#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2100281.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100281_Fobs loop_ _publ_author_name 'Nichol, Gary S.' 'Clegg, William' _publ_section_title ; A variable-temperature study of a phase transition in barbituric acid dihydrate ; _journal_coeditor_code WS5026 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 464 _journal_page_last 472 _journal_volume 61 _journal_year 2005 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2bc 2a' _symmetry_space_group_name_H-M 'P m n b' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1665 _cell_length_b 12.7626 _cell_length_c 8.8814 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.7476 _[local]_cod_data_source_file ws5026220sup13.hkl _[local]_cod_data_source_block 220 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 220 in Pmnb' _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' 'x+1/2, -y, -z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y-1/2, -z-1/2' '-x-1/2, y, z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5896.08 4520.51 243.69 o 0 2 0 987.89 1155.18 52.35 o 1 2 0 2278.20 2163.91 61.61 o 2 2 0 767.05 693.46 16.73 o 3 2 0 472.37 449.66 19.28 o 4 2 0 229.25 182.51 5.40 o 5 2 0 108.93 100.26 3.38 o 6 2 0 33.16 33.09 2.91 o 7 2 0 27.95 24.69 1.84 o 0 4 0 38.70 42.14 1.95 o 1 4 0 652.27 621.23 13.09 o 2 4 0 4.98 4.48 0.33 o 3 4 0 94.18 76.21 2.07 o 4 4 0 1.39 1.63 0.38 o 5 4 0 9.57 8.51 0.75 o 6 4 0 2.63 1.23 0.98 o 7 4 0 1.01 1.55 1.01 o 8 4 0 0.89 1.84 1.29 o 0 6 0 41.43 56.67 1.90 o 1 6 0 230.35 227.16 5.74 o 2 6 0 27.37 34.13 0.96 o 3 6 0 61.94 65.51 1.69 o 4 6 0 10.15 12.73 0.69 o 5 6 0 23.59 26.55 1.10 o 6 6 0 3.05 4.50 0.58 o 7 6 0 7.47 8.00 1.11 o 0 8 0 567.86 624.08 20.65 o 1 8 0 395.66 480.54 18.48 o 2 8 0 285.40 293.20 7.41 o 3 8 0 100.15 100.52 2.74 o 4 8 0 48.83 50.70 2.14 o 5 8 0 3.20 2.87 0.61 o 6 8 0 4.74 6.31 0.93 o 7 8 0 0.27 1.59 2.27 o 0 10 0 491.50 563.64 19.53 o 1 10 0 152.12 150.87 4.44 o 2 10 0 325.29 341.07 10.25 o 3 10 0 46.25 41.29 1.39 o 4 10 0 125.95 128.40 3.53 o 5 10 0 3.56 3.42 0.67 o 6 10 0 37.56 35.88 1.60 o 0 12 0 121.00 119.93 4.72 o 1 12 0 150.22 151.57 5.42 o 2 12 0 63.26 61.94 1.91 o 3 12 0 89.10 83.87 2.47 o 4 12 0 10.43 12.96 0.88 o 5 12 0 31.57 31.07 1.24 o 0 14 0 42.69 54.05 3.18 o 1 14 0 4.91 4.78 0.99 o 2 14 0 30.79 33.65 2.48 o 3 14 0 0.30 1.98 0.65 o 4 14 0 14.30 15.34 0.90 o 0 16 0 298.86 322.60 15.21 o 1 16 0 6.72 9.10 1.20 o 2 16 0 231.77 223.68 10.74 o 1 0 1 3282.78 2991.94 101.97 o 3 0 1 718.76 752.91 19.55 o 5 0 1 203.80 192.48 7.96 o 0 1 1 18.41 18.83 0.48 o 1 1 1 224.62 209.92 5.06 o 2 1 1 16.54 15.74 1.51 o 3 1 1 73.11 62.31 1.44 o 4 1 1 6.32 6.74 1.25 o 5 1 1 3.95 3.58 0.46 o 6 1 1 1.21 2.69 0.67 o 7 1 1 0.01 0.32 0.63 o 0 2 1 1294.30 1326.63 30.30 o 1 2 1 259.18 236.70 5.14 o 2 2 1 553.54 521.37 8.56 o 3 2 1 119.91 103.14 2.60 o 4 2 1 133.57 128.32 3.39 o 5 2 1 19.84 16.83 0.62 o 6 2 1 35.29 37.25 1.18 o 7 2 1 2.52 4.29 0.84 o 0 3 1 5.27 6.46 0.36 o 1 3 1 2052.82 2194.36 50.35 o 2 3 1 0.40 2.04 0.18 o 3 3 1 540.06 519.44 8.67 o 4 3 1 1.23 0.45 0.24 o 5 3 1 51.14 47.40 0.99 o 6 3 1 0.00 -0.45 0.45 o 7 3 1 2.80 3.61 0.79 o 8 3 1 0.03 1.49 1.60 o 0 4 1 480.96 554.73 12.67 o 1 4 1 3451.31 3740.03 61.81 o 2 4 1 221.74 216.94 3.53 o 3 4 1 752.42 694.40 11.62 o 4 4 1 15.34 11.41 0.38 o 5 4 1 90.60 80.27 1.67 o 6 4 1 0.08 -0.34 0.39 o 7 4 1 10.27 8.09 0.58 o 0 5 1 374.92 470.57 13.36 o 1 5 1 1849.47 2112.88 34.93 o 2 5 1 128.00 133.61 2.14 o 3 5 1 484.24 457.25 7.95 o 4 5 1 8.17 9.04 0.43 o 5 5 1 64.60 63.09 1.33 o 6 5 1 0.13 -0.41 0.52 o 7 5 1 6.57 8.75 0.68 o 0 6 1 413.94 461.16 9.68 o 1 6 1 98.00 120.62 1.95 o 2 6 1 205.48 202.68 3.32 o 3 6 1 63.14 67.18 1.20 o 4 6 1 14.02 11.28 0.47 o 5 6 1 23.29 23.57 0.66 o 6 6 1 0.98 0.78 0.43 o 7 6 1 5.28 7.35 0.78 o 0 7 1 626.78 721.29 15.17 o 1 7 1 443.57 509.03 7.95 o 2 7 1 295.35 304.26 5.34 o 3 7 1 157.92 146.15 2.70 o 4 7 1 60.23 54.93 1.17 o 5 7 1 27.46 23.60 0.80 o 6 7 1 13.20 11.92 0.58 o 7 7 1 3.11 5.27 1.02 o 0 8 1 333.86 341.97 7.33 o 1 8 1 20.84 18.78 0.43 o 2 8 1 166.76 157.81 2.93 o 3 8 1 7.96 8.22 0.44 o 4 8 1 34.96 34.12 0.86 o 5 8 1 2.00 2.74 0.47 o 6 8 1 6.10 7.22 0.57 o 7 8 1 0.34 0.76 1.54 o 0 9 1 22.51 27.34 0.80 o 1 9 1 35.55 35.48 0.72 o 2 9 1 33.65 34.52 0.93 o 3 9 1 28.53 26.42 0.75 o 4 9 1 30.91 27.75 0.75 o 5 9 1 17.03 17.35 0.72 o 6 9 1 12.21 11.54 0.55 o 0 10 1 184.48 192.90 4.24 o 1 10 1 465.87 517.56 11.16 o 2 10 1 91.97 93.71 1.87 o 3 10 1 217.84 218.43 4.57 o 4 10 1 14.74 15.89 0.87 o 5 10 1 67.42 69.11 1.64 o 6 10 1 1.16 1.23 0.51 o 0 11 1 0.40 0.40 0.37 o 1 11 1 861.02 928.80 21.18 o 2 11 1 2.12 1.97 0.35 o 3 11 1 402.86 390.91 6.98 o 4 11 1 3.90 3.57 0.51 o 5 11 1 104.56 102.56 3.06 o 6 11 1 1.92 1.99 1.22 o 0 12 1 209.18 224.64 6.61 o 1 12 1 7.19 10.68 0.54 o 2 12 1 153.44 163.83 3.87 o 3 12 1 0.05 0.61 0.36 o 4 12 1 61.77 58.25 1.97 o 5 12 1 0.84 0.98 0.63 o 0 13 1 17.15 18.17 1.02 o 1 13 1 51.54 52.37 1.46 o 2 13 1 14.51 15.02 0.68 o 3 13 1 23.81 26.40 0.86 o 4 13 1 8.98 9.58 0.67 o 5 13 1 6.50 10.16 1.75 o 0 14 1 31.20 29.98 1.61 o 1 14 1 341.21 340.47 7.40 o 2 14 1 21.83 23.59 0.85 o 3 14 1 142.99 136.94 2.86 o 4 14 1 7.84 10.58 0.66 o 0 15 1 3.96 6.86 1.23 o 1 15 1 82.19 81.46 2.26 o 2 15 1 2.31 3.63 0.53 o 3 15 1 35.93 36.46 1.64 o 0 16 1 23.30 23.31 1.90 o 1 16 1 45.68 51.45 1.66 o 2 16 1 19.40 16.98 1.55 o 0 0 2 971.99 876.89 26.21 o 2 0 2 358.20 328.50 7.46 o 4 0 2 39.10 36.67 1.11 o 6 0 2 4.16 3.54 0.77 o 8 0 2 0.58 3.04 1.01 o 0 1 2 147.84 159.36 3.89 o 1 1 2 162.07 176.67 2.93 o 2 1 2 134.06 136.14 2.52 o 3 1 2 62.09 61.68 1.75 o 4 1 2 26.63 19.99 0.47 o 5 1 2 9.88 9.43 0.44 o 6 1 2 0.53 -0.49 0.49 o 7 1 2 0.99 0.66 0.56 o 0 2 2 1446.84 1594.16 33.47 o 1 2 2 128.88 117.86 1.84 o 2 2 2 641.99 646.61 10.68 o 3 2 2 41.93 30.66 0.60 o 4 2 2 87.30 82.21 2.00 o 5 2 2 6.22 5.22 0.45 o 6 2 2 7.06 7.23 0.53 o 7 2 2 0.58 1.17 0.58 o 8 2 2 0.46 1.67 1.15 o 0 3 2 313.62 328.95 6.95 o 1 3 2 877.95 911.97 15.48 o 2 3 2 199.48 203.25 4.16 o 3 3 2 134.10 139.35 2.30 o 4 3 2 38.11 36.82 0.89 o 5 3 2 11.99 12.95 0.50 o 6 3 2 2.61 2.56 0.54 o 7 3 2 1.59 1.59 0.72 o 8 3 2 0.18 0.31 0.71 o 0 4 2 27.62 33.49 0.81 o 1 4 2 2112.14 2192.29 36.02 o 2 4 2 4.62 5.84 0.27 o 3 4 2 517.90 492.37 7.89 o 4 4 2 3.07 3.21 0.28 o 5 4 2 64.31 60.14 2.19 o 6 4 2 5.01 5.43 0.64 o 7 4 2 7.15 7.06 0.66 o 0 5 2 8.89 8.33 0.36 o 1 5 2 674.69 754.83 12.04 o 2 5 2 6.40 7.89 0.31 o 3 5 2 91.82 85.74 1.55 o 4 5 2 0.41 0.97 0.27 o 5 5 2 2.30 3.29 0.43 o 6 5 2 0.15 0.27 0.49 o 7 5 2 0.06 0.30 0.46 o 0 6 2 1704.44 1997.43 45.18 o 1 6 2 950.15 1060.89 17.81 o 2 6 2 913.04 983.21 16.22 o 3 6 2 303.54 306.93 5.19 o 4 6 2 198.02 201.39 3.51 o 5 6 2 51.85 52.46 1.96 o 6 6 2 30.02 31.73 1.11 o 7 6 2 6.96 7.54 0.68 o 0 7 2 55.06 63.48 1.92 o 1 7 2 277.75 302.18 5.10 o 2 7 2 32.82 34.36 0.74 o 3 7 2 70.13 72.19 1.43 o 4 7 2 8.25 8.48 0.45 o 5 7 2 18.22 18.60 0.80 o 6 7 2 1.26 2.13 0.56 o 7 7 2 5.71 4.25 0.65 o 0 8 2 484.05 485.86 12.52 o 1 8 2 64.59 79.91 1.42 o 2 8 2 275.89 274.89 4.87 o 3 8 2 15.65 16.77 0.54 o 4 8 2 58.50 58.75 1.39 o 5 8 2 1.21 0.82 0.41 o 6 8 2 5.73 7.56 0.78 o 7 8 2 0.04 -0.65 0.65 o 0 9 2 113.54 109.56 2.78 o 1 9 2 22.22 22.43 0.57 o 2 9 2 88.16 78.99 1.50 o 3 9 2 37.57 36.27 0.88 o 4 9 2 49.16 47.28 1.22 o 5 9 2 23.98 23.29 0.81 o 6 9 2 19.63 19.73 1.09 o 0 10 2 876.67 932.42 21.34 o 1 10 2 344.40 326.92 5.35 o 2 10 2 564.18 574.44 9.73 o 3 10 2 121.50 120.51 2.33 o 4 10 2 171.48 165.64 4.07 o 5 10 2 20.06 22.42 0.81 o 6 10 2 30.77 31.27 1.07 o 0 11 2 870.07 849.89 21.06 o 1 11 2 133.20 126.13 2.39 o 2 11 2 600.91 597.42 13.36 o 3 11 2 74.23 72.18 1.53 o 4 11 2 215.72 200.37 5.88 o 5 11 2 22.06 22.24 1.04 o 6 11 2 49.25 50.11 3.15 o 0 12 2 201.69 219.54 6.45 o 1 12 2 3.91 4.19 0.64 o 2 12 2 125.68 132.98 3.87 o 3 12 2 1.17 1.86 0.38 o 4 12 2 34.69 37.39 1.24 o 5 12 2 0.05 0.92 0.43 o 0 13 2 53.13 51.68 1.93 o 1 13 2 66.88 58.18 1.45 o 2 13 2 30.88 29.67 1.02 o 3 13 2 37.58 35.17 1.50 o 4 13 2 5.29 6.07 0.60 o 5 13 2 13.69 14.10 1.81 o 0 14 2 14.71 16.05 0.99 o 1 14 2 5.64 6.08 0.54 o 2 14 2 6.13 8.99 0.62 o 3 14 2 1.14 1.60 0.41 o 4 14 2 0.11 1.25 0.55 o 0 15 2 68.35 70.45 2.89 o 1 15 2 2.52 2.56 0.51 o 2 15 2 46.60 49.16 1.97 o 3 15 2 1.29 1.24 1.22 o 0 16 2 0.69 0.26 0.63 o 1 16 2 18.53 20.64 0.99 o 2 16 2 0.66 1.55 1.18 o 1 0 3 8216.18 8458.30 201.77 o 3 0 3 1762.15 1634.61 42.12 o 5 0 3 213.91 199.97 7.99 o 7 0 3 26.95 25.01 1.31 o 0 1 3 75.26 76.60 1.68 o 1 1 3 925.78 984.85 16.03 o 2 1 3 34.64 31.29 0.63 o 3 1 3 240.51 240.11 4.18 o 4 1 3 7.18 6.13 0.33 o 5 1 3 15.83 15.08 0.60 o 6 1 3 1.34 0.21 0.43 o 7 1 3 0.14 -0.45 0.52 o 0 2 3 0.29 -0.07 0.15 o 1 2 3 320.90 359.10 6.67 o 2 2 3 0.03 -0.04 0.14 o 3 2 3 23.53 24.31 0.84 o 4 2 3 3.32 4.22 0.36 o 5 2 3 0.10 0.47 0.41 o 6 2 3 6.26 6.25 0.43 o 7 2 3 0.70 -0.15 0.70 o 0 3 3 23.93 29.19 0.72 o 1 3 3 209.74 234.89 3.52 o 2 3 3 7.43 8.23 0.29 o 3 3 3 40.76 38.57 0.82 o 4 3 3 2.10 2.04 0.36 o 5 3 3 3.60 4.75 0.69 o 6 3 3 1.52 1.66 0.42 o 7 3 3 0.14 -0.66 0.81 o 0 4 3 172.68 181.33 3.90 o 1 4 3 1189.62 1315.80 20.08 o 2 4 3 52.13 43.74 0.84 o 3 4 3 419.56 416.29 6.69 o 4 4 3 0.48 0.77 0.29 o 5 4 3 68.99 67.61 1.50 o 6 4 3 1.07 1.86 0.45 o 7 4 3 7.95 11.04 0.99 o 0 5 3 37.49 36.67 0.98 o 1 5 3 795.35 825.70 12.26 o 2 5 3 35.49 42.63 0.81 o 3 5 3 280.56 266.66 4.51 o 4 5 3 15.25 18.89 0.59 o 5 5 3 46.44 39.65 1.23 o 6 5 3 3.08 4.31 0.58 o 7 5 3 5.05 5.18 0.71 o 0 6 3 207.70 257.96 5.50 o 1 6 3 215.01 274.09 4.34 o 2 6 3 134.79 152.05 2.62 o 3 6 3 93.25 102.07 1.83 o 4 6 3 30.54 28.66 0.79 o 5 6 3 26.63 28.60 0.91 o 6 6 3 2.48 3.20 0.55 o 7 6 3 5.47 8.40 0.71 o 0 7 3 46.61 43.38 1.09 o 1 7 3 445.03 480.31 8.05 o 2 7 3 16.01 17.36 0.48 o 3 7 3 133.21 141.41 2.48 o 4 7 3 1.67 3.19 0.45 o 5 7 3 17.45 18.39 0.78 o 6 7 3 0.51 0.60 0.51 o 7 7 3 1.43 1.73 0.81 o 0 8 3 173.44 174.48 4.65 o 1 8 3 33.62 30.51 0.65 o 2 8 3 93.49 92.76 1.68 o 3 8 3 8.46 9.03 0.46 o 4 8 3 12.47 11.28 0.52 o 5 8 3 0.96 0.57 0.58 o 6 8 3 0.13 0.42 0.46 o 0 9 3 46.75 51.22 1.55 o 1 9 3 5.27 4.43 0.30 o 2 9 3 12.71 13.20 0.50 o 3 9 3 7.23 6.41 0.45 o 4 9 3 0.16 -0.41 0.41 o 5 9 3 6.38 6.99 0.69 o 6 9 3 1.60 1.12 0.46 o 0 10 3 61.03 57.49 1.73 o 1 10 3 56.58 42.50 0.87 o 2 10 3 31.05 30.11 0.78 o 3 10 3 15.45 15.64 0.61 o 4 10 3 3.01 2.27 0.47 o 5 10 3 1.88 3.36 0.63 o 6 10 3 0.02 -0.44 0.72 o 0 11 3 18.48 12.06 0.66 o 1 11 3 20.37 15.50 0.56 o 2 11 3 19.27 15.35 0.54 o 3 11 3 17.32 15.58 0.61 o 4 11 3 13.33 11.34 0.55 o 5 11 3 8.80 10.02 0.69 o 0 12 3 76.62 58.30 1.78 o 1 12 3 82.83 77.68 1.69 o 2 12 3 54.24 46.38 1.38 o 3 12 3 31.40 31.18 1.18 o 4 12 3 19.70 17.70 0.72 o 5 12 3 6.12 8.31 0.84 o 0 13 3 7.46 5.86 0.63 o 1 13 3 92.17 86.91 1.88 o 2 13 3 5.27 5.35 0.54 o 3 13 3 43.84 36.66 1.11 o 4 13 3 2.12 2.50 0.51 o 0 14 3 147.17 145.29 4.47 o 1 14 3 15.60 14.83 0.68 o 2 14 3 94.44 90.89 2.40 o 3 14 3 8.72 8.97 0.64 o 4 14 3 27.07 28.97 1.76 o 0 15 3 39.25 33.95 1.86 o 1 15 3 1.87 3.08 0.48 o 2 15 3 25.04 23.79 1.48 o 3 15 3 3.27 6.48 1.58 o 0 16 3 4.51 9.74 1.57 o 1 16 3 3.41 5.30 1.36 o 0 0 4 37.00 44.31 1.47 o 2 0 4 28.30 24.62 1.13 o 4 0 4 0.06 1.04 0.38 o 6 0 4 11.13 10.67 0.86 o 0 1 4 522.58 533.04 12.02 o 1 1 4 1707.59 1787.27 29.31 o 2 1 4 248.39 241.28 4.12 o 3 1 4 508.34 484.76 8.54 o 4 1 4 35.42 38.55 0.92 o 5 1 4 73.62 70.81 1.70 o 6 1 4 2.75 3.62 0.59 o 7 1 4 7.73 11.17 1.79 o 0 2 4 1020.99 1108.88 23.25 o 1 2 4 315.03 354.90 5.63 o 2 2 4 411.50 403.48 7.16 o 3 2 4 133.22 143.60 2.77 o 4 2 4 44.29 40.80 1.02 o 5 2 4 48.00 53.42 1.25 o 6 2 4 2.37 2.67 0.43 o 7 2 4 12.83 14.47 1.09 o 0 3 4 1.93 1.48 0.60 o 1 3 4 39.52 37.01 0.67 o 2 3 4 0.44 0.56 0.17 o 3 3 4 13.60 16.01 0.48 o 4 3 4 0.10 0.20 0.32 o 5 3 4 1.93 2.52 0.43 o 6 3 4 0.22 0.40 0.53 o 7 3 4 0.08 1.43 0.78 o 0 4 4 295.75 259.89 5.53 o 1 4 4 497.03 544.17 8.34 o 2 4 4 109.50 91.29 1.67 o 3 4 4 159.71 155.05 3.02 o 4 4 4 8.98 8.87 0.44 o 5 4 4 19.37 18.09 0.65 o 6 4 4 0.49 0.75 0.51 o 7 4 4 1.68 1.60 0.64 o 0 5 4 559.85 602.15 12.63 o 1 5 4 2.19 2.14 0.19 o 2 5 4 319.46 329.08 5.55 o 3 5 4 0.42 0.54 0.28 o 4 5 4 80.89 76.79 1.72 o 5 5 4 0.01 -0.10 0.39 o 6 5 4 14.63 14.86 0.82 o 7 5 4 0.00 1.02 0.70 o 0 6 4 2.76 5.79 0.40 o 1 6 4 280.24 308.40 4.79 o 2 6 4 0.40 1.10 0.24 o 3 6 4 67.95 71.10 1.47 o 4 6 4 0.02 0.02 0.33 o 5 6 4 0.89 0.76 0.40 o 6 6 4 0.00 0.13 0.49 o 7 6 4 1.01 1.61 0.96 o 0 7 4 0.01 0.55 0.29 o 1 7 4 47.66 44.74 0.87 o 2 7 4 0.61 1.41 0.25 o 3 7 4 25.73 25.50 0.66 o 4 7 4 1.74 1.57 0.50 o 5 7 4 10.64 11.89 0.79 o 6 7 4 0.91 1.05 0.88 o 0 8 4 25.11 20.64 0.79 o 1 8 4 28.67 22.35 0.55 o 2 8 4 17.49 15.58 0.50 o 3 8 4 7.50 7.29 0.39 o 4 8 4 7.84 8.36 0.53 o 5 8 4 1.86 2.40 0.49 o 6 8 4 2.69 4.93 0.75 o 0 9 4 5.15 6.11 0.52 o 1 9 4 185.80 180.51 3.03 o 2 9 4 4.87 6.19 0.39 o 3 9 4 50.43 51.36 1.19 o 4 9 4 3.21 4.32 0.59 o 5 9 4 3.65 4.54 0.50 o 6 9 4 1.14 1.42 0.50 o 0 10 4 295.74 261.92 6.64 o 1 10 4 29.52 26.08 0.66 o 2 10 4 180.47 155.57 2.98 o 3 10 4 7.38 7.93 0.48 o 4 10 4 51.51 47.09 1.38 o 5 10 4 0.87 1.41 0.60 o 0 11 4 51.43 53.05 2.02 o 1 11 4 12.42 13.08 0.49 o 2 11 4 36.15 39.06 1.07 o 3 11 4 5.81 7.41 0.50 o 4 11 4 13.52 14.98 0.76 o 5 11 4 1.88 2.88 0.70 o 0 12 4 10.53 8.92 0.67 o 1 12 4 104.00 94.10 2.00 o 2 12 4 3.49 3.84 0.42 o 3 12 4 57.78 48.82 1.72 o 4 12 4 0.02 1.03 0.43 o 0 13 4 71.09 58.32 2.04 o 1 13 4 5.83 9.89 0.49 o 2 13 4 48.73 39.37 1.20 o 3 13 4 4.57 6.17 0.58 o 4 13 4 17.10 17.92 2.25 o 0 14 4 89.52 85.38 2.85 o 1 14 4 0.45 2.91 0.58 o 2 14 4 50.77 45.73 1.46 o 3 14 4 0.41 0.77 0.53 o 0 15 4 98.77 106.88 3.47 o 1 15 4 0.83 0.91 0.62 o 2 15 4 75.73 82.90 2.77 o 0 16 4 33.97 33.97 2.64 o 1 0 5 1221.22 1250.90 29.80 o 3 0 5 350.22 351.74 9.32 o 5 0 5 65.82 62.11 2.28 o 7 0 5 11.66 10.87 1.57 o 0 1 5 276.88 338.04 7.19 o 1 1 5 4.51 5.20 0.27 o 2 1 5 182.20 196.09 3.59 o 3 1 5 5.87 5.81 0.32 o 4 1 5 57.24 52.10 1.12 o 5 1 5 0.68 0.44 0.45 o 6 1 5 10.77 12.00 0.84 o 7 1 5 0.00 -0.84 0.84 o 0 2 5 196.15 200.01 4.30 o 1 2 5 396.76 406.80 6.45 o 2 2 5 109.47 113.79 2.14 o 3 2 5 105.76 96.05 1.94 o 4 2 5 31.67 34.20 0.90 o 5 2 5 16.74 14.78 0.62 o 6 2 5 7.82 8.00 0.56 o 7 2 5 2.19 2.36 0.68 o 0 3 5 1102.50 1090.23 22.80 o 1 3 5 14.32 18.30 0.40 o 2 3 5 541.98 528.88 9.38 o 3 3 5 2.83 6.19 0.41 o 4 3 5 94.29 92.33 1.93 o 5 3 5 0.61 1.48 0.44 o 6 3 5 11.27 11.19 0.58 o 7 3 5 0.09 0.00 0.72 o 0 4 5 40.68 44.67 1.09 o 1 4 5 1.48 2.98 0.21 o 2 4 5 24.50 28.34 0.73 o 3 4 5 0.00 0.03 0.32 o 4 4 5 2.86 4.78 0.41 o 5 4 5 1.42 1.01 0.45 o 6 4 5 0.04 0.10 0.66 o 0 5 5 162.89 172.84 3.74 o 1 5 5 170.76 164.62 2.62 o 2 5 5 51.34 56.50 1.15 o 3 5 5 39.48 37.84 0.99 o 4 5 5 0.21 1.20 0.49 o 5 5 5 0.90 0.55 0.45 o 6 5 5 1.63 2.19 0.66 o 7 5 5 0.31 2.01 0.91 o 0 6 5 1657.73 1628.48 34.01 o 1 6 5 75.08 75.50 1.29 o 2 6 5 1015.01 973.56 16.62 o 3 6 5 34.93 36.95 0.95 o 4 6 5 301.53 302.62 5.84 o 5 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47.67 3.88 o 1 0 9 51.84 45.10 1.95 o 3 0 9 25.78 21.16 1.00 o 5 0 9 5.90 8.53 1.82 o 0 1 9 185.65 163.25 4.97 o 1 1 9 109.44 107.74 2.58 o 2 1 9 128.74 114.07 3.21 o 3 1 9 34.23 32.15 0.95 o 4 1 9 46.96 43.70 1.31 o 5 1 9 2.77 3.20 1.57 o 0 2 9 21.28 17.09 0.93 o 1 2 9 7.11 10.16 0.52 o 2 2 9 17.91 14.34 0.72 o 3 2 9 1.05 2.67 0.40 o 4 2 9 9.42 7.55 0.51 o 5 2 9 0.00 1.77 1.98 o 0 3 9 43.91 41.36 1.84 o 1 3 9 7.22 6.40 0.53 o 2 3 9 31.11 28.91 1.05 o 3 3 9 4.45 5.60 0.56 o 4 3 9 11.03 10.48 0.60 o 0 4 9 108.36 110.56 4.06 o 1 4 9 94.08 87.03 2.37 o 2 4 9 67.22 68.53 1.94 o 3 4 9 49.27 45.38 1.18 o 4 4 9 18.04 22.03 0.88 o 5 4 9 16.15 16.56 1.93 o 0 5 9 9.51 11.62 0.96 o 1 5 9 21.10 20.17 1.06 o 2 5 9 8.66 9.91 0.61 o 3 5 9 9.66 11.23 0.78 o 4 5 9 4.95 7.33 0.79 o 0 6 9 31.92 29.00 1.93 o 1 6 9 57.23 59.85 1.95 o 2 6 9 17.64 18.34 0.87 o 3 6 9 28.52 31.41 1.06 o 4 6 9 2.14 3.07 0.68 o 0 7 9 143.38 146.70 9.79 o 1 7 9 65.19 75.04 2.66 o 2 7 9 92.04 92.24 2.75 o 3 7 9 31.25 38.36 1.22 o 4 7 9 28.47 28.43 1.20 o 0 8 9 0.84 2.77 0.97 o 1 8 9 42.84 43.23 1.80 o 2 8 9 1.24 3.59 0.56 o 3 8 9 19.54 22.07 0.91 o 0 9 9 97.06 111.01 7.51 o 1 9 9 0.10 0.99 0.83 o 2 9 9 59.97 68.28 3.20 o 3 9 9 0.37 0.94 0.76 o 0 10 9 0.37 1.16 0.79 o 1 10 9 4.76 6.42 1.08 o 0 0 10 0.71 1.13 0.83 o 2 0 10 0.20 0.40 0.74 o 0 1 10 43.74 45.55 1.73 o 1 1 10 1.15 1.45 0.40 o 2 1 10 29.01 32.40 1.12 o 3 1 10 0.25 1.29 0.55 o 0 2 10 1.92 0.74 0.46 o 1 2 10 85.11 76.98 1.98 o 2 2 10 0.17 0.06 0.63 o 3 2 10 37.43 36.17 1.36 o 4 2 10 0.88 4.00 1.48 o 0 3 10 26.32 25.22 1.34 o 1 3 10 124.32 124.14 3.55 o 2 3 10 19.81 18.08 0.80 o 3 3 10 50.66 51.31 1.77 o 4 3 10 8.14 6.79 1.48 o 0 4 10 5.82 8.99 0.99 o 1 4 10 137.52 140.51 4.46 o 2 4 10 2.88 4.75 0.52 o 3 4 10 75.77 73.89 2.30 o 4 4 10 0.24 -1.01 1.54 o 0 5 10 72.16 74.94 3.83 o 1 5 10 17.78 18.23 0.90 o 2 5 10 46.28 46.61 1.83 o 3 5 10 2.29 4.83 0.64 o 0 6 10 3.16 2.40 1.05 o 1 6 10 27.66 33.43 1.51 o 2 6 10 0.92 1.02 0.57 o 3 6 10 13.29 21.58 1.48 o 0 7 10 69.94 82.60 6.22 o 1 7 10 0.68 1.39 0.55 o 2 7 10 55.62 66.76 3.31 o 0 8 10 1.02 3.34 1.21 o 1 0 11 0.66 0.52 0.68 o 0 1 11 1.53 1.43 1.12 o 1 1 11 0.17 0.84 0.46 o 2 1 11 0.93 0.94 0.61 o 0 2 11 209.16 205.23 7.17 o 1 2 11 42.78 53.49 1.85 o 2 2 11 137.95 130.63 4.21 o 0 3 11 8.44 10.67 0.91 o 1 3 11 2.15 5.83 0.78 o 2 3 11 7.64 8.82 0.75 o 0 4 11 68.84 74.85 4.31 o 1 4 11 16.99 19.39 1.36 o 2 4 11 51.42 55.72 3.85 o 0 5 11 10.93 14.13 2.45 o 1 5 11 10.57 11.20 2.17 o