#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/03/2100343.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100343_Fobs loop_ _publ_author_name 'Hao, Xiang' 'Parkin, Sean' 'Brock, Carolyn Pratt' _publ_section_title ; The unusual phases of anhydrous and hydrated pinacol ; _journal_coeditor_code WS5034 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 689 _journal_page_last 699 _journal_volume 61 _journal_year 2005 _space_group_IT_number 58 _symmetry_space_group_name_Hall '-P 2 2n' _symmetry_space_group_name_H-M 'P n n m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.3080 _cell_length_b 6.3210 _cell_length_c 15.7590 _exptl_crystal_F_000 252.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file ws5034k03226osup5.hkl _[local]_cod_data_source_block k03226o #BEGIN Tags that were not found in dictionaries: _shelx_title ' k03226o in Pnnm' _shelx_refln_list_code 4 _shelx_f_calc_maximum 56.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z' 'x-1/2, -y-1/2, z-1/2' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 595.51 588.76 13.94 o 4 0 0 92.10 91.46 3.69 o 6 0 0 491.79 528.85 26.73 o 8 0 0 16.73 12.87 2.64 o 1 1 0 157.42 143.02 2.31 o 2 1 0 2853.81 2886.75 39.69 o 3 1 0 1860.39 1882.01 25.27 o 4 1 0 153.82 136.74 2.89 o 5 1 0 18.36 16.81 0.90 o 6 1 0 16.49 14.80 1.19 o 7 1 0 3.09 3.20 1.53 o 8 1 0 41.81 49.65 4.61 o 0 2 0 662.02 672.31 20.97 o 1 2 0 2894.79 2862.35 60.95 o 2 2 0 1898.53 1954.95 33.97 o 3 2 0 177.51 203.98 3.85 o 4 2 0 260.13 271.62 7.97 o 5 2 0 353.22 361.96 9.49 o 6 2 0 8.81 9.01 1.77 o 7 2 0 61.32 62.44 4.41 o 1 3 0 1965.04 1978.02 36.58 o 2 3 0 191.00 195.81 4.63 o 3 3 0 400.71 388.02 10.21 o 4 3 0 15.75 15.45 1.39 o 5 3 0 247.96 253.69 6.95 o 6 3 0 0.29 -0.76 1.54 o 7 3 0 75.18 74.75 4.74 o 0 4 0 88.55 91.06 3.39 o 1 4 0 163.07 148.25 4.60 o 2 4 0 229.59 244.11 5.84 o 3 4 0 15.45 17.01 1.22 o 4 4 0 46.70 51.46 2.48 o 5 4 0 132.31 148.56 12.63 o 6 4 0 0.77 0.92 2.66 o 7 4 0 22.36 23.15 4.14 o 1 5 0 20.93 21.33 2.12 o 2 5 0 389.92 397.12 11.37 o 3 5 0 264.43 262.70 10.02 o 4 5 0 136.16 151.59 6.44 o 5 5 0 9.49 6.46 3.57 o 6 5 0 0.94 1.13 2.36 o 1 6 0 16.61 18.83 4.82 o 2 6 0 7.98 9.46 1.75 o 3 6 0 0.17 -0.75 2.01 o 4 6 0 1.18 -1.87 2.77 o 5 6 0 1.02 -0.26 3.48 o 1 7 0 1.76 0.89 2.59 o 2 7 0 66.85 68.40 4.25 o 4 7 0 26.95 38.39 7.23 o 1 0 1 821.57 791.76 12.51 o 3 0 1 55.71 58.55 0.99 o 5 0 1 22.97 19.69 1.38 o 7 0 1 0.83 1.17 1.39 o 0 1 1 774.32 727.34 13.40 o 1 1 1 253.29 242.66 3.06 o 2 1 1 3.08 2.39 0.17 o 3 1 1 71.89 78.02 1.11 o 4 1 1 14.84 13.24 0.54 o 5 1 1 9.36 7.95 0.54 o 6 1 1 2.03 0.14 0.69 o 7 1 1 0.51 1.03 0.87 o 8 1 1 3.85 5.75 2.30 o 1 2 1 6.36 7.65 0.41 o 2 2 1 15.04 12.60 0.60 o 3 2 1 45.52 44.51 1.29 o 4 2 1 38.87 44.97 1.21 o 5 2 1 32.96 29.25 1.02 o 6 2 1 2.63 2.88 0.65 o 7 2 1 1.76 0.80 1.70 o 0 3 1 56.22 63.56 1.85 o 1 3 1 74.34 81.23 1.51 o 2 3 1 32.72 31.58 0.91 o 3 3 1 0.66 1.22 0.55 o 4 3 1 107.18 107.06 2.34 o 5 3 1 0.37 0.12 0.65 o 6 3 1 2.95 4.09 1.07 o 7 3 1 2.54 5.30 2.34 o 1 4 1 11.20 11.40 0.59 o 2 4 1 36.70 39.28 1.24 o 3 4 1 119.49 131.50 3.15 o 4 4 1 2.99 6.42 1.31 o 5 4 1 2.00 1.29 0.98 o 6 4 1 0.55 0.25 1.21 o 7 4 1 4.07 6.79 1.91 o 0 5 1 22.46 16.13 1.41 o 1 5 1 6.49 4.05 0.70 o 2 5 1 34.88 31.05 1.22 o 3 5 1 0.51 -0.39 0.73 o 4 5 1 3.08 1.29 1.08 o 5 5 1 0.07 0.90 1.66 o 6 5 1 0.29 -1.96 1.96 o 1 6 1 2.56 1.78 0.82 o 2 6 1 2.09 1.58 1.52 o 3 6 1 2.75 5.27 0.99 o 4 6 1 0.60 3.09 1.92 o 5 6 1 0.50 2.43 3.11 o 1 7 1 1.08 0.70 1.49 o 2 7 1 1.95 3.30 1.62 o 3 7 1 1.87 1.70 3.26 o 4 7 1 4.66 8.61 2.60 o 0 0 2 398.97 405.29 9.53 o 2 0 2 1580.40 1665.42 31.92 o 4 0 2 23.34 23.71 0.77 o 6 0 2 28.35 21.22 1.44 o 8 0 2 2.35 3.98 2.87 o 1 1 2 1607.18 1562.24 23.42 o 2 1 2 165.83 153.79 1.70 o 3 1 2 340.56 366.83 4.39 o 4 1 2 76.47 76.32 1.31 o 5 1 2 65.68 58.91 1.27 o 6 1 2 1.58 2.22 0.71 o 7 1 2 13.77 14.95 1.44 o 8 1 2 0.70 0.34 2.01 o 0 2 2 1691.35 1700.33 29.95 o 1 2 2 153.18 143.76 2.01 o 2 2 2 30.99 27.01 0.52 o 3 2 2 45.28 51.81 0.86 o 4 2 2 190.56 189.88 3.54 o 5 2 2 4.09 3.74 0.57 o 6 2 2 44.47 40.06 1.39 o 7 2 2 3.78 4.15 1.38 o 1 3 2 325.87 332.98 5.36 o 2 3 2 52.22 56.61 1.10 o 3 3 2 39.12 33.64 1.08 o 4 3 2 2.34 1.99 0.43 o 5 3 2 0.48 0.51 0.76 o 6 3 2 0.55 1.07 1.09 o 7 3 2 36.74 41.93 2.40 o 0 4 2 19.74 25.11 1.17 o 1 4 2 69.49 68.75 1.37 o 2 4 2 216.63 214.65 5.15 o 3 4 2 1.90 2.83 1.59 o 4 4 2 220.31 242.64 7.12 o 5 4 2 0.11 -1.14 1.14 o 6 4 2 0.46 -1.68 1.68 o 7 4 2 1.03 3.21 1.91 o 1 5 2 66.39 58.58 1.59 o 2 5 2 2.43 1.58 0.76 o 3 5 2 0.25 0.67 0.76 o 4 5 2 0.13 1.39 1.24 o 5 5 2 16.80 18.94 1.75 o 6 5 2 5.49 9.56 2.82 o 1 6 2 1.39 1.13 1.51 o 2 6 2 44.50 42.94 4.95 o 3 6 2 0.33 -0.45 1.19 o 4 6 2 0.75 1.89 1.51 o 5 6 2 5.38 5.24 2.13 o 1 7 2 12.10 12.41 2.37 o 2 7 2 4.36 6.42 1.89 o 3 7 2 40.50 45.06 7.01 o 4 7 2 1.54 2.74 2.44 o 1 0 3 3182.13 3175.41 55.86 o 3 0 3 1732.54 1834.56 33.96 o 5 0 3 71.79 69.85 2.23 o 7 0 3 53.26 53.97 2.60 o 0 1 3 3091.15 3038.59 62.79 o 1 1 3 421.92 433.70 6.52 o 2 1 3 130.76 116.72 1.42 o 3 1 3 183.38 177.59 2.31 o 4 1 3 38.38 36.17 1.15 o 5 1 3 121.89 124.34 2.36 o 6 1 3 24.10 21.94 1.03 o 7 1 3 21.52 18.66 1.53 o 8 1 3 2.62 4.21 1.68 o 1 2 3 140.64 130.45 1.90 o 2 2 3 829.97 888.60 10.82 o 3 2 3 352.43 372.67 5.78 o 4 2 3 96.13 89.12 2.05 o 5 2 3 39.41 39.34 1.35 o 6 2 3 5.65 5.54 1.37 o 7 2 3 2.35 1.24 1.47 o 0 3 3 1760.04 1845.80 40.69 o 1 3 3 186.93 189.18 2.63 o 2 3 3 332.92 340.48 5.24 o 3 3 3 3.86 4.78 0.43 o 4 3 3 7.48 9.02 0.70 o 5 3 3 7.83 5.84 0.84 o 6 3 3 63.40 64.54 2.73 o 7 3 3 6.93 6.35 1.76 o 1 4 3 37.76 39.45 0.98 o 2 4 3 94.74 91.30 2.16 o 3 4 3 5.75 6.61 0.59 o 4 4 3 36.92 36.17 1.66 o 5 4 3 10.27 9.11 1.04 o 6 4 3 3.30 4.13 1.63 o 7 4 3 3.69 3.02 1.90 o 0 5 3 69.79 69.25 3.10 o 1 5 3 135.32 138.64 2.89 o 2 5 3 42.02 40.28 2.99 o 3 5 3 7.35 4.14 0.93 o 4 5 3 11.86 10.59 1.23 o 5 5 3 78.55 88.53 4.06 o 6 5 3 0.71 4.77 2.35 o 1 6 3 22.02 19.15 1.79 o 2 6 3 7.57 6.22 2.39 o 3 6 3 60.82 61.92 3.13 o 4 6 3 3.76 0.96 1.96 o 5 6 3 0.52 0.21 4.46 o 0 7 3 47.48 55.62 4.55 o 1 7 3 22.92 15.62 2.59 o 2 7 3 2.51 1.57 2.01 o 3 7 3 5.82 1.85 4.45 o 4 7 3 3.80 3.54 3.49 o 0 0 4 200.68 205.53 7.32 o 2 0 4 755.08 761.58 13.42 o 4 0 4 741.02 761.12 16.05 o 6 0 4 3.87 3.45 1.22 o 8 0 4 18.19 24.55 8.88 o 1 1 4 974.21 977.60 13.49 o 2 1 4 1419.82 1464.43 17.01 o 3 1 4 3.31 2.87 0.32 o 4 1 4 347.65 334.19 5.41 o 5 1 4 63.53 58.78 1.49 o 6 1 4 8.87 6.41 0.88 o 7 1 4 32.15 30.35 1.90 o 0 2 4 694.95 711.34 12.36 o 1 2 4 1369.18 1405.21 19.37 o 2 2 4 472.38 537.99 7.55 o 3 2 4 11.82 14.90 0.65 o 4 2 4 3.05 2.98 0.40 o 5 2 4 84.91 78.94 2.41 o 6 2 4 34.34 39.09 1.48 o 7 2 4 0.82 0.64 1.62 o 1 3 4 4.02 4.04 0.27 o 2 3 4 14.83 18.72 0.61 o 3 3 4 784.59 808.87 16.51 o 4 3 4 0.93 1.06 0.89 o 5 3 4 68.51 69.00 2.52 o 6 3 4 1.66 0.42 1.49 o 7 3 4 6.10 5.93 1.77 o 0 4 4 782.32 773.84 32.03 o 1 4 4 332.86 324.61 6.06 o 2 4 4 1.90 1.37 0.54 o 3 4 4 0.44 -0.16 0.55 o 4 4 4 31.45 29.07 1.74 o 5 4 4 23.95 25.17 1.57 o 6 4 4 83.88 95.69 3.93 o 1 5 4 69.24 63.12 2.27 o 2 5 4 81.08 79.30 2.85 o 3 5 4 70.42 65.93 3.02 o 4 5 4 22.39 23.29 2.91 o 5 5 4 17.81 23.62 2.37 o 6 5 4 10.23 13.56 2.89 o 0 6 4 6.62 6.07 1.96 o 1 6 4 7.13 6.54 1.64 o 2 6 4 38.15 44.79 2.52 o 3 6 4 1.34 0.49 1.17 o 4 6 4 84.74 89.78 4.63 o 5 6 4 8.86 8.50 3.27 o 1 7 4 36.75 24.64 4.46 o 2 7 4 1.43 -0.80 2.28 o 3 7 4 6.32 3.51 2.67 o 1 0 5 7.80 7.28 0.53 o 3 0 5 99.47 99.05 3.08 o 5 0 5 4.25 4.62 0.98 o 7 0 5 5.35 5.80 2.86 o 0 1 5 8.73 8.64 0.41 o 1 1 5 2019.63 2086.46 25.94 o 2 1 5 52.37 59.91 1.19 o 3 1 5 15.24 13.76 0.92 o 4 1 5 33.92 31.02 0.86 o 5 1 5 74.24 66.45 1.64 o 6 1 5 11.47 9.15 0.97 o 7 1 5 2.10 3.17 1.31 o 1 2 5 41.82 47.62 0.75 o 2 2 5 186.93 180.32 2.46 o 3 2 5 2.48 1.28 0.39 o 4 2 5 119.86 115.06 2.94 o 5 2 5 18.63 17.94 0.92 o 6 2 5 5.23 1.89 1.11 o 7 2 5 4.01 3.49 1.57 o 0 3 5 94.21 94.80 2.38 o 1 3 5 17.58 18.13 0.67 o 2 3 5 2.53 2.27 0.50 o 3 3 5 6.17 6.40 0.70 o 4 3 5 161.55 166.84 3.85 o 5 3 5 1.61 1.36 0.76 o 6 3 5 24.42 25.76 1.69 o 7 3 5 2.68 2.76 1.62 o 1 4 5 32.86 26.18 0.82 o 2 4 5 125.64 119.05 2.60 o 3 4 5 173.49 173.44 4.27 o 4 4 5 27.11 25.30 1.42 o 5 4 5 0.12 1.35 1.08 o 6 4 5 0.76 3.26 1.76 o 0 5 5 3.01 5.71 1.70 o 1 5 5 65.64 60.18 2.16 o 2 5 5 18.72 15.79 1.21 o 3 5 5 1.19 1.04 1.03 o 4 5 5 0.10 -1.76 1.84 o 5 5 5 5.07 6.82 1.56 o 6 5 5 2.54 3.92 2.95 o 1 6 5 15.59 12.02 1.65 o 2 6 5 3.11 1.65 1.78 o 3 6 5 27.98 29.01 2.08 o 4 6 5 0.47 1.58 1.45 o 5 6 5 3.18 7.33 3.06 o 1 7 5 3.03 5.89 3.57 o 2 7 5 4.18 2.66 2.91 o 3 7 5 1.97 1.10 1.69 o 0 0 6 755.70 825.47 20.53 o 2 0 6 740.62 740.99 14.61 o 4 0 6 250.54 240.01 5.96 o 6 0 6 2.15 1.62 1.56 o 1 1 6 1516.82 1609.43 20.46 o 2 1 6 32.97 28.62 0.92 o 3 1 6 20.62 21.40 0.71 o 4 1 6 7.16 6.77 0.69 o 5 1 6 51.03 46.35 1.92 o 6 1 6 7.79 8.47 1.15 o 7 1 6 42.19 43.67 2.30 o 0 2 6 796.81 779.20 14.05 o 1 2 6 40.14 35.28 0.60 o 2 2 6 31.83 30.58 1.23 o 3 2 6 127.55 131.93 2.24 o 4 2 6 69.60 68.49 1.80 o 5 2 6 46.00 43.89 2.30 o 6 2 6 55.88 52.56 2.23 o 7 2 6 14.90 13.65 2.06 o 1 3 6 17.53 16.49 0.65 o 2 3 6 136.45 140.92 2.93 o 3 3 6 287.28 300.49 5.20 o 4 3 6 14.02 14.86 1.35 o 5 3 6 1.11 0.96 0.83 o 6 3 6 0.23 0.88 1.12 o 7 3 6 0.61 0.66 1.62 o 0 4 6 260.70 254.53 8.27 o 1 4 6 5.69 5.74 0.55 o 2 4 6 77.12 69.65 4.45 o 3 4 6 11.96 11.56 0.79 o 4 4 6 63.34 64.97 2.21 o 5 4 6 17.13 19.97 1.79 o 6 4 6 23.54 30.50 2.22 o 1 5 6 47.01 46.72 2.36 o 2 5 6 49.98 48.23 2.05 o 3 5 6 1.28 1.58 1.04 o 4 5 6 19.08 20.77 1.63 o 5 5 6 7.58 5.84 1.54 o 6 5 6 0.36 -2.43 2.43 o 0 6 6 1.45 3.12 1.87 o 1 6 6 11.51 8.52 1.59 o 2 6 6 54.52 48.46 5.03 o 3 6 6 0.12 3.77 1.79 o 4 6 6 24.05 28.25 2.51 o 5 6 6 0.61 0.16 2.62 o 1 7 6 42.08 41.33 5.27 o 2 7 6 11.96 9.01 2.17 o 3 7 6 0.70 1.34 2.06 o 1 0 7 81.21 74.97 1.93 o 3 0 7 555.91 601.86 15.87 o 5 0 7 4.74 3.74 1.02 o 7 0 7 16.71 18.63 2.74 o 0 1 7 95.54 89.96 1.82 o 1 1 7 2192.30 2389.11 29.82 o 2 1 7 64.87 65.33 1.11 o 3 1 7 23.59 22.49 0.82 o 4 1 7 47.71 45.60 1.17 o 5 1 7 189.83 196.50 4.22 o 6 1 7 35.58 30.96 1.45 o 7 1 7 17.17 18.13 1.54 o 1 2 7 60.01 62.74 0.91 o 2 2 7 558.52 553.77 10.17 o 3 2 7 44.54 45.12 1.74 o 4 2 7 250.98 248.95 5.20 o 5 2 7 2.20 3.74 0.80 o 6 2 7 4.34 4.37 1.15 o 7 2 7 7.93 4.14 1.55 o 0 3 7 528.58 549.80 16.81 o 1 3 7 28.79 27.67 1.40 o 2 3 7 53.73 52.56 1.32 o 3 3 7 6.41 5.23 0.48 o 4 3 7 247.49 270.93 9.03 o 5 3 7 0.42 -0.58 0.88 o 6 3 7 75.39 81.84 2.86 o 7 3 7 2.31 1.55 1.99 o 1 4 7 47.33 42.78 1.29 o 2 4 7 254.33 259.47 5.93 o 3 4 7 255.38 269.95 10.88 o 4 4 7 94.88 110.19 3.15 o 5 4 7 0.55 0.63 1.24 o 6 4 7 0.77 2.64 2.19 o 0 5 7 8.32 2.50 1.52 o 1 5 7 177.28 181.97 5.79 o 2 5 7 2.73 1.96 1.00 o 3 5 7 0.34 0.04 0.94 o 4 5 7 0.33 0.77 1.79 o 5 5 7 26.20 30.27 2.21 o 1 6 7 40.29 37.05 2.92 o 2 6 7 2.58 0.09 2.86 o 3 6 7 83.28 89.86 4.20 o 4 6 7 0.57 -0.24 1.77 o 0 7 7 20.03 18.75 3.30 o 1 7 7 20.03 22.14 4.55 o 2 7 7 7.74 5.67 1.96 o 3 7 7 1.77 0.59 5.04 o 0 0 8 700.49 733.45 38.12 o 2 0 8 318.18 354.47 8.55 o 4 0 8 152.92 140.53 4.20 o 6 0 8 5.25 7.15 1.50 o 1 1 8 96.79 89.83 1.41 o 2 1 8 187.20 191.89 3.23 o 3 1 8 62.42 61.89 1.59 o 4 1 8 132.16 132.39 3.04 o 5 1 8 57.54 49.49 1.81 o 6 1 8 0.79 0.20 1.04 o 7 1 8 7.17 7.08 1.69 o 0 2 8 305.39 333.72 7.52 o 1 2 8 180.79 177.06 2.76 o 2 2 8 234.41 215.08 3.60 o 3 2 8 69.52 63.40 1.54 o 4 2 8 10.83 11.39 0.85 o 5 2 8 4.36 3.49 1.11 o 6 2 8 20.85 23.78 1.70 o 7 2 8 0.11 2.24 1.38 o 1 3 8 71.86 74.04 1.49 o 2 3 8 72.45 70.96 2.17 o 3 3 8 234.44 221.62 5.01 o 4 3 8 4.66 5.30 0.80 o 5 3 8 31.71 32.78 1.46 o 6 3 8 0.25 0.55 2.13 o 0 4 8 148.80 139.03 5.64 o 1 4 8 132.58 127.11 4.48 o 2 4 8 8.82 9.35 0.72 o 3 4 8 4.19 2.60 0.89 o 4 4 8 0.03 0.45 0.99 o 5 4 8 3.37 2.55 2.45 o 6 4 8 27.30 37.47 3.62 o 1 5 8 62.97 51.47 2.58 o 2 5 8 3.07 1.37 1.11 o 3 5 8 33.92 35.56 2.19 o 4 5 8 3.02 5.38 1.81 o 5 5 8 24.88 26.33 2.63 o 1 6 8 1.55 2.46 1.70 o 2 6 8 23.37 30.06 2.60 o 3 6 8 0.15 1.10 1.54 o 4 6 8 27.02 25.00 3.52 o 2 7 8 0.21 3.25 2.05 o 1 0 9 701.83 762.04 18.21 o 3 0 9 450.71 455.71 14.82 o 5 0 9 1.54 -0.37 1.07 o 7 0 9 52.36 54.34 3.59 o 0 1 9 704.76 779.39 22.62 o 1 1 9 9.73 8.01 0.48 o 2 1 9 9.06 9.53 0.71 o 3 1 9 101.94 105.91 2.09 o 4 1 9 24.74 20.95 0.98 o 5 1 9 46.06 44.32 2.92 o 6 1 9 11.70 12.39 1.44 o 7 1 9 2.27 1.95 1.53 o 1 2 9 14.04 13.77 0.69 o 2 2 9 325.49 329.82 6.21 o 3 2 9 48.27 42.23 1.35 o 4 2 9 7.61 8.67 1.68 o 5 2 9 6.69 4.61 0.86 o 6 2 9 15.88 13.29 1.56 o 7 2 9 2.36 -1.42 1.78 o 0 3 9 443.75 454.61 12.23 o 1 3 9 111.70 116.57 2.15 o 2 3 9 43.01 41.28 1.91 o 3 3 9 3.34 3.26 0.81 o 4 3 9 10.16 10.45 1.03 o 5 3 9 16.22 18.30 1.27 o 6 3 9 20.54 21.44 1.94 o 1 4 9 28.51 26.36 1.91 o 2 4 9 8.71 7.98 0.88 o 3 4 9 7.10 7.02 1.19 o 4 4 9 0.95 0.76 1.24 o 5 4 9 4.21 4.12 1.84 o 6 4 9 9.49 10.71 2.16 o 0 5 9 1.25 -0.62 1.87 o 1 5 9 52.89 50.38 4.69 o 2 5 9 6.29 3.99 1.35 o 3 5 9 16.33 18.45 1.66 o 4 5 9 4.70 3.72 1.90 o 5 5 9 57.12 71.01 3.70 o 1 6 9 9.77 12.23 2.50 o 2 6 9 17.82 20.55 2.56 o 3 6 9 20.98 23.03 2.30 o 4 6 9 9.71 14.38 3.00 o 1 7 9 2.49 0.18 2.95 o 2 7 9 2.15 -1.87 5.00 o 0 0 10 177.41 196.43 9.11 o 2 0 10 66.74 58.84 2.23 o 4 0 10 0.07 1.13 1.14 o 6 0 10 83.96 79.75 4.03 o 1 1 10 147.67 147.80 2.78 o 2 1 10 251.37 268.91 5.28 o 3 1 10 231.88 230.37 4.78 o 4 1 10 158.52 166.65 3.55 o 5 1 10 13.83 15.21 1.04 o 6 1 10 0.01 -0.71 1.04 o 7 1 10 6.69 7.11 1.89 o 0 2 10 70.22 66.34 2.15 o 1 2 10 251.14 256.76 4.84 o 2 2 10 74.97 78.48 1.84 o 3 2 10 16.01 10.17 0.80 o 4 2 10 102.95 99.98 2.42 o 5 2 10 28.02 27.37 2.67 o 6 2 10 5.70 3.84 1.57 o 1 3 10 221.47 220.03 3.90 o 2 3 10 16.31 13.59 0.91 o 3 3 10 18.79 14.21 1.22 o 4 3 10 2.44 3.96 1.38 o 5 3 10 17.85 17.24 1.50 o 6 3 10 0.81 -0.58 1.46 o 0 4 10 0.06 0.52 1.18 o 1 4 10 158.05 147.04 4.24 o 2 4 10 112.48 105.00 3.85 o 3 4 10 2.73 1.97 1.05 o 4 4 10 142.23 146.45 5.68 o 5 4 10 11.58 13.71 2.48 o 1 5 10 14.94 11.78 2.54 o 2 5 10 25.13 23.36 1.85 o 3 5 10 15.45 15.88 1.80 o 4 5 10 10.75 11.48 1.96 o 5 5 10 1.61 2.08 2.42 o 1 6 10 0.02 -1.74 1.74 o 2 6 10 5.65 3.62 2.57 o 3 6 10 0.69 1.68 2.17 o 1 7 10 5.61 5.62 4.11 o 1 0 11 159.05 163.26 4.34 o 3 0 11 63.59 53.37 3.88 o 5 0 11 3.35 7.72 2.24 o 0 1 11 144.96 139.74 6.33 o 1 1 11 17.21 20.84 1.14 o 2 1 11 1.31 1.61 0.51 o 3 1 11 36.00 34.95 1.21 o 4 1 11 3.09 3.48 1.02 o 5 1 11 2.59 2.80 1.02 o 6 1 11 0.79 0.85 1.34 o 1 2 11 1.43 1.79 0.60 o 2 2 11 23.08 21.52 0.96 o 3 2 11 17.29 16.26 1.01 o 4 2 11 0.30 0.39 0.65 o 5 2 11 4.77 4.45 1.20 o 6 2 11 2.18 -0.34 1.31 o 0 3 11 68.30 67.52 3.42 o 1 3 11 39.16 36.59 1.46 o 2 3 11 12.09 12.01 0.81 o 3 3 11 3.77 5.60 1.92 o 4 3 11 3.49 3.34 1.26 o 5 3 11 4.09 3.42 1.23 o 6 3 11 1.85 2.57 1.76 o 1 4 11 2.73 4.05 1.23 o 2 4 11 0.14 -0.77 1.11 o 3 4 11 4.22 6.65 1.76 o 4 4 11 0.70 -1.31 1.58 o 5 4 11 2.69 5.97 2.18 o 0 5 11 3.06 4.46 1.52 o 1 5 11 4.05 4.06 1.61 o 2 5 11 5.94 7.35 1.62 o 3 5 11 4.04 2.99 1.90 o 4 5 11 3.91 0.38 1.60 o 1 6 11 0.85 3.47 1.93 o 2 6 11 2.27 1.82 2.10 o 3 6 11 1.79 1.74 2.21 o 0 0 12 2562.23 2644.36 179.09 o 2 0 12 6.30 5.16 0.95 o 4 0 12 9.60 11.17 1.60 o 6 0 12 161.67 167.17 7.71 o 1 1 12 3.52 4.29 0.67 o 2 1 12 164.80 160.53 3.21 o 3 1 12 284.04 291.04 7.27 o 4 1 12 16.44 13.97 1.37 o 5 1 12 10.51 10.52 1.54 o 6 1 12 8.96 6.69 1.46 o 0 2 12 7.80 7.34 0.89 o 1 2 12 168.16 165.73 3.69 o 2 2 12 198.68 211.60 7.19 o 3 2 12 42.82 38.21 1.90 o 4 2 12 66.23 69.08 3.31 o 5 2 12 88.38 91.61 3.17 o 6 2 12 0.52 -1.71 1.71 o 1 3 12 298.17 302.20 10.98 o 2 3 12 43.56 43.07 1.97 o 3 3 12 41.55 46.77 2.24 o 4 3 12 9.06 7.09 1.34 o 5 3 12 73.07 80.95 3.43 o 0 4 12 9.26 8.30 1.96 o 1 4 12 18.32 16.15 1.40 o 2 4 12 61.67 60.38 3.33 o 3 4 12 8.91 9.65 1.92 o 4 4 12 13.73 16.57 2.27 o 5 4 12 39.92 46.30 4.25 o 1 5 12 10.67 8.73 1.93 o 2 5 12 96.41 98.81 4.31 o 3 5 12 79.30 88.89 3.99 o 4 5 12 41.49 49.05 3.81 o 1 6 12 9.28 5.80 4.55 o 2 6 12 0.50 4.74 2.13 o 1 0 13 0.57 0.91 1.07 o 3 0 13 16.52 13.80 1.37 o 5 0 13 2.42 2.93 2.21 o 0 1 13 0.86 1.16 0.87 o 1 1 13 136.61 143.29 3.77 o 2 1 13 2.66 3.32 0.66 o 3 1 13 1.23 0.42 0.70 o 4 1 13 17.08 16.41 1.59 o 5 1 13 28.19 23.33 2.03 o 6 1 13 5.18 4.42 1.57 o 1 2 13 1.37 2.13 0.70 o 2 2 13 49.50 55.02 2.42 o 3 2 13 0.04 -0.26 0.89 o 4 2 13 31.67 30.99 1.87 o 5 2 13 6.71 5.87 2.01 o 6 2 13 5.61 5.16 3.13 o 0 3 13 16.60 15.48 1.83 o 1 3 13 1.64 1.70 1.47 o 2 3 13 0.03 0.86 1.37 o 3 3 13 0.01 0.66 1.35 o 4 3 13 69.76 72.90 3.86 o 5 3 13 0.29 -1.12 2.05 o 1 4 13 14.30 13.26 1.52 o 2 4 13 30.44 27.87 2.21 o 3 4 13 76.19 85.10 3.52 o 4 4 13 5.81 6.38 2.03 o 0 5 13 2.90 2.14 2.05 o 1 5 13 23.94 24.23 2.40 o 2 5 13 6.77 8.64 2.49 o 3 5 13 0.35 1.83 2.07 o 1 6 13 6.39 12.59 6.07 o 2 6 13 5.00 4.08 2.99 o 0 0 14 129.88 118.11 7.95 o 2 0 14 151.78 141.77 5.18 o 4 0 14 37.91 36.39 2.87 o 1 1 14 162.64 160.28 4.70 o 2 1 14 4.26 2.60 0.80 o 3 1 14 11.40 10.59 1.22 o 4 1 14 0.08 0.70 1.14 o 5 1 14 28.47 26.56 1.79 o 0 2 14 159.75 150.20 5.48 o 1 2 14 5.32 4.35 1.01 o 2 2 14 2.37 1.76 0.86 o 3 2 14 9.08 8.71 1.82 o 4 2 14 24.73 21.89 2.01 o 5 2 14 5.55 6.65 1.65 o 1 3 14 9.92 11.00 1.25 o 2 3 14 10.68 8.36 1.54 o 3 3 14 69.68 71.96 4.19 o 4 3 14 0.48 0.16 1.66 o 5 3 14 1.23 2.80 2.27 o 0 4 14 41.03 37.94 4.82 o 1 4 14 0.14 1.04 2.14 o 2 4 14 27.24 29.56 2.40 o 3 4 14 0.30 -1.99 1.99 o 4 4 14 54.32 59.59 3.48 o 1 5 14 27.32 28.15 3.20 o 2 5 14 7.23 3.23 2.49 o 3 5 14 1.32 -0.31 1.94 o 1 0 15 151.14 168.20 9.37 o 3 0 15 144.97 145.45 5.05 o 5 0 15 25.84 23.06 2.65 o 0 1 15 141.99 147.12 7.22 o 1 1 15 21.75 18.84 1.42 o 2 1 15 6.84 5.97 0.99 o 3 1 15 7.65 5.59 1.08 o 4 1 15 2.74 0.62 1.83 o 5 1 15 15.06 14.75 1.72 o 1 2 15 6.20 6.14 1.37 o 2 2 15 65.44 58.10 4.08 o 3 2 15 40.67 44.18 2.72 o 4 2 15 14.30 13.81 1.85 o 5 2 15 13.95 11.34 2.12 o 0 3 15 158.18 148.45 6.91 o 1 3 15 8.95 5.39 1.28 o 2 3 15 36.91 38.65 2.63 o 3 3 15 1.73 2.91 2.31 o 4 3 15 0.31 0.53 1.65 o 1 4 15 2.89 1.19 1.86 o 2 4 15 13.87 13.62 2.92 o 3 4 15 0.20 1.74 2.26 o 0 5 15 21.92 26.25 4.82 o 1 5 15 18.81 14.55 4.55 o 2 5 15 16.00 12.40 3.20 o 0 0 16 9.97 9.20 2.41 o 2 0 16 55.18 51.88 3.03 o 4 0 16 161.77 173.79 8.29 o 1 1 16 51.68 53.26 2.54 o 2 1 16 115.59 125.34 5.20 o 3 1 16 0.53 0.31 1.34 o 4 1 16 47.58 41.40 2.67 o 5 1 16 13.20 12.38 2.29 o 0 2 16 52.29 54.34 6.38 o 1 2 16 110.83 119.88 4.06 o 2 2 16 51.05 50.62 3.17 o 3 2 16 0.13 -1.23 1.93 o 4 2 16 0.12 0.88 2.17 o 1 3 16 0.32 2.32 1.37 o 2 3 16 0.12 2.06 2.03 o 3 3 16 170.32 176.35 7.70 o 4 3 16 1.48 4.87 2.72 o 0 4 16 159.01 169.80 10.62 o 1 4 16 46.63 40.30 4.87 o 2 4 16 0.06 -0.38 2.12 o 3 4 16 2.05 2.95 2.12 o 1 5 16 15.54 16.04 3.52 o 1 0 17 28.74 29.24 2.99 o 3 0 17 13.14 8.53 2.21 o 0 1 17 30.87 32.62 2.96 o 1 1 17 3.95 4.43 1.34 o 2 1 17 0.21 -0.61 2.25 o 3 1 17 2.66 4.10 1.49 o 4 1 17 0.34 -0.38 2.39 o 1 2 17 0.28 0.17 1.38 o 2 2 17 2.26 5.22 2.20 o 3 2 17 5.42 3.53 1.67 o 4 2 17 0.33 -0.20 2.34 o 0 3 17 12.59 11.61 3.39 o 1 3 17 3.33 1.45 1.73 o 2 3 17 5.94 6.67 1.98 o 3 3 17 2.13 2.52 2.47 o 1 4 17 0.21 -0.13 2.12 o 2 4 17 0.47 -1.51 2.68 o 0 0 18 54.24 54.10 6.87 o 2 0 18 59.44 65.35 7.41 o 1 1 18 77.15 73.36 4.64 o 2 1 18 2.56 3.25 1.93 o 3 1 18 4.78 4.31 2.75 o 0 2 18 63.04 73.32 4.93 o 1 2 18 2.91 1.99 1.57 o 2 2 18 1.43 0.55 2.23 o 3 2 18 7.87 4.65 3.61 o 1 3 18 4.26 3.62 1.97 o 2 3 18 8.70 9.32 4.49 o 1 0 19 4.98 6.78 3.20 o 3 0 19 63.92 76.53 7.59 o 0 1 19 6.78 6.64 2.92 o 1 1 19 111.55 114.52 5.94 o 2 1 19 6.60 4.26 4.09 o 1 2 19 6.88 6.33 3.42 o 2 2 19 58.54 55.24 4.67 o 0 3 19 59.91 72.05 8.03 o 0 0 20 182.81 215.16 17.50 o 1 1 20 0.45 1.86 2.60 o