#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2100303.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100303_Fobs loop_ _publ_author_name 'Cowan, John. A.' 'Howard, Judith A. K.' 'McIntyre, Garry, J.' 'Lo, Samuel M.-F' 'Williams, Ian D.' _publ_section_title ; Variable-temperature neutron diffraction studies of the short, strong hydrogen bonds in the crystal structure of pyridine-3,5-dicarboxylic acid ; _journal_coeditor_code BS5020 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 724 _journal_page_last 730 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.754 _cell_angle_gamma 90.000 _cell_length_a 9.7196 _cell_length_b 11.1396 _cell_length_c 6.4540 _exptl_crystal_F_000 254.94 _reflns_d_resolution_high 0.7158 _[local]_cod_data_source_file bs5020dad15sup4.hkl _[local]_cod_data_source_block dad15 #BEGIN Tags that were not found in dictionaries: _shelx_title ' PDA P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 321.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 354.29 436.96 23.54 o 3 0 0 588.66 540.87 28.70 o 4 0 0 13333.94 13053.91 117.03 o 5 0 0 162.16 177.11 17.18 o 6 0 0 3007.48 2909.61 59.28 o 7 0 0 2200.76 2301.40 55.79 o 8 0 0 6855.06 6999.96 102.16 o 9 0 0 39.81 78.18 23.35 o 10 0 0 7514.16 8280.90 142.96 o 11 0 0 276.43 310.14 52.66 o 12 0 0 2.48 8.82 30.57 o 1 1 0 105.54 260.41 38.55 o 2 1 0 58.09 117.43 13.07 o 3 1 0 2.10 37.73 11.47 o 4 1 0 188.18 186.30 17.42 o 5 1 0 415.15 349.73 21.76 o 6 1 0 4245.00 4261.80 70.80 o 7 1 0 4.80 8.35 14.01 o 8 1 0 37.78 40.41 17.58 o 9 1 0 1621.33 1853.04 66.08 o 10 1 0 18.72 77.40 27.04 o 11 1 0 3368.62 3853.60 112.45 o 12 1 0 582.72 648.28 67.54 o 0 2 0 54.39 82.20 9.32 o 1 2 0 4433.40 4670.07 43.40 o 2 2 0 263.45 243.19 17.72 o 3 2 0 212.68 185.99 17.29 o 4 2 0 0.72 -3.77 10.38 o 5 2 0 1894.94 1870.47 46.19 o 6 2 0 38.28 73.06 21.96 o 7 2 0 386.32 312.68 24.02 o 8 2 0 872.00 777.26 39.53 o 9 2 0 99.32 61.43 34.48 o 10 2 0 598.16 498.35 42.78 o 11 2 0 996.85 984.01 64.11 o 12 2 0 1749.21 1668.84 87.27 o 1 3 0 205.84 255.22 17.71 o 2 3 0 5.78 35.76 19.58 o 3 3 0 1026.25 988.20 35.74 o 4 3 0 1.89 42.41 18.53 o 5 3 0 806.96 944.27 36.49 o 6 3 0 2264.47 2257.25 53.47 o 7 3 0 5770.52 5829.36 118.18 o 8 3 0 2477.11 2784.54 70.19 o 9 3 0 7.55 17.24 33.49 o 10 3 0 277.19 403.69 48.59 o 11 3 0 464.96 577.76 61.58 o 12 3 0 503.84 355.09 49.80 o 0 4 0 169.68 153.54 16.31 o 1 4 0 83.01 89.16 12.02 o 2 4 0 751.29 855.02 34.49 o 3 4 0 85.70 146.47 21.49 o 4 4 0 5053.85 4670.99 71.15 o 5 4 0 99.24 99.04 23.22 o 6 4 0 1039.86 1030.27 41.20 o 7 4 0 172.32 189.15 28.28 o 8 4 0 14232.14 14912.38 164.90 o 9 4 0 1.25 53.68 22.46 o 10 4 0 282.26 368.99 50.25 o 11 4 0 11.24 133.95 37.39 o 12 4 0 2065.50 2429.05 106.99 o 1 5 0 1492.26 1456.46 106.65 o 2 5 0 444.87 462.81 24.45 o 3 5 0 8450.53 8148.79 93.25 o 4 5 0 611.73 570.31 30.17 o 5 5 0 19.79 76.28 23.18 o 6 5 0 322.67 248.35 22.38 o 7 5 0 54105.52 57086.68 502.13 o 8 5 0 45.78 53.51 22.46 o 9 5 0 60.17 22.50 37.53 o 10 5 0 1331.60 1252.69 66.92 o 11 5 0 4039.52 4706.70 131.08 o 0 6 0 2199.58 2178.37 48.95 o 1 6 0 384.70 381.29 22.09 o 2 6 0 37.95 49.20 13.37 o 3 6 0 2317.15 2535.53 56.75 o 4 6 0 159.94 97.37 16.16 o 5 6 0 61.08 75.03 16.42 o 6 6 0 767.76 855.39 41.70 o 7 6 0 8.08 88.76 35.56 o 8 6 0 4049.09 4245.73 98.49 o 9 6 0 0.30 -10.93 38.31 o 10 6 0 2357.11 2739.05 98.43 o 11 6 0 1455.78 1108.04 71.76 o 1 7 0 121.77 111.31 16.26 o 2 7 0 7.59 27.79 13.78 o 3 7 0 69.30 86.20 17.14 o 4 7 0 32.02 45.77 15.17 o 5 7 0 410.29 454.62 28.88 o 6 7 0 5928.61 6175.10 101.75 o 7 7 0 1044.15 744.15 43.72 o 8 7 0 3352.81 3526.96 96.61 o 9 7 0 2941.86 3459.24 103.84 o 10 7 0 88.62 148.27 37.26 o 11 7 0 1995.27 1407.89 100.84 o 0 8 0 22595.83 21933.83 352.20 o 1 8 0 1419.46 1361.79 45.69 o 2 8 0 490.90 517.07 28.34 o 3 8 0 976.00 919.17 40.27 o 4 8 0 1278.03 1294.08 47.18 o 5 8 0 392.53 438.87 32.41 o 6 8 0 46.21 53.61 43.71 o 7 8 0 105.14 82.03 41.27 o 8 8 0 1453.90 1488.38 71.20 o 9 8 0 170.33 428.12 58.52 o 10 8 0 1518.89 1555.49 83.85 o 1 9 0 20050.67 20131.31 167.54 o 2 9 0 142.67 109.98 26.24 o 3 9 0 3388.32 3268.85 72.15 o 4 9 0 12.18 52.86 29.28 o 5 9 0 4858.03 5254.74 103.01 o 6 9 0 160.47 165.27 41.65 o 7 9 0 62.15 79.00 41.54 o 8 9 0 47.40 89.28 33.83 o 9 9 0 2929.27 2879.12 107.01 o 10 9 0 464.76 622.93 72.92 o 0 10 0 31929.53 32123.85 311.32 o 1 10 0 625.72 698.52 38.75 o 2 10 0 74.07 41.54 31.05 o 3 10 0 0.64 57.27 32.03 o 4 10 0 1213.23 1291.64 58.89 o 5 10 0 721.19 831.19 59.83 o 6 10 0 1736.96 1915.17 78.34 o 7 10 0 129.12 245.18 50.23 o 8 10 0 3033.77 3177.38 109.40 o 9 10 0 9.10 34.68 36.44 o 1 11 0 32.52 52.56 22.33 o 2 11 0 1511.31 1538.69 64.05 o 3 11 0 315.24 371.39 44.59 o 4 11 0 1422.48 1592.43 69.98 o 5 11 0 170.41 294.76 48.03 o 6 11 0 1331.69 1416.32 78.97 o 7 11 0 306.17 296.58 57.69 o 8 11 0 369.19 527.01 88.29 o 0 12 0 1.99 89.61 28.36 o 1 12 0 108.13 113.93 40.69 o 2 12 0 10.07 109.12 40.75 o 3 12 0 2135.07 2255.67 84.66 o 4 12 0 1571.27 1701.25 77.38 o 5 12 0 209.87 197.09 37.37 o 6 12 0 3.05 -29.01 29.01 o 7 12 0 288.42 338.86 55.48 o 1 13 0 22.57 12.72 27.82 o 2 13 0 274.32 256.60 39.96 o 3 13 0 501.94 550.88 62.03 o 4 13 0 0.94 39.43 29.62 o 5 13 0 27.56 94.84 35.08 o 6 13 0 617.45 558.59 55.79 o 0 14 0 325.39 342.26 57.62 o 1 14 0 331.53 352.31 57.93 o 2 14 0 5690.02 5910.36 145.45 o 3 14 0 6213.68 5579.47 146.15 o 4 14 0 2628.13 2546.85 106.61 o 1 15 0 3175.45 3243.92 121.12 o 2 15 0 114.48 231.76 46.83 o -12 1 1 1232.01 1135.38 69.24 o -11 1 1 77.39 182.06 41.54 o -10 1 1 162.50 428.80 46.74 o -9 1 1 6377.49 6285.23 107.49 o -8 1 1 542.28 551.03 30.42 o -7 1 1 138.36 146.81 24.78 o -6 1 1 373.43 728.06 28.71 o -5 1 1 6615.39 6309.13 79.45 o -4 1 1 741.00 781.92 32.54 o -3 1 1 331.29 501.20 23.50 o 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2 1 999.26 1072.92 31.25 o 8 2 1 17.30 16.35 18.93 o 9 2 1 1095.73 786.09 49.75 o 10 2 1 440.75 500.75 55.70 o 11 2 1 66.15 67.26 32.51 o -12 3 1 1148.48 807.16 62.01 o -11 3 1 107.35 442.44 54.88 o -10 3 1 4346.61 4550.04 108.54 o -9 3 1 872.81 1044.27 51.36 o -8 3 1 5147.70 5256.77 90.20 o -7 3 1 200.57 213.15 27.23 o -6 3 1 744.42 747.12 35.49 o -5 3 1 145.73 182.62 18.03 o -4 3 1 211.05 277.29 20.04 o -3 3 1 329.25 348.29 21.45 o -2 3 1 2652.37 2532.00 51.57 o -1 3 1 5.41 1.83 10.15 o 0 3 1 27.29 56.96 10.33 o 1 3 1 452.81 563.53 25.15 o 2 3 1 206.53 216.73 13.92 o 3 3 1 1178.34 1095.39 36.01 o 4 3 1 661.90 625.87 31.88 o 5 3 1 32.80 31.18 22.06 o 6 3 1 39.29 43.60 14.83 o 7 3 1 149.95 126.27 29.43 o 8 3 1 6436.28 6614.24 89.28 o 9 3 1 1212.82 938.50 53.06 o 10 3 1 2740.86 3070.60 99.72 o 11 3 1 316.52 385.95 60.57 o -12 4 1 6683.33 6886.67 160.20 o -11 4 1 4094.07 4224.22 118.63 o -10 4 1 579.56 488.23 43.15 o -9 4 1 2989.59 3465.81 87.73 o -8 4 1 10153.28 10023.09 128.75 o -7 4 1 1617.43 2187.44 55.73 o -6 4 1 11433.33 11105.83 83.04 o -5 4 1 482.50 452.75 25.50 o -4 4 1 1312.92 1204.99 38.71 o -2 4 1 15550.56 15221.61 127.10 o -1 4 1 1152.91 1343.68 39.51 o 0 4 1 3049.32 3023.73 40.37 o 1 4 1 2829.11 3254.01 41.91 o 2 4 1 14675.28 13624.22 119.96 o 3 4 1 396.41 558.07 26.41 o 4 4 1 416.26 325.59 18.45 o 5 4 1 1937.31 2240.02 38.85 o 6 4 1 11953.89 11302.34 490.18 o 7 4 1 2055.96 2319.02 52.70 o 8 4 1 9150.28 9110.86 137.73 o 9 4 1 289.27 260.97 46.48 o 10 4 1 1032.72 893.19 63.19 o 11 4 1 3182.93 3568.91 120.52 o -12 5 1 1834.93 1687.73 94.09 o -11 5 1 674.74 581.67 62.05 o -10 5 1 12.26 3.70 23.38 o -9 5 1 168.94 358.62 35.13 o -8 5 1 6473.67 6492.72 110.11 o -7 5 1 4861.76 4761.32 83.78 o -6 5 1 1161.60 1042.08 41.22 o -5 5 1 854.12 819.91 36.66 o -4 5 1 842.02 773.85 34.35 o -3 5 1 782.26 827.04 33.37 o -2 5 1 1359.18 1348.14 39.83 o -1 5 1 1559.60 1598.74 42.04 o 0 5 1 63.70 149.77 11.61 o 1 5 1 1371.57 1519.91 41.58 o 2 5 1 959.41 973.07 35.34 o 3 5 1 251.76 245.28 14.22 o 4 5 1 581.60 560.58 29.55 o 5 5 1 287.47 324.10 31.25 o 6 5 1 921.69 996.11 47.13 o 7 5 1 3554.27 3698.51 84.27 o 8 5 1 3910.51 4310.50 101.15 o 9 5 1 433.73 371.07 41.30 o 10 5 1 18.80 52.83 31.11 o 11 5 1 507.07 534.74 55.88 o -11 6 1 453.34 661.42 67.45 o -10 6 1 1190.29 1169.44 64.24 o -9 6 1 2073.63 2461.10 82.95 o -8 6 1 4587.93 5162.07 103.68 o -7 6 1 2255.31 2160.93 64.00 o -6 6 1 2292.98 2280.33 57.42 o -5 6 1 1222.93 1143.94 42.52 o -4 6 1 71.28 233.93 20.63 o -3 6 1 727.47 826.45 36.99 o -2 6 1 3761.87 3556.04 62.69 o -1 6 1 182.47 126.42 10.87 o 0 6 1 41.47 44.32 18.27 o 1 6 1 140.45 278.86 20.03 o 2 6 1 3042.00 2871.93 58.50 o 3 6 1 2729.45 2589.70 57.01 o 4 6 1 395.06 452.11 26.94 o 5 6 1 1110.41 1181.62 43.72 o 6 6 1 376.67 392.45 30.88 o 7 6 1 4876.58 5172.81 105.17 o 8 6 1 6448.76 6629.05 129.36 o 9 6 1 426.75 471.55 56.45 o 10 6 1 3107.31 3208.07 111.02 o 11 6 1 974.50 965.44 87.52 o -11 7 1 2570.56 2692.99 109.40 o -10 7 1 1139.77 949.63 72.84 o 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8 1 150.43 211.17 27.73 o 4 8 1 53.43 8.69 26.06 o 5 8 1 214.92 218.53 26.55 o 6 8 1 708.01 646.96 42.80 o 7 8 1 130.13 230.52 51.01 o 8 8 1 2253.67 2323.06 91.22 o 9 8 1 3699.50 4206.00 124.75 o 10 8 1 4383.05 4789.28 142.64 o -10 9 1 1564.70 2289.00 99.86 o -9 9 1 3557.24 3528.89 112.45 o -8 9 1 49.58 10.42 48.39 o -7 9 1 58.31 36.24 37.97 o -6 9 1 270.99 685.34 190.39 o -5 9 1 12592.10 11514.54 118.73 o -4 9 1 86.83 225.24 32.44 o -3 9 1 550.20 492.11 31.27 o -2 9 1 3546.85 3859.27 74.20 o -1 9 1 5273.45 4862.94 65.85 o 0 9 1 331.62 584.70 53.94 o 1 9 1 4761.52 4666.41 83.60 o 2 9 1 1224.48 1358.28 49.76 o 3 9 1 982.11 896.81 47.03 o 4 9 1 459.83 833.74 268.96 o 5 9 1 10543.08 9900.14 103.37 o 6 9 1 225.61 224.43 45.42 o 7 9 1 2.16 124.62 39.19 o 8 9 1 133.50 241.04 60.28 o 9 9 1 3294.21 3635.50 123.52 o -9 10 1 190.42 260.58 65.65 o -8 10 1 96.80 144.40 51.58 o -7 10 1 162.61 243.37 48.81 o -6 10 1 1559.99 1643.45 73.20 o -5 10 1 806.66 873.05 61.58 o -4 10 1 1770.27 1841.28 67.03 o -3 10 1 3563.68 3455.30 82.62 o -1 10 1 14322.48 13825.49 152.06 o 0 10 1 5125.79 5682.38 110.40 o 1 10 1 14095.21 13290.26 152.15 o 2 10 1 1175.67 1261.58 56.20 o 3 10 1 4051.13 3953.32 91.76 o 4 10 1 1656.33 1652.04 67.54 o 5 10 1 836.37 801.34 49.78 o 6 10 1 1243.39 1379.18 72.62 o 7 10 1 222.21 324.73 52.24 o 8 10 1 6.71 -5.46 31.55 o -9 11 1 3262.92 3446.43 124.93 o -7 11 1 525.39 521.96 60.91 o -6 11 1 44.16 161.21 51.17 o -5 11 1 1380.14 1574.93 73.44 o -4 11 1 970.24 605.54 44.52 o -3 11 1 31.51 34.81 24.57 o -2 11 1 167.27 355.07 130.46 o -1 11 1 2313.60 2497.58 76.99 o 0 11 1 979.55 1001.91 35.27 o 1 11 1 5951.30 6019.34 114.40 o 2 11 1 90.63 51.75 36.99 o 3 11 1 355.19 432.38 46.83 o 4 11 1 40.29 243.23 45.94 o 5 11 1 1530.17 1468.34 75.50 o 6 11 1 46.16 8.48 49.47 o 7 11 1 652.12 692.02 68.33 o 8 11 1 1147.64 1076.87 71.87 o -8 12 1 1735.37 1702.32 90.39 o -7 12 1 9.41 90.39 40.44 o -6 12 1 694.28 708.93 54.61 o -5 12 1 219.49 428.98 59.78 o -4 12 1 4933.84 4940.23 120.38 o -3 12 1 2510.76 2444.84 86.79 o -2 12 1 1146.37 1136.06 60.47 o -1 12 1 352.34 550.96 220.55 o 0 12 1 9519.70 9091.25 221.48 o 1 12 1 410.66 535.65 44.15 o 2 12 1 496.00 723.75 52.08 o 3 12 1 1909.87 2070.21 82.76 o 4 12 1 2528.65 2501.15 94.89 o 5 12 1 896.41 897.72 62.05 o 6 12 1 368.20 355.46 59.83 o 7 12 1 775.17 835.40 78.34 o -6 13 1 37.82 123.68 42.04 o -5 13 1 1738.91 2060.79 94.73 o -4 13 1 244.49 533.53 62.67 o -3 13 1 2995.32 3169.84 104.80 o -2 13 1 367.69 520.18 48.66 o -1 13 1 1891.55 1901.73 83.44 o 0 13 1 247.09 428.34 30.30 o 1 13 1 1256.13 1340.98 71.50 o 2 13 1 1977.66 1964.74 88.18 o 3 13 1 4197.79 3910.28 118.37 o 4 13 1 942.70 908.23 64.16 o 5 13 1 1453.41 1629.94 92.14 o -5 14 1 2159.83 2082.73 103.77 o -4 14 1 953.02 942.65 69.67 o -3 14 1 219.80 593.10 67.45 o -2 14 1 5946.29 5601.28 142.33 o -1 14 1 359.50 367.24 46.72 o 0 14 1 299.71 473.14 44.27 o 1 14 1 245.26 566.49 64.57 o 2 14 1 5336.83 5437.92 143.67 o 3 14 1 30.83 137.08 41.57 o 4 14 1 363.76 514.84 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