#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:57:46 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180871 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/03/2100367.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100367_Fobs loop_ _publ_author_name 'Britton, Doyle' _publ_section_title ; 3,5-Dihalo-4-hydroxybenzonitriles: isostructures, polymorphs and solvates ; _journal_coeditor_code DE5020 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 109 _journal_page_last 117 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.820 _cell_angle_beta 66.990 _cell_angle_gamma 79.040 _cell_length_a 7.4200 _cell_length_b 8.3860 _cell_length_c 8.8080 _exptl_crystal_F_000 169.00 _reflns_d_resolution_high 0.7705 _cod_data_source_file de5020MCl-Bzsup3.hkl _cod_data_source_block MCl-Bz #BEGIN Tags that were not found in dictionaries: _shelx_title 'MCl-Bz in P1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 120.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 257.40 258.43 2.47 o 2 0 0 151.24 129.20 1.29 o 3 0 0 0.07 0.36 0.07 o 4 0 0 198.19 198.82 2.25 o 5 0 0 223.41 221.17 2.28 o 6 0 0 34.40 35.54 0.61 o 7 0 0 208.50 199.88 3.00 o 8 0 0 54.47 56.20 1.17 o -8 1 0 48.25 49.38 1.13 o -7 1 0 7.70 7.38 0.40 o -6 1 0 148.23 142.74 2.23 o -5 1 0 162.74 166.47 1.96 o -4 1 0 1019.52 1016.59 9.28 o -3 1 0 294.84 289.04 2.71 o -2 1 0 205.26 212.65 2.01 o -1 1 0 92.68 92.75 0.95 o 0 1 0 74.20 78.87 0.80 o 1 1 0 0.44 3.66 0.11 o 2 1 0 2363.13 2332.74 27.67 o 3 1 0 1934.52 1961.74 17.80 o 4 1 0 143.41 140.80 1.42 o 5 1 0 45.97 44.57 0.56 o 6 1 0 62.86 63.81 0.92 o 7 1 0 206.86 210.07 2.53 o 8 1 0 5.32 6.75 0.57 o -8 2 0 327.10 330.69 4.78 o -7 2 0 1.79 1.77 0.24 o -6 2 0 0.71 0.86 0.24 o -5 2 0 188.20 184.28 2.67 o -4 2 0 49.94 49.88 0.60 o -3 2 0 645.91 627.09 6.47 o -2 2 0 469.16 485.16 4.49 o -1 2 0 2379.33 2400.28 33.79 o 0 2 0 573.75 582.35 5.40 o 1 2 0 664.15 715.14 7.59 o 2 2 0 2178.17 2293.52 24.05 o 3 2 0 180.19 196.98 1.89 o 4 2 0 194.07 187.09 2.45 o 5 2 0 393.33 383.55 3.63 o 6 2 0 131.08 132.36 2.15 o 7 2 0 701.84 708.49 9.50 o 8 2 0 25.14 28.14 0.77 o -8 3 0 6.75 6.50 1.03 o -7 3 0 72.43 74.03 1.41 o -6 3 0 142.54 134.69 2.14 o -5 3 0 145.52 145.40 3.09 o -4 3 0 83.55 80.70 1.03 o -3 3 0 11.55 12.23 0.23 o -2 3 0 333.89 341.00 5.01 o -1 3 0 2145.18 2175.24 19.75 o 0 3 0 408.29 408.40 3.80 o 1 3 0 2097.10 2095.82 21.98 o 2 3 0 1261.15 1328.50 13.98 o 3 3 0 1019.55 1115.87 10.19 o 4 3 0 128.87 132.42 1.34 o 5 3 0 278.89 278.74 4.06 o 6 3 0 70.62 71.06 1.29 o 7 3 0 9.45 9.32 0.40 o 8 3 0 112.13 119.66 2.02 o -7 4 0 2.68 2.64 0.32 o -6 4 0 708.29 683.56 9.18 o -5 4 0 106.08 110.68 1.78 o -4 4 0 39.60 36.86 0.61 o -3 4 0 570.76 551.79 5.93 o -2 4 0 23.05 29.69 0.56 o -1 4 0 170.55 180.07 1.75 o 0 4 0 55.60 59.83 0.66 o 1 4 0 296.53 287.26 3.16 o 2 4 0 1344.95 1363.26 14.33 o 3 4 0 4.49 5.99 0.20 o 4 4 0 285.68 279.80 3.15 o 5 4 0 41.85 45.66 1.02 o 6 4 0 131.03 126.64 2.29 o 7 4 0 51.01 49.14 1.05 o 8 4 0 1.56 2.24 0.36 o -7 5 0 29.03 31.29 0.89 o -6 5 0 93.75 97.33 1.95 o -5 5 0 195.81 196.52 2.95 o -4 5 0 96.99 89.38 1.21 o -3 5 0 253.20 246.99 3.28 o -2 5 0 250.86 242.17 2.73 o -1 5 0 21.45 28.35 0.52 o 0 5 0 815.80 825.40 9.53 o 1 5 0 7.54 6.47 0.26 o 2 5 0 26.99 28.93 0.48 o 3 5 0 425.85 433.63 5.18 o 4 5 0 82.57 79.55 1.10 o 5 5 0 421.78 407.33 4.52 o 6 5 0 86.11 80.18 1.19 o 7 5 0 8.59 10.20 0.49 o 8 5 0 19.32 21.35 0.73 o -6 6 0 88.79 92.34 1.70 o -5 6 0 0.27 0.49 0.69 o -4 6 0 16.22 15.67 0.42 o -3 6 0 134.30 125.85 1.61 o -2 6 0 13.53 16.06 0.37 o -1 6 0 401.44 396.47 4.35 o 0 6 0 7.93 7.80 0.24 o 1 6 0 2393.11 2401.42 25.16 o 2 6 0 699.98 670.77 7.24 o 3 6 0 68.79 67.23 0.97 o 4 6 0 7.69 7.03 0.26 o 5 6 0 0.59 1.27 0.20 o 6 6 0 222.70 219.91 3.01 o 7 6 0 50.28 52.07 1.13 o -6 7 0 0.05 0.57 0.46 o -5 7 0 170.08 178.31 2.79 o -4 7 0 7.98 7.99 0.43 o -3 7 0 350.52 334.92 3.82 o -2 7 0 34.12 35.59 0.64 o -1 7 0 3.72 5.11 0.32 o 0 7 0 22.17 21.76 0.69 o 1 7 0 139.74 145.72 1.78 o 2 7 0 92.56 90.21 2.84 o 3 7 0 109.73 104.81 1.39 o 4 7 0 171.01 170.13 2.09 o 5 7 0 38.92 41.12 0.75 o 6 7 0 7.13 5.78 0.33 o 7 7 0 6.47 5.15 0.57 o -5 8 0 1.10 0.57 0.46 o -4 8 0 43.04 41.85 1.32 o -3 8 0 75.93 67.85 1.33 o -2 8 0 87.79 96.02 1.66 o -1 8 0 234.87 233.39 3.78 o 0 8 0 134.47 135.13 2.19 o 1 8 0 19.13 19.01 0.46 o 2 8 0 18.19 16.51 0.42 o 3 8 0 39.89 40.03 0.73 o 4 8 0 52.92 52.52 0.90 o 5 8 0 78.45 78.47 1.23 o 6 8 0 142.54 140.15 1.66 o -3 9 0 10.66 11.11 0.49 o -2 9 0 18.91 16.87 0.60 o -1 9 0 30.10 31.89 1.09 o 0 9 0 154.79 158.95 2.51 o 1 9 0 6.34 7.03 0.40 o 2 9 0 406.73 396.31 4.52 o 3 9 0 46.58 48.24 0.86 o 4 9 0 105.97 115.41 1.63 o 5 9 0 4.04 2.59 0.28 o -1 10 0 0.76 1.66 0.32 o 0 10 0 0.56 1.39 0.32 o 1 10 0 0.94 1.20 0.32 o 2 10 0 19.82 20.08 0.68 o 3 10 0 194.56 192.67 4.35 o -1 -10 1 99.48 101.50 2.63 o -4 -9 1 0.53 1.40 0.28 o -3 -9 1 0.19 1.29 0.26 o -2 -9 1 74.48 78.03 1.50 o -1 -9 1 1.56 1.60 0.32 o 0 -9 1 107.45 109.82 1.90 o 1 -9 1 48.41 49.48 1.13 o 2 -9 1 52.27 59.61 1.25 o 3 -9 1 5.88 5.16 0.40 o -5 -8 1 20.44 23.08 0.57 o -4 -8 1 241.29 244.73 2.58 o -3 -8 1 147.48 151.12 1.96 o -2 -8 1 1.36 1.49 0.21 o -1 -8 1 50.19 47.86 1.83 o 0 -8 1 14.22 13.86 0.49 o 1 -8 1 105.68 101.80 1.74 o 2 -8 1 91.10 87.42 2.23 o 3 -8 1 53.49 54.95 1.37 o 4 -8 1 77.10 81.87 1.72 o -6 -7 1 23.65 22.19 0.73 o -5 -7 1 58.62 54.66 1.10 o -4 -7 1 0.60 1.03 0.20 o -3 -7 1 185.27 183.89 2.27 o -2 -7 1 173.96 183.01 2.25 o -1 -7 1 54.96 57.41 0.88 o 0 -7 1 1.28 1.94 0.24 o 1 -7 1 7.35 7.50 0.32 o 2 -7 1 1.28 2.07 0.24 o 3 -7 1 68.21 63.41 0.97 o 4 -7 1 7.20 8.90 0.40 o 5 -7 1 56.85 57.59 1.60 o 6 -7 1 0.54 1.03 0.46 o -7 -6 1 49.76 50.56 1.72 o -6 -6 1 253.66 245.06 3.68 o -5 -6 1 1.93 2.00 0.31 o -4 -6 1 96.41 97.15 1.30 o -3 -6 1 48.26 48.29 0.77 o -2 -6 1 274.78 264.13 3.51 o -1 -6 1 123.99 114.49 1.45 o 0 -6 1 222.70 218.99 2.53 o 1 -6 1 485.25 486.24 7.69 o 2 -6 1 32.11 31.98 0.73 o 3 -6 1 140.75 139.53 1.78 o 4 -6 1 0.18 0.27 0.20 o 5 -6 1 22.93 22.93 0.55 o 6 -6 1 9.86 10.65 0.86 o -7 -5 1 1.78 2.24 0.51 o -6 -5 1 1.02 2.35 0.51 o -5 -5 1 84.15 93.21 1.27 o -4 -5 1 169.11 143.98 1.78 o -3 -5 1 329.70 312.20 3.51 o -2 -5 1 136.75 149.45 1.78 o -1 -5 1 203.85 195.21 2.25 o 0 -5 1 60.02 55.45 0.64 o 1 -5 1 15.91 14.64 0.25 o 2 -5 1 480.01 461.49 6.51 o 3 -5 1 12.33 9.92 0.28 o 4 -5 1 195.45 196.72 2.34 o 5 -5 1 64.86 62.60 0.97 o 6 -5 1 3.18 3.31 0.40 o 7 -5 1 121.83 119.54 2.10 o -8 -4 1 9.35 11.09 0.74 o -7 -4 1 163.77 162.66 2.59 o -6 -4 1 2.25 2.94 0.32 o -5 -4 1 4.14 5.21 0.39 o -4 -4 1 181.93 174.38 2.07 o -3 -4 1 70.74 66.19 1.12 o -2 -4 1 830.30 808.89 8.61 o -1 -4 1 80.03 95.54 1.17 o 0 -4 1 5.69 4.55 0.40 o 1 -4 1 736.67 800.27 7.33 o 2 -4 1 331.73 377.12 4.08 o 3 -4 1 125.20 143.74 1.72 o 4 -4 1 103.24 107.34 1.38 o 5 -4 1 478.76 477.27 5.28 o 6 -4 1 102.56 117.53 2.75 o 7 -4 1 0.12 0.57 0.40 o -8 -3 1 16.06 15.29 1.72 o -7 -3 1 40.21 41.33 1.14 o -6 -3 1 42.92 44.27 0.97 o -5 -3 1 54.33 57.83 1.14 o -4 -3 1 252.63 237.56 2.71 o -3 -3 1 0.16 2.02 0.10 o -2 -3 1 38.64 57.56 0.77 o -1 -3 1 467.92 462.79 4.96 o 0 -3 1 249.95 240.67 2.52 o 1 -3 1 1230.19 1223.97 12.92 o 2 -3 1 137.66 112.36 1.32 o 3 -3 1 154.10 159.57 1.85 o 4 -3 1 14.53 16.36 0.35 o 5 -3 1 4.42 5.22 0.24 o 6 -3 1 13.69 12.81 0.49 o 7 -3 1 27.73 29.32 0.77 o 8 -3 1 56.82 53.77 1.21 o -8 -2 1 0.05 0.57 0.32 o -7 -2 1 39.93 41.61 0.93 o -6 -2 1 80.50 81.74 1.41 o -5 -2 1 624.27 618.19 6.65 o -4 -2 1 299.65 287.67 2.75 o -3 -2 1 972.87 991.65 10.49 o -2 -2 1 993.53 1064.50 9.75 o -1 -2 1 982.19 1040.03 13.05 o 0 -2 1 0.25 3.34 0.10 o 1 -2 1 239.43 254.49 2.76 o 3 -2 1 1298.33 1273.60 13.35 o 4 -2 1 99.08 100.78 1.26 o 5 -2 1 398.55 389.20 4.28 o 6 -2 1 56.38 58.30 1.13 o 7 -2 1 24.76 25.25 0.86 o 8 -2 1 0.38 0.51 0.32 o -8 -1 1 61.10 63.38 1.83 o -7 -1 1 210.76 210.34 4.58 o -6 -1 1 249.28 245.83 2.89 o -5 -1 1 0.65 1.20 0.15 o -4 -1 1 61.81 61.12 0.70 o -3 -1 1 217.68 213.85 2.03 o -2 -1 1 818.35 795.16 7.92 o -1 -1 1 1732.12 1686.13 18.47 o 0 -1 1 0.78 5.60 0.23 o 1 -1 1 1530.63 1573.65 18.60 o 2 -1 1 6.75 6.74 0.29 o 3 -1 1 87.24 91.78 1.10 o 4 -1 1 141.24 148.08 1.72 o 5 -1 1 47.95 54.73 0.66 o 6 -1 1 178.37 173.20 2.59 o 7 -1 1 3.84 4.18 0.32 o 8 -1 1 73.34 70.54 1.38 o -8 0 1 9.69 9.16 0.49 o -7 0 1 20.40 20.76 0.65 o -6 0 1 17.71 17.67 0.42 o -5 0 1 657.51 662.01 7.14 o -4 0 1 26.18 30.53 0.43 o -3 0 1 151.79 139.59 1.61 o -2 0 1 296.99 328.84 3.56 o -1 0 1 1643.06 1599.61 15.39 o 0 0 1 422.63 405.56 3.97 o 1 0 1 9.01 26.67 0.33 o 2 0 1 5386.54 5377.97 49.08 o 3 0 1 144.37 152.21 1.33 o 4 0 1 266.52 276.61 2.35 o 5 0 1 0.18 0.20 0.11 o 6 0 1 134.86 140.92 1.46 o 7 0 1 152.97 153.03 6.35 o 8 0 1 9.23 8.36 0.40 o 9 0 1 22.46 22.72 0.73 o -8 1 1 0.42 0.97 0.32 o -7 1 1 0.13 0.57 0.46 o -6 1 1 18.72 21.03 2.12 o -5 1 1 60.49 60.19 0.81 o -4 1 1 45.74 32.87 0.71 o -3 1 1 147.84 179.42 2.03 o -2 1 1 1804.26 1858.22 16.98 o -1 1 1 311.42 301.80 3.77 o 0 1 1 1326.51 1270.01 11.99 o 1 1 1 414.49 396.31 5.16 o 2 1 1 2286.15 2366.87 28.79 o 3 1 1 108.46 89.47 0.98 o 4 1 1 765.27 782.83 7.18 o 5 1 1 456.62 437.42 4.98 o 6 1 1 113.56 109.52 1.19 o 7 1 1 10.19 10.80 0.33 o 8 1 1 196.64 193.79 3.55 o 9 1 1 42.11 39.69 1.37 o -8 2 1 125.28 127.22 2.63 o -7 2 1 86.98 87.25 1.62 o -6 2 1 126.13 119.67 1.94 o -5 2 1 59.04 57.02 1.49 o -4 2 1 60.65 63.29 0.85 o -3 2 1 913.20 909.05 8.34 o -2 2 1 58.52 57.98 0.70 o -1 2 1 2083.48 2143.87 19.54 o 0 2 1 0.85 1.09 0.08 o 1 2 1 266.49 270.08 4.02 o 2 2 1 911.16 946.48 8.68 o 3 2 1 66.11 71.64 0.67 o 4 2 1 1109.49 1184.16 10.78 o 5 2 1 28.90 29.32 0.43 o 6 2 1 166.03 164.03 1.52 o 7 2 1 301.04 301.96 3.46 o 8 2 1 3.40 4.35 0.46 o 9 2 1 10.46 10.07 0.69 o -7 3 1 8.29 8.17 0.44 o -6 3 1 0.24 0.93 0.51 o -5 3 1 22.14 22.14 0.57 o -4 3 1 357.89 358.82 6.82 o -3 3 1 50.48 41.87 0.56 o -2 3 1 100.72 103.35 1.06 o -1 3 1 245.15 252.74 2.38 o 0 3 1 1494.90 1445.82 13.16 o 1 3 1 405.57 400.27 3.71 o 2 3 1 857.33 836.36 11.71 o 3 3 1 66.53 50.95 0.57 o 4 3 1 0.62 0.43 0.12 o 5 3 1 328.74 351.02 3.34 o 6 3 1 176.10 177.32 2.12 o 7 3 1 51.95 52.06 1.05 o 8 3 1 0.89 1.90 0.32 o 9 3 1 81.21 81.35 2.29 o -7 4 1 0.26 0.86 0.32 o -6 4 1 7.33 7.28 0.40 o -5 4 1 10.44 9.80 0.40 o -4 4 1 806.37 788.64 10.37 o -3 4 1 280.87 269.10 4.45 o -2 4 1 233.36 259.76 2.85 o -1 4 1 848.21 920.86 8.41 o 0 4 1 923.31 1039.23 11.02 o 1 4 1 176.06 203.31 1.93 o 2 4 1 4.43 4.16 0.12 o 3 4 1 15.28 10.98 0.33 o 4 4 1 782.13 767.10 9.02 o 5 4 1 17.15 17.85 0.40 o 6 4 1 85.07 81.97 1.14 o 7 4 1 18.17 17.89 0.46 o 8 4 1 5.13 4.69 0.32 o -6 5 1 44.23 40.04 0.97 o -5 5 1 191.41 192.05 5.27 o -4 5 1 72.57 69.91 1.25 o -3 5 1 3.25 3.00 0.20 o -2 5 1 565.19 559.20 5.18 o -1 5 1 470.66 435.27 4.06 o 0 5 1 520.96 489.73 5.55 o 1 5 1 29.13 38.81 0.48 o 2 5 1 50.57 50.56 0.73 o 3 5 1 4.68 7.49 0.26 o 4 5 1 65.19 69.48 0.95 o 5 5 1 108.77 104.06 1.92 o 6 5 1 60.38 55.23 0.88 o 7 5 1 207.61 197.06 4.24 o 8 5 1 2.93 2.52 0.46 o -6 6 1 57.80 59.72 1.29 o -5 6 1 39.57 36.55 0.89 o -4 6 1 89.89 85.60 1.50 o -3 6 1 2.73 3.40 0.20 o -2 6 1 0.88 1.72 0.34 o -1 6 1 7.98 8.57 0.21 o 0 6 1 3.25 4.10 0.15 o 1 6 1 695.40 670.66 12.10 o 2 6 1 0.13 1.84 0.24 o 3 6 1 733.45 712.83 7.66 o 4 6 1 134.89 133.80 4.96 o 5 6 1 21.19 23.02 1.09 o 6 6 1 0.02 1.31 0.25 o 7 6 1 33.86 30.52 1.72 o 8 6 1 122.90 123.71 3.09 o -5 7 1 0.72 1.32 0.32 o -4 7 1 17.84 15.56 0.57 o -3 7 1 97.70 96.70 1.34 o -2 7 1 10.11 13.30 0.35 o -1 7 1 552.16 525.25 8.21 o 1 7 1 8.58 9.07 0.32 o 2 7 1 98.04 96.30 1.26 o 3 7 1 119.39 125.32 3.21 o 4 7 1 152.33 154.57 1.94 o 5 7 1 208.13 205.79 2.49 o 6 7 1 61.06 59.38 0.97 o 7 7 1 40.34 40.15 1.37 o -4 8 1 10.31 11.04 0.49 o -3 8 1 0.01 0.30 0.20 o -2 8 1 116.31 114.46 1.90 o -1 8 1 12.68 13.12 0.51 o 0 8 1 179.18 179.82 3.32 o 1 8 1 330.32 312.14 4.28 o 2 8 1 10.47 11.18 0.33 o 3 8 1 61.70 60.74 1.24 o 4 8 1 10.72 10.98 0.37 o 5 8 1 121.89 124.90 1.70 o 6 8 1 51.91 55.47 1.17 o -3 9 1 133.11 126.01 3.09 o -2 9 1 1.94 1.56 0.32 o -1 9 1 0.49 1.19 0.27 o 0 9 1 16.43 17.74 0.57 o 1 9 1 172.82 174.02 2.67 o 2 9 1 45.53 48.17 0.86 o 3 9 1 1.57 2.61 0.26 o 4 9 1 164.53 164.22 2.11 o 5 9 1 9.03 11.91 0.49 o -1 10 1 4.69 5.91 0.91 o 0 10 1 109.81 124.91 2.10 o 1 10 1 47.71 53.69 1.17 o 2 10 1 44.86 44.73 1.05 o 3 10 1 61.53 60.32 1.38 o 4 10 1 20.39 20.70 1.03 o -3 -9 2 9.26 6.56 0.44 o -2 -9 2 31.41 35.56 0.93 o -1 -9 2 29.78 29.41 0.81 o 0 -9 2 191.05 188.28 4.87 o 1 -9 2 2.47 3.24 0.34 o 2 -9 2 148.88 150.00 2.51 o -4 -8 2 106.98 105.46 1.52 o -3 -8 2 65.73 65.46 1.08 o -2 -8 2 230.22 235.51 3.31 o -1 -8 2 83.19 82.96 1.54 o 0 -8 2 54.92 51.36 2.35 o 1 -8 2 0.26 0.34 0.24 o 2 -8 2 22.76 23.32 0.97 o 3 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219.18 3.89 o 0 0 9 10.17 12.75 0.49 o 1 0 9 13.09 13.44 0.49 o 2 0 9 11.22 11.44 0.49 o 3 0 9 16.80 16.37 0.42 o 4 0 9 104.28 96.41 1.70 o 5 0 9 56.97 54.89 1.32 o 6 0 9 40.82 43.10 1.20 o 7 0 9 16.15 18.42 0.65 o -2 1 9 84.31 88.38 1.66 o -1 1 9 0.01 0.57 0.32 o 0 1 9 56.68 61.04 1.21 o 1 1 9 31.89 30.41 1.09 o 2 1 9 20.89 19.11 0.57 o 3 1 9 30.61 33.54 0.64 o 4 1 9 27.18 26.85 0.69 o 5 1 9 5.37 4.87 0.32 o 6 1 9 44.22 42.56 0.97 o 7 1 9 23.13 23.40 1.26 o -2 2 9 31.87 29.89 1.03 o -1 2 9 20.99 19.68 0.65 o 0 2 9 6.12 6.75 0.40 o 1 2 9 215.88 208.10 3.32 o 2 2 9 41.96 43.88 0.97 o 3 2 9 6.55 7.05 0.28 o 4 2 9 45.74 45.11 0.79 o 5 2 9 79.32 75.12 1.38 o 6 2 9 28.51 28.78 0.77 o 7 2 9 7.25 6.88 0.44 o 8 2 9 0.12 0.34 0.46 o -2 3 9 141.33 149.74 3.61 o -1 3 9 65.74 63.05 1.29 o 0 3 9 196.81 183.42 2.83 o 1 3 9 38.49 40.44 0.97 o 2 3 9 7.23 6.98 0.40 o 3 3 9 11.18 11.13 0.37 o 4 3 9 25.98 22.46 0.53 o 5 3 9 126.66 121.67 1.65 o 6 3 9 12.48 12.81 0.49 o 7 3 9 62.66 68.25 1.38 o 8 3 9 5.21 4.52 0.40 o -1 4 9 34.12 33.82 0.89 o 0 4 9 18.27 18.08 0.65 o 1 4 9 67.60 69.44 1.33 o 2 4 9 2.88 2.54 0.32 o 3 4 9 3.62 3.99 0.40 o 4 4 9 4.85 4.86 0.26 o 5 4 9 7.42 7.12 0.33 o 6 4 9 50.98 50.80 0.86 o 7 4 9 1.47 1.94 0.36 o 8 4 9 47.20 51.36 1.60 o -1 5 9 80.61 79.59 1.54 o 0 5 9 6.53 7.84 0.40 o 1 5 9 10.57 10.69 0.49 o 2 5 9 62.42 61.32 1.32 o 3 5 9 94.26 91.09 1.62 o 4 5 9 366.27 365.42 4.17 o 5 5 9 85.39 87.31 1.28 o 6 5 9 13.12 13.79 0.44 o 7 5 9 24.55 25.66 0.60 o 8 5 9 0.61 1.60 0.57 o -1 6 9 5.06 8.12 0.69 o 0 6 9 85.06 87.61 3.49 o 1 6 9 63.92 64.53 1.43 o 2 6 9 5.31 5.44 0.40 o 3 6 9 7.59 7.61 0.40 o 4 6 9 6.89 7.25 0.37 o 5 6 9 51.70 50.96 1.20 o 6 6 9 63.51 67.74 1.08 o 7 6 9 13.91 13.92 0.46 o 0 7 9 35.68 39.01 0.97 o 1 7 9 144.26 142.46 2.39 o 2 7 9 30.56 30.26 0.81 o 3 7 9 7.87 7.73 0.44 o 4 7 9 0.33 0.46 0.26 o 5 7 9 22.01 22.25 0.57 o 6 7 9 1.55 2.29 0.36 o 7 7 9 48.89 50.45 1.72 o 1 8 9 0.78 0.91 0.46 o 2 8 9 48.68 48.84 1.09 o 3 8 9 91.62 99.36 3.09 o 4 8 9 14.45 13.63 0.75 o 5 8 9 35.24 35.99 0.93 o 4 -2 10 17.16 19.44 0.65 o 1 -1 10 1.52 2.52 0.57 o 2 -1 10 15.09 15.67 0.80 o 3 -1 10 253.54 251.03 5.27 o 4 -1 10 0.33 0.57 0.32 o 5 -1 10 39.66 41.78 1.01 o 0 0 10 19.56 16.79 0.60 o 1 0 10 102.96 102.71 2.29 o 2 0 10 0.01 0.51 0.40 o 3 0 10 181.72 176.87 3.89 o 4 0 10 2.09 3.35 0.34 o 5 0 10 26.79 26.95 0.77 o 6 0 10 40.51 45.88 1.05 o 0 1 10 9.28 9.40 0.49 o 1 1 10 16.62 19.29 0.65 o 2 1 10 66.37 71.84 1.77 o 3 1 10 125.79 118.51 2.02 o 4 1 10 41.03 41.41 0.97 o 5 1 10 34.46 33.28 0.85 o 6 1 10 7.80 7.23 0.44 o -1 2 10 60.26 61.89 1.83 o 0 2 10 0.16 0.86 0.32 o 1 2 10 0.02 0.63 0.32 o 2 2 10 96.33 93.50 1.70 o 3 2 10 36.51 33.07 0.81 o 4 2 10 62.68 67.59 1.44 o 5 2 10 21.34 22.72 0.68 o 6 2 10 52.27 54.52 1.17 o 7 2 10 4.62 5.22 0.40 o 0 3 10 118.63 126.69 2.18 o 1 3 10 25.18 23.74 0.73 o 2 3 10 302.29 299.61 4.33 o 3 3 10 12.51 12.02 0.52 o 4 3 10 15.67 14.49 0.44 o 5 3 10 111.12 106.92 1.95 o 6 3 10 0.94 1.03 0.32 o 7 3 10 27.21 30.09 0.81 o 0 4 10 14.03 15.00 0.57 o 1 4 10 9.33 10.18 0.49 o 2 4 10 1.87 2.52 0.32 o 3 4 10 193.58 196.25 3.04 o 4 4 10 24.78 23.58 0.73 o 5 4 10 3.03 4.45 0.43 o 6 4 10 2.59 2.94 0.28 o 7 4 10 1.06 2.05 0.46 o 1 5 10 19.11 19.62 0.65 o 2 5 10 9.14 10.37 0.49 o 3 5 10 8.26 8.60 0.49 o 4 5 10 218.17 221.62 3.36 o 5 5 10 52.72 56.78 0.97 o 6 5 10 81.96 80.09 1.54 o 7 5 10 2.69 3.34 0.33 o 1 6 10 19.94 19.85 0.68 o 2 6 10 12.31 12.89 0.57 o 3 6 10 28.71 28.92 1.09 o 4 6 10 196.33 191.87 3.03 o 5 6 10 22.98 21.46 0.55 o 6 6 10 2.58 3.84 0.33 o 2 7 10 31.34 36.60 1.37 o 3 7 10 49.37 49.59 1.26 o 4 7 10 99.94 101.51 1.95 o 5 7 10 2.60 2.77 0.33 o 2 1 11 14.09 12.13 0.57 o 3 1 11 5.50 5.60 0.57 o 4 1 11 16.02 17.96 0.92 o 5 1 11 17.40 19.44 0.92 o 2 2 11 2.79 3.79 0.40 o 3 2 11 70.66 74.60 1.46 o 4 2 11 7.55 7.21 0.69 o 5 2 11 7.74 7.55 0.69 o 2 3 11 109.44 112.19 2.29 o 3 3 11 1.14 1.51 0.32 o 4 3 11 19.05 20.03 0.65 o 5 3 11 0.52 1.77 0.51 o 6 3 11 4.87 4.80 0.69 o 3 4 11 6.30 6.76 0.49 o 4 4 11 2.41 3.67 0.40 o 5 4 11 5.35 5.49 0.57 o 4 5 11 7.31 8.69 0.69 o 5 5 11 112.16 109.40 2.86 o