#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2100283.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100283_Fobs loop_ _publ_author_name 'Nichol, Gary S.' 'Clegg, William' _publ_section_title ; A variable-temperature study of a phase transition in barbituric acid dihydrate ; _journal_coeditor_code WS5026 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 464 _journal_page_last 472 _journal_volume 61 _journal_year 2005 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2bc 2a' _symmetry_space_group_name_H-M 'P m n b' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.2144 _cell_length_b 12.7512 _cell_length_c 8.8841 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.7501 _[local]_cod_data_source_file ws5026270sup15.hkl _[local]_cod_data_source_block 270 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 270 in Pmnb' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' 'x+1/2, -y, -z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y-1/2, -z-1/2' '-x-1/2, y, z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 43881.55 37761.26 1607.67 o 4 0 0 4924.72 4880.39 58.49 o 6 0 0 467.75 397.47 12.68 o 8 0 0 44.59 35.61 1.84 o 0 2 0 975.63 1004.31 15.25 o 1 2 0 2249.74 2243.70 20.03 o 2 2 0 743.16 753.34 6.51 o 3 2 0 459.57 494.07 5.02 o 4 2 0 203.59 185.14 1.84 o 5 2 0 94.51 92.15 1.10 o 6 2 0 24.78 22.47 0.75 o 7 2 0 19.68 18.54 1.29 o 8 2 0 2.58 5.81 1.08 o 0 4 0 37.78 34.29 0.60 o 1 4 0 591.18 549.76 6.21 o 2 4 0 5.71 5.29 0.18 o 3 4 0 77.49 69.81 0.80 o 4 4 0 1.97 2.20 0.22 o 5 4 0 5.99 5.85 0.38 o 6 4 0 2.56 2.35 0.58 o 7 4 0 0.42 0.24 0.89 o 0 6 0 38.63 47.32 0.95 o 1 6 0 205.44 182.38 2.34 o 2 6 0 27.70 32.38 0.46 o 3 6 0 51.64 56.08 0.81 o 4 6 0 10.74 11.63 0.46 o 5 6 0 16.79 19.49 0.60 o 6 6 0 2.82 2.71 0.57 o 7 6 0 4.48 4.89 1.14 o 0 8 0 464.48 445.76 5.65 o 1 8 0 335.27 361.35 3.30 o 2 8 0 223.40 221.98 2.74 o 3 8 0 70.49 73.02 1.18 o 4 8 0 32.10 35.34 0.80 o 5 8 0 1.16 1.08 0.45 o 6 8 0 2.18 1.69 0.55 o 7 8 0 0.29 1.28 1.61 o 0 10 0 409.99 400.67 6.62 o 1 10 0 120.55 105.39 1.34 o 2 10 0 268.16 262.63 3.20 o 3 10 0 31.01 28.95 0.74 o 4 10 0 96.81 96.08 1.55 o 5 10 0 1.57 0.68 0.35 o 6 10 0 24.78 24.53 1.50 o 0 12 0 93.91 88.43 2.05 o 1 12 0 121.71 114.11 1.73 o 2 12 0 46.14 44.17 1.13 o 3 12 0 68.77 64.73 1.33 o 4 12 0 5.78 7.48 0.52 o 5 12 0 21.49 22.63 0.78 o 0 14 0 35.35 42.04 2.53 o 1 14 0 2.32 1.11 0.43 o 2 14 0 24.91 28.64 1.02 o 3 14 0 0.01 -0.54 0.84 o 4 14 0 10.42 12.93 0.87 o 0 16 0 186.69 190.41 5.71 o 1 16 0 4.36 6.20 0.80 o 2 16 0 139.68 149.23 6.29 o 1 0 1 3328.16 3289.73 54.12 o 3 0 1 735.80 830.89 7.20 o 5 0 1 185.02 180.70 1.86 o 7 0 1 40.71 35.75 1.22 o 0 1 1 20.59 19.55 0.29 o 1 1 1 216.03 219.56 1.41 o 2 1 1 17.85 17.86 0.32 o 3 1 1 64.36 58.27 0.53 o 4 1 1 6.46 5.85 0.22 o 5 1 1 3.19 2.39 0.19 o 6 1 1 1.11 1.04 0.27 o 7 1 1 0.01 -0.27 0.27 o 8 1 1 0.14 1.42 0.58 o 0 2 1 1293.81 1246.08 10.78 o 1 2 1 257.68 243.62 1.69 o 2 2 1 547.96 573.34 3.68 o 3 2 1 114.50 105.09 0.80 o 4 2 1 119.77 134.42 0.99 o 5 2 1 17.53 15.04 0.30 o 6 2 1 25.93 27.56 0.50 o 7 2 1 1.96 2.88 0.42 o 8 2 1 3.97 5.99 1.20 o 0 3 1 5.36 5.81 0.37 o 1 3 1 1965.95 2129.50 19.79 o 2 3 1 0.20 -0.03 0.10 o 3 3 1 461.57 480.67 3.02 o 4 3 1 0.87 0.12 0.13 o 5 3 1 34.71 32.96 0.44 o 6 3 1 0.00 -0.24 0.24 o 7 3 1 1.34 1.62 0.54 o 8 3 1 0.02 -0.70 0.70 o 0 4 1 446.42 483.72 6.10 o 1 4 1 3329.37 3472.05 21.89 o 2 4 1 184.16 194.72 1.58 o 3 4 1 648.11 633.60 3.94 o 4 4 1 8.83 7.33 0.21 o 5 4 1 64.24 56.36 0.63 o 6 4 1 0.16 0.42 0.32 o 7 4 1 6.03 5.89 0.51 o 0 5 1 349.51 413.76 3.95 o 1 5 1 1735.93 1875.91 12.82 o 2 5 1 114.37 120.42 0.91 o 3 5 1 403.94 413.73 2.64 o 4 5 1 5.66 6.15 0.22 o 5 5 1 43.20 42.33 0.61 o 6 5 1 0.01 -0.24 0.24 o 7 5 1 3.30 3.54 0.46 o 0 6 1 380.42 388.44 3.59 o 1 6 1 91.12 104.45 0.80 o 2 6 1 168.38 166.72 1.21 o 3 6 1 59.53 63.10 0.62 o 4 6 1 6.97 6.07 0.25 o 5 6 1 19.16 19.76 0.43 o 6 6 1 1.43 2.21 0.32 o 7 6 1 3.42 6.09 0.53 o 0 7 1 561.86 601.35 5.29 o 1 7 1 406.21 428.74 2.85 o 2 7 1 254.92 264.55 1.85 o 3 7 1 133.45 123.27 1.12 o 4 7 1 46.13 44.44 0.62 o 5 7 1 18.67 16.56 0.41 o 6 7 1 8.67 7.44 0.40 o 7 7 1 1.46 1.86 0.44 o 0 8 1 275.65 254.55 2.39 o 1 8 1 19.73 16.14 0.26 o 2 8 1 130.10 119.35 1.14 o 3 8 1 6.78 6.73 0.26 o 4 8 1 23.08 23.00 0.45 o 5 8 1 1.19 1.38 0.29 o 6 8 1 3.25 3.63 0.37 o 7 8 1 0.12 0.87 0.97 o 0 9 1 19.25 20.22 0.65 o 1 9 1 27.68 27.07 0.39 o 2 9 1 29.17 29.19 0.45 o 3 9 1 23.46 22.10 0.44 o 4 9 1 25.23 23.84 0.54 o 5 9 1 12.47 12.69 0.43 o 6 9 1 8.50 9.37 0.44 o 0 10 1 139.11 131.30 1.59 o 1 10 1 399.61 401.54 3.11 o 2 10 1 63.68 62.62 0.73 o 3 10 1 177.91 177.23 1.67 o 4 10 1 7.82 9.18 0.36 o 5 10 1 48.46 47.70 0.80 o 6 10 1 0.41 0.93 0.33 o 0 11 1 0.37 -0.25 0.34 o 1 11 1 680.34 668.95 5.31 o 2 11 1 1.95 1.65 0.25 o 3 11 1 290.49 297.41 2.60 o 4 11 1 3.18 3.43 0.31 o 5 11 1 65.01 65.66 0.99 o 6 11 1 1.23 1.80 0.38 o 0 12 1 163.66 168.83 2.32 o 1 12 1 3.98 5.98 0.34 o 2 12 1 115.42 118.08 1.36 o 3 12 1 0.00 -0.20 0.24 o 4 12 1 41.19 40.30 0.74 o 5 12 1 0.76 1.14 0.44 o 0 13 1 14.19 14.76 0.88 o 1 13 1 33.00 34.01 0.65 o 2 13 1 11.51 11.41 0.44 o 3 13 1 14.01 15.04 0.47 o 4 13 1 6.42 6.80 0.39 o 5 13 1 3.16 5.53 0.53 o 0 14 1 22.10 19.90 1.70 o 1 14 1 220.97 218.43 2.45 o 2 14 1 14.92 15.19 0.53 o 3 14 1 84.03 88.38 1.32 o 4 14 1 4.73 7.30 0.51 o 0 15 1 2.21 2.46 0.49 o 1 15 1 55.69 56.12 1.11 o 2 15 1 1.25 1.48 0.35 o 3 15 1 21.56 22.24 0.67 o 0 16 1 13.67 13.37 0.92 o 1 16 1 32.37 37.58 1.13 o 2 16 1 11.51 14.30 0.83 o 0 0 2 995.88 950.02 11.59 o 2 0 2 345.42 333.05 3.25 o 4 0 2 32.26 31.13 0.51 o 6 0 2 3.05 2.96 0.39 o 8 0 2 0.38 0.91 0.78 o 0 1 2 152.98 160.53 1.47 o 1 1 2 162.98 175.36 1.45 o 2 1 2 129.26 136.56 1.00 o 3 1 2 56.40 56.29 0.50 o 4 1 2 23.22 17.97 0.27 o 5 1 2 7.66 7.18 0.30 o 6 1 2 0.45 0.11 0.21 o 7 1 2 0.64 0.49 0.31 o 8 1 2 0.00 1.27 0.48 o 0 2 2 1420.50 1567.76 13.42 o 1 2 2 127.61 118.29 0.92 o 2 2 2 589.20 625.68 4.22 o 3 2 2 37.15 29.47 0.34 o 4 2 2 65.25 67.08 0.64 o 5 2 2 4.28 4.40 0.27 o 6 2 2 3.81 3.85 0.32 o 7 2 2 0.27 0.43 0.37 o 8 2 2 0.16 0.66 0.78 o 0 3 2 309.55 320.27 2.84 o 1 3 2 810.03 868.93 5.56 o 2 3 2 186.31 202.69 1.60 o 3 3 2 110.42 121.20 0.92 o 4 3 2 31.21 29.53 0.41 o 5 3 2 7.74 8.21 0.29 o 6 3 2 1.78 1.17 0.26 o 7 3 2 0.88 0.51 0.29 o 8 3 2 0.11 0.82 1.36 o 0 4 2 28.91 32.07 0.42 o 1 4 2 1965.65 2063.42 12.52 o 2 4 2 3.04 3.97 0.14 o 3 4 2 431.34 444.27 2.94 o 4 4 2 4.91 4.47 0.19 o 5 4 2 44.34 42.07 0.61 o 6 4 2 4.91 5.65 0.34 o 7 4 2 4.02 3.09 0.65 o 0 5 2 7.04 7.52 0.22 o 1 5 2 613.11 672.20 4.35 o 2 5 2 5.08 5.84 0.19 o 3 5 2 71.30 70.69 0.67 o 4 5 2 0.25 -0.03 0.15 o 5 5 2 0.72 0.74 0.22 o 6 5 2 0.13 0.06 0.24 o 7 5 2 0.20 -0.29 0.29 o 0 6 2 1568.40 1746.40 14.94 o 1 6 2 855.43 940.12 7.40 o 2 6 2 803.55 881.35 5.70 o 3 6 2 247.26 260.67 1.94 o 4 6 2 153.50 159.85 1.31 o 5 6 2 35.48 36.74 0.69 o 6 6 2 19.34 19.13 0.55 o 7 6 2 3.84 4.27 0.41 o 0 7 2 49.06 57.52 0.81 o 1 7 2 248.76 267.63 1.86 o 2 7 2 29.55 28.42 0.38 o 3 7 2 59.36 60.99 0.63 o 4 7 2 6.73 5.90 0.27 o 5 7 2 13.66 12.24 0.44 o 6 7 2 0.72 0.35 0.34 o 7 7 2 3.67 3.73 0.45 o 0 8 2 425.09 405.55 3.67 o 1 8 2 52.31 64.73 0.60 o 2 8 2 227.73 220.71 1.69 o 3 8 2 10.63 11.92 0.31 o 4 8 2 39.65 40.36 0.61 o 5 8 2 0.53 0.05 0.27 o 6 8 2 2.71 4.46 0.39 o 7 8 2 0.01 -0.22 0.87 o 0 9 2 90.41 85.23 1.13 o 1 9 2 20.11 18.69 0.31 o 2 9 2 71.72 65.55 0.73 o 3 9 2 32.94 30.76 0.52 o 4 9 2 37.83 37.25 0.78 o 5 9 2 18.89 16.95 0.51 o 6 9 2 12.66 11.89 0.48 o 0 10 2 717.01 724.64 7.18 o 1 10 2 268.11 240.20 2.11 o 2 10 2 439.57 440.80 3.39 o 3 10 2 84.08 82.99 0.90 o 4 10 2 116.20 112.22 1.42 o 5 10 2 11.17 12.85 0.48 o 6 10 2 16.89 17.33 0.56 o 0 11 2 702.15 649.67 7.38 o 1 11 2 97.57 84.70 0.97 o 2 11 2 462.46 442.98 3.67 o 3 11 2 51.30 48.83 0.72 o 4 11 2 148.39 144.32 1.49 o 5 11 2 13.16 12.87 0.51 o 6 11 2 29.35 30.37 1.05 o 0 12 2 153.91 152.61 2.52 o 1 12 2 2.59 2.32 0.28 o 2 12 2 91.81 93.76 1.08 o 3 12 2 0.57 0.36 0.26 o 4 12 2 22.36 22.42 0.56 o 5 12 2 0.00 0.02 0.37 o 0 13 2 39.61 35.17 1.27 o 1 13 2 49.90 45.08 0.76 o 2 13 2 21.16 19.89 0.63 o 3 13 2 25.69 23.87 0.57 o 4 13 2 2.85 2.75 0.55 o 5 13 2 8.17 7.76 1.08 o 0 14 2 5.47 6.76 0.62 o 1 14 2 2.82 3.06 0.35 o 2 14 2 1.55 2.80 0.35 o 3 14 2 0.33 0.03 0.29 o 4 14 2 0.08 -0.14 0.33 o 0 15 2 46.68 50.52 1.57 o 1 15 2 1.39 1.49 0.37 o 2 15 2 30.18 32.49 0.75 o 3 15 2 0.69 1.28 0.33 o 0 16 2 0.92 0.87 0.44 o 1 16 2 11.37 15.37 1.06 o 2 16 2 0.82 1.56 0.47 o 1 0 3 7909.99 8506.41 76.81 o 3 0 3 1525.28 1555.67 25.35 o 5 0 3 151.97 145.14 1.97 o 7 0 3 15.70 12.28 0.68 o 0 1 3 70.35 75.42 0.77 o 1 1 3 865.77 943.56 6.04 o 2 1 3 32.42 30.36 0.34 o 3 1 3 198.40 205.43 1.62 o 4 1 3 6.26 5.59 0.23 o 5 1 3 10.08 9.21 0.35 o 6 1 3 0.91 0.42 0.24 o 7 1 3 0.04 -0.08 0.25 o 8 1 3 0.08 -0.76 0.76 o 0 2 3 0.34 -0.10 0.10 o 1 2 3 293.53 326.83 2.15 o 2 2 3 0.44 0.40 0.09 o 3 2 3 17.01 18.20 0.26 o 4 2 3 5.27 5.24 0.24 o 5 2 3 0.35 -0.03 0.22 o 6 2 3 5.99 6.03 0.35 o 7 2 3 0.63 0.43 0.28 o 0 3 3 26.66 29.28 0.40 o 1 3 3 194.71 214.81 1.40 o 2 3 3 8.86 8.41 0.18 o 3 3 3 31.25 30.79 0.35 o 4 3 3 2.15 2.14 0.20 o 5 3 3 1.64 2.01 0.24 o 6 3 3 1.11 0.69 0.27 o 7 3 3 0.01 -0.29 0.29 o 0 4 3 152.62 152.55 1.47 o 1 4 3 1112.40 1216.14 7.40 o 2 4 3 41.04 34.81 0.36 o 3 4 3 357.33 365.92 2.47 o 4 4 3 0.01 0.21 0.19 o 5 4 3 49.01 50.17 0.69 o 6 4 3 1.48 1.69 0.27 o 7 4 3 4.35 6.00 0.46 o 0 5 3 36.26 31.91 0.46 o 1 5 3 716.72 754.91 4.65 o 2 5 3 32.39 38.46 0.42 o 3 5 3 233.30 223.55 1.69 o 4 5 3 12.96 15.74 0.37 o 5 5 3 31.96 26.95 0.50 o 6 5 3 2.50 3.65 0.36 o 7 5 3 2.60 2.66 0.41 o 0 6 3 195.50 231.56 2.18 o 1 6 3 203.37 249.05 1.74 o 2 6 3 119.30 133.99 1.09 o 3 6 3 80.72 89.84 0.83 o 4 6 3 23.57 22.96 0.44 o 5 6 3 19.62 20.89 0.49 o 6 6 3 1.52 0.98 0.38 o 7 6 3 3.21 4.82 0.53 o 0 7 3 43.19 39.41 0.56 o 1 7 3 386.32 411.42 2.77 o 2 7 3 14.27 13.54 0.29 o 3 7 3 101.83 111.55 0.99 o 4 7 3 1.27 1.46 0.23 o 5 7 3 10.94 11.10 0.43 o 6 7 3 0.34 -0.12 0.27 o 7 7 3 0.75 -0.21 0.58 o 0 8 3 147.30 145.56 1.68 o 1 8 3 27.48 25.17 0.37 o 2 8 3 72.74 74.45 0.73 o 3 8 3 6.95 6.67 0.25 o 4 8 3 7.52 7.23 0.33 o 5 8 3 0.73 0.31 0.26 o 6 8 3 0.03 0.15 0.28 o 7 8 3 0.06 1.71 0.90 o 0 9 3 36.74 37.27 0.67 o 1 9 3 5.18 4.15 0.23 o 2 9 3 8.21 8.89 0.27 o 3 9 3 6.81 6.18 0.31 o 4 9 3 0.55 0.44 0.23 o 5 9 3 4.85 4.99 0.39 o 6 9 3 1.49 1.96 0.34 o 0 10 3 43.87 41.92 0.74 o 1 10 3 36.67 27.67 0.45 o 2 10 3 19.81 19.51 0.43 o 3 10 3 8.55 8.04 0.30 o 4 10 3 1.11 1.21 0.29 o 5 10 3 0.71 0.99 0.30 o 6 10 3 0.08 1.03 0.36 o 0 11 3 15.47 9.90 0.47 o 1 11 3 19.46 15.45 0.39 o 2 11 3 15.68 11.90 0.36 o 3 11 3 14.98 12.99 0.38 o 4 11 3 9.62 8.33 0.61 o 5 11 3 6.82 7.09 0.43 o 0 12 3 59.25 45.06 1.13 o 1 12 3 65.69 60.73 0.81 o 2 12 3 40.56 33.24 0.59 o 3 12 3 22.93 23.08 0.55 o 4 12 3 13.22 12.62 0.54 o 5 12 3 3.63 5.77 0.44 o 0 13 3 5.41 2.78 0.50 o 1 13 3 70.28 65.73 1.04 o 2 13 3 3.66 3.43 0.29 o 3 13 3 29.64 26.96 0.61 o 4 13 3 1.34 2.14 0.42 o 0 14 3 94.93 91.92 1.88 o 1 14 3 9.32 8.51 0.48 o 2 14 3 57.06 58.66 1.01 o 3 14 3 4.88 5.70 0.46 o 4 14 3 13.74 17.73 2.02 o 0 15 3 21.77 21.50 0.89 o 1 15 3 2.25 4.29 0.44 o 2 15 3 13.10 13.23 0.57 o 3 15 3 3.03 5.86 1.64 o 0 16 3 1.98 3.10 0.67 o 1 16 3 1.34 3.69 0.54 o 0 0 4 40.94 46.54 0.80 o 2 0 4 22.96 21.61 0.55 o 4 0 4 0.96 2.68 0.32 o 6 0 4 10.87 10.89 0.52 o 0 1 4 491.12 505.00 4.44 o 1 1 4 1580.70 1720.80 11.40 o 2 1 4 216.76 226.74 1.66 o 3 1 4 427.57 425.93 2.99 o 4 1 4 25.23 28.83 0.46 o 5 1 4 51.28 48.80 0.68 o 6 1 4 1.47 2.32 0.31 o 7 1 4 4.10 5.33 0.46 o 0 2 4 971.78 1056.70 9.10 o 1 2 4 298.67 331.36 2.12 o 2 2 4 369.24 371.74 2.60 o 3 2 4 120.91 133.61 1.15 o 4 2 4 31.16 30.32 0.46 o 5 2 4 37.40 43.16 0.69 o 6 2 4 0.87 0.92 0.25 o 7 2 4 8.07 9.01 0.41 o 0 3 4 0.83 0.27 0.13 o 1 3 4 31.90 30.13 0.31 o 2 3 4 0.06 0.13 0.12 o 3 3 4 10.66 9.57 0.26 o 4 3 4 0.25 0.54 0.19 o 5 3 4 1.25 1.24 0.27 o 6 3 4 0.22 0.20 0.25 o 7 3 4 0.03 0.44 0.34 o 0 4 4 258.93 219.71 2.07 o 1 4 4 449.86 479.75 3.02 o 2 4 4 85.85 73.26 0.63 o 3 4 4 127.70 133.97 1.27 o 4 4 4 4.56 4.76 0.30 o 5 4 4 13.32 12.19 0.37 o 6 4 4 0.14 -0.16 0.25 o 7 4 4 1.07 1.08 0.34 o 0 5 4 514.18 547.15 4.85 o 1 5 4 1.15 1.20 0.14 o 2 5 4 280.17 285.49 2.19 o 3 5 4 0.06 -0.18 0.18 o 4 5 4 62.08 59.75 0.76 o 5 5 4 0.01 -0.19 0.20 o 6 5 4 9.23 7.95 0.36 o 7 5 4 0.01 -0.20 0.40 o 0 6 4 4.08 7.20 0.27 o 1 6 4 239.62 258.67 1.82 o 2 6 4 0.71 1.71 0.17 o 3 6 4 46.25 50.00 0.66 o 4 6 4 0.00 -0.13 0.19 o 5 6 4 0.08 -0.16 0.21 o 6 6 4 0.01 0.24 0.29 o 7 6 4 0.97 0.41 0.43 o 0 7 4 0.24 0.71 0.20 o 1 7 4 40.61 39.34 0.47 o 2 7 4 1.22 1.68 0.18 o 3 7 4 21.61 21.24 0.43 o 4 7 4 1.97 1.81 0.28 o 5 7 4 8.19 8.45 0.37 o 6 7 4 0.74 0.40 0.28 o 0 8 4 20.41 17.48 0.45 o 1 8 4 20.12 16.13 0.32 o 2 8 4 14.67 13.71 0.31 o 3 8 4 4.42 4.47 0.27 o 4 8 4 6.26 7.44 0.34 o 5 8 4 0.83 0.99 0.30 o 6 8 4 1.74 3.21 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