#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:57:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180870 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/02/2100295.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100295_Fobs loop_ _publ_author_name 'Hao, Xiang' 'Parkin, Sean' 'Brock, Carolyn Pratt' _publ_section_title ; Three modulation patterns in four related [M(H~2~O)~2~(15-crown-5)](NO~3~)~2~ structures ; _journal_coeditor_code BM5026 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 675 _journal_page_last 688 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.483 _cell_angle_gamma 90.000 _cell_length_a 14.6330 _cell_length_b 14.0340 _cell_length_c 25.5610 _exptl_crystal_F_000 2784.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file bm5026k04160sup5.hkl _cod_data_source_block k04160 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k04160 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 621.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10.88 33.37 16.68 o 2 0 0 198948.27 186167.81 4003.97 o 3 0 0 38.06 16.68 16.68 o 4 0 0 16141.83 16249.44 300.30 o 5 0 0 3.88 33.37 33.37 o 6 0 0 88468.42 89104.96 1518.17 o 7 0 0 3112.63 3269.91 116.78 o 8 0 0 7062.53 6556.50 216.88 o 9 0 0 4633.47 4788.08 216.88 o 10 0 0 41174.79 40606.91 1000.99 o 11 0 0 66.62 200.20 133.47 o 12 0 0 31985.86 32098.47 867.53 o 13 0 0 0.38 16.68 166.83 o 14 0 0 25039.13 25508.61 800.79 o 15 0 0 522.62 383.71 183.52 o 16 0 0 7121.48 6856.79 417.08 o 17 0 0 9.16 -150.15 250.25 o 1 1 0 7.83 52.43 16.68 o 2 1 0 36318.68 38253.99 434.57 o 3 1 0 94.53 70.90 16.68 o 4 1 0 92.26 112.02 25.02 o 5 1 0 48.33 41.71 23.59 o 6 1 0 59689.02 62517.26 714.98 o 7 1 0 1061.97 1007.25 66.73 o 8 1 0 948.44 761.38 58.98 o 9 1 0 327.04 421.93 64.08 o 10 1 0 823.87 772.33 116.78 o 11 1 0 204.96 109.63 80.08 o 12 1 0 3165.42 2865.24 147.99 o 13 1 0 125.38 91.76 108.44 o 14 1 0 86.01 50.05 87.89 o 15 1 0 0.08 1.76 125.12 o 16 1 0 82.34 77.24 191.86 o 17 1 0 11.00 107.05 325.32 o 0 2 0 287187.41 263937.16 4249.57 o 1 2 0 38.61 59.58 11.80 o 2 2 0 339524.88 324820.16 4718.02 o 3 2 0 293.29 275.07 25.02 o 4 2 0 62783.27 60141.94 652.76 o 5 2 0 233.35 234.76 23.59 o 6 2 0 145498.66 151904.98 1868.52 o 7 2 0 3097.98 3097.45 91.76 o 8 2 0 88618.62 89538.14 1308.81 o 9 2 0 686.91 744.85 83.42 o 10 2 0 6665.24 5949.54 165.16 o 11 2 0 85.60 150.15 82.58 o 12 2 0 19292.58 18548.97 400.40 o 13 2 0 220.27 243.38 99.75 o 14 2 0 12726.57 12542.42 475.47 o 15 2 0 295.18 304.85 128.16 o 16 2 0 19983.37 20948.66 667.33 o 17 2 0 2.25 -182.32 218.76 o 1 3 0 202.11 193.53 66.73 o 2 3 0 169776.72 174906.23 1985.14 o 3 3 0 189.87 192.22 11.80 o 4 3 0 16259.20 14605.19 225.22 o 5 3 0 755.17 712.07 75.07 o 6 3 0 29369.82 30402.02 642.30 o 7 3 0 1923.76 1990.72 100.10 o 8 3 0 26837.33 28107.56 600.60 o 9 3 0 135.76 96.39 52.11 o 10 3 0 1679.37 1477.49 250.25 o 11 3 0 974.34 918.82 107.94 o 12 3 0 7055.83 6973.06 228.00 o 13 3 0 305.10 175.17 106.17 o 14 3 0 3701.34 3575.84 433.76 o 15 3 0 34.65 -21.35 144.30 o 16 3 0 1405.15 1279.87 194.38 o 17 3 0 44.02 73.15 228.00 o 0 4 0 296.30 335.18 50.05 o 1 4 0 67.34 50.05 14.92 o 2 4 0 71637.94 73638.91 900.89 o 3 4 0 1.51 -14.92 14.92 o 4 4 0 90783.34 89185.91 1027.10 o 5 4 0 2331.46 2417.80 76.00 o 6 4 0 37367.71 34921.05 459.62 o 7 4 0 2340.27 2536.29 94.37 o 8 4 0 115867.36 116500.24 1801.78 o 9 4 0 1120.49 1143.84 99.75 o 10 4 0 32946.43 33676.02 984.31 o 11 4 0 801.39 892.74 241.91 o 12 4 0 2395.98 2447.90 152.00 o 13 4 0 11.05 -72.00 107.94 o 14 4 0 21962.38 22737.89 742.40 o 15 4 0 0.20 139.64 151.22 o 16 4 0 7774.28 7686.80 339.67 o 1 5 0 35.12 55.61 14.92 o 2 5 0 781.11 694.87 41.71 o 3 5 0 436.50 469.55 27.76 o 4 5 0 2413.73 2731.33 72.92 o 5 5 0 1447.73 1498.27 55.53 o 6 5 0 1258.60 1451.26 125.12 o 7 5 0 73.94 108.44 58.98 o 8 5 0 14701.92 15255.62 284.53 o 9 5 0 387.60 284.21 175.17 o 10 5 0 1741.27 1330.01 158.49 o 11 5 0 0.01 -18.77 150.15 o 12 5 0 190.91 232.58 99.75 o 13 5 0 98.96 106.77 266.93 o 14 5 0 36.65 -2.38 120.12 o 15 5 0 0.15 -12.19 147.99 o 16 5 0 301.34 354.80 175.78 o 0 6 0 1609.21 1222.52 59.69 o 1 6 0 73.52 83.42 15.83 o 2 6 0 31405.86 29941.62 725.72 o 3 6 0 384.05 381.33 66.73 o 4 6 0 48379.68 47722.77 649.08 o 5 6 0 1198.83 1229.47 55.53 o 6 6 0 70987.22 68653.91 1017.69 o 7 6 0 135.43 125.12 91.76 o 8 6 0 53965.96 52972.75 849.35 o 9 6 0 1079.37 1000.23 113.67 o 10 6 0 3108.05 3029.13 158.82 o 11 6 0 677.17 590.24 141.81 o 12 6 0 6370.64 6247.23 255.93 o 13 6 0 241.12 115.27 128.16 o 14 6 0 15830.15 15796.16 533.86 o 15 6 0 2.77 -103.73 135.28 o 16 6 0 8399.32 8570.20 428.28 o 1 7 0 233.93 298.14 33.37 o 2 7 0 6740.13 6954.60 225.22 o 3 7 0 278.46 324.13 55.53 o 4 7 0 5492.19 5169.90 383.71 o 5 7 0 268.67 330.51 55.53 o 6 7 0 698.26 859.33 75.07 o 7 7 0 210.40 213.85 57.94 o 8 7 0 6.48 -17.97 76.00 o 9 7 0 474.08 465.04 158.49 o 10 7 0 8632.30 8595.63 264.47 o 11 7 0 484.00 531.29 125.12 o 12 7 0 3.46 77.06 183.52 o 13 7 0 469.55 38.44 135.28 o 14 7 0 1744.57 1428.75 233.56 o 15 7 0 253.61 141.81 212.34 o 0 8 0 152846.38 153286.86 2892.99 o 1 8 0 321.80 311.05 100.10 o 2 8 0 78508.50 76102.26 1743.39 o 3 8 0 56.05 14.83 58.39 o 4 8 0 18687.21 17254.44 359.66 o 5 8 0 339.14 357.52 44.77 o 6 8 0 7663.16 7235.98 156.59 o 7 8 0 6.55 56.12 64.08 o 8 8 0 4754.75 4679.43 163.90 o 9 8 0 15.91 -89.67 92.18 o 10 8 0 28870.48 31161.04 608.01 o 11 8 0 62.03 59.15 116.78 o 12 8 0 21429.40 21394.26 1651.64 o 13 8 0 26.45 -96.97 184.36 o 14 8 0 5371.18 5208.16 342.01 o 15 8 0 11.93 75.07 291.96 o 1 9 0 174.21 243.42 46.00 o 2 9 0 773.91 923.31 116.78 o 3 9 0 263.94 259.18 141.81 o 4 9 0 11071.87 11554.29 274.68 o 5 9 0 94.89 66.73 91.76 o 6 9 0 1807.59 1886.25 87.88 o 7 9 0 197.39 234.26 183.52 o 8 9 0 1011.80 842.01 116.21 o 9 9 0 111.12 205.76 104.22 o 10 9 0 1709.91 1845.71 172.28 o 11 9 0 55.01 -114.22 152.00 o 12 9 0 83.58 169.81 154.07 o 13 9 0 72.95 -8.05 170.75 o 14 9 0 476.53 658.14 325.32 o 0 10 0 155266.31 159829.05 2939.62 o 1 10 0 69.91 7.15 75.07 o 2 10 0 22189.49 21563.57 625.62 o 3 10 0 0.32 175.17 85.83 o 4 10 0 34603.09 33886.12 626.36 o 5 10 0 67.59 161.27 87.89 o 6 10 0 41270.63 42213.09 867.53 o 7 10 0 301.28 199.32 111.60 o 8 10 0 2389.35 2504.27 158.93 o 9 10 0 539.14 389.52 135.28 o 10 10 0 16997.83 18475.88 525.52 o 11 10 0 41.60 -27.98 208.54 o 12 10 0 29349.20 30238.98 928.37 o 13 10 0 117.56 -3.65 178.99 o 1 11 0 2489.32 2432.43 119.38 o 2 11 0 527.50 628.64 95.67 o 3 11 0 43.98 120.12 83.29 o 4 11 0 1615.45 1640.52 135.76 o 5 11 0 26.83 35.45 92.18 o 6 11 0 8545.37 8242.50 263.66 o 7 11 0 151.40 433.76 135.76 o 8 11 0 3989.85 3607.93 204.18 o 9 11 0 232.24 464.66 158.93 o 10 11 0 214.42 37.22 152.00 o 11 11 0 24.05 -216.88 291.96 o 12 11 0 4047.61 4514.67 401.09 o 13 11 0 21.77 138.88 218.00 o 0 12 0 12559.19 12538.57 489.99 o 1 12 0 56.30 -54.68 158.49 o 2 12 0 40641.03 41671.28 942.60 o 3 12 0 212.71 183.52 104.45 o 4 12 0 22818.78 23254.41 581.08 o 5 12 0 21.20 86.75 111.05 o 6 12 0 32340.34 34457.80 683.00 o 7 12 0 46.23 -50.81 123.45 o 8 12 0 38494.46 39988.75 864.39 o 9 12 0 295.35 -51.38 147.11 o 10 12 0 9725.44 9872.82 416.88 o 11 12 0 48.62 -117.66 215.88 o 12 12 0 10456.27 11542.79 586.66 o 1 13 0 1004.96 978.57 175.17 o 2 13 0 176.72 133.47 225.22 o 3 13 0 63.75 -83.42 163.90 o 4 13 0 446.96 599.80 166.58 o 5 13 0 175.56 211.32 135.76 o 6 13 0 396.22 183.52 132.70 o 7 13 0 55.08 134.70 158.93 o 8 13 0 4049.54 4174.40 287.40 o 9 13 0 92.78 88.63 184.36 o 10 13 0 48.06 -115.31 196.42 o 0 14 0 2207.02 2440.69 308.15 o 1 14 0 482.61 640.37 168.32 o 2 14 0 27093.04 28971.30 862.20 o 3 14 0 81.70 115.22 187.65 o 4 14 0 44498.48 48012.05 1209.13 o 5 14 0 73.58 -100.10 176.95 o 6 14 0 15486.90 15624.79 571.32 o 7 14 0 57.31 -86.93 223.21 o 8 14 0 18313.08 18328.13 601.28 o 9 14 0 229.82 70.39 241.62 o 1 15 0 48.20 -139.03 208.44 o 2 15 0 2926.53 3413.52 282.95 o 3 15 0 4.49 -61.17 233.56 o 4 15 0 265.82 306.36 300.30 o 5 15 0 0.36 444.89 244.38 o 6 15 0 607.51 787.82 342.01 o 7 15 0 30.84 -329.22 350.35 o 0 16 0 24653.83 25309.99 1592.57 o 1 16 0 17.13 -235.94 235.94 o 2 16 0 13361.80 13582.45 615.21 o 3 16 0 13.98 120.75 266.93 o 4 16 0 14663.04 15468.05 600.25 o -17 1 1 1931.63 1901.40 312.45 o -16 1 1 164.36 217.55 147.11 o -15 1 1 549.30 450.45 129.76 o -14 1 1 109.65 88.98 104.22 o -13 1 1 4751.27 4753.15 200.20 o -12 1 1 14.57 58.39 92.18 o -11 1 1 2007.19 1821.92 116.21 o -10 1 1 55.06 116.78 58.98 o -9 1 1 4684.93 4913.22 141.56 o -8 1 1 56.70 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12823.36 12758.40 235.05 o -8 3 1 3.37 64.65 42.92 o -7 3 1 1636.76 1834.17 58.39 o -6 3 1 49.35 71.50 40.04 o -5 3 1 424.85 377.04 35.39 o -4 3 1 25.07 8.34 23.59 o -3 3 1 3602.44 3348.34 52.11 o -2 3 1 112.19 97.72 25.02 o -1 3 1 871.02 859.27 23.59 o 0 3 1 0.14 0.00 14.92 o 1 3 1 2669.16 2673.07 52.11 o 2 3 1 269.22 297.11 14.92 o 3 3 1 202.83 163.93 50.05 o 4 3 1 473.12 506.23 33.37 o 5 3 1 2105.55 2110.46 47.19 o 6 3 1 90.16 85.98 33.37 o 7 3 1 28.15 -11.12 29.84 o 8 3 1 498.80 490.58 66.73 o 9 3 1 5618.75 5365.06 200.20 o 10 3 1 3.63 -33.37 55.53 o 11 3 1 2093.57 2120.96 132.24 o 12 3 1 5.04 8.34 94.37 o 13 3 1 3206.46 3153.46 168.32 o 14 3 1 401.12 543.86 116.21 o 15 3 1 4916.64 5160.18 239.90 o 16 3 1 496.13 319.86 163.56 o -16 4 1 20.95 -14.38 183.52 o -15 4 1 781.80 847.97 156.33 o -14 4 1 63.44 -48.29 111.60 o -13 4 1 34.00 -111.60 111.60 o -12 4 1 71.51 -19.63 99.75 o -11 4 1 604.07 562.92 99.75 o -10 4 1 9.69 -70.78 70.78 o -9 4 1 331.51 331.47 64.08 o -8 4 1 51.10 84.93 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