#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/02/2100297.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100297_Fobs loop_ _publ_author_name 'Hao, Xiang' 'Parkin, Sean' 'Brock, Carolyn Pratt' _publ_section_title ; Three modulation patterns in four related [M(H~2~O)~2~(15-crown-5)](NO~3~)~2~ structures ; _journal_coeditor_code BM5026 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 675 _journal_page_last 688 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.461 _cell_angle_gamma 90.000 _cell_length_a 14.4970 _cell_length_b 14.1810 _cell_length_c 25.7000 _exptl_crystal_F_000 2568.00 _reflns_d_resolution_high 0.7693 _[local]_cod_data_source_file bm5026k02119sup7.hkl _[local]_cod_data_source_block k02119 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k02119 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 564.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3.80 23.24 6.57 o 2 0 0 52406.09 49795.37 746.12 o 3 0 0 7.15 13.95 13.95 o 4 0 0 117422.48 114223.14 1767.09 o 5 0 0 80.99 69.73 19.72 o 6 0 0 7539.97 6981.18 255.69 o 7 0 0 2284.58 2349.61 68.80 o 8 0 0 4524.58 4960.44 144.12 o 9 0 0 4900.73 4916.61 251.04 o 10 0 0 9265.13 8830.71 183.17 o 11 0 0 8.37 92.98 58.21 o 12 0 0 7772.03 7782.35 177.13 o 13 0 0 47.87 54.10 71.43 o 14 0 0 5442.03 5827.11 239.36 o 15 0 0 390.10 423.71 111.57 o 16 0 0 384.36 212.72 131.80 o 17 0 0 4.77 34.92 223.15 o 18 0 0 1832.49 1785.11 198.51 o 1 1 0 4.57 41.02 4.65 o 2 1 0 35415.83 37372.20 365.70 o 3 1 0 87.18 83.07 8.05 o 4 1 0 36.08 58.89 10.02 o 5 1 0 49.37 26.03 30.87 o 6 1 0 58897.05 61735.45 743.73 o 7 1 0 926.36 919.97 37.58 o 8 1 0 2474.58 2169.57 100.65 o 9 1 0 298.95 368.18 41.87 o 10 1 0 1782.65 1958.01 87.47 o 11 1 0 305.63 321.02 40.26 o 12 1 0 3838.40 3803.69 84.17 o 13 1 0 87.01 122.96 61.73 o 14 1 0 10.69 144.18 106.02 o 15 1 0 42.31 64.24 75.76 o 16 1 0 1.58 92.14 95.18 o 17 1 0 13.93 33.90 106.96 o 18 1 0 849.96 784.31 166.41 o 0 2 0 106439.27 100095.33 1969.07 o 1 2 0 37.66 40.47 6.32 o 2 2 0 149187.00 147101.55 1573.70 o 3 2 0 434.45 402.16 12.72 o 4 2 0 2854.47 2376.84 56.36 o 5 2 0 46.88 8.63 15.78 o 6 2 0 37078.90 39400.89 458.73 o 7 2 0 2539.77 2602.56 48.05 o 8 2 0 21946.98 22164.11 296.23 o 9 2 0 685.81 632.85 37.44 o 10 2 0 928.31 1031.56 64.42 o 11 2 0 140.98 136.32 37.00 o 12 2 0 1191.19 1135.12 60.63 o 13 2 0 23.87 16.68 49.55 o 14 2 0 296.88 219.34 71.66 o 15 2 0 208.01 205.10 75.62 o 16 2 0 5483.98 5542.32 165.29 o 17 2 0 1.46 -123.81 123.81 o 18 2 0 502.54 514.06 142.38 o 1 3 0 302.66 299.30 24.16 o 2 3 0 170015.66 172994.17 1871.27 o 3 3 0 185.53 163.48 12.17 o 4 3 0 13937.32 12734.06 147.96 o 5 3 0 769.57 815.43 25.25 o 6 3 0 30575.09 32145.17 367.57 o 7 3 0 1821.57 1857.32 44.93 o 8 3 0 24858.61 26822.39 339.32 o 9 3 0 63.82 77.08 69.01 o 10 3 0 2543.92 2547.50 70.81 o 11 3 0 979.35 970.00 67.10 o 12 3 0 7801.54 8111.06 149.68 o 13 3 0 224.53 176.47 53.06 o 14 3 0 3721.16 3739.37 128.36 o 15 3 0 150.14 244.05 79.18 o 16 3 0 530.42 647.98 121.30 o 17 3 0 12.60 -14.49 117.78 o 18 3 0 14.34 -113.08 132.43 o 0 4 0 45102.76 43409.45 653.55 o 1 4 0 57.72 67.67 5.88 o 2 4 0 8267.62 8335.66 97.73 o 3 4 0 8.46 18.60 16.10 o 4 4 0 20265.33 18976.23 213.97 o 5 4 0 1564.80 1586.07 36.23 o 6 4 0 705.72 556.49 27.30 o 7 4 0 2131.90 2147.01 76.50 o 8 4 0 38552.33 38445.37 488.62 o 9 4 0 1426.68 1388.35 67.96 o 10 4 0 3878.01 3716.84 89.06 o 11 4 0 1064.67 1047.63 64.89 o 12 4 0 3261.08 2980.95 87.50 o 13 4 0 1.58 -21.54 58.91 o 14 4 0 3182.13 2956.82 106.73 o 15 4 0 19.00 12.02 88.03 o 16 4 0 193.50 259.65 115.13 o 17 4 0 15.91 126.67 122.27 o 18 4 0 2021.18 2357.84 242.91 o 1 5 0 0.66 -3.98 12.08 o 2 5 0 1703.20 1347.61 29.52 o 3 5 0 340.52 321.14 30.76 o 4 5 0 1437.50 1546.35 37.08 o 5 5 0 1657.23 1802.00 45.63 o 6 5 0 3076.10 2991.88 53.86 o 7 5 0 146.62 173.72 26.75 o 8 5 0 7593.63 8206.27 144.94 o 9 5 0 352.91 386.65 38.21 o 10 5 0 861.49 757.97 54.23 o 11 5 0 4.02 -26.44 45.29 o 12 5 0 82.58 92.11 57.28 o 13 5 0 102.63 190.74 65.90 o 14 5 0 36.99 52.61 83.10 o 15 5 0 0.04 52.75 98.02 o 16 5 0 284.34 61.66 151.65 o 17 5 0 21.34 -136.07 136.07 o 18 5 0 1051.12 1124.08 199.57 o 0 6 0 23895.72 26499.23 468.61 o 1 6 0 164.54 171.05 15.22 o 2 6 0 56.18 129.15 33.84 o 3 6 0 474.17 488.45 42.94 o 4 6 0 3846.73 3537.86 65.62 o 5 6 0 905.95 880.01 39.90 o 6 6 0 16058.86 16085.25 199.43 o 7 6 0 31.68 33.81 21.93 o 8 6 0 9429.14 9245.74 149.70 o 9 6 0 1125.63 1125.00 49.65 o 10 6 0 2713.62 2543.84 72.66 o 11 6 0 905.03 803.36 59.90 o 12 6 0 110.88 45.00 62.35 o 13 6 0 365.30 275.58 70.80 o 14 6 0 2445.12 2292.78 203.99 o 15 6 0 7.90 -91.53 91.53 o 16 6 0 916.54 885.39 143.00 o 17 6 0 0.42 -135.85 142.69 o 1 7 0 72.73 86.63 18.79 o 2 7 0 5838.85 6491.44 150.31 o 3 7 0 211.02 171.83 33.69 o 4 7 0 6968.89 7010.77 224.12 o 5 7 0 388.36 452.95 58.29 o 6 7 0 1204.80 1212.07 55.50 o 7 7 0 156.54 170.56 24.27 o 8 7 0 565.74 614.77 42.11 o 9 7 0 463.63 498.59 52.95 o 10 7 0 6001.51 5836.80 148.96 o 11 7 0 481.36 525.02 73.81 o 12 7 0 10.00 -5.93 63.56 o 13 7 0 440.17 572.06 92.53 o 14 7 0 1847.40 1805.21 158.36 o 15 7 0 216.61 387.70 111.39 o 16 7 0 1164.33 1153.30 148.96 o 17 7 0 68.47 123.89 144.20 o 0 8 0 44277.87 45322.55 798.30 o 1 8 0 208.61 210.42 22.23 o 2 8 0 13764.52 13081.20 198.87 o 3 8 0 13.95 -12.52 40.67 o 4 8 0 23.42 90.67 37.51 o 5 8 0 272.58 226.83 34.89 o 6 8 0 1635.91 1551.59 65.76 o 7 8 0 38.43 -41.07 41.07 o 8 8 0 2806.87 2710.84 81.16 o 9 8 0 0.56 19.42 49.55 o 10 8 0 4829.95 4825.53 118.96 o 11 8 0 114.31 83.35 66.94 o 12 8 0 6071.77 6252.02 240.22 o 13 8 0 76.56 80.41 96.66 o 14 8 0 113.52 261.31 105.84 o 15 8 0 4.93 -4.12 113.23 o 16 8 0 932.92 1062.24 203.31 o 1 9 0 249.22 219.40 23.08 o 2 9 0 576.77 568.03 38.87 o 3 9 0 223.05 217.08 18.38 o 4 9 0 12675.31 13140.51 231.00 o 5 9 0 13.15 -41.35 42.54 o 6 9 0 1073.88 959.37 65.98 o 7 9 0 251.08 257.49 67.10 o 8 9 0 866.63 783.21 61.06 o 9 9 0 73.14 -5.88 55.48 o 10 9 0 1526.75 1621.81 83.94 o 11 9 0 89.12 76.12 74.88 o 12 9 0 43.87 -95.38 100.65 o 13 9 0 118.88 102.15 108.70 o 14 9 0 193.15 56.70 100.00 o 15 9 0 1.21 -102.12 122.50 o 16 9 0 1.44 16.80 201.30 o 0 10 0 80603.60 82998.62 1701.76 o 1 10 0 15.90 1.77 33.81 o 2 10 0 333.43 326.27 40.26 o 3 10 0 3.57 57.51 55.02 o 4 10 0 3812.35 3585.56 109.06 o 5 10 0 6.58 11.67 55.75 o 6 10 0 7688.11 7823.62 184.10 o 7 10 0 168.41 176.80 69.50 o 8 10 0 3481.50 3098.32 107.65 o 9 10 0 443.29 487.58 69.90 o 10 10 0 1917.43 2069.61 140.91 o 11 10 0 2.95 100.78 92.83 o 12 10 0 10027.68 10554.84 240.04 o 13 10 0 104.12 162.64 130.18 o 14 10 0 1518.71 1422.42 130.63 o 15 10 0 124.06 144.73 181.00 o 1 11 0 2646.12 2769.72 115.41 o 2 11 0 1478.78 1673.62 78.05 o 3 11 0 38.01 97.39 58.32 o 4 11 0 616.47 663.97 100.65 o 5 11 0 28.52 -10.22 64.15 o 6 11 0 9067.35 8889.78 203.99 o 7 11 0 40.28 72.12 73.78 o 8 11 0 2161.11 1956.98 104.80 o 9 11 0 122.30 111.89 71.69 o 10 11 0 347.56 417.35 89.79 o 11 11 0 16.24 0.90 84.50 o 12 11 0 4083.12 4054.12 154.09 o 13 11 0 0.11 61.80 115.31 o 14 11 0 254.27 275.44 227.81 o 15 11 0 17.51 -204.55 529.98 o 0 12 0 228.38 76.07 129.16 o 1 12 0 187.90 207.81 59.95 o 2 12 0 10580.88 10647.34 242.91 o 3 12 0 176.20 133.88 62.58 o 4 12 0 1825.92 1720.35 87.81 o 5 12 0 144.16 88.83 81.72 o 6 12 0 8986.71 9075.46 213.15 o 7 12 0 88.11 -11.12 72.93 o 8 12 0 12573.82 13052.05 297.86 o 9 12 0 293.89 196.76 85.16 o 10 12 0 91.83 100.98 96.19 o 11 12 0 4.17 21.15 134.20 o 12 12 0 1454.44 1618.18 138.05 o 13 12 0 72.38 -36.60 126.64 o 14 12 0 714.88 718.10 169.27 o 1 13 0 1163.80 1152.02 111.57 o 2 13 0 434.67 540.60 97.27 o 3 13 0 156.66 195.25 83.00 o 4 13 0 198.78 207.76 70.73 o 5 13 0 207.95 164.99 106.89 o 6 13 0 82.78 56.96 72.53 o 7 13 0 119.64 3.71 83.21 o 8 13 0 6323.85 6261.94 194.22 o 9 13 0 41.93 10.86 104.68 o 10 13 0 170.77 171.34 115.41 o 11 13 0 93.12 -38.10 129.91 o 12 13 0 52.83 96.96 140.59 o 13 13 0 23.17 -183.60 223.46 o 0 14 0 1375.94 1498.14 194.06 o 1 14 0 579.92 599.32 116.63 o 2 14 0 5387.10 5479.83 224.12 o 3 14 0 199.54 181.58 95.34 o 4 14 0 15377.75 16750.80 404.93 o 5 14 0 6.70 -84.17 84.17 o 6 14 0 1720.30 1731.27 134.36 o 7 14 0 11.44 -112.85 112.85 o 8 14 0 4554.59 4433.18 178.88 o 9 14 0 157.10 167.22 125.54 o 10 14 0 41.34 169.09 123.89 o 11 14 0 16.83 13.97 166.41 o 12 14 0 587.01 667.24 277.09 o 1 15 0 74.03 75.75 108.94 o 2 15 0 3367.53 3277.72 195.96 o 3 15 0 59.35 -5.36 115.07 o 4 15 0 159.07 -39.04 131.70 o 5 15 0 18.37 -99.03 130.44 o 6 15 0 1251.63 1174.60 120.87 o 7 15 0 107.63 38.51 116.75 o 8 15 0 486.17 436.33 236.39 o 9 15 0 7.19 125.86 124.27 o 10 15 0 195.39 -65.56 156.39 o 0 16 0 3394.48 3840.90 369.33 o 1 16 0 2.26 176.34 179.83 o 2 16 0 1354.59 1587.04 170.03 o 3 16 0 36.14 -113.61 170.44 o 4 16 0 3032.22 2977.00 178.24 o 5 16 0 1.84 -73.74 120.94 o 6 16 0 4509.03 4195.50 295.25 o 7 16 0 189.56 432.56 182.92 o 8 16 0 144.57 420.29 184.54 o 9 16 0 36.06 130.06 172.16 o 1 17 0 263.51 568.23 222.94 o 2 17 0 336.48 207.82 195.82 o 3 17 0 1.57 -105.69 166.41 o 4 17 0 131.29 237.32 150.55 o 5 17 0 4.50 -105.11 138.67 o 6 17 0 0.36 -74.04 206.44 o 7 17 0 45.43 -46.03 188.49 o 0 18 0 5208.35 4914.33 466.79 o 1 18 0 4.83 166.24 194.87 o 2 18 0 930.82 1035.70 199.98 o 3 18 0 0.29 -68.16 204.43 o 4 18 0 1329.09 1387.23 311.29 o -18 1 1 81.94 -101.88 118.49 o -17 1 1 150.81 113.39 106.28 o -16 1 1 51.56 139.08 108.85 o -15 1 1 116.20 84.68 85.49 o -14 1 1 100.26 88.43 68.78 o -13 1 1 1914.66 1888.54 75.46 o -12 1 1 64.06 122.75 50.20 o -11 1 1 445.97 495.14 62.41 o -10 1 1 56.91 96.39 40.26 o -9 1 1 8732.13 9400.73 138.19 o -8 1 1 61.45 64.31 26.75 o -7 1 1 2401.55 2578.13 55.79 o -6 1 1 3.16 11.83 20.04 o -5 1 1 734.89 741.19 23.24 o -4 1 1 0.01 4.23 10.74 o -3 1 1 238.59 198.10 9.30 o -2 1 1 4.94 13.95 4.65 o -1 1 1 46.42 50.21 6.44 o 0 1 1 1.91 6.97 4.65 o 1 1 1 355.29 303.76 7.60 o 2 1 1 0.32 -6.71 6.71 o 3 1 1 212.85 225.28 11.35 o 4 1 1 2.78 28.38 11.33 o 5 1 1 10981.88 10728.77 123.89 o 6 1 1 2.61 23.99 17.69 o 7 1 1 12165.76 12493.33 160.14 o 8 1 1 459.52 476.97 30.71 o 9 1 1 18215.28 19158.73 247.97 o 10 1 1 0.31 -17.85 36.45 o 11 1 1 2041.08 2029.01 63.01 o 12 1 1 34.14 0.61 44.11 o 13 1 1 481.20 479.29 64.81 o 14 1 1 89.04 118.84 70.23 o 15 1 1 261.23 398.46 87.70 o 16 1 1 10.52 -67.27 100.02 o 17 1 1 442.27 300.20 105.61 o 18 1 1 24.41 6.69 114.07 o -18 2 1 21.39 10.64 143.21 o -17 2 1 72.34 -97.78 114.17 o -16 2 1 117.92 243.02 89.72 o -15 2 1 182.79 188.55 82.56 o -14 2 1 53.31 47.23 60.92 o -13 2 1 149.27 118.99 52.79 o -12 2 1 7.17 -0.31 40.66 o -11 2 1 89.00 85.50 40.26 o -10 2 1 17.13 -14.16 34.22 o -9 2 1 2559.92 2450.66 65.76 o -8 2 1 20.30 2.74 25.50 o -7 2 1 3688.44 3800.90 63.34 o -6 2 1 173.26 164.10 44.29 o -5 2 1 7.87 -15.78 15.78 o -4 2 1 7.32 9.30 10.94 o -3 2 1 62.33 61.99 10.02 o -2 2 1 4.59 -3.72 7.03 o -1 2 1 110.24 105.17 4.65 o 0 2 1 36.09 32.54 5.37 o 1 2 1 20.89 24.32 4.65 o 2 2 1 134.95 135.00 9.39 o 3 2 1 1146.99 1202.25 19.49 o 4 2 1 30.95 35.33 10.94 o 5 2 1 2385.28 2320.93 36.75 o 6 2 1 516.00 477.88 21.59 o 7 2 1 108.09 184.03 27.30 o 8 2 1 935.02 872.02 37.00 o 9 2 1 409.45 429.31 35.84 o 10 2 1 207.84 185.80 33.26 o 11 2 1 3905.45 3999.27 80.75 o 12 2 1 1087.19 1093.06 59.43 o 13 2 1 107.76 103.74 77.84 o 14 2 1 16.26 35.98 63.63 o 15 2 1 1830.15 1992.96 110.99 o 16 2 1 4.02 -8.48 94.10 o 17 2 1 62.47 95.89 114.51 o 18 2 1 17.88 15.88 124.24 o -18 3 1 202.76 387.42 123.33 o -17 3 1 358.20 283.51 114.98 o -16 3 1 160.08 221.07 95.36 o -15 3 1 14.56 81.35 77.82 o -14 3 1 23.58 102.59 67.89 o -13 3 1 1273.58 1339.47 77.15 o -12 3 1 199.08 172.72 48.05 o -11 3 1 2870.15 2682.24 74.53 o -10 3 1 226.12 231.68 36.75 o -9 3 1 6130.89 6089.73 106.12 o -8 3 1 11.29 23.05 38.92 o -7 3 1 5884.04 6412.01 92.11 o -6 3 1 38.68 68.47 20.04 o -5 3 1 2.02 -15.22 15.22 o -4 3 1 48.31 44.63 14.78 o -3 3 1 2654.92 2254.73 32.04 o -2 3 1 85.34 105.66 10.74 o -1 3 1 630.38 667.76 15.22 o 0 3 1 4.90 0.00 9.30 o 1 3 1 1498.15 1548.21 22.53 o 2 3 1 133.43 122.61 20.13 o 3 3 1 95.46 92.20 24.16 o 4 3 1 136.77 114.23 15.53 o 5 3 1 4382.92 4324.08 60.74 o 6 3 1 0.17 -13.95 18.60 o 7 3 1 1116.45 1348.49 42.45 o 8 3 1 102.41 99.81 29.52 o 9 3 1 919.21 812.36 74.81 o 10 3 1 94.04 55.22 48.31 o 11 3 1 28.26 17.40 42.77 o 12 3 1 126.51 117.79 57.69 o 13 3 1 482.41 440.44 63.03 o 14 3 1 55.92 -19.56 68.19 o 15 3 1 875.70 794.83 92.42 o 16 3 1 99.36 87.18 107.04 o 17 3 1 147.11 221.70 116.42 o 18 3 1 92.06 60.86 123.19 o -18 4 1 19.02 45.98 191.91 o -17 4 1 199.99 292.84 119.33 o -16 4 1 0.57 101.33 92.37 o -15 4 1 1059.68 1112.08 113.55 o -14 4 1 3.51 45.80 66.90 o -13 4 1 2.65 0.20 77.78 o -12 4 1 13.77 8.62 47.19 o -11 4 1 454.93 510.45 52.70 o -10 4 1 32.16 26.72 38.75 o -9 4 1 478.17 542.88 68.44 o -8 4 1 157.43 157.71 29.95 o -7 4 1 904.95 914.77 35.39 o -6 4 1 95.38 177.30 32.21 o -5 4 1 9529.79 9735.65 163.73 o -4 4 1 129.34 140.04 18.79 o -3 4 1 2205.27 2147.23 42.94 o -2 4 1 4.96 11.50 17.45 o -1 4 1 3598.77 3496.36 50.82 o 0 4 1 58.80 51.70 9.30 o 1 4 1 0.08 8.45 13.42 o 2 4 1 6.71 17.92 25.50 o 3 4 1 580.44 554.40 38.92 o 4 4 1 230.38 226.78 26.55 o 5 4 1 5485.31 5648.72 95.37 o 6 4 1 3.38 32.06 23.95 o 7 4 1 974.45 1101.89 37.19 o 8 4 1 116.06 76.45 26.47 o 9 4 1 1405.73 1488.36 53.06 o 10 4 1 353.41 302.86 51.00 o 11 4 1 2752.30 2732.91 115.60 o 12 4 1 73.73 37.03 53.40 o 13 4 1 1367.86 1393.88 81.03 o 14 4 1 434.38 441.16 77.72 o 15 4 1 128.09 35.58 89.33 o 16 4 1 1.69 -42.20 119.58 o 17 4 1 178.46 184.62 116.81 o 18 4 1 30.95 -13.35 131.07 o -18 5 1 0.18 118.87 175.23 o -17 5 1 0.03 -86.85 132.09 o -16 5 1 0.23 -96.41 96.41 o -15 5 1 769.48 573.20 83.05 o -14 5 1 66.37 35.94 92.60 o -13 5 1 55.83 33.84 61.28 o -12 5 1 34.19 21.41 56.02 o -11 5 1 2794.88 2638.93 85.75 o -10 5 1 616.10 630.72 52.78 o -9 5 1 12642.01 12402.59 183.66 o -8 5 1 306.90 313.16 33.69 o -7 5 1 2263.44 2410.52 53.86 o -6 5 1 52.65 40.09 24.99 o -5 5 1 5734.57 5871.55 111.39 o -4 5 1 0.17 3.40 16.10 o -3 5 1 864.24 887.77 23.63 o -2 5 1 0.37 10.19 17.45 o -1 5 1 515.39 502.74 30.87 o 0 5 1 11.46 16.27 14.09 o 1 5 1 3002.22 2937.04 46.14 o 2 5 1 114.22 125.69 21.52 o 3 5 1 347.56 351.39 26.96 o 4 5 1 298.54 331.91 26.03 o 5 5 1 3755.96 3991.05 85.21 o 6 5 1 15.17 -17.91 21.47 o 7 5 1 1223.95 1057.58 37.44 o 8 5 1 321.86 301.19 34.28 o 9 5 1 4689.89 4657.72 118.24 o 10 5 1 3.86 65.00 42.13 o 11 5 1 380.15 437.86 70.03 o 12 5 1 484.93 449.30 58.91 o 13 5 1 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