#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:57:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180870 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/02/2100280.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100280_Fobs loop_ _publ_author_name 'Nichol, Gary S.' 'Clegg, William' _publ_section_title ; A variable-temperature study of a phase transition in barbituric acid dihydrate ; _journal_coeditor_code WS5026 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 464 _journal_page_last 472 _journal_volume 61 _journal_year 2005 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2bc 2a' _symmetry_space_group_name_H-M 'P m n b' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1624 _cell_length_b 12.7569 _cell_length_c 8.8782 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.7502 _cod_data_source_file ws5026219sup12.hkl _cod_data_source_block 219 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 219 in Pmnb' _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' 'x+1/2, -y, -z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y-1/2, -z-1/2' '-x-1/2, y, z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 6020.16 4710.04 338.64 o 6 0 0 722.59 686.79 24.76 o 0 2 0 1010.30 1199.97 40.38 o 1 2 0 2317.91 2198.98 52.34 o 2 2 0 782.87 706.24 18.30 o 3 2 0 476.56 469.22 13.48 o 4 2 0 238.85 196.21 5.13 o 5 2 0 111.86 99.13 3.65 o 6 2 0 35.83 38.48 2.20 o 7 2 0 30.47 35.87 6.25 o 0 4 0 38.00 42.54 1.61 o 1 4 0 657.87 618.99 16.07 o 2 4 0 5.60 4.56 0.40 o 3 4 0 94.93 74.60 2.24 o 4 4 0 1.76 1.13 0.61 o 5 4 0 9.93 10.21 0.82 o 6 4 0 3.06 3.98 0.83 o 7 4 0 1.16 7.06 2.77 o 0 6 0 42.01 58.42 2.41 o 1 6 0 246.92 230.88 6.18 o 2 6 0 25.66 33.10 1.25 o 3 6 0 68.12 64.07 1.83 o 4 6 0 9.32 12.48 0.81 o 5 6 0 26.74 28.91 1.21 o 6 6 0 3.21 6.05 0.63 o 7 6 0 9.11 12.02 3.19 o 0 8 0 602.78 652.26 20.30 o 1 8 0 401.51 475.42 15.30 o 2 8 0 299.35 290.42 7.78 o 3 8 0 100.61 96.97 2.96 o 4 8 0 50.99 53.04 1.90 o 5 8 0 3.12 5.09 0.81 o 6 8 0 5.34 10.10 1.07 o 7 8 0 0.32 0.69 2.83 o 0 10 0 532.77 588.09 18.39 o 1 10 0 159.83 153.49 4.36 o 2 10 0 352.89 349.87 13.08 o 3 10 0 47.81 43.49 1.68 o 4 10 0 138.85 133.07 3.92 o 5 10 0 3.71 6.61 1.12 o 6 10 0 43.25 43.10 2.16 o 0 12 0 123.18 128.26 5.58 o 1 12 0 152.54 161.80 7.59 o 2 12 0 63.94 62.59 2.41 o 3 12 0 92.05 86.71 3.55 o 4 12 0 10.25 12.34 0.84 o 5 12 0 34.56 30.77 1.71 o 0 14 0 49.13 56.63 3.93 o 1 14 0 5.04 5.49 1.30 o 2 14 0 35.77 39.61 2.92 o 3 14 0 0.36 1.07 0.79 o 4 14 0 16.96 19.79 1.88 o 0 16 0 327.07 329.28 17.34 o 1 16 0 8.51 12.68 2.68 o 2 16 0 255.58 257.95 13.78 o 1 0 1 3316.34 3095.18 125.97 o 3 0 1 745.71 795.50 23.46 o 5 0 1 218.26 200.38 5.70 o 0 1 1 18.59 19.59 0.54 o 1 1 1 222.93 206.36 4.01 o 3 1 1 72.01 62.40 1.42 o 4 1 1 7.31 11.95 0.80 o 5 1 1 3.96 2.74 0.71 o 6 1 1 1.52 5.38 1.05 o 7 1 1 0.01 6.77 1.20 o 0 2 1 1295.56 1332.44 36.09 o 1 2 1 255.37 242.35 4.29 o 2 2 1 564.21 500.85 13.06 o 3 2 1 118.22 88.75 5.21 o 4 2 1 142.13 140.09 2.47 o 5 2 1 20.14 18.58 0.66 o 6 2 1 39.31 36.48 3.28 o 7 2 1 2.67 10.26 0.68 o 0 3 1 5.42 6.01 0.50 o 1 3 1 2045.33 2153.96 53.41 o 2 3 1 0.32 3.25 0.27 o 3 3 1 538.42 520.71 10.08 o 4 3 1 1.06 0.68 0.31 o 5 3 1 52.07 49.29 1.59 o 6 3 1 0.00 -0.38 0.61 o 7 3 1 2.97 11.58 1.35 o 0 4 1 502.14 574.85 15.32 o 1 4 1 3461.07 3685.00 63.41 o 2 4 1 230.40 216.24 4.07 o 3 4 1 768.09 686.09 12.62 o 4 4 1 15.81 12.33 0.53 o 5 4 1 95.44 83.17 1.84 o 6 4 1 0.11 0.47 0.59 o 7 4 1 11.50 16.28 1.28 o 0 5 1 389.34 489.17 12.87 o 1 5 1 1846.49 2133.32 37.03 o 2 5 1 132.92 134.27 2.37 o 3 5 1 489.74 470.64 7.95 o 4 5 1 8.19 8.88 0.52 o 5 5 1 65.84 64.89 1.53 o 6 5 1 0.08 0.76 0.82 o 7 5 1 6.75 12.11 1.01 o 0 6 1 411.92 482.45 11.67 o 1 6 1 101.86 121.40 2.16 o 2 6 1 203.51 203.28 3.50 o 3 6 1 66.48 67.99 1.41 o 4 6 1 13.10 12.34 0.58 o 5 6 1 25.67 24.92 0.80 o 6 6 1 1.42 3.83 0.51 o 7 6 1 6.16 11.57 1.02 o 0 7 1 642.31 740.73 19.49 o 1 7 1 453.95 512.09 8.31 o 2 7 1 303.66 298.56 6.51 o 3 7 1 160.13 146.92 2.93 o 4 7 1 62.33 56.92 1.37 o 5 7 1 28.09 25.86 0.88 o 6 7 1 14.14 14.55 0.70 o 7 7 1 3.23 7.63 0.90 o 0 8 1 337.01 361.47 9.43 o 1 8 1 21.40 19.76 0.57 o 2 8 1 169.08 155.53 3.08 o 3 8 1 8.47 8.89 0.59 o 4 8 1 35.72 33.64 1.06 o 5 8 1 2.45 3.75 0.64 o 6 8 1 6.36 8.96 0.59 o 7 8 1 0.50 3.05 2.83 o 0 9 1 24.76 28.67 0.97 o 1 9 1 37.78 38.13 0.89 o 2 9 1 35.83 35.66 0.97 o 3 9 1 30.24 27.32 0.88 o 4 9 1 32.91 29.07 0.92 o 5 9 1 18.83 18.80 0.85 o 6 9 1 13.48 17.56 0.84 o 0 10 1 187.33 211.99 6.98 o 1 10 1 485.99 542.21 12.32 o 2 10 1 93.89 94.49 2.07 o 3 10 1 228.20 218.64 4.29 o 4 10 1 15.12 18.23 0.75 o 5 10 1 72.80 71.39 1.87 o 6 10 1 1.19 5.78 1.39 o 0 11 1 0.39 0.66 0.62 o 1 11 1 900.51 974.83 19.58 o 2 11 1 2.15 2.17 0.52 o 3 11 1 428.30 403.37 7.67 o 4 11 1 4.25 6.79 0.57 o 5 11 1 114.55 107.34 3.26 o 6 11 1 2.24 8.72 1.01 o 0 12 1 224.89 247.58 7.94 o 1 12 1 6.62 11.28 0.76 o 2 12 1 165.71 162.88 4.00 o 3 12 1 0.00 1.68 0.59 o 4 12 1 68.43 61.97 1.61 o 5 12 1 1.19 7.08 1.19 o 0 13 1 18.82 20.79 1.38 o 1 13 1 55.75 57.62 1.80 o 2 13 1 16.32 16.30 0.88 o 3 13 1 26.12 29.17 1.09 o 4 13 1 10.37 12.32 0.66 o 5 13 1 7.40 16.27 2.88 o 0 14 1 32.10 34.73 2.08 o 1 14 1 374.40 361.93 8.66 o 2 14 1 22.32 25.84 1.13 o 3 14 1 158.61 143.07 3.29 o 4 14 1 8.06 12.19 0.78 o 0 15 1 6.69 10.82 1.28 o 1 15 1 88.01 86.27 2.70 o 2 15 1 4.00 6.94 0.71 o 3 15 1 38.85 36.39 1.31 o 0 16 1 25.17 26.27 1.79 o 1 16 1 54.17 60.24 2.11 o 2 16 1 21.14 26.53 2.39 o 0 0 2 969.88 866.91 26.84 o 2 0 2 357.41 322.81 11.60 o 4 0 2 39.95 40.18 1.59 o 6 0 2 4.65 6.70 1.04 o 8 0 2 0.73 10.03 1.20 o 0 1 2 154.16 159.49 4.01 o 1 1 2 166.55 176.89 3.56 o 2 1 2 137.07 137.85 2.49 o 3 1 2 65.68 63.10 1.65 o 4 1 2 27.64 20.80 0.62 o 5 1 2 10.96 9.81 0.60 o 6 1 2 0.57 0.53 0.74 o 7 1 2 1.19 7.68 1.24 o 8 1 2 0.01 12.40 1.53 o 0 2 2 1467.63 1636.91 35.78 o 1 2 2 124.28 116.93 1.99 o 2 2 2 649.23 644.04 11.03 o 3 2 2 42.06 29.93 1.19 o 4 2 2 88.67 88.60 1.95 o 5 2 2 6.35 6.64 0.71 o 6 2 2 7.48 8.76 0.65 o 7 2 2 0.57 8.62 0.84 o 0 3 2 319.99 338.96 7.89 o 1 3 2 896.16 923.62 16.67 o 2 3 2 201.76 206.22 3.67 o 3 3 2 136.48 139.49 2.89 o 4 3 2 39.41 33.91 1.11 o 5 3 2 12.59 13.94 0.68 o 6 3 2 2.92 2.81 0.97 o 7 3 2 1.92 6.77 0.76 o 0 4 2 26.05 34.74 0.95 o 1 4 2 2166.76 2253.74 40.95 o 2 4 2 4.19 5.69 0.31 o 3 4 2 530.10 509.01 8.96 o 4 4 2 3.36 3.51 0.37 o 5 4 2 66.61 61.32 1.76 o 6 4 2 5.42 8.91 0.73 o 7 4 2 7.77 12.42 1.06 o 0 5 2 9.07 8.04 0.63 o 1 5 2 684.91 756.82 13.07 o 2 5 2 5.75 8.29 0.38 o 3 5 2 91.03 83.75 1.59 o 4 5 2 0.28 0.59 0.36 o 5 5 2 1.88 4.26 0.60 o 6 5 2 0.17 -0.55 0.93 o 7 5 2 0.13 6.65 1.24 o 0 6 2 1769.09 2099.26 51.29 o 1 6 2 976.79 1099.40 19.50 o 2 6 2 948.26 969.61 20.04 o 3 6 2 317.42 305.51 5.47 o 4 6 2 207.06 200.82 5.15 o 5 6 2 56.48 50.65 1.65 o 6 6 2 32.22 32.46 1.33 o 7 6 2 8.06 14.10 1.48 o 0 7 2 58.63 70.07 2.34 o 1 7 2 284.84 317.70 5.72 o 2 7 2 33.30 34.43 0.84 o 3 7 2 73.22 71.56 1.51 o 4 7 2 7.94 9.60 0.71 o 5 7 2 19.74 18.75 0.88 o 6 7 2 1.23 3.24 0.77 o 7 7 2 6.63 11.13 0.96 o 0 8 2 493.59 518.25 13.67 o 1 8 2 69.50 83.66 1.70 o 2 8 2 283.71 275.11 5.04 o 3 8 2 17.35 16.92 0.62 o 4 8 2 61.40 60.32 1.64 o 5 8 2 1.45 1.10 0.62 o 6 8 2 6.13 11.48 0.78 o 7 8 2 0.06 2.97 1.23 o 0 9 2 119.60 113.44 3.04 o 1 9 2 21.17 23.10 0.70 o 2 9 2 92.38 78.98 1.66 o 3 9 2 37.80 35.00 1.01 o 4 9 2 52.71 47.14 1.34 o 5 9 2 25.80 25.95 1.08 o 6 9 2 22.41 22.79 1.14 o 0 10 2 917.73 1000.62 24.12 o 1 10 2 344.74 343.46 7.54 o 2 10 2 593.96 563.86 10.06 o 3 10 2 122.27 118.02 2.83 o 4 10 2 183.83 163.73 4.23 o 5 10 2 20.46 24.54 1.60 o 6 10 2 34.10 37.73 1.66 o 0 11 2 901.54 908.04 23.80 o 1 11 2 143.44 132.36 2.63 o 2 11 2 628.81 589.74 12.23 o 3 11 2 79.79 70.62 1.67 o 4 11 2 231.85 204.27 4.52 o 5 11 2 24.41 26.51 0.99 o 6 11 2 55.27 64.49 4.00 o 0 12 2 212.47 228.29 7.38 o 1 12 2 4.22 4.91 0.69 o 2 12 2 132.13 137.31 3.20 o 3 12 2 1.29 2.27 0.72 o 4 12 2 36.30 39.40 1.95 o 5 12 2 0.05 3.59 0.92 o 0 13 2 55.59 53.77 2.30 o 1 13 2 74.46 63.72 1.78 o 2 13 2 32.12 31.92 1.05 o 3 13 2 42.79 34.07 1.12 o 4 13 2 5.29 8.10 0.85 o 5 13 2 15.80 20.40 2.30 o 0 14 2 15.30 18.25 1.24 o 1 14 2 6.78 9.16 0.79 o 2 14 2 6.31 11.18 0.65 o 3 14 2 1.34 3.42 0.71 o 4 14 2 0.10 4.55 0.72 o 0 15 2 72.58 81.08 6.31 o 1 15 2 5.18 7.78 0.75 o 2 15 2 49.92 53.48 1.74 o 3 15 2 2.64 6.04 1.14 o 0 16 2 1.28 6.68 2.05 o 1 16 2 22.11 29.33 1.88 o 2 16 2 1.18 4.46 1.80 o 1 0 3 8246.74 8669.63 209.81 o 3 0 3 1790.92 1673.01 52.87 o 5 0 3 223.45 213.23 6.64 o 7 0 3 29.85 32.10 3.19 o 0 1 3 77.29 78.00 1.80 o 1 1 3 924.70 988.79 16.59 o 2 1 3 36.18 30.98 0.71 o 3 1 3 240.84 242.76 4.70 o 4 1 3 7.78 7.28 0.49 o 5 1 3 15.99 15.17 0.81 o 6 1 3 1.46 2.28 0.67 o 7 1 3 0.13 2.48 0.77 o 0 2 3 0.82 0.11 0.22 o 1 2 3 321.85 351.48 7.09 o 2 2 3 0.10 0.42 0.20 o 3 2 3 22.44 24.54 0.91 o 4 2 3 3.35 4.01 0.49 o 5 2 3 0.29 0.73 0.54 o 6 2 3 6.56 6.50 0.87 o 7 2 3 1.02 7.12 1.51 o 0 3 3 23.51 29.69 0.81 o 1 3 3 218.34 236.04 3.70 o 2 3 3 7.28 8.27 0.35 o 3 3 3 42.91 38.96 0.99 o 4 3 3 2.19 2.44 0.49 o 5 3 3 3.74 5.07 0.56 o 6 3 3 1.76 0.57 0.63 o 7 3 3 0.14 5.12 1.03 o 0 4 3 176.80 183.13 4.13 o 1 4 3 1207.97 1317.29 20.87 o 2 4 3 52.49 44.41 0.94 o 3 4 3 425.87 412.16 6.99 o 4 4 3 0.32 1.16 0.43 o 5 4 3 71.12 67.82 1.83 o 6 4 3 1.38 3.31 0.93 o 7 4 3 8.31 15.04 0.97 o 0 5 3 36.05 38.65 1.15 o 1 5 3 800.86 835.56 13.96 o 2 5 3 35.56 43.65 0.96 o 3 5 3 284.90 262.25 4.70 o 4 5 3 16.31 20.12 0.77 o 5 5 3 48.70 40.00 1.43 o 6 5 3 3.56 7.58 1.21 o 7 5 3 5.61 9.22 1.42 o 0 6 3 210.70 264.64 5.91 o 1 6 3 221.55 283.56 5.12 o 2 6 3 136.34 149.47 2.63 o 3 6 3 100.48 99.10 1.85 o 4 6 3 30.84 29.78 1.15 o 5 6 3 29.43 26.62 1.04 o 6 6 3 2.41 3.40 0.80 o 7 6 3 6.12 13.69 1.57 o 0 7 3 49.49 45.62 1.24 o 1 7 3 457.96 491.62 10.14 o 2 7 3 17.35 17.43 0.63 o 3 7 3 138.60 140.85 2.65 o 4 7 3 1.96 4.90 0.54 o 5 7 3 18.34 20.84 1.16 o 6 7 3 0.67 3.40 0.88 o 7 7 3 1.54 6.23 3.76 o 0 8 3 175.22 179.74 4.66 o 1 8 3 36.89 31.80 0.78 o 2 8 3 93.81 91.70 1.74 o 3 8 3 8.94 10.25 0.61 o 4 8 3 12.43 12.01 0.75 o 5 8 3 1.03 2.46 0.85 o 6 8 3 0.12 1.98 0.70 o 0 9 3 52.15 52.79 1.77 o 1 9 3 5.90 4.86 0.45 o 2 9 3 14.38 13.42 0.62 o 3 9 3 7.94 7.20 0.65 o 4 9 3 0.19 0.27 0.54 o 5 9 3 7.36 8.01 0.97 o 6 9 3 1.97 5.29 1.02 o 0 10 3 67.72 59.99 2.01 o 1 10 3 60.12 45.48 1.15 o 2 10 3 34.21 30.68 0.92 o 3 10 3 16.10 14.30 0.80 o 4 10 3 3.39 3.44 0.69 o 5 10 3 1.93 6.57 0.75 o 6 10 3 0.01 6.06 1.18 o 0 11 3 25.26 14.63 0.89 o 1 11 3 20.12 16.50 0.73 o 2 11 3 24.97 16.90 0.67 o 3 11 3 18.32 17.00 1.03 o 4 11 3 16.46 14.08 1.14 o 5 11 3 9.93 11.80 0.95 o 0 12 3 75.56 62.10 2.09 o 1 12 3 90.63 83.56 2.04 o 2 12 3 53.14 44.68 1.33 o 3 12 3 34.67 31.35 1.16 o 4 12 3 19.38 19.19 0.89 o 5 12 3 6.81 13.19 1.19 o 0 13 3 7.56 6.03 0.76 o 1 13 3 99.04 93.33 2.25 o 2 13 3 5.54 7.76 0.62 o 3 13 3 47.82 40.52 1.39 o 4 13 3 2.34 5.98 0.65 o 0 14 3 154.70 153.00 5.24 o 1 14 3 17.21 17.24 0.91 o 2 14 3 100.28 100.47 2.86 o 3 14 3 9.59 9.72 0.95 o 4 14 3 29.55 30.76 2.36 o 0 15 3 46.12 43.56 3.16 o 1 15 3 2.19 7.10 0.71 o 2 15 3 29.49 27.88 1.36 o 3 15 3 3.90 7.84 2.02 o 0 16 3 6.18 11.95 1.63 o 1 16 3 2.33 8.55 2.48 o 0 0 4 38.46 44.34 1.60 o 2 0 4 28.03 25.41 0.98 o 4 0 4 0.17 0.47 0.54 o 6 0 4 13.06 11.92 1.26 o 0 1 4 538.84 538.51 12.60 o 1 1 4 1742.98 1830.68 30.82 o 2 1 4 253.55 242.00 4.28 o 3 1 4 520.06 480.39 9.27 o 4 1 4 35.62 39.30 1.06 o 5 1 4 76.02 73.09 1.89 o 6 1 4 2.77 4.04 0.72 o 7 1 4 8.11 14.35 1.70 o 0 2 4 1022.04 1128.56 24.52 o 1 2 4 309.40 356.55 5.85 o 2 2 4 413.73 396.53 7.66 o 3 2 4 136.01 144.60 2.91 o 4 2 4 44.07 43.16 1.20 o 5 2 4 51.72 51.60 1.41 o 6 2 4 2.15 6.22 0.87 o 7 2 4 14.63 20.92 1.47 o 0 3 4 1.45 1.52 0.53 o 1 3 4 36.20 37.69 0.74 o 2 3 4 0.26 0.75 0.23 o 3 3 4 13.19 16.77 0.64 o 4 3 4 0.14 1.11 0.47 o 5 3 4 1.92 5.14 0.63 o 6 3 4 0.22 0.75 0.60 o 7 3 4 0.07 6.59 1.21 o 0 4 4 301.70 269.10 6.00 o 1 4 4 503.92 546.82 8.74 o 2 4 4 114.57 89.29 1.67 o 3 4 4 164.85 154.48 3.16 o 4 4 4 10.22 11.07 0.65 o 5 4 4 20.85 17.86 0.75 o 6 4 4 0.70 1.96 0.63 o 7 4 4 1.94 7.77 1.34 o 0 5 4 569.46 620.13 13.57 o 1 5 4 2.33 2.63 0.25 o 2 5 4 327.80 325.09 5.75 o 3 5 4 0.39 0.75 0.42 o 4 5 4 85.19 77.48 2.02 o 5 5 4 0.01 0.28 0.55 o 6 5 4 16.12 14.73 0.97 o 7 5 4 0.00 2.42 1.32 o 0 6 4 2.08 7.11 0.73 o 1 6 4 289.20 305.42 5.15 o 2 6 4 0.25 1.04 0.32 o 3 6 4 69.32 68.55 1.48 o 4 6 4 0.05 0.36 0.53 o 5 6 4 0.71 0.55 0.61 o 6 6 4 0.01 0.58 0.78 o 7 6 4 1.38 4.20 1.98 o 0 7 4 0.03 0.29 0.32 o 1 7 4 51.58 45.14 0.99 o 2 7 4 0.80 1.70 0.35 o 3 7 4 27.97 26.68 0.82 o 4 7 4 2.07 1.95 0.65 o 5 7 4 11.64 11.03 0.97 o 6 7 4 1.06 3.74 1.16 o 0 8 4 28.37 20.98 0.86 o 1 8 4 29.63 23.82 0.68 o 2 8 4 19.55 15.45 0.61 o 3 8 4 7.77 7.52 0.47 o 4 8 4 8.93 9.56 0.73 o 5 8 4 1.88 4.68 1.26 o 6 8 4 3.24 6.11 0.85 o 0 9 4 5.16 7.22 0.82 o 1 9 4 191.11 189.35 4.00 o 2 9 4 4.91 7.01 0.56 o 3 9 4 51.96 51.39 1.31 o 4 9 4 3.27 5.52 0.78 o 5 9 4 3.76 6.51 1.05 o 6 9 4 1.18 5.95 1.52 o 0 10 4 297.11 274.24 7.49 o 1 10 4 29.97 28.26 0.86 o 2 10 4 180.34 162.61 3.53 o 3 10 4 7.60 8.44 0.53 o 4 10 4 51.66 50.49 1.60 o 5 10 4 0.89 2.53 0.61 o 0 11 4 54.76 57.11 1.98 o 1 11 4 14.74 12.93 0.60 o 2 11 4 38.90 40.65 1.66 o 3 11 4 7.10 8.70 0.74 o 4 11 4 14.94 16.99 1.17 o 5 11 4 2.41 5.65 0.95 o 0 12 4 13.58 10.75 0.81 o 1 12 4 109.79 97.18 2.29 o 2 12 4 4.69 5.61 0.54 o 3 12 4 61.35 51.55 2.04 o 4 12 4 0.05 2.16 0.96 o 0 13 4 77.00 63.94 2.54 o 1 13 4 6.21 9.32 0.79 o 2 13 4 53.40 42.33 1.46 o 3 13 4 4.93 7.07 0.84 o 4 13 4 19.46 19.62 3.02 o 0 14 4 96.32 89.73 3.37 o 1 14 4 0.69 4.22 0.55 o 2 14 4 54.76 49.48 1.85 o 3 14 4 0.59 2.49 1.27 o 0 15 4 105.96 120.95 4.37 o 1 15 4 1.21 1.92 0.62 o 2 15 4 81.95 89.30 7.49 o 1 0 5 1221.58 1260.99 30.66 o 3 0 5 353.08 343.56 9.19 o 5 0 5 69.04 63.51 2.45 o 7 0 5 13.38 14.05 2.15 o 0 1 5 279.43 343.96 7.61 o 1 1 5 5.21 5.67 0.43 o 2 1 5 185.38 196.18 3.73 o 3 1 5 6.40 6.38 0.43 o 4 1 5 59.38 53.58 1.23 o 5 1 5 0.79 1.27 0.55 o 6 1 5 11.46 11.99 1.00 o 7 1 5 0.00 6.05 2.59 o 0 2 5 199.09 203.98 4.57 o 1 2 5 406.72 417.30 6.87 o 2 2 5 110.61 114.08 2.25 o 3 2 5 109.17 96.08 2.04 o 4 2 5 32.32 34.53 1.07 o 5 2 5 17.59 15.01 0.70 o 6 2 5 8.46 10.08 0.81 o 7 2 5 2.39 9.23 0.98 o 0 3 5 1117.74 1116.93 24.28 o 1 3 5 13.37 18.93 0.47 o 2 3 5 547.69 526.05 9.58 o 3 3 5 2.67 7.77 0.53 o 4 3 5 94.69 94.12 2.08 o 5 3 5 0.55 2.91 0.60 o 6 3 5 11.53 12.49 1.30 o 7 3 5 0.07 0.28 1.89 o 0 4 5 42.46 45.50 1.22 o 1 4 5 1.30 3.26 0.28 o 2 4 5 25.97 30.52 0.85 o 3 4 5 0.00 -0.04 0.40 o 4 4 5 3.11 6.50 0.63 o 5 4 5 1.67 1.46 0.61 o 6 4 5 0.06 0.91 0.54 o 0 5 5 167.10 179.12 4.11 o 1 5 5 175.39 167.05 3.07 o 2 5 5 52.07 57.01 1.32 o 3 5 5 39.02 38.07 1.13 o 4 5 5 0.12 1.14 0.47 o 5 5 5 0.73 1.17 0.73 o 6 5 5 2.04 2.61 1.02 o 7 5 5 0.41 2.91 1.79 o 0 6 5 1728.32 1683.12 36.55 o 1 6 5 78.23 78.18 1.52 o 2 6 5 1063.60 991.04 17.62 o 3 6 5 36.45 37.66 1.09 o 4 6 5 321.98 308.84 6.52 o 5 6 5 10.60 13.12 1.00 o 6 6 5 68.17 71.23 3.62 o 0 7 5 707.58 693.26 16.36 o 1 7 5 2.12 5.42 0.47 o 2 7 5 448.02 423.19 7.72 o 3 7 5 1.92 2.83 0.55 o 4 7 5 155.47 150.98 4.67 o 5 7 5 0.86 1.35 0.72 o 6 7 5 42.49 43.08 2.65 o 0 8 5 216.14 218.53 6.04 o 1 8 5 74.34 63.83 1.52 o 2 8 5 133.32 129.41 2.59 o 3 8 5 42.18 37.24 1.09 o 4 8 5 31.97 27.20 1.31 o 5 8 5 17.17 16.94 0.95 o 6 8 5 3.46 5.04 0.89 o 0 9 5 144.86 116.74 3.45 o 1 9 5 67.12 62.03 1.48 o 2 9 5 114.63 93.08 2.05 o 3 9 5 42.79 38.46 1.21 o 4 9 5 53.60 49.22 1.44 o 5 9 5 19.50 19.83 1.36 o 0 10 5 282.78 258.61 7.10 o 1 10 5 145.73 122.37 2.77 o 2 10 5 182.02 168.35 3.71 o 3 10 5 67.90 59.15 2.65 o 4 10 5 51.48 48.55 1.67 o 5 10 5 19.33 18.93 0.98 o 0 11 5 0.92 1.61 0.58 o 1 11 5 153.37 128.34 2.91 o 2 11 5 1.17 0.93 0.51 o 3 11 5 77.27 61.00 1.84 o 4 11 5 1.56 4.64 1.19 o 5 11 5 23.38 20.97 2.29 o 0 12 5 18.43 19.11 1.02 o 1 12 5 28.62 22.54 0.90 o 2 12 5 8.32 8.98 0.61 o 3 12 5 10.66 10.78 1.25 o 4 12 5 0.28 2.31 0.93 o 0 13 5 21.55 20.85 1.19 o 1 13 5 64.75 66.30 2.17 o 2 13 5 16.32 14.31 0.78 o 3 13 5 16.40 18.64 1.11 o 4 13 5 7.68 15.78 2.42 o 0 14 5 4.72 5.06 0.96 o 1 14 5 24.41 24.08 0.97 o 2 14 5 3.46 5.14 0.69 o 0 15 5 0.07 1.14 0.84 o 1 15 5 14.12 21.50 1.33 o 0 0 6 119.61 112.70 4.79 o 2 0 6 54.90 56.09 1.91 o 4 0 6 5.53 8.85 0.84 o 6 0 6 0.06 2.40 0.95 o 0 1 6 337.56 308.53 6.88 o 1 1 6 104.86 92.35 1.78 o 2 1 6 180.09 163.71 3.14 o 3 1 6 26.56 24.78 0.75 o 4 1 6 22.49 20.06 0.78 o 5 1 6 1.78 2.71 0.97 o 6 1 6 0.09 1.13 0.71 o 7 1 6 0.00 1.68 1.52 o 0 2 6 18.57 17.37 0.74 o 1 2 6 111.22 105.04 2.16 o 2 2 6 24.23 21.82 0.65 o 3 2 6 34.99 33.28 0.90 o 4 2 6 24.66 22.11 0.82 o 5 2 6 4.20 6.07 0.57 o 6 2 6 12.11 13.86 1.27 o 7 2 6 0.17 0.51 1.18 o 0 3 6 38.64 43.07 1.27 o 1 3 6 29.14 36.91 0.87 o 2 3 6 28.25 31.52 0.86 o 3 3 6 21.61 22.40 0.76 o 4 3 6 8.38 10.59 0.62 o 5 3 6 15.29 14.09 0.73 o 6 3 6 1.16 2.53 0.82 o 0 4 6 377.60 380.65 8.44 o 1 4 6 104.72 100.53 2.18 o 2 4 6 244.46 229.34 4.64 o 3 4 6 71.56 67.83 1.62 o 4 4 6 77.97 72.89 1.74 o 5 4 6 33.80 34.44 1.15 o 6 4 6 16.16 20.44 0.86 o 0 5 6 24.77 21.29 0.85 o 1 5 6 358.94 379.09 7.15 o 2 5 6 9.73 10.08 0.60 o 3 5 6 203.35 195.31 4.02 o 4 5 6 0.75 2.38 0.58 o 5 5 6 64.07 64.06 1.70 o 6 5 6 0.02 3.64 1.12 o 0 6 6 63.68 67.29 1.97 o 1 6 6 276.20 273.76 5.37 o 2 6 6 50.49 51.28 1.33 o 3 6 6 147.26 137.49 2.97 o 4 6 6 26.42 28.04 0.96 o 5 6 6 49.39 48.04 1.55 o 6 6 6 9.34 13.31 0.98 o 0 7 6 90.05 93.79 2.83 o 1 7 6 1233.64 1174.76 21.89 o 2 7 6 53.52 55.21 1.47 o 3 7 6 515.46 453.52 9.41 o 4 7 6 14.15 16.01 0.72 o 5 7 6 130.09 119.78 3.37 o 6 7 6 2.71 6.02 1.69 o 0 8 6 476.70 473.65 15.03 o 1 8 6 18.88 16.06 0.68 o 2 8 6 335.27 313.19 6.26 o 3 8 6 5.12 6.91 0.68 o 4 8 6 127.15 123.84 3.15 o 5 8 6 0.27 2.26 0.79 o 0 9 6 0.78 0.08 0.75 o 1 9 6 90.36 84.21 2.05 o 2 9 6 2.93 1.70 0.57 o 3 9 6 77.54 68.84 1.83 o 4 9 6 7.78 9.08 0.84 o 5 9 6 36.42 39.66 1.55 o 0 10 6 37.66 34.99 1.76 o 1 10 6 7.35 9.37 0.56 o 2 10 6 18.83 18.28 0.94 o 3 10 6 1.15 2.70 0.61 o 4 10 6 1.82 5.34 0.62 o 5 10 6 0.02 1.60 1.85 o 0 11 6 49.28 40.79 1.95 o 1 11 6 284.08 259.89 5.53 o 2 11 6 39.22 31.14 1.42 o 3 11 6 118.51 112.21 2.96 o 4 11 6 18.88 18.59 1.41 o 0 12 6 2.85 5.53 0.70 o 1 12 6 25.43 29.11 1.07 o 2 12 6 3.05 5.20 0.83 o 3 12 6 16.88 19.08 1.01 o 4 12 6 2.51 18.64 3.48 o 0 13 6 6.08 6.35 0.87 o 1 13 6 51.27 45.85 1.67 o 2 13 6 4.61 7.86 0.66 o 0 14 6 0.04 1.52 0.85 o 1 14 6 46.47 44.93 1.95 o 1 0 7 14.21 16.67 0.91 o 3 0 7 2.26 5.78 0.72 o 5 0 7 0.61 1.66 1.51 o 0 1 7 13.71 13.50 0.87 o 1 1 7 251.65 230.23 4.18 o 2 1 7 4.26 5.64 0.44 o 3 1 7 84.89 80.38 1.72 o 4 1 7 0.02 0.06 0.62 o 5 1 7 16.82 20.37 1.09 o 6 1 7 0.57 4.48 1.03 o 0 2 7 327.72 328.60 9.58 o 1 2 7 60.18 60.11 1.28 o 2 2 7 199.58 189.90 3.64 o 3 2 7 64.78 58.37 1.47 o 4 2 7 55.11 57.95 1.53 o 5 2 7 36.79 32.96 1.26 o 6 2 7 9.53 14.81 0.96 o 0 3 7 578.73 561.25 16.11 o 1 3 7 89.22 92.22 1.94 o 2 3 7 365.61 344.11 6.42 o 3 3 7 42.08 39.89 1.17 o 4 3 7 119.72 113.30 2.64 o 5 3 7 9.44 11.39 0.65 o 6 3 7 29.70 32.80 1.17 o 0 4 7 1736.18 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0.71 o 4 10 7 0.39 8.05 1.94 o 0 11 7 15.48 15.08 1.23 o 1 11 7 1.26 1.35 0.58 o 2 11 7 12.94 14.37 0.92 o 3 11 7 0.32 1.16 1.17 o 0 12 7 60.53 59.03 2.56 o 1 12 7 12.72 17.24 1.46 o 2 12 7 44.74 44.13 1.95 o 3 12 7 13.97 13.75 1.73 o 0 13 7 83.97 83.27 3.31 o 1 13 7 12.70 16.47 1.36 o 2 13 7 66.93 65.75 5.60 o 0 0 8 105.78 123.31 5.59 o 2 0 8 54.74 58.13 2.49 o 4 0 8 11.20 12.43 0.96 o 0 1 8 6.62 8.54 0.77 o 1 1 8 418.65 369.65 7.62 o 2 1 8 2.30 4.61 0.54 o 3 1 8 175.62 154.75 3.21 o 4 1 8 0.00 -0.03 0.52 o 5 1 8 38.87 41.55 1.35 o 0 2 8 36.76 28.89 1.33 o 1 2 8 59.61 42.92 1.30 o 2 2 8 41.25 35.16 1.06 o 3 2 8 22.89 19.09 0.85 o 4 2 8 31.89 30.71 1.09 o 5 2 8 3.45 8.29 1.04 o 0 3 8 15.11 8.82 1.02 o 1 3 8 129.56 126.69 3.25 o 2 3 8 8.85 7.86 0.56 o 3 3 8 90.60 78.13 1.85 o 4 3 8 1.96 5.92 0.60 o 5 3 8 38.62 37.61 1.15 o 0 4 8 17.02 16.71 1.24 o 1 4 8 366.15 356.94 7.89 o 2 4 8 11.19 10.02 0.64 o 3 4 8 182.08 169.96 3.77 o 4 4 8 5.15 7.52 0.77 o 5 4 8 50.05 51.09 1.41 o 0 5 8 1.53 3.69 0.88 o 1 5 8 255.76 266.63 6.43 o 2 5 8 3.73 5.79 0.65 o 3 5 8 100.79 104.29 2.38 o 4 5 8 6.75 8.21 0.68 o 5 5 8 19.77 27.43 1.30 o 0 6 8 5.43 6.62 1.24 o 1 6 8 57.90 59.16 1.79 o 2 6 8 2.84 3.46 0.67 o 3 6 8 27.90 29.33 0.99 o 4 6 8 0.48 2.43 0.70 o 5 6 8 8.99 15.04 1.44 o 0 7 8 23.77 17.28 2.40 o 1 7 8 113.85 121.30 3.24 o 2 7 8 13.09 12.55 0.78 o 3 7 8 49.61 51.76 1.41 o 4 7 8 2.34 4.89 0.77 o 0 8 8 17.47 20.50 3.73 o 1 8 8 111.94 120.68 3.51 o 2 8 8 12.84 17.13 0.99 o 3 8 8 55.89 52.94 1.40 o 4 8 8 4.97 9.07 1.15 o 0 9 8 1.26 2.93 1.13 o 1 9 8 97.98 94.20 3.28 o 2 9 8 1.13 2.90 0.73 o 3 9 8 36.24 35.71 1.46 o 4 9 8 0.76 3.28 0.89 o 0 10 8 10.82 11.84 2.27 o 1 10 8 62.72 70.01 2.38 o 2 10 8 4.84 7.52 1.22 o 3 10 8 30.13 36.98 3.44 o 0 11 8 33.10 35.77 3.04 o 1 11 8 1.15 2.43 0.65 o 2 11 8 22.30 23.26 2.05 o 0 12 8 0.20 6.74 2.49 o 1 12 8 54.10 61.77 4.52 o 1 0 9 57.46 46.51 1.82 o 3 0 9 28.85 25.38 1.11 o 5 0 9 6.60 19.17 2.01 o 0 1 9 195.26 178.61 5.56 o 1 1 9 117.62 116.54 2.87 o 2 1 9 136.16 120.94 3.49 o 3 1 9 36.73 36.98 1.15 o 4 1 9 50.36 50.19 1.51 o 5 1 9 3.00 11.32 1.35 o 0 2 9 24.71 20.82 1.12 o 1 2 9 7.34 10.75 0.71 o 2 2 9 20.76 15.67 0.82 o 3 2 9 0.93 4.67 0.79 o 4 2 9 10.88 9.80 0.63 o 5 2 9 0.03 8.70 1.18 o 0 3 9 46.93 44.29 2.05 o 1 3 9 7.36 6.91 0.60 o 2 3 9 33.05 30.70 1.21 o 3 3 9 4.50 6.19 0.89 o 4 3 9 11.62 13.01 0.75 o 0 4 9 115.02 119.31 4.51 o 1 4 9 98.21 90.77 2.58 o 2 4 9 70.95 76.71 2.67 o 3 4 9 52.86 46.84 1.42 o 4 4 9 18.78 26.19 1.10 o 0 5 9 11.87 14.37 1.27 o 1 5 9 22.61 22.39 1.34 o 2 5 9 10.68 12.02 0.82 o 3 5 9 10.48 10.98 0.76 o 4 5 9 6.15 9.60 1.30 o 0 6 9 34.75 32.94 2.37 o 1 6 9 62.02 65.67 2.27 o 2 6 9 19.31 21.28 1.12 o 3 6 9 30.86 33.24 1.36 o 4 6 9 2.35 10.24 1.15 o 0 7 9 159.42 150.54 10.82 o 1 7 9 70.17 83.09 3.11 o 2 7 9 103.20 101.76 3.16 o 3 7 9 34.00 41.56 1.46 o 4 7 9 32.80 30.62 1.98 o 0 8 9 0.92 5.56 1.10 o 1 8 9 46.10 48.13 2.18 o 2 8 9 1.37 5.71 1.01 o 3 8 9 21.12 28.84 2.72 o 0 9 9 105.29 121.92 5.97 o 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