2, -z-1/2' '-x-1/2, y, z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 990.99 1190.69 60.65 o 1 2 0 2281.43 2177.85 59.56 o 2 2 0 784.86 681.21 21.60 o 3 2 0 474.94 443.60 29.09 o 4 2 0 240.81 194.96 13.64 o 6 2 0 36.60 40.91 2.09 o 7 2 0 29.99 30.42 6.25 o 0 4 0 38.56 40.60 1.53 o 1 4 0 647.67 600.75 18.50 o 2 4 0 4.94 4.04 0.37 o 3 4 0 95.33 78.03 2.36 o 4 4 0 1.63 0.97 0.45 o 5 4 0 10.49 11.67 0.99 o 6 4 0 3.19 2.59 0.97 o 7 4 0 1.18 1.09 4.08 o 0 6 0 39.20 56.43 2.10 o 1 6 0 243.44 230.27 5.84 o 2 6 0 26.31 32.06 1.28 o 3 6 0 64.82 63.47 1.89 o 4 6 0 10.25 12.60 1.10 o 5 6 0 25.00 29.06 1.26 o 6 6 0 3.44 6.42 1.34 o 7 6 0 8.13 11.75 2.66 o 0 8 0 580.95 630.27 23.57 o 1 8 0 400.85 466.36 13.20 o 2 8 0 291.73 284.73 11.43 o 3 8 0 102.54 97.40 2.92 o 4 8 0 49.56 53.20 1.85 o 5 8 0 3.32 4.18 0.92 o 6 8 0 4.53 6.41 1.32 o 7 8 0 0.26 -1.21 1.91 o 0 10 0 515.18 582.75 18.80 o 1 10 0 154.43 152.37 4.41 o 2 10 0 342.13 343.82 10.46 o 3 10 0 45.65 41.98 1.61 o 4 10 0 135.01 131.75 3.96 o 5 10 0 2.88 3.07 1.31 o 6 10 0 41.89 42.39 2.85 o 0 12 0 127.17 127.97 5.59 o 1 12 0 154.44 161.45 6.94 o 2 12 0 67.06 63.47 2.33 o 3 12 0 94.77 86.97 4.82 o 4 12 0 11.60 15.95 1.31 o 5 12 0 35.68 37.61 2.01 o 0 14 0 45.15 54.22 3.84 o 1 14 0 3.67 2.82 1.28 o 2 14 0 32.71 36.22 2.14 o 3 14 0 0.13 0.23 0.93 o 4 14 0 15.51 16.03 1.46 o 0 16 0 326.92 357.03 18.71 o 1 16 0 7.26 10.26 1.38 o 2 16 0 255.53 258.31 13.79 o 1 0 1 3289.60 2969.26 121.20 o 3 0 1 731.82 706.44 69.41 o 5 0 1 215.90 205.15 7.79 o 0 1 1 19.14 19.07 0.53 o 1 1 1 224.95 205.04 5.83 o 4 1 1 8.39 12.94 1.14 o 5 1 1 4.21 3.64 0.49 o 6 1 1 2.00 3.09 0.93 o 7 1 1 0.02 1.98 1.06 o 0 2 1 1294.57 1300.79 35.06 o 1 2 1 262.55 232.84 4.46 o 2 2 1 556.14 520.64 10.23 o 4 2 1 137.38 120.97 8.00 o 5 2 1 21.36 20.70 0.80 o 6 2 1 37.55 25.49 3.68 o 7 2 1 2.98 11.04 1.14 o 0 3 1 5.24 6.47 0.45 o 1 3 1 2054.53 2251.81 42.37 o 2 3 1 0.40 3.41 0.27 o 3 3 1 544.95 508.03 15.03 o 4 3 1 1.09 0.72 0.33 o 5 3 1 51.59 51.15 5.19 o 6 3 1 0.00 -0.61 0.61 o 7 3 1 2.72 7.45 1.43 o 8 3 1 0.05 4.34 2.65 o 0 4 1 486.65 558.72 13.95 o 1 4 1 3486.62 3637.96 62.47 o 2 4 1 226.16 216.86 4.19 o 3 4 1 769.97 660.80 17.65 o 4 4 1 15.70 12.64 0.49 o 5 4 1 96.39 85.61 1.89 o 6 4 1 0.09 -0.18 0.69 o 7 4 1 11.70 11.71 1.25 o 0 5 1 384.92 485.55 12.32 o 1 5 1 1863.89 2091.01 47.11 o 2 5 1 131.66 134.99 2.69 o 3 5 1 494.89 475.21 8.70 o 4 5 1 8.70 10.09 0.57 o 5 5 1 67.91 68.93 1.61 o 6 5 1 0.15 -0.81 0.81 o 7 5 1 7.08 9.41 0.91 o 0 6 1 414.85 470.14 10.81 o 1 6 1 100.74 120.51 2.12 o 2 6 1 207.49 203.48 3.78 o 3 6 1 65.94 67.11 1.41 o 4 6 1 13.99 11.63 0.62 o 5 6 1 25.16 26.94 0.86 o 6 6 1 1.18 0.50 0.64 o 7 6 1 6.10 8.43 1.05 o 0 7 1 635.04 731.13 19.39 o 1 7 1 459.23 512.82 8.65 o 2 7 1 298.58 301.97 6.65 o 3 7 1 165.34 151.67 3.06 o 4 7 1 61.46 58.43 1.38 o 5 7 1 29.42 25.68 1.02 o 6 7 1 13.96 14.83 0.82 o 7 7 1 3.42 4.04 1.28 o 0 8 1 343.15 353.49 10.53 o 1 8 1 21.81 18.92 0.56 o 2 8 1 171.52 158.09 3.33 o 3 8 1 8.14 9.68 0.61 o 4 8 1 36.31 35.10 0.99 o 5 8 1 1.94 3.55 0.69 o 6 8 1 6.38 10.52 0.94 o 7 8 1 0.27 -0.73 2.62 o 0 9 1 24.63 29.04 1.32 o 1 9 1 35.99 37.23 0.87 o 2 9 1 36.11 35.45 0.97 o 3 9 1 29.54 27.13 0.92 o 4 9 1 32.88 29.74 0.92 o 5 9 1 18.34 18.36 0.85 o 6 9 1 13.35 16.53 0.87 o 0 10 1 187.92 212.64 6.19 o 1 10 1 480.40 531.06 10.85 o 2 10 1 94.74 92.25 2.03 o 3 10 1 227.49 218.78 4.84 o 4 10 1 16.17 17.91 0.93 o 5 10 1 72.73 75.36 1.96 o 6 10 1 1.57 4.74 1.21 o 0 11 1 0.36 -0.20 0.60 o 1 11 1 889.53 973.40 24.07 o 2 11 1 2.16 1.91 0.55 o 3 11 1 423.69 407.89 8.34 o 4 11 1 4.13 5.05 0.69 o 5 11 1 113.90 113.64 4.10 o 6 11 1 2.06 6.73 1.32 o 0 12 1 219.18 232.05 7.56 o 1 12 1 7.39 11.89 0.78 o 2 12 1 162.36 161.83 3.67 o 3 12 1 0.06 0.68 0.54 o 4 12 1 67.30 61.95 1.61 o 5 12 1 0.85 3.84 0.90 o 0 13 1 18.39 21.58 1.37 o 1 13 1 54.89 55.76 1.78 o 2 13 1 15.67 14.33 0.72 o 3 13 1 26.08 28.91 1.17 o 4 13 1 9.88 11.96 0.85 o 5 13 1 7.60 19.07 4.34 o 0 14 1 33.70 35.57 2.08 o 1 14 1 361.72 358.52 8.68 o 2 14 1 23.67 23.16 0.99 o 3 14 1 153.33 142.46 3.25 o 4 14 1 8.58 12.72 0.90 o 0 15 1 5.09 6.80 1.29 o 1 15 1 87.30 90.94 2.80 o 2 15 1 2.99 5.16 0.83 o 3 15 1 38.82 39.74 2.02 o 0 16 1 25.25 28.20 2.38 o 1 16 1 52.14 55.83 2.00 o 2 16 1 21.23 22.92 2.18 o 0 0 2 970.65 891.92 28.62 o 2 0 2 356.25 339.29 10.43 o 6 0 2 4.10 6.85 1.18 o 0 1 2 150.05 159.17 4.15 o 1 1 2 162.76 172.30 3.14 o 2 1 2 138.96 138.88 2.49 o 3 1 2 66.73 65.09 1.55 o 4 1 2 28.23 21.41 0.64 o 5 1 2 12.11 11.08 0.70 o 6 1 2 0.68 0.42 0.59 o 7 1 2 1.64 4.80 0.91 o 0 2 2 1465.87 1625.56 36.75 o 1 2 2 127.13 117.48 2.19 o 2 2 2 653.61 640.14 14.21 o 3 2 2 41.72 32.56 0.82 o 4 2 2 90.56 90.07 3.07 o 5 2 2 6.27 6.11 0.78 o 6 2 2 7.60 8.61 0.73 o 7 2 2 0.60 2.76 2.47 o 8 2 2 0.52 1.48 1.67 o 0 3 2 315.91 329.98 9.26 o 1 3 2 881.32 909.18 16.89 o 2 3 2 202.43 208.11 3.81 o 3 3 2 135.92 138.66 2.97 o 4 3 2 38.27 37.92 1.27 o 5 3 2 12.97 13.25 0.77 o 6 3 2 2.41 3.84 1.00 o 7 3 2 1.92 4.02 1.68 o 0 4 2 27.48 33.63 1.04 o 1 4 2 2135.66 2183.94 39.68 o 2 4 2 4.50 6.14 0.36 o 3 4 2 523.82 512.30 9.96 o 4 4 2 3.36 3.13 0.41 o 5 4 2 65.31 63.36 1.92 o 6 4 2 5.54 8.49 1.30 o 7 4 2 7.38 10.58 1.75 o 0 5 2 8.66 8.43 0.66 o 1 5 2 678.00 752.17 14.24 o 2 5 2 6.26 8.23 0.40 o 3 5 2 91.53 86.24 1.71 o 4 5 2 0.37 1.02 0.38 o 5 5 2 2.21 2.69 0.56 o 6 5 2 0.16 -0.67 0.67 o 7 5 2 0.10 2.71 0.79 o 0 6 2 1743.44 2060.33 53.01 o 1 6 2 970.10 1095.09 21.81 o 2 6 2 939.45 985.57 18.86 o 3 6 2 316.10 309.40 5.67 o 4 6 2 207.48 205.67 4.76 o 5 6 2 56.34 51.81 1.97 o 6 6 2 32.42 33.75 1.81 o 7 6 2 8.05 10.79 1.20 o 0 7 2 56.05 67.72 1.91 o 1 7 2 282.14 311.04 5.85 o 2 7 2 33.49 34.03 0.82 o 3 7 2 71.57 71.90 1.58 o 4 7 2 8.47 9.93 0.61 o 5 7 2 19.42 20.25 0.86 o 6 7 2 1.27 2.63 0.82 o 7 7 2 6.41 6.07 2.02 o 0 8 2 493.38 512.92 12.85 o 1 8 2 66.92 81.35 1.67 o 2 8 2 283.29 271.98 4.99 o 3 8 2 16.68 17.05 0.67 o 4 8 2 61.34 60.56 1.93 o 5 8 2 1.39 0.62 0.56 o 6 8 2 6.19 9.75 1.02 o 7 8 2 0.05 2.91 1.69 o 0 9 2 117.57 110.71 3.00 o 1 9 2 21.96 23.93 0.69 o 2 9 2 91.70 79.19 1.94 o 3 9 2 38.81 36.10 1.04 o 4 9 2 52.30 48.36 1.40 o 5 9 2 25.71 24.34 0.97 o 6 9 2 21.69 23.30 1.07 o 0 10 2 912.14 995.93 27.17 o 1 10 2 350.22 339.27 6.23 o 2 10 2 590.69 580.99 11.17 o 3 10 2 125.51 120.44 2.55 o 4 10 2 182.96 169.06 4.30 o 5 10 2 21.44 23.60 0.98 o 6 10 2 33.87 38.30 1.55 o 0 11 2 889.64 892.90 24.10 o 1 11 2 141.06 130.53 3.08 o 2 11 2 620.59 600.77 12.12 o 3 11 2 79.05 71.19 1.67 o 4 11 2 229.05 200.53 5.25 o 5 11 2 23.59 23.29 1.73 o 6 11 2 54.88 64.39 3.92 o 0 12 2 212.04 220.74 7.21 o 1 12 2 3.95 4.68 0.55 o 2 12 2 133.05 137.90 3.49 o 3 12 2 1.25 2.69 0.58 o 4 12 2 37.54 38.64 1.86 o 5 12 2 0.07 3.56 1.12 o 0 13 2 55.60 55.14 2.33 o 1 13 2 71.38 64.09 1.77 o 2 13 2 32.21 30.49 1.07 o 3 13 2 40.57 35.53 1.10 o 4 13 2 5.27 8.56 1.05 o 5 13 2 15.08 16.24 1.74 o 0 14 2 14.70 17.46 1.31 o 1 14 2 6.53 8.52 0.81 o 2 14 2 6.03 9.31 0.73 o 3 14 2 1.34 1.89 0.85 o 4 14 2 0.08 2.93 1.15 o 0 15 2 71.14 78.39 3.51 o 1 15 2 3.77 6.50 0.82 o 2 15 2 49.08 52.72 1.71 o 3 15 2 1.90 2.54 1.11 o 0 16 2 0.98 1.78 1.59 o 1 16 2 21.44 28.12 3.71 o 2 16 2 0.88 3.95 1.23 o 1 0 3 8228.23 8533.96 215.45 o 3 0 3 1792.34 1798.09 58.21 o 5 0 3 226.97 205.99 11.80 o 0 1 3 75.67 77.95 1.85 o 1 1 3 927.18 974.88 18.19 o 2 1 3 34.82 32.16 0.76 o 3 1 3 245.92 249.21 4.96 o 4 1 3 7.21 7.54 0.50 o 5 1 3 16.76 16.10 0.82 o 6 1 3 1.24 0.43 0.64 o 7 1 3 0.20 0.75 1.37 o 0 2 3 0.48 0.18 0.22 o 1 2 3 325.80 362.15 7.23 o 2 2 3 0.06 0.37 0.22 o 3 2 3 23.01 25.04 0.77 o 4 2 3 3.55 3.44 0.44 o 5 2 3 0.19 -0.03 0.54 o 6 2 3 6.75 5.76 0.92 o 7 2 3 0.93 4.25 0.98 o 0 3 3 24.87 29.42 0.82 o 1 3 3 213.40 233.42 4.00 o 2 3 3 7.58 8.35 0.40 o 3 3 3 42.21 39.22 1.00 o 4 3 3 2.20 2.04 0.48 o 5 3 3 4.06 3.64 0.60 o 6 3 3 1.72 1.03 0.54 o 7 3 3 0.19 1.97 1.13 o 0 4 3 173.37 182.90 4.26 o 1 4 3 1196.08 1309.02 22.50 o 2 4 3 52.52 45.37 1.05 o 3 4 3 426.05 410.51 7.60 o 4 4 3 0.54 0.37 0.47 o 5 4 3 70.94 68.41 1.98 o 6 4 3 1.07 0.94 0.62 o 7 4 3 8.29 13.96 1.72 o 0 5 3 38.04 38.82 1.16 o 1 5 3 801.12 830.25 14.34 o 2 5 3 37.38 44.93 0.97 o 3 5 3 288.13 268.55 4.92 o 4 5 3 16.92 20.39 0.73 o 5 5 3 49.50 39.59 1.71 o 6 5 3 3.76 4.28 0.76 o 7 5 3 5.78 7.44 0.84 o 0 6 3 208.39 262.50 6.05 o 1 6 3 219.22 273.66 4.66 o 2 6 3 137.07 150.69 2.73 o 3 6 3 96.34 101.18 1.92 o 4 6 3 31.81 31.66 1.10 o 5 6 3 27.88 28.44 1.42 o 6 6 3 2.70 2.80 0.67 o 7 6 3 5.71 8.24 0.95 o 0 7 3 48.05 44.78 1.31 o 1 7 3 457.17 479.02 10.04 o 2 7 3 16.66 18.95 0.61 o 3 7 3 139.75 141.72 2.90 o 4 7 3 1.93 5.38 0.71 o 5 7 3 19.38 20.31 1.03 o 6 7 3 0.67 1.85 0.84 o 7 7 3 1.82 1.54 1.85 o 0 8 3 173.33 175.29 4.14 o 1 8 3 34.88 30.47 0.78 o 2 8 3 94.02 90.48 1.81 o 3 8 3 8.69 10.76 0.63 o 4 8 3 12.67 11.74 0.68 o 5 8 3 0.90 1.69 0.72 o 6 8 3 0.14 -0.22 0.97 o 0 9 3 50.72 52.04 1.77 o 1 9 3 5.52 5.27 0.41 o 2 9 3 13.84 14.44 0.64 o 3 9 3 7.64 7.72 0.60 o 4 9 3 0.18 -0.56 0.60 o 5 9 3 6.96 8.58 1.27 o 6 9 3 1.84 3.36 0.76 o 0 10 3 65.56 59.69 1.98 o 1 10 3 57.40 43.97 1.02 o 2 10 3 33.10 29.65 0.89 o 3 10 3 15.61 16.18 0.80 o 4 10 3 2.94 1.38 0.69 o 5 10 3 1.94 4.05 1.06 o 6 10 3 0.07 2.11 1.36 o 0 11 3 22.96 13.97 0.90 o 1 11 3 19.66 16.47 0.73 o 2 11 3 22.99 16.62 0.80 o 3 11 3 17.41 14.31 0.76 o 4 11 3 15.02 13.93 0.97 o 5 11 3 9.32 10.90 1.02 o 0 12 3 77.14 60.00 2.07 o 1 12 3 88.31 81.17 1.96 o 2 12 3 55.38 44.81 1.36 o 3 12 3 34.28 32.94 1.16 o 4 12 3 21.03 18.50 0.90 o 5 12 3 7.10 13.76 1.41 o 0 13 3 7.85 7.23 1.09 o 1 13 3 98.67 92.83 2.23 o 2 13 3 5.58 5.27 0.67 o 3 13 3 47.40 40.32 1.43 o 4 13 3 2.27 4.17 0.66 o 0 14 3 151.70 152.68 5.25 o 1 14 3 17.18 16.98 0.96 o 2 14 3 97.96 97.81 2.78 o 3 14 3 9.78 10.93 0.98 o 4 14 3 28.65 33.34 2.94 o 0 15 3 44.01 42.05 3.21 o 1 15 3 1.97 5.82 0.84 o 2 15 3 28.34 25.84 1.33 o 3 15 3 3.60 5.35 2.29 o 0 16 3 5.29 6.70 1.40 o 1 16 3 3.18 7.65 1.33 o 0 0 4 38.24 45.23 1.62 o 2 0 4 29.61 25.56 1.18 o 4 0 4 0.09 2.29 0.61 o 6 0 4 12.53 13.01 1.27 o 0 1 4 526.74 541.52 13.09 o 1 1 4 1721.58 1842.13 34.44 o 2 1 4 250.16 242.73 4.44 o 3 1 4 520.37 487.89 8.77 o 4 1 4 35.76 40.18 1.10 o 5 1 4 77.83 73.46 1.99 o 6 1 4 2.82 5.47 0.81 o 7 1 4 8.59 11.08 1.64 o 0 2 4 1026.80 1114.94 25.12 o 1 2 4 311.58 359.16 6.48 o 2 2 4 412.56 389.24 8.60 o 3 2 4 134.96 145.38 3.00 o 4 2 4 44.33 45.04 1.30 o 5 2 4 50.73 54.20 1.87 o 6 2 4 2.24 4.84 0.79 o 7 2 4 14.09 20.17 2.09 o 0 3 4 2.11 1.57 0.48 o 1 3 4 39.05 39.07 0.83 o 2 3 4 0.50 1.47 0.23 o 3 3 4 13.78 17.47 0.79 o 4 3 4 0.10 0.95 0.47 o 5 3 4 2.01 3.01 0.56 o 6 3 4 0.25 0.36 0.67 o 7 3 4 0.08 3.73 1.25 o 0 4 4 300.72 265.78 6.12 o 1 4 4 504.09 550.59 9.44 o 2 4 4 112.29 88.81 1.79 o 3 4 4 165.44 154.88 3.57 o 4 4 4 9.94 9.69 0.60 o 5 4 4 20.75 17.87 0.72 o 6 4 4 0.74 1.49 0.66 o 7 4 4 1.94 3.80 0.81 o 0 5 4 562.60 609.43 13.78 o 1 5 4 2.43 2.29 0.25 o 2 5 4 325.02 324.99 6.37 o 3 5 4 0.36 1.42 0.41 o 4 5 4 85.22 79.45 1.85 o 5 5 4 0.00 -0.06 0.54 o 6 5 4 16.18 15.49 1.13 o 7 5 4 0.01 2.81 0.87 o 0 6 4 2.78 6.94 0.50 o 1 6 4 283.47 313.00 5.52 o 2 6 4 0.35 0.77 0.34 o 3 6 4 68.40 68.21 1.48 o 4 6 4 0.05 0.25 0.46 o 5 6 4 0.70 0.80 0.57 o 6 6 4 0.02 0.29 0.68 o 7 6 4 1.30 2.59 1.19 o 0 7 4 0.04 -0.14 0.36 o 1 7 4 49.00 45.18 0.98 o 2 7 4 0.85 2.54 0.38 o 3 7 4 26.56 26.17 0.80 o 4 7 4 2.25 3.12 0.69 o 5 7 4 11.13 9.80 1.21 o 6 7 4 1.25 3.73 0.92 o 0 8 4 26.80 21.26 0.89 o 1 8 4 29.92 23.41 0.71 o 2 8 4 18.30 15.40 0.59 o 3 8 4 7.66 8.17 0.60 o 4 8 4 7.85 10.98 0.77 o 5 8 4 1.83 2.59 1.14 o 6 8 4 2.53 5.15 0.95 o 0 9 4 5.04 7.49 0.74 o 1 9 4 189.41 180.04 3.40 o 2 9 4 4.86 7.39 0.54 o 3 9 4 51.82 51.32 1.32 o 4 9 4 3.32 4.35 0.77 o 5 9 4 3.76 5.61 1.10 o 6 9 4 1.23 1.18 1.28 o 0 10 4 302.33 266.14 7.41 o 1 10 4 30.57 27.53 0.84 o 2 10 4 185.44 160.62 3.75 o 3 10 4 8.01 10.09 0.67 o 4 10 4 54.29 49.63 2.74 o 5 10 4 1.17 3.45 0.87 o 0 11 4 54.08 56.63 1.92 o 1 11 4 13.83 12.54 0.64 o 2 11 4 38.46 40.23 1.19 o 3 11 4 6.49 8.60 0.86 o 4 11 4 14.86 17.76 1.13 o 5 11 4 2.09 3.83 0.99 o 0 12 4 12.06 9.87 0.78 o 1 12 4 108.16 96.93 2.29 o 2 12 4 4.15 4.35 0.60 o 3 12 4 61.11 53.44 1.68 o 4 12 4 0.05 1.56 0.96 o 0 13 4 74.95 62.94 2.49 o 1 13 4 6.85 9.61 0.61 o 2 13 4 52.01 42.55 1.61 o 3 13 4 5.26 8.50 1.03 o 4 13 4 18.88 21.55 3.08 o 0 14 4 93.65 89.02 3.32 o 1 14 4 0.46 2.70 0.71 o 2 14 4 53.14 48.62 1.66 o 3 14 4 0.42 2.86 0.86 o 0 15 4 105.96 119.21 4.26 o 1 15 4 1.15 3.49 0.90 o 2 15 4 81.75 91.56 5.18 o 1 0 5 1237.73 1266.82 32.09 o 3 0 5 355.21 348.52 8.92 o 5 0 5 68.24 66.59 2.60 o 7 0 5 12.66 12.43 1.72 o 0 1 5 276.39 351.71 8.05 o 1 1 5 5.10 6.05 0.33 o 2 1 5 183.91 198.42 3.90 o 3 1 5 6.43 6.72 0.44 o 4 1 5 59.66 55.17 1.29 o 5 1 5 0.77 1.21 0.59 o 6 1 5 12.02 14.29 0.88 o 7 1 5 0.00 0.00 0.81 o 0 2 5 202.64 203.78 4.71 o 1 2 5 403.51 414.17 8.09 o 2 2 5 113.28 115.39 2.32 o 3 2 5 108.06 94.87 2.05 o 4 2 5 33.23 34.99 1.07 o 5 2 5 17.37 14.61 0.76 o 6 2 5 8.40 10.82 1.07 o 7 2 5 2.24 5.38 0.90 o 0 3 5 1107.17 1109.85 24.95 o 1 3 5 13.83 19.65 0.55 o 2 3 5 545.75 530.89 10.04 o 3 3 5 2.96 8.90 0.57 o 4 3 5 96.55 92.85 2.09 o 5 3 5 0.81 3.04 0.60 o 6 3 5 12.11 11.50 1.01 o 7 3 5 0.16 3.36 2.66 o 0 4 5 42.95 46.00 1.25 o 1 4 5 1.38 2.98 0.31 o 2 4 5 26.64 30.49 0.84 o 3 4 5 0.00 -0.35 0.44 o 4 4 5 3.45 6.22 0.61 o 5 4 5 1.85 1.40 0.64 o 6 4 5 0.02 1.75 0.74 o 0 5 5 164.57 175.55 4.14 o 1 5 5 173.57 165.92 2.95 o 2 5 5 51.75 56.79 1.27 o 3 5 5 40.44 37.84 1.11 o 4 5 5 0.20 1.44 0.56 o 5 5 5 0.94 1.47 0.61 o 6 5 5 1.72 3.23 0.86 o 7 5 5 0.31 0.28 1.02 o 0 6 5 1709.74 1675.99 37.72 o 1 6 5 78.04 78.25 1.54 o 2 6 5 1054.09 983.78 18.07 o 3 6 5 37.26 38.49 1.14 o 4 6 5 321.34 306.31 6.31 o 5 6 5 10.89 13.68 0.92 o 6 6 5 68.36 71.70 2.87 o 0 7 5 704.73 691.13 16.81 o 1 7 5 1.91 5.21 0.46 o 2 7 5 444.52 417.26 7.80 o 3 7 5 1.49 2.34 0.64 o 4 7 5 153.82 146.45 3.57 o 5 7 5 0.63 1.03 0.80 o 6 7 5 41.90 41.55 2.20 o 0 8 5 212.59 214.81 6.07 o 1 8 5 71.88 63.09 1.49 o 2 8 5 131.92 126.84 2.68 o 3 8 5 41.26 35.89 1.10 o 4 8 5 31.95 28.84 1.40 o 5 8 5 16.56 17.30 1.01 o 6 8 5 3.56 3.08 1.23 o 0 9 5 144.17 116.79 3.48 o 1 9 5 67.20 60.12 1.43 o 2 9 5 115.40 91.22 1.94 o 3 9 5 43.12 39.06 1.29 o 4 9 5 54.59 46.91 1.40 o 5 9 5 19.50 17.02 1.00 o 0 10 5 282.48 257.24 7.22 o 1 10 5 143.31 119.92 2.75 o 2 10 5 182.41 165.73 3.51 o 3 10 5 67.23 56.66 1.72 o 4 10 5 51.52 48.54 1.72 o 5 10 5 19.13 18.62 1.69 o 0 11 5 0.58 1.26 0.55 o 1 11 5 151.29 124.99 2.86 o 2 11 5 0.78 0.33 0.53 o 3 11 5 76.34 66.12 1.95 o 4 11 5 1.23 1.72 0.72 o 5 11 5 23.11 18.10 2.87 o 0 12 5 17.25 18.18 1.02 o 1 12 5 27.02 21.37 0.91 o 2 12 5 7.70 9.96 0.76 o 3 12 5 9.89 9.19 0.89 o 4 12 5 0.26 3.03 0.96 o 0 13 5 20.71 20.55 1.24 o 1 13 5 64.53 65.22 2.04 o 2 13 5 15.50 14.27 0.81 o 3 13 5 16.91 21.12 1.85 o 0 14 5 4.50 5.09 1.11 o 1 14 5 23.44 24.33 1.01 o 2 14 5 3.32 3.81 0.78 o 0 15 5 0.11 0.67 0.91 o 1 15 5 14.31 19.67 1.31 o 0 0 6 121.49 114.60 3.91 o 2 0 6 56.01 58.91 2.27 o 4 0 6 5.95 7.16 0.80 o 6 0 6 0.12 0.17 1.41 o 0 1 6 333.53 313.16 7.24 o 1 1 6 104.18 93.43 1.84 o 2 1 6 180.26 165.68 3.25 o 3 1 6 26.29 25.77 0.75 o 4 1 6 22.93 20.32 0.78 o 5 1 6 1.69 2.40 0.75 o 6 1 6 0.11 0.15 0.86 o 7 1 6 0.01 6.31 2.41 o 0 2 6 17.75 17.47 0.65 o 1 2 6 109.22 105.62 2.22 o 2 2 6 23.18 22.18 0.65 o 3 2 6 33.66 33.97 0.91 o 4 2 6 23.30 22.39 0.85 o 5 2 6 3.74 4.67 0.70 o 6 2 6 11.20 11.62 0.84 o 7 2 6 0.10 1.25 2.06 o 0 3 6 40.48 41.98 1.26 o 1 3 6 29.37 36.81 0.87 o 2 3 6 29.77 31.83 0.86 o 3 3 6 21.40 21.95 0.79 o 4 3 6 8.55 9.36 0.60 o 5 3 6 15.30 14.79 0.70 o 6 3 6 1.06 2.27 0.81 o 0 4 6 381.41 385.15 8.78 o 1 4 6 102.78 99.69 2.19 o 2 4 6 247.42 225.99 4.70 o 3 4 6 69.26 68.96 1.65 o 4 4 6 79.17 72.28 1.75 o 5 4 6 31.92 33.07 1.06 o 6 4 6 16.51 18.80 1.95 o 0 5 6 24.04 20.97 0.83 o 1 5 6 355.02 369.18 7.07 o 2 5 6 9.14 9.45 0.59 o 3 5 6 202.14 196.81 4.15 o 4 5 6 0.63 0.73 0.53 o 5 5 6 63.78 64.24 1.76 o 6 5 6 0.01 1.22 0.94 o 0 6 6 61.48 66.44 1.92 o 1 6 6 277.45 275.43 5.57 o 2 6 6 48.43 50.50 1.31 o 3 6 6 148.49 137.58 3.01 o 4 6 6 25.05 27.29 0.95 o 5 6 6 49.86 48.01 1.56 o 6 6 6 8.73 10.78 0.94 o 0 7 6 87.76 92.20 3.34 o 1 7 6 1214.40 1164.76 23.11 o 2 7 6 52.09 54.69 1.47 o 3 7 6 509.18 463.58 9.90 o 4 7 6 13.94 14.97 0.73 o 5 7 6 129.46 111.11 3.51 o 6 7 6 2.77 1.46 1.13 o 0 8 6 473.27 469.27 15.33 o 1 8 6 18.90 14.74 0.69 o 2 8 6 332.49 312.80 6.76 o 3 8 6 5.14 6.03 0.66 o 4 8 6 125.88 121.94 3.12 o 5 8 6 0.26 1.58 0.74 o 0 9 6 0.71 -0.29 0.70 o 1 9 6 93.41 81.80 2.10 o 2 9 6 2.79 1.59 0.47 o 3 9 6 79.62 68.46 1.85 o 4 9 6 7.45 8.04 0.72 o 5 9 6 37.07 35.93 1.76 o 0 10 6 34.92 34.91 1.68 o 1 10 6 7.58 9.97 0.67 o 2 10 6 17.50 17.65 0.87 o 3 10 6 1.20 2.46 0.70 o 4 10 6 1.75 3.80 0.71 o 5 10 6 0.03 0.42 1.66 o 0 11 6 47.35 39.71 1.90 o 1 11 6 284.45 262.91 6.11 o 2 11 6 37.30 32.00 1.57 o 3 11 6 119.58 111.18 3.11 o 4 11 6 17.61 18.30 1.05 o 0 12 6 3.10 7.72 1.09 o 1 12 6 26.05 29.07 1.06 o 2 12 6 3.20 5.24 0.73 o 3 12 6 16.65 19.58 0.99 o 4 12 6 2.44 11.35 2.96 o 0 13 6 5.26 6.04 1.06 o 1 13 6 49.78 45.11 1.59 o 2 13 6 4.05 5.60 0.84 o 0 14 6 0.07 2.01 1.62 o 1 14 6 45.98 44.24 1.60 o 1 0 7 14.46 16.79 0.80 o 3 0 7 2.45 5.81 0.78 o 5 0 7 0.77 0.82 0.90 o 0 1 7 13.22 12.26 0.82 o 1 1 7 249.76 233.12 4.36 o 2 1 7 4.19 4.87 0.42 o 3 1 7 85.22 83.40 1.80 o 4 1 7 0.01 -0.21 0.61 o 5 1 7 17.19 20.12 0.93 o 6 1 7 0.55 1.63 0.74 o 0 2 7 327.08 336.43 10.17 o 1 2 7 59.70 60.10 1.41 o 2 2 7 199.94 191.10 3.75 o 3 2 7 63.88 57.14 1.42 o 4 2 7 56.01 57.73 1.55 o 5 2 7 35.52 34.03 1.22 o 6 2 7 9.89 11.17 0.90 o 0 3 7 577.20 559.80 17.74 o 1 3 7 89.03 91.74 1.95 o 2 3 7 367.00 345.11 6.65 o 3 3 7 42.27 39.88 1.14 o 4 3 7 121.93 115.77 2.71 o 5 3 7 9.57 11.19 0.70 o 6 3 7 30.52 31.09 1.53 o 0 4 7 1724.88 1735.57 51.27 o 1 4 7 79.73 72.99 1.62 o 2 4 7 1148.64 1051.29 20.92 o 3 4 7 19.44 19.02 0.79 o 4 4 7 375.93 335.72 6.90 o 5 4 7 1.52 3.56 0.79 o 6 4 7 75.44 68.11 5.69 o 0 5 7 36.73 39.48 2.34 o 1 5 7 117.19 112.18 2.68 o 2 5 7 43.56 46.14 1.37 o 3 5 7 53.16 47.84 1.32 o 4 5 7 36.91 37.45 1.14 o 5 5 7 13.52 14.89 1.28 o 6 5 7 15.73 19.21 3.07 o 0 6 7 61.59 66.49 2.25 o 1 6 7 7.09 11.17 0.62 o 2 6 7 42.20 41.46 1.19 o 3 6 7 5.42 7.37 0.63 o 4 6 7 13.08 13.46 0.73 o 5 6 7 3.30 4.37 0.73 o 0 7 7 152.53 175.03 7.33 o 1 7 7 0.06 0.56 0.54 o 2 7 7 101.91 102.87 2.36 o 3 7 7 0.84 1.02 0.56 o 4 7 7 37.33 37.90 1.17 o 5 7 7 2.03 3.66 0.74 o 0 8 7 64.92 67.60 2.73 o 1 8 7 4.44 6.09 0.70 o 2 8 7 43.37 41.16 1.20 o 3 8 7 7.39 7.03 0.71 o 4 8 7 12.40 13.01 0.79 o 5 8 7 6.15 3.51 1.29 o 0 9 7 278.92 272.05 9.11 o 1 9 7 4.83 6.30 0.83 o 2 9 7 188.87 170.06 3.86 o 3 9 7 3.23 5.05 0.60 o 4 9 7 61.63 63.33 1.76 o 0 10 7 2.45 5.18 0.94 o 1 10 7 3.22 5.26 0.87 o 2 10 7 1.74 3.10 0.73 o 3 10 7 3.52 4.83 0.75 o 4 10 7 0.45 3.10 0.78 o 0 11 7 14.51 15.78 1.10 o 1 11 7 1.25 1.56 0.78 o 2 11 7 12.15 13.82 0.81 o 3 11 7 0.31 2.07 0.83 o 0 12 7 60.11 61.16 2.56 o 1 12 7 13.19 16.22 1.07 o 2 12 7 44.22 43.24 1.83 o 3 12 7 13.98 19.56 2.27 o 0 13 7 83.17 82.07 3.40 o 1 13 7 12.46 17.38 2.42 o 2 13 7 66.60 65.22 5.35 o 0 0 8 112.34 125.22 5.77 o 2 0 8 58.25 56.59 1.79 o 4 0 8 12.11 12.38 1.02 o 0 1 8 6.80 8.95 0.99 o 1 1 8 422.61 374.22 8.03 o 2 1 8 2.44 3.15 0.50 o 3 1 8 178.96 157.23 3.33 o 4 1 8 0.01 -0.29 0.55 o 5 1 8 40.08 40.89 1.38 o 0 2 8 37.01 27.16 1.28 o 1 2 8 57.61 42.75 1.28 o 2 2 8 41.46 35.15 1.04 o 3 2 8 21.95 19.25 0.86 o 4 2 8 31.59 29.26 1.13 o 5 2 8 3.26 6.03 1.10 o 0 3 8 14.77 8.77 0.84 o 1 3 8 129.20 127.13 3.33 o 2 3 8 8.56 7.75 0.59 o 3 3 8 89.81 78.89 1.85 o 4 3 8 1.76 3.04 0.70 o 5 3 8 38.15 38.05 1.23 o 0 4 8 16.38 15.38 1.15 o 1 4 8 361.67 360.35 8.25 o 2 4 8 10.87 10.97 0.65 o 3 4 8 179.76 168.78 3.82 o 4 4 8 5.33 8.10 0.85 o 5 4 8 49.02 50.30 1.46 o 0 5 8 1.61 2.02 0.70 o 1 5 8 251.42 266.74 7.55 o 2 5 8 3.67 5.23 0.55 o 3 5 8 100.39 104.43 2.41 o 4 5 8 6.42 8.63 0.72 o 5 5 8 20.45 26.39 1.00 o 0 6 8 5.57 4.45 1.31 o 1 6 8 57.49 59.74 1.83 o 2 6 8 2.80 3.64 0.60 o 3 6 8 28.12 27.00 0.94 o 4 6 8 0.40 1.23 0.55 o 5 6 8 9.40 13.97 1.14 o 1 7 8 113.11 121.65 3.21 o 2 7 8 13.09 11.12 0.73 o 3 7 8 49.27 52.96 1.44 o 4 7 8 2.59 3.14 0.66 o 0 8 8 16.94 19.55 2.16 o 1 8 8 109.74 120.78 3.54 o 2 8 8 12.26 14.06 0.95 o 3 8 8 54.79 54.35 1.52 o 4 8 8 4.62 9.62 1.28 o 0 9 8 1.09 1.91 2.05 o 1 9 8 95.17 91.23 3.17 o 2 9 8 1.00 2.44 0.73 o 3 9 8 35.90 35.67 1.23 o 4 9 8 0.72 4.37 1.48 o 0 10 8 10.03 11.40 3.10 o 1 10 8 65.40 68.21 2.27 o 2 10 8 4.56 6.24 0.99 o 3 10 8 31.55 33.72 2.52 o 0 11 8 32.50 35.68 4.57 o 1 11 8 1.14 2.30 0.84 o 2 11 8 21.98 26.77 2.74 o 0 12 8 0.41 2.99 2.04 o 1 12 8 53.32 55.48 3.26 o 1 0 9 55.25 47.09 1.88 o 3 0 9 27.34 25.18 1.53 o 5 0 9 6.10 10.61 1.91 o 0 1 9 197.89 183.25 5.82 o 1 1 9 113.01 116.12 2.91 o 2 1 9 138.00 121.58 3.57 o 3 1 9 35.38 35.45 1.13 o 4 1 9 51.08 47.25 1.51 o 5 1 9 2.80 4.90 1.50 o 0 2 9 22.90 19.00 1.09 o 1 2 9 7.34 11.24 0.65 o 2 2 9 19.46 13.56 0.79 o 3 2 9 0.95 2.33 0.49 o 4 2 9 10.48 11.02 0.79 o 5 2 9 0.03 4.05 2.27 o 0 3 9 46.03 44.63 2.14 o 1 3 9 8.42 7.91 0.66 o 2 3 9 32.60 30.27 1.21 o 3 3 9 5.00 7.30 0.69 o 4 3 9 11.44 13.10 1.01 o 0 4 9 113.65 114.37 4.40 o 1 4 9 98.20 90.83 2.62 o 2 4 9 70.76 73.55 2.24 o 3 4 9 52.80 48.19 1.54 o 4 4 9 19.23 26.26 1.01 o 0 5 9 11.19 14.08 1.08 o 1 5 9 22.64 20.08 1.46 o 2 5 9 10.16 11.65 0.86 o 3 5 9 10.28 11.53 0.72 o 4 5 9 5.81 8.04 0.77 o 0 6 9 35.26 34.16 2.31 o 1 6 9 59.94 62.44 2.18 o 2 6 9 19.61 20.89 1.15 o 3 6 9 30.23 33.18 1.41 o 4 6 9 2.38 5.44 1.36 o 0 7 9 155.21 147.18 10.82 o 1 7 9 69.28 82.67 3.10 o 2 7 9 100.49 101.26 3.19 o 3 7 9 33.63 40.09 1.95 o 4 7 9 32.00 34.56 1.73 o 0 8 9 0.55 2.08 1.20 o 1 8 9 45.56 46.13 2.11 o 2 8 9 1.00 4.72 1.50 o 3 8 9 21.08 29.03 2.61 o 0 9 9 101.71 121.93 6.11 o 1 9 9 0.08 0.31 0.74 o 2 9 9 62.83 75.01 2.96 o 3 9 9 0.46 4.36 1.21 o 0 10 9 0.70 3.17 1.60 o 1 10 9 4.48 9.68 2.37 o 0 0 10 0.50 1.30 2.34 o 2 0 10 0.10 -0.72 0.96 o 0 1 10 46.60 52.32 2.09 o 1 1 10 1.44 2.33 0.51 o 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