#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:57:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180870 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/02/2100282.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100282_Fobs loop_ _publ_author_name 'Nichol, Gary S.' 'Clegg, William' _publ_section_title ; A variable-temperature study of a phase transition in barbituric acid dihydrate ; _journal_coeditor_code WS5026 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 464 _journal_page_last 472 _journal_volume 61 _journal_year 2005 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2bc 2a' _symmetry_space_group_name_H-M 'P m n b' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1739 _cell_length_b 12.7594 _cell_length_c 8.8831 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.7501 _cod_data_source_file ws5026230sup14.hkl _cod_data_source_block 230 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 230 in Pmnb' _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' 'x+1/2, -y, -z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y-1/2, -z-1/2' '-x-1/2, y, z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5860.63 5688.82 98.23 o 6 0 0 675.25 610.55 18.80 o 0 2 0 979.31 950.72 17.16 o 1 2 0 2259.60 2114.48 22.33 o 2 2 0 758.86 777.15 7.24 o 3 2 0 473.94 524.51 4.98 o 4 2 0 225.50 204.68 2.15 o 5 2 0 109.95 109.08 1.34 o 6 2 0 32.79 32.07 0.81 o 7 2 0 28.29 25.77 1.04 o 0 4 0 36.46 31.71 1.02 o 1 4 0 622.97 564.64 5.95 o 2 4 0 4.86 4.40 0.18 o 3 4 0 87.59 78.43 0.94 o 4 4 0 1.74 2.88 0.32 o 5 4 0 8.27 8.15 0.46 o 6 4 0 3.08 2.25 0.36 o 7 4 0 0.78 1.26 0.59 o 8 4 0 1.05 3.65 0.57 o 0 6 0 36.00 47.91 0.90 o 1 6 0 223.06 203.97 2.07 o 2 6 0 25.68 33.46 0.50 o 3 6 0 60.63 63.71 0.94 o 4 6 0 10.31 11.87 0.50 o 5 6 0 23.35 26.16 0.73 o 6 6 0 3.12 3.92 0.41 o 7 6 0 7.56 6.67 0.91 o 0 8 0 528.19 498.74 6.79 o 1 8 0 376.27 395.65 3.87 o 2 8 0 267.50 269.72 3.46 o 3 8 0 93.91 94.09 1.53 o 4 8 0 45.85 46.40 1.01 o 5 8 0 2.76 4.22 0.74 o 6 8 0 4.33 5.12 0.54 o 7 8 0 0.31 2.54 0.78 o 0 10 0 457.91 459.91 6.44 o 1 10 0 136.88 126.52 1.66 o 2 10 0 307.63 305.63 3.95 o 3 10 0 41.96 38.98 0.93 o 4 10 0 121.72 121.60 1.98 o 5 10 0 3.25 4.42 0.78 o 6 10 0 36.53 36.25 1.19 o 0 12 0 105.78 104.74 2.35 o 1 12 0 131.56 128.39 2.01 o 2 12 0 55.20 54.91 1.15 o 3 12 0 79.14 77.04 1.46 o 4 12 0 8.79 9.77 0.57 o 5 12 0 28.10 27.68 1.09 o 0 14 0 39.16 43.93 2.29 o 1 14 0 3.78 2.71 0.71 o 2 14 0 28.67 31.56 1.06 o 3 14 0 0.16 1.15 0.42 o 4 14 0 13.71 16.37 0.71 o 0 16 0 247.29 257.37 7.80 o 1 16 0 4.86 6.01 0.76 o 2 16 0 191.25 187.43 6.04 o 1 0 1 3304.32 3154.06 35.01 o 3 0 1 745.43 841.75 10.78 o 5 0 1 213.45 213.31 3.09 o 0 1 1 19.03 18.82 0.27 o 1 1 1 220.98 225.72 1.62 o 2 1 1 16.43 17.10 0.26 o 3 1 1 73.35 67.15 0.61 o 4 1 1 6.07 6.16 0.23 o 5 1 1 4.18 3.58 0.22 o 6 1 1 1.15 1.37 0.45 o 7 1 1 0.02 0.77 0.41 o 0 2 1 1293.04 1147.42 13.01 o 1 2 1 256.20 242.14 1.83 o 2 2 1 557.39 580.44 4.03 o 3 2 1 117.67 111.60 0.92 o 4 2 1 135.09 146.09 1.14 o 5 2 1 19.63 17.26 0.37 o 6 2 1 35.47 36.33 0.72 o 7 2 1 2.61 5.28 0.46 o 0 3 1 5.41 5.67 0.28 o 1 3 1 2021.31 2168.99 15.46 o 2 3 1 0.25 0.05 0.09 o 3 3 1 532.75 546.06 3.85 o 4 3 1 0.99 0.42 0.13 o 5 3 1 50.51 47.16 0.60 o 6 3 1 0.00 -0.05 0.22 o 7 3 1 2.87 3.96 0.47 o 8 3 1 0.03 2.84 0.57 o 0 4 1 472.49 501.64 7.52 o 1 4 1 3395.53 3405.56 27.44 o 2 4 1 214.32 216.97 1.68 o 3 4 1 736.87 708.59 5.52 o 4 4 1 14.22 11.09 0.27 o 5 4 1 88.84 79.50 0.91 o 6 4 1 0.08 0.38 0.26 o 7 4 1 10.27 8.80 0.41 o 0 5 1 366.04 432.34 4.65 o 1 5 1 1814.40 1929.75 12.63 o 2 5 1 125.30 130.72 1.04 o 3 5 1 465.86 469.05 3.53 o 4 5 1 7.72 7.99 0.28 o 5 5 1 60.64 57.52 0.80 o 6 5 1 0.06 -0.03 0.23 o 7 5 1 6.04 6.70 0.37 o 0 6 1 401.83 420.06 4.51 o 1 6 1 96.35 110.89 0.86 o 2 6 1 196.24 191.98 1.47 o 3 6 1 63.50 67.78 0.70 o 4 6 1 12.35 10.75 0.35 o 5 6 1 23.22 24.48 0.49 o 6 6 1 1.20 1.28 0.27 o 7 6 1 5.18 7.35 0.44 o 0 7 1 603.11 641.94 6.33 o 1 7 1 422.98 456.84 3.11 o 2 7 1 285.08 291.12 2.28 o 3 7 1 150.24 140.91 1.33 o 4 7 1 58.43 56.32 0.78 o 5 7 1 25.18 21.79 0.49 o 6 7 1 12.77 10.55 0.43 o 7 7 1 2.62 4.17 0.63 o 0 8 1 312.80 300.37 3.00 o 1 8 1 20.08 17.25 0.28 o 2 8 1 155.05 141.89 1.52 o 3 8 1 7.93 7.85 0.32 o 4 8 1 32.08 31.49 0.58 o 5 8 1 1.92 2.76 0.32 o 6 8 1 5.62 6.25 0.36 o 7 8 1 0.30 -0.07 0.89 o 0 9 1 21.34 22.43 0.47 o 1 9 1 31.95 30.57 0.42 o 2 9 1 31.95 32.55 0.51 o 3 9 1 26.55 25.47 0.52 o 4 9 1 29.25 27.12 0.54 o 5 9 1 15.89 15.66 0.49 o 6 9 1 11.55 11.99 0.46 o 0 10 1 165.65 163.31 1.83 o 1 10 1 436.46 445.71 3.63 o 2 10 1 81.19 79.96 0.99 o 3 10 1 207.06 207.25 2.06 o 4 10 1 12.43 14.41 0.45 o 5 10 1 64.70 62.14 1.00 o 6 10 1 0.92 3.14 0.45 o 0 11 1 0.40 0.19 0.29 o 1 11 1 785.43 777.54 6.12 o 2 11 1 2.08 1.71 0.26 o 3 11 1 366.08 367.41 3.37 o 4 11 1 3.73 4.77 0.33 o 5 11 1 95.12 91.12 1.31 o 6 11 1 1.78 4.74 1.17 o 0 12 1 187.34 190.96 3.97 o 1 12 1 5.30 7.35 0.36 o 2 12 1 137.58 139.41 1.72 o 3 12 1 0.01 0.05 0.24 o 4 12 1 55.12 53.34 0.85 o 5 12 1 0.89 1.51 0.29 o 0 13 1 15.26 15.84 0.95 o 1 13 1 44.19 45.37 0.95 o 2 13 1 12.82 12.97 0.41 o 3 13 1 20.04 22.08 0.54 o 4 13 1 8.01 8.82 0.45 o 5 13 1 5.31 9.20 1.50 o 0 14 1 25.20 28.00 1.36 o 1 14 1 289.46 281.55 3.51 o 2 14 1 17.75 20.33 0.56 o 3 14 1 121.88 121.60 1.53 o 4 14 1 6.41 8.01 0.45 o 0 15 1 3.66 5.06 0.82 o 1 15 1 69.85 68.53 1.50 o 2 15 1 2.23 4.39 0.51 o 3 15 1 30.38 31.03 0.72 o 0 16 1 17.54 18.27 1.16 o 1 16 1 39.84 44.95 1.19 o 2 16 1 14.91 19.19 1.48 o 0 0 2 980.18 907.99 17.84 o 2 0 2 362.26 351.29 3.37 o 4 0 2 40.02 38.58 0.63 o 6 0 2 4.45 4.32 0.49 o 8 0 2 0.66 3.57 1.04 o 0 1 2 154.33 167.97 1.81 o 1 1 2 167.05 180.12 1.59 o 2 1 2 139.43 148.56 1.07 o 3 1 2 61.79 62.09 0.56 o 4 1 2 28.31 22.00 0.33 o 5 1 2 9.56 9.06 0.31 o 6 1 2 0.71 0.36 0.25 o 7 1 2 0.94 2.29 0.93 o 8 1 2 0.00 4.63 1.22 o 0 2 2 1428.82 1548.86 14.30 o 1 2 2 131.00 120.07 1.03 o 2 2 2 630.29 663.87 4.40 o 3 2 2 41.58 33.13 0.39 o 4 2 2 83.71 84.13 0.78 o 5 2 2 5.91 5.19 0.29 o 6 2 2 6.50 6.42 0.35 o 7 2 2 0.51 1.26 0.31 o 8 2 2 0.41 2.96 0.51 o 0 3 2 309.48 312.31 2.99 o 1 3 2 865.32 908.82 7.32 o 2 3 2 199.87 211.11 1.57 o 3 3 2 133.07 144.15 1.15 o 4 3 2 39.40 36.41 0.48 o 5 3 2 11.60 12.08 0.35 o 6 3 2 2.99 2.56 0.31 o 7 3 2 1.45 1.31 0.43 o 0 4 2 27.82 31.57 0.49 o 1 4 2 2073.23 2118.87 14.41 o 2 4 2 4.23 4.94 0.19 o 3 4 2 506.08 505.99 3.78 o 4 4 2 3.54 3.38 0.20 o 5 4 2 62.49 56.56 0.78 o 6 4 2 5.32 5.98 0.38 o 7 4 2 6.99 6.48 0.42 o 0 5 2 7.38 8.23 0.28 o 1 5 2 651.48 713.52 4.96 o 2 5 2 5.91 7.30 0.30 o 3 5 2 87.78 84.78 0.82 o 4 5 2 0.42 0.23 0.17 o 5 5 2 1.78 2.56 0.28 o 6 5 2 0.14 0.13 0.27 o 7 5 2 0.16 0.52 0.29 o 0 6 2 1640.90 1830.80 16.84 o 1 6 2 911.42 1005.87 6.92 o 2 6 2 877.31 948.32 6.90 o 3 6 2 290.28 302.52 2.39 o 4 6 2 189.78 196.84 1.79 o 5 6 2 49.23 49.28 0.81 o 6 6 2 28.86 28.10 0.73 o 7 6 2 6.58 7.33 0.43 o 0 7 2 52.48 59.90 0.78 o 1 7 2 265.71 280.56 1.98 o 2 7 2 31.80 31.27 0.44 o 3 7 2 68.19 70.20 1.24 o 4 7 2 7.76 6.92 0.31 o 5 7 2 17.82 16.06 0.47 o 6 7 2 1.01 2.06 0.36 o 7 7 2 5.53 5.64 0.59 o 0 8 2 464.66 444.72 4.32 o 1 8 2 61.19 72.78 0.75 o 2 8 2 263.76 255.37 2.20 o 3 8 2 14.29 15.71 0.38 o 4 8 2 55.20 55.70 0.79 o 5 8 2 1.01 0.97 0.26 o 6 8 2 5.31 6.69 0.37 o 7 8 2 0.02 1.00 0.66 o 0 9 2 103.19 95.74 1.18 o 1 9 2 19.86 19.68 0.37 o 2 9 2 81.44 75.11 0.86 o 3 9 2 34.66 32.60 0.58 o 4 9 2 45.84 44.55 0.78 o 5 9 2 22.47 21.29 0.56 o 6 9 2 18.15 17.38 0.55 o 0 10 2 812.11 835.59 8.70 o 1 10 2 310.61 286.85 2.32 o 2 10 2 521.35 519.04 4.21 o 3 10 2 108.03 105.29 1.23 o 4 10 2 157.58 149.85 1.76 o 5 10 2 17.39 19.63 0.56 o 6 10 2 28.21 29.40 0.73 o 0 11 2 788.98 752.50 8.97 o 1 11 2 124.31 105.91 1.12 o 2 11 2 544.21 531.20 4.63 o 3 11 2 69.24 63.40 0.90 o 4 11 2 196.16 188.72 2.31 o 5 11 2 20.35 20.72 0.59 o 6 11 2 45.59 44.86 2.21 o 0 12 2 183.26 185.17 3.11 o 1 12 2 3.35 4.01 0.34 o 2 12 2 113.93 114.26 1.34 o 3 12 2 0.96 1.78 0.26 o 4 12 2 31.23 31.87 0.71 o 5 12 2 0.03 0.84 0.29 o 0 13 2 47.80 44.70 1.29 o 1 13 2 59.69 51.38 0.94 o 2 13 2 27.85 27.61 0.61 o 3 13 2 33.36 29.51 0.63 o 4 13 2 4.87 6.19 0.44 o 5 13 2 12.36 14.35 1.24 o 0 14 2 10.63 11.80 1.26 o 1 14 2 4.54 5.25 0.50 o 2 14 2 4.10 6.28 0.47 o 3 14 2 0.85 1.06 0.32 o 4 14 2 0.01 1.11 0.39 o 0 15 2 56.65 58.56 3.13 o 1 15 2 2.60 3.59 0.46 o 2 15 2 38.69 41.00 0.96 o 3 15 2 1.40 3.47 0.54 o 0 16 2 0.75 -0.56 0.56 o 1 16 2 15.62 19.32 0.82 o 2 16 2 0.72 0.40 0.70 o 1 0 3 8169.85 7859.44 155.74 o 3 0 3 1740.53 1682.79 15.53 o 5 0 3 208.86 201.53 2.77 o 7 0 3 26.18 21.66 1.06 o 0 1 3 75.43 78.55 0.99 o 1 1 3 909.23 983.83 7.05 o 2 1 3 35.02 32.82 0.38 o 3 1 3 235.22 241.98 1.73 o 4 1 3 7.22 5.97 0.23 o 5 1 3 15.75 13.69 0.39 o 6 1 3 1.27 1.77 0.27 o 7 1 3 0.19 0.39 0.31 o 0 2 3 0.31 -0.07 0.11 o 1 2 3 316.22 351.15 3.78 o 2 2 3 0.06 -0.06 0.08 o 3 2 3 22.91 23.96 0.35 o 4 2 3 3.68 4.32 0.23 o 5 2 3 0.12 -0.20 0.21 o 6 2 3 6.50 5.89 0.40 o 7 2 3 0.74 1.37 0.49 o 0 3 3 24.22 28.05 0.43 o 1 3 3 206.15 229.18 1.60 o 2 3 3 7.92 8.36 0.19 o 3 3 3 38.23 36.80 0.43 o 4 3 3 2.18 2.89 0.24 o 5 3 3 2.88 4.03 0.30 o 6 3 3 1.37 1.87 0.42 o 7 3 3 0.06 -0.29 0.29 o 0 4 3 166.37 167.66 1.72 o 1 4 3 1160.85 1280.67 8.38 o 2 4 3 48.52 42.32 0.48 o 3 4 3 407.95 411.23 3.29 o 4 4 3 0.21 0.17 0.18 o 5 4 3 66.24 66.13 0.87 o 6 4 3 1.42 1.71 0.29 o 7 4 3 7.53 9.58 0.69 o 0 5 3 38.51 35.85 0.57 o 1 5 3 765.48 794.31 5.27 o 2 5 3 35.29 41.85 0.49 o 3 5 3 269.05 258.51 2.18 o 4 5 3 15.16 18.18 0.38 o 5 5 3 43.76 36.40 0.68 o 6 5 3 3.36 4.90 0.43 o 7 5 3 4.62 4.88 0.54 o 0 6 3 206.03 247.61 2.50 o 1 6 3 213.69 260.69 1.85 o 2 6 3 133.27 147.55 1.27 o 3 6 3 91.43 98.48 0.96 o 4 6 3 29.93 28.50 0.53 o 5 6 3 26.14 25.96 0.57 o 6 6 3 2.35 3.62 0.46 o 7 6 3 5.43 6.45 0.37 o 0 7 3 44.82 42.59 0.63 o 1 7 3 423.20 448.78 3.58 o 2 7 3 15.57 14.02 0.31 o 3 7 3 124.77 133.87 1.23 o 4 7 3 1.62 2.12 0.27 o 5 7 3 16.34 17.16 0.52 o 6 7 3 0.45 0.23 0.29 o 7 7 3 1.42 1.93 0.76 o 0 8 3 158.97 164.40 1.79 o 1 8 3 31.21 28.22 0.42 o 2 8 3 85.74 85.60 0.87 o 3 8 3 8.41 8.06 0.30 o 4 8 3 11.34 11.43 0.40 o 5 8 3 1.06 1.35 0.30 o 6 8 3 0.11 -0.25 0.25 o 0 9 3 44.47 45.50 0.93 o 1 9 3 4.51 3.82 0.23 o 2 9 3 12.07 12.31 0.33 o 3 9 3 6.63 5.99 0.30 o 4 9 3 0.16 -0.06 0.23 o 5 9 3 5.82 6.54 0.37 o 6 9 3 1.57 2.53 0.65 o 0 10 3 52.61 51.91 1.05 o 1 10 3 49.89 38.28 0.54 o 2 10 3 26.86 26.43 0.52 o 3 10 3 13.69 12.99 0.43 o 4 10 3 2.59 2.90 0.42 o 5 10 3 1.60 3.11 0.38 o 6 10 3 0.02 0.91 0.52 o 0 11 3 19.19 12.10 0.54 o 1 11 3 18.46 14.99 0.43 o 2 11 3 19.65 14.41 0.38 o 3 11 3 16.08 13.46 0.46 o 4 11 3 13.16 11.08 0.42 o 5 11 3 8.58 8.82 0.47 o 0 12 3 66.88 52.59 1.12 o 1 12 3 75.90 69.42 1.01 o 2 12 3 47.62 40.29 0.69 o 3 12 3 29.04 29.18 0.73 o 4 12 3 17.31 16.29 0.49 o 5 12 3 5.60 7.69 0.46 o 0 13 3 6.98 6.31 0.63 o 1 13 3 83.99 78.42 1.12 o 2 13 3 4.94 4.24 0.38 o 3 13 3 39.70 36.46 0.74 o 4 13 3 2.05 3.88 0.31 o 0 14 3 125.41 121.96 2.60 o 1 14 3 13.30 12.10 0.55 o 2 14 3 80.03 79.10 1.29 o 3 14 3 7.33 8.46 0.54 o 4 14 3 22.79 26.25 1.13 o 0 15 3 32.53 30.02 1.33 o 1 15 3 1.69 4.71 0.64 o 2 15 3 20.78 20.67 0.81 o 3 15 3 2.93 6.25 0.58 o 0 16 3 3.74 5.46 0.87 o 1 16 3 1.99 6.11 0.78 o 0 0 4 39.08 43.91 0.82 o 2 0 4 27.04 24.75 0.51 o 4 0 4 0.28 1.61 0.32 o 6 0 4 12.25 11.88 0.69 o 0 1 4 509.89 531.81 7.56 o 1 1 4 1667.07 1788.06 12.23 o 2 1 4 241.89 251.96 1.96 o 3 1 4 491.77 491.80 3.68 o 4 1 4 33.65 36.04 0.53 o 5 1 4 69.77 66.15 0.95 o 6 1 4 2.36 4.27 0.38 o 7 1 4 7.07 7.81 0.48 o 0 2 4 998.06 1104.92 10.86 o 1 2 4 309.65 351.37 2.41 o 2 2 4 402.07 407.58 2.91 o 3 2 4 131.96 146.13 1.34 o 4 2 4 42.81 40.68 0.63 o 5 2 4 47.42 50.86 0.76 o 6 2 4 2.11 2.31 0.32 o 7 2 4 12.67 14.67 0.74 o 0 3 4 0.83 0.49 0.22 o 1 3 4 36.58 34.27 0.45 o 2 3 4 0.12 0.07 0.11 o 3 3 4 12.96 12.36 0.31 o 4 3 4 0.21 0.53 0.22 o 5 3 4 1.99 2.68 0.28 o 6 3 4 0.28 0.22 0.27 o 7 3 4 0.11 0.82 0.30 o 0 4 4 283.14 248.04 2.48 o 1 4 4 487.57 516.35 3.48 o 2 4 4 103.45 86.61 0.77 o 3 4 4 155.65 155.39 1.43 o 4 4 4 8.17 7.72 0.32 o 5 4 4 19.21 17.51 0.45 o 6 4 4 0.44 0.77 0.31 o 7 4 4 1.80 2.36 0.36 o 0 5 4 539.98 562.84 5.37 o 1 5 4 1.66 1.50 0.13 o 2 5 4 305.99 315.87 2.47 o 3 5 4 0.27 0.24 0.19 o 4 5 4 76.47 71.63 0.90 o 5 5 4 0.00 -0.25 0.25 o 6 5 4 13.72 13.14 0.50 o 7 5 4 0.00 1.31 0.41 o 0 6 4 2.56 5.61 0.27 o 1 6 4 266.55 290.17 2.65 o 2 6 4 0.33 1.11 0.16 o 3 6 4 63.17 63.86 0.77 o 4 6 4 0.01 -0.18 0.18 o 5 6 4 0.68 0.64 0.28 o 6 6 4 0.00 0.55 0.26 o 7 6 4 1.08 1.33 0.55 o 0 7 4 0.00 -0.03 0.19 o 1 7 4 46.25 42.86 0.54 o 2 7 4 0.50 1.13 0.18 o 3 7 4 25.46 25.35 0.47 o 4 7 4 1.64 1.93 0.27 o 5 7 4 10.88 10.62 0.44 o 6 7 4 0.88 1.47 0.33 o 0 8 4 23.25 19.67 0.51 o 1 8 4 26.59 20.56 0.39 o 2 8 4 16.98 14.77 0.36 o 3 8 4 6.72 6.42 0.28 o 4 8 4 8.00 8.00 0.39 o 5 8 4 1.63 2.78 0.35 o 6 8 4 2.73 4.81 0.42 o 0 9 4 4.73 5.42 0.42 o 1 9 4 170.10 163.31 1.46 o 2 9 4 4.53 5.14 0.30 o 3 9 4 45.25 45.40 0.71 o 4 9 4 3.07 3.88 0.36 o 5 9 4 3.11 4.31 0.35 o 6 9 4 1.15 1.53 0.39 o 0 10 4 266.74 238.82 3.23 o 1 10 4 25.29 23.50 0.45 o 2 10 4 163.49 145.71 1.54 o 3 10 4 5.93 6.44 0.31 o 4 10 4 46.68 43.20 0.96 o 5 10 4 0.63 1.41 0.30 o 0 11 4 46.06 49.50 1.06 o 1 11 4 11.43 10.82 0.36 o 2 11 4 32.16 33.38 0.62 o 3 11 4 5.42 5.80 0.31 o 4 11 4 11.71 13.35 0.52 o 5 11 4 1.80 3.01 0.47 o 0 12 4 9.79 8.83 0.54 o 1 12 4 91.13 84.47 1.16 o 2 12 4 3.47 4.24 0.36 o 3 12 4 50.80 47.01 0.86 o 4 12 4 0.05 0.19 0.28 o 5 12 4 15.73 16.21 1.42 o 0 13 4 60.79 54.12 1.40 o 1 13 4 5.00 8.31 0.38 o 2 13 4 41.60 35.41 0.86 o 3 13 4 3.81 5.83 0.41 o 4 13 4 14.63 14.65 0.70 o 0 14 4 70.72 70.73 2.10 o 1 14 4 0.68 2.84 0.39 o 2 14 4 39.93 40.46 0.96 o 3 14 4 0.54 2.34 0.63 o 0 15 4 81.49 93.63 2.06 o 1 15 4 0.81 1.85 0.46 o 2 15 4 62.37 71.63 1.55 o 0 16 4 28.26 31.06 1.67 o 1 0 5 1182.23 1244.13 12.52 o 3 0 5 340.30 349.82 4.30 o 5 0 5 64.27 58.80 1.40 o 7 0 5 11.55 9.74 0.77 o 0 1 5 271.01 339.53 3.60 o 1 1 5 4.07 4.99 0.15 o 2 1 5 177.28 196.87 1.61 o 3 1 5 5.68 5.35 0.24 o 4 1 5 54.91 51.81 0.69 o 5 1 5 0.62 0.24 0.25 o 6 1 5 10.12 9.59 0.49 o 7 1 5 0.00 0.45 0.92 o 0 2 5 185.40 195.05 2.01 o 1 2 5 383.48 394.34 2.71 o 2 2 5 104.10 110.54 1.08 o 3 2 5 102.41 94.18 0.99 o 4 2 5 30.45 31.88 0.57 o 5 2 5 16.02 13.15 0.43 o 6 2 5 7.59 7.85 0.39 o 7 2 5 2.03 2.44 0.44 o 0 3 5 1057.58 1028.76 9.60 o 1 3 5 12.91 17.25 0.28 o 2 3 5 520.61 513.30 4.08 o 3 3 5 2.27 4.14 0.26 o 4 3 5 91.09 90.10 1.08 o 5 3 5 0.45 0.99 0.26 o 6 3 5 11.10 9.79 0.38 o 7 3 5 0.05 0.29 0.41 o 0 4 5 40.25 43.39 0.65 o 1 4 5 1.15 3.14 0.20 o 2 4 5 23.68 25.92 0.40 o 3 4 5 0.00 -0.08 0.17 o 4 4 5 2.64 3.79 0.29 o 5 4 5 1.52 1.46 0.26 o 6 4 5 0.04 0.06 0.37 o 0 5 5 157.18 157.65 2.26 o 1 5 5 160.82 153.13 1.26 o 2 5 5 49.61 51.13 0.65 o 3 5 5 36.82 33.72 0.58 o 4 5 5 0.20 0.88 0.25 o 5 5 5 0.73 1.14 0.25 o 6 5 5 1.64 1.35 0.28 o 7 5 5 0.34 2.16 0.88 o 0 6 5 1555.22 1472.18 13.67 o 1 6 5 66.84 70.02 0.70 o 2 6 5 950.70 913.33 7.09 o 3 6 5 31.20 33.90 0.59 o 4 6 5 280.68 271.77 2.56 o 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16.54 15.85 0.62 o 1 13 5 50.96 54.01 1.00 o 2 13 5 12.16 13.22 0.58 o 3 13 5 13.06 14.31 0.64 o 4 13 5 5.47 8.78 0.91 o 0 14 5 3.44 3.97 0.73 o 1 14 5 16.90 19.49 0.68 o 2 14 5 2.52 3.62 0.54 o 0 15 5 0.06 1.73 1.02 o 1 15 5 11.25 13.25 0.76 o 0 0 6 114.81 110.97 1.81 o 2 0 6 51.67 53.95 0.90 o 4 0 6 5.09 6.63 0.42 o 6 0 6 0.08 0.34 0.57 o 0 1 6 313.18 305.60 3.06 o 1 1 6 95.91 86.93 0.85 o 2 1 6 166.31 160.22 1.39 o 3 1 6 23.74 23.12 0.44 o 4 1 6 20.16 18.31 0.49 o 5 1 6 1.48 2.05 0.45 o 6 1 6 0.06 -0.03 0.33 o 7 1 6 0.00 3.77 1.15 o 0 2 6 17.45 17.30 0.39 o 1 2 6 103.96 99.95 1.00 o 2 2 6 22.90 19.77 0.36 o 3 2 6 31.90 31.55 0.52 o 4 2 6 22.57 19.58 0.47 o 5 2 6 3.52 5.29 0.38 o 6 2 6 10.51 9.70 0.46 o 7 2 6 0.10 -0.99 0.99 o 0 3 6 37.14 38.83 0.67 o 1 3 6 27.97 33.93 0.46 o 2 3 6 27.99 30.35 0.49 o 3 3 6 21.01 21.91 0.47 o 4 3 6 8.73 8.71 0.35 o 5 3 6 14.20 13.44 0.47 o 6 3 6 1.31 2.17 0.35 o 0 4 6 344.45 340.03 3.40 o 1 4 6 95.97 89.36 0.89 o 2 4 6 221.62 214.42 2.04 o 3 4 6 65.05 66.55 0.88 o 4 4 6 68.72 65.38 0.90 o 5 4 6 29.57 31.67 0.62 o 6 4 6 13.53 14.76 0.54 o 0 5 6 22.47 18.12 0.44 o 1 5 6 324.91 332.60 3.28 o 2 5 6 8.64 7.89 0.34 o 3 5 6 179.60 182.03 1.83 o 4 5 6 0.71 1.76 0.29 o 5 5 6 55.02 55.52 0.86 o 6 5 6 0.04 0.51 0.31 o 0 6 6 56.48 58.77 0.97 o 1 6 6 251.71 240.08 2.28 o 2 6 6 43.90 47.19 0.72 o 3 6 6 133.83 127.70 1.41 o 4 6 6 22.12 24.52 0.65 o 5 6 6 43.56 41.42 0.79 o 6 6 6 7.48 10.11 0.51 o 0 7 6 79.59 81.73 1.23 o 1 7 6 1079.94 1002.01 8.27 o 2 7 6 45.98 48.57 0.74 o 3 7 6 447.45 417.64 3.74 o 4 7 6 11.54 12.31 0.39 o 5 7 6 110.48 102.05 1.38 o 6 7 6 2.13 3.84 0.50 o 0 8 6 412.78 404.98 5.91 o 1 8 6 15.13 13.09 0.40 o 2 8 6 287.32 277.48 2.61 o 3 8 6 4.16 4.97 0.33 o 4 8 6 105.91 103.74 1.38 o 5 8 6 0.21 0.70 0.28 o 0 9 6 0.67 -0.14 0.34 o 1 9 6 79.03 69.88 1.09 o 2 9 6 2.61 2.11 0.24 o 3 9 6 66.29 59.46 0.96 o 4 9 6 6.59 5.87 0.37 o 5 9 6 30.04 30.85 0.76 o 0 10 6 30.14 29.04 0.94 o 1 10 6 4.82 7.34 0.35 o 2 10 6 14.91 16.35 0.51 o 3 10 6 0.67 1.47 0.29 o 4 10 6 1.40 2.70 0.36 o 0 11 6 40.55 35.61 1.09 o 1 11 6 234.29 221.91 2.43 o 2 11 6 31.79 26.58 0.74 o 3 11 6 95.91 96.66 1.46 o 4 11 6 14.95 13.36 0.54 o 0 12 6 2.15 4.27 0.47 o 1 12 6 20.17 23.78 0.63 o 2 12 6 2.32 4.42 0.57 o 3 12 6 12.68 15.98 0.79 o 4 12 6 1.91 6.20 1.03 o 0 13 6 3.50 4.27 0.46 o 1 13 6 38.28 37.71 0.82 o 2 13 6 2.73 4.50 0.60 o 3 13 6 18.85 22.77 1.38 o 0 14 6 0.03 0.23 0.93 o 1 14 6 35.38 36.67 0.93 o 2 14 6 0.01 0.00 0.53 o 1 0 7 14.99 17.10 0.48 o 3 0 7 2.98 4.89 0.41 o 5 0 7 0.98 1.14 0.40 o 0 1 7 12.26 13.25 0.55 o 1 1 7 228.34 216.42 1.81 o 2 1 7 3.88 4.82 0.27 o 3 1 7 76.76 77.84 0.92 o 4 1 7 0.01 0.08 0.21 o 5 1 7 14.70 17.26 0.56 o 6 1 7 0.48 0.76 0.47 o 0 2 7 294.61 295.08 4.65 o 1 2 7 56.21 56.90 0.67 o 2 2 7 177.60 177.25 2.16 o 3 2 7 59.51 55.15 0.80 o 4 2 7 47.77 49.61 0.83 o 5 2 7 32.57 29.95 0.75 o 6 2 7 8.00 9.07 0.47 o 0 3 7 519.61 497.69 6.00 o 1 3 7 84.20 84.90 0.94 o 2 3 7 328.75 313.76 2.69 o 3 3 7 39.15 37.89 0.65 o 4 3 7 106.54 104.66 1.27 o 5 3 7 8.72 9.18 0.44 o 6 3 7 25.31 25.42 0.67 o 0 4 7 1539.94 1473.33 15.03 o 1 4 7 69.48 63.57 0.79 o 2 4 7 1018.53 976.56 8.07 o 3 4 7 16.27 16.50 0.44 o 4 4 7 327.56 301.33 3.80 o 5 4 7 1.12 2.28 0.41 o 6 4 7 64.23 60.92 1.59 o 0 5 7 33.48 33.41 0.82 o 1 5 7 105.23 97.86 1.06 o 2 5 7 38.78 40.89 0.67 o 3 5 7 46.10 42.58 0.72 o 4 5 7 31.92 33.20 0.66 o 5 5 7 11.00 11.29 0.47 o 6 5 7 13.12 15.84 1.04 o 0 6 7 55.58 55.61 1.09 o 1 6 7 6.19 7.51 0.32 o 2 6 7 38.34 38.64 0.66 o 3 6 7 4.93 5.93 0.33 o 4 6 7 12.14 12.25 0.42 o 5 6 7 3.20 4.34 0.40 o 0 7 7 133.38 139.71 3.01 o 1 7 7 0.12 0.18 0.20 o 2 7 7 89.03 92.99 1.15 o 3 7 7 0.54 0.50 0.23 o 4 7 7 32.03 32.78 0.65 o 5 7 7 1.45 2.47 0.32 o 0 8 7 55.56 53.28 1.86 o 1 8 7 4.13 5.63 0.32 o 2 8 7 36.97 36.30 0.65 o 3 8 7 6.15 5.65 0.33 o 4 8 7 10.35 11.58 0.60 o 5 8 7 4.75 5.44 0.42 o 0 9 7 236.79 224.13 3.71 o 1 9 7 3.78 4.28 0.41 o 2 9 7 159.00 149.06 1.78 o 3 9 7 2.53 4.09 0.44 o 4 9 7 51.02 53.01 0.94 o 0 10 7 1.80 2.82 0.47 o 1 10 7 2.12 3.68 0.42 o 2 10 7 1.34 2.69 0.54 o 3 10 7 2.52 4.47 0.64 o 4 10 7 0.40 1.61 0.42 o 0 11 7 12.80 12.84 0.66 o 1 11 7 0.99 0.05 0.62 o 2 11 7 10.54 10.96 0.47 o 3 11 7 0.26 0.43 0.49 o 0 12 7 46.25 49.43 1.69 o 1 12 7 9.82 12.13 0.81 o 2 12 7 33.56 35.90 0.88 o 3 12 7 10.38 13.32 2.79 o 0 13 7 62.61 70.25 1.72 o 1 13 7 10.02 11.00 0.79 o 2 13 7 49.99 53.04 2.43 o 0 0 8 98.07 109.46 2.46 o 2 0 8 51.23 53.83 0.97 o 4 0 8 10.77 10.35 0.67 o 0 1 8 6.53 7.57 0.45 o 1 1 8 365.19 329.74 2.98 o 2 1 8 2.28 3.38 0.31 o 3 1 8 151.99 141.53 1.66 o 4 1 8 0.01 0.03 0.23 o 5 1 8 33.24 35.41 0.82 o 0 2 8 33.68 25.60 0.71 o 1 2 8 49.50 35.64 0.66 o 2 2 8 37.09 31.77 0.59 o 3 2 8 18.26 15.44 0.51 o 4 2 8 27.67 25.48 0.65 o 5 2 8 2.52 3.63 0.45 o 0 3 8 11.51 5.93 0.43 o 1 3 8 111.01 110.75 1.47 o 2 3 8 6.86 5.20 0.32 o 3 3 8 76.21 72.21 0.97 o 4 3 8 1.52 2.25 0.34 o 5 3 8 31.29 31.10 0.71 o 0 4 8 15.54 14.09 0.74 o 1 4 8 321.80 313.16 2.89 o 2 4 8 10.11 9.11 0.36 o 3 4 8 157.41 151.04 1.65 o 4 4 8 4.52 5.38 0.32 o 5 4 8 42.12 39.96 0.82 o 0 5 8 1.32 1.75 0.45 o 1 5 8 223.07 223.03 2.60 o 2 5 8 3.11 3.91 0.27 o 3 5 8 87.65 93.56 1.20 o 4 5 8 5.54 6.51 0.36 o 5 5 8 17.33 20.73 0.60 o 0 6 8 4.72 5.04 0.56 o 1 6 8 46.67 47.86 0.95 o 2 6 8 2.40 3.59 0.38 o 3 6 8 21.92 23.45 0.54 o 4 6 8 0.41 1.13 0.32 o 5 6 8 6.75 9.04 0.50 o 0 7 8 18.10 14.00 1.25 o 1 7 8 93.62 93.92 1.39 o 2 7 8 10.08 9.43 0.44 o 3 7 8 39.93 42.87 0.75 o 4 7 8 1.88 3.10 0.34 o 5 7 8 8.72 13.18 1.57 o 0 8 8 15.26 17.10 2.12 o 1 8 8 90.66 93.16 1.54 o 2 8 8 10.58 11.57 0.45 o 3 8 8 44.37 44.65 0.78 o 4 8 8 3.63 6.31 0.39 o 0 9 8 1.02 2.36 0.96 o 1 9 8 74.70 68.30 1.43 o 2 9 8 0.96 2.24 0.44 o 3 9 8 26.66 26.11 0.64 o 4 9 8 0.72 1.42 0.45 o 0 10 8 7.59 6.84 1.16 o 1 10 8 51.43 51.92 1.11 o 2 10 8 3.41 4.84 0.44 o 3 10 8 24.64 27.15 0.98 o 0 11 8 25.85 26.12 1.23 o 1 11 8 0.56 1.11 0.48 o 2 11 8 17.49 20.38 2.19 o 0 12 8 0.36 2.53 0.96 o 1 12 8 39.41 44.20 1.29 o 1 0 9 45.88 39.36 0.95 o 3 0 9 22.48 19.42 0.71 o 5 0 9 5.03 9.83 1.61 o 0 1 9 167.11 151.91 2.30 o 1 1 9 98.10 96.29 1.26 o 2 1 9 116.07 104.78 2.52 o 3 1 9 29.96 29.82 0.66 o 4 1 9 42.54 39.82 1.16 o 5 1 9 2.16 3.34 0.77 o 0 2 9 19.77 15.10 0.58 o 1 2 9 5.97 8.85 0.35 o 2 2 9 16.51 12.84 0.48 o 3 2 9 0.80 1.98 0.32 o 4 2 9 8.57 7.36 0.37 o 5 2 9 0.02 1.21 0.48 o 0 3 9 39.50 37.12 1.10 o 1 3 9 6.18 5.57 0.33 o 2 3 9 27.52 24.64 0.65 o 3 3 9 3.96 4.03 0.34 o 4 3 9 9.36 9.93 0.40 o 0 4 9 95.14 97.39 1.99 o 1 4 9 82.98 72.62 1.17 o 2 4 9 58.55 60.36 1.05 o 3 4 9 43.42 40.44 0.72 o 4 4 9 15.22 20.88 0.57 o 0 5 9 8.52 10.29 0.56 o 1 5 9 19.80 18.77 0.71 o 2 5 9 7.51 8.69 0.41 o 3 5 9 8.94 8.44 0.41 o 4 5 9 4.04 5.71 0.55 o 0 6 9 27.64 26.26 1.66 o 1 6 9 49.58 50.05 1.06 o 2 6 9 15.01 14.69 0.59 o 3 6 9 24.51 27.12 0.66 o 4 6 9 1.69 1.96 0.37 o 0 7 9 127.67 127.71 4.36 o 1 7 9 56.93 63.09 1.41 o 2 7 9 82.26 81.79 1.46 o 3 7 9 26.98 32.08 0.72 o 4 7 9 25.83 26.35 0.78 o 0 8 9 0.75 3.79 1.20 o 1 8 9 36.04 36.16 1.04 o 2 8 9 1.09 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