#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/18/2101894.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2101894_Fobs loop_ _publ_author_name 'Harada, J.' 'Ogawa, K.' 'Tomoda, S.' _publ_section_title ; Molecular Motion and Conformational Interconversion of Azobenzenes in Crystals as Studied by X-ray Diffraction ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 662 _journal_page_last 672 _journal_volume 53 _journal_year 1997 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _exptl_crystal_F_000 448.00 _[local]_cod_data_source_file oa00073200sup9.hkl _[local]_cod_data_source_block 3200 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3,3'-Dimethylazobenzene 200K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4505.18 2838.14 13.33 o 4 0 0 232.67 268.39 2.80 o 6 0 0 1682.74 2093.78 12.26 o 8 0 0 7.88 8.47 0.66 o 10 0 0 354.00 378.14 5.49 o 12 0 0 291.41 264.68 4.99 o 2 1 0 2056.87 1985.43 9.75 o 4 1 0 62.34 62.21 1.52 o 6 1 0 780.57 912.09 6.85 o 8 1 0 210.54 237.08 3.73 o 10 1 0 315.82 320.59 4.90 o 12 1 0 124.38 136.11 3.62 o 0 2 0 2787.09 2486.63 12.02 o 2 2 0 2688.86 2633.56 12.95 o 4 2 0 6.67 14.18 1.15 o 6 2 0 301.11 355.11 4.00 o 8 2 0 0.83 0.60 0.57 o 10 2 0 63.21 76.41 2.59 o 12 2 0 730.35 675.06 7.81 o 2 3 0 1663.58 1687.48 9.38 o 4 3 0 4.19 4.91 0.54 o 6 3 0 168.60 201.75 3.05 o 8 3 0 75.09 75.86 2.36 o 10 3 0 45.65 51.77 2.42 o 12 3 0 17.39 14.46 1.23 o 0 4 0 3539.67 3812.41 19.10 o 2 4 0 54.29 60.68 1.63 o 4 4 0 509.90 470.15 4.56 o 6 4 0 355.21 375.15 4.47 o 8 4 0 152.29 168.79 3.34 o 10 4 0 232.42 214.13 4.15 o 12 4 0 1.78 3.86 0.79 o 2 5 0 4.99 8.17 0.74 o 4 5 0 2037.44 2302.06 13.85 o 6 5 0 26.09 36.53 1.74 o 8 5 0 0.38 0.95 1.42 o 10 5 0 2.29 1.55 1.61 o 12 5 0 1.97 6.96 0.81 o 0 6 0 275.20 253.24 3.66 o 2 6 0 1178.33 1337.40 9.69 o 4 6 0 356.43 372.42 4.71 o 6 6 0 79.81 106.79 2.76 o 8 6 0 91.94 96.68 2.93 o 10 6 0 38.88 37.92 2.17 o 2 7 0 176.23 193.36 3.52 o 4 7 0 77.26 90.47 2.64 o 6 7 0 2.08 2.50 0.69 o 8 7 0 806.75 792.32 8.37 o 10 7 0 44.99 45.04 2.37 o 0 8 0 90.45 97.60 2.91 o 2 8 0 12.31 11.95 1.00 o 4 8 0 431.97 449.38 6.02 o 6 8 0 392.16 400.06 5.86 o 8 8 0 380.02 385.24 5.87 o 2 9 0 36.98 37.60 2.21 o 4 9 0 745.99 760.42 8.48 o 6 9 0 53.53 51.83 2.57 o 8 9 0 115.72 121.68 3.43 o 0 10 0 3.98 4.31 0.80 o 2 10 0 0.92 0.91 0.72 o 4 10 0 321.36 331.19 5.66 o 6 10 0 35.95 34.82 2.26 o 2 11 0 245.49 239.96 4.89 o 4 11 0 8.04 7.34 0.87 o 0 12 0 22.39 21.92 2.08 o 2 12 0 99.75 107.73 3.10 o 4 12 0 171.54 162.51 3.53 o 6 12 0 3.95 4.38 0.53 o 2 13 0 5.56 6.45 0.72 o 1 1 1 2610.57 2405.85 11.81 o 2 1 1 175.55 159.13 1.88 o 3 1 1 397.76 385.94 3.31 o 4 1 1 186.89 177.13 2.38 o 5 1 1 165.51 185.02 2.65 o 6 1 1 195.42 226.25 3.20 o 7 1 1 61.99 48.75 1.86 o 8 1 1 4.51 3.80 0.64 o 9 1 1 64.17 75.07 2.53 o 10 1 1 7.49 8.23 0.84 o 11 1 1 48.06 50.98 2.52 o 12 1 1 19.39 23.71 2.28 o 13 1 1 51.37 56.12 2.57 o 0 2 1 2619.18 2478.89 12.48 o 1 2 1 11906.12 6143.87 28.83 o 2 2 1 70.43 62.11 1.54 o 3 2 1 367.24 341.04 3.25 o 4 2 1 0.28 1.31 0.49 o 5 2 1 20.66 23.43 1.32 o 6 2 1 251.52 268.86 3.54 o 7 2 1 1245.44 1402.32 9.93 o 8 2 1 19.30 19.31 1.62 o 9 2 1 134.37 135.57 3.17 o 10 2 1 29.74 23.93 1.84 o 11 2 1 328.79 302.04 5.18 o 12 2 1 0.08 3.21 1.12 o 13 2 1 1.31 -1.68 1.65 o 1 3 1 630.79 575.70 4.57 o 2 3 1 193.18 189.97 2.59 o 3 3 1 2.48 1.85 0.51 o 4 3 1 336.84 375.92 3.84 o 5 3 1 2350.37 2809.93 15.46 o 6 3 1 28.37 29.91 1.55 o 7 3 1 499.06 530.55 5.58 o 8 3 1 1.18 2.46 0.60 o 9 3 1 1.83 1.16 0.69 o 10 3 1 23.28 23.88 1.95 o 11 3 1 379.14 392.91 5.95 o 12 3 1 30.08 30.25 2.21 o 13 3 1 11.34 9.28 0.87 o 0 4 1 410.67 442.34 4.23 o 1 4 1 948.71 948.92 6.81 o 2 4 1 16.75 15.16 1.22 o 3 4 1 92.94 80.85 2.02 o 4 4 1 39.09 35.96 1.58 o 5 4 1 766.98 866.22 7.03 o 6 4 1 138.72 149.11 2.85 o 7 4 1 265.33 274.36 4.07 o 8 4 1 4.31 6.09 0.77 o 9 4 1 40.44 44.64 2.07 o 10 4 1 2.05 3.63 0.78 o 11 4 1 307.23 304.19 5.09 o 12 4 1 19.56 17.86 1.26 o 13 4 1 39.93 25.18 2.01 o 1 5 1 1892.70 1807.05 11.42 o 2 5 1 48.31 40.45 1.72 o 3 5 1 1.76 2.01 0.57 o 4 5 1 6.56 6.09 0.67 o 5 5 1 194.08 252.72 3.78 o 6 5 1 1.92 1.64 0.59 o 7 5 1 371.04 375.32 5.01 o 8 5 1 0.44 0.19 1.34 o 9 5 1 0.87 0.96 1.51 o 10 5 1 17.39 17.09 1.25 o 11 5 1 7.25 8.52 0.89 o 12 5 1 14.34 10.59 0.94 o 13 5 1 38.57 34.42 2.16 o 0 6 1 367.24 397.21 4.76 o 1 6 1 690.04 755.92 6.89 o 2 6 1 42.63 48.76 1.85 o 3 6 1 25.85 23.14 1.58 o 4 6 1 20.98 22.87 1.59 o 5 6 1 73.61 84.90 2.52 o 6 6 1 29.57 32.92 1.88 o 7 6 1 410.48 411.72 5.62 o 8 6 1 14.81 17.22 1.22 o 9 6 1 4.31 4.93 0.82 o 10 6 1 2.26 2.80 0.77 o 11 6 1 27.78 31.04 2.03 o 12 6 1 1.88 0.89 0.71 o 13 6 1 2.14 2.12 0.66 o 1 7 1 195.36 157.85 3.34 o 2 7 1 4.05 4.60 0.67 o 3 7 1 46.17 50.54 2.19 o 4 7 1 0.32 -0.53 1.37 o 5 7 1 30.78 35.80 2.10 o 6 7 1 6.61 6.30 0.76 o 7 7 1 117.49 119.30 3.30 o 8 7 1 30.50 29.21 2.49 o 9 7 1 0.68 1.25 1.74 o 10 7 1 6.32 5.24 0.82 o 11 7 1 29.09 28.29 2.14 o 12 7 1 7.89 8.51 0.75 o 0 8 1 37.34 39.24 2.00 o 1 8 1 96.92 99.13 2.96 o 2 8 1 135.85 145.60 3.43 o 3 8 1 0.04 0.81 1.38 o 4 8 1 67.10 67.15 2.66 o 5 8 1 138.70 125.36 3.44 o 6 8 1 1.38 1.95 0.77 o 7 8 1 10.02 10.52 0.94 o 8 8 1 1.58 4.25 0.87 o 9 8 1 80.88 92.85 3.05 o 10 8 1 8.99 8.44 0.92 o 11 8 1 0.67 -0.31 1.34 o 1 9 1 15.05 14.87 1.21 o 2 9 1 29.60 31.73 2.19 o 3 9 1 182.54 195.48 4.32 o 4 9 1 22.35 22.16 2.17 o 5 9 1 0.11 -0.78 1.52 o 6 9 1 0.66 -1.10 1.56 o 7 9 1 85.55 80.10 3.11 o 8 9 1 56.81 55.28 2.62 o 9 9 1 193.67 180.50 3.96 o 0 10 1 0.09 1.10 0.74 o 1 10 1 0.19 -0.21 1.53 o 2 10 1 42.27 48.37 2.53 o 3 10 1 868.09 858.52 9.47 o 4 10 1 44.43 39.32 2.52 o 5 10 1 0.00 0.44 1.59 o 6 10 1 14.29 12.35 1.24 o 1 11 1 3.75 5.54 0.82 o 2 11 1 0.03 1.14 1.61 o 3 11 1 77.24 85.19 3.17 o 4 11 1 21.71 21.89 1.41 o 0 12 1 1.44 0.53 1.57 o 1 12 1 0.28 1.24 1.34 o 2 12 1 1.65 2.00 0.64 o 1 13 1 4.21 3.54 0.65 o 0 0 2 30584.49 11517.89 52.44 o 1 0 2 11535.58 7474.73 34.56 o 2 0 2 18.27 22.11 1.21 o 3 0 2 9.74 7.31 0.56 o 4 0 2 3.54 10.23 0.74 o 5 0 2 0.00 0.93 1.04 o 6 0 2 1104.95 1229.05 8.79 o 7 0 2 194.12 211.86 3.41 o 8 0 2 27.77 28.19 1.76 o 9 0 2 25.32 26.88 1.79 o 10 0 2 229.28 239.19 4.46 o 11 0 2 2.47 2.12 0.79 o 12 0 2 585.98 550.93 7.16 o 13 0 2 40.97 33.68 2.28 o 1 1 2 1770.75 1737.25 9.77 o 2 1 2 300.23 305.99 3.14 o 3 1 2 228.66 231.32 2.76 o 4 1 2 176.41 192.43 2.65 o 5 1 2 549.02 641.91 5.47 o 6 1 2 116.17 156.51 2.91 o 7 1 2 136.31 152.89 2.98 o 8 1 2 0.51 -1.46 1.26 o 9 1 2 87.36 92.91 2.79 o 10 1 2 4.18 3.05 0.75 o 11 1 2 219.75 231.69 4.60 o 12 1 2 0.67 1.38 1.83 o 13 1 2 18.07 20.43 1.36 o 0 2 2 15903.66 8942.03 41.79 o 1 2 2 3567.76 3466.75 17.70 o 2 2 2 0.00 0.53 1.02 o 3 2 2 140.67 139.08 2.38 o 4 2 2 14.77 13.28 1.24 o 5 2 2 54.42 51.23 1.72 o 6 2 2 10.22 9.31 0.87 o 7 2 2 19.81 20.81 1.72 o 8 2 2 17.51 18.16 1.65 o 9 2 2 0.00 1.20 1.42 o 10 2 2 24.91 25.08 2.10 o 11 2 2 41.04 38.13 2.46 o 12 2 2 255.26 235.71 4.76 o 13 2 2 49.86 38.95 2.30 o 1 3 2 25.94 21.17 1.32 o 2 3 2 17.49 71.91 1.77 o 3 3 2 172.97 173.61 2.85 o 4 3 2 153.96 152.96 2.85 o 5 3 2 197.05 223.36 3.56 o 6 3 2 85.94 97.17 2.49 o 7 3 2 6.55 5.97 0.71 o 8 3 2 10.33 10.13 0.98 o 9 3 2 110.53 115.03 3.27 o 10 3 2 14.95 17.12 1.27 o 11 3 2 26.93 23.05 1.49 o 12 3 2 0.01 -0.55 1.75 o 13 3 2 0.07 -0.26 1.57 o 14 3 2 0.01 -0.95 1.30 o 0 4 2 226.05 193.22 3.09 o 1 4 2 258.44 271.27 3.57 o 2 4 2 512.60 483.99 5.04 o 3 4 2 214.77 204.15 3.28 o 4 4 2 220.94 210.09 3.51 o 5 4 2 100.87 101.26 2.62 o 6 4 2 2.14 3.33 0.61 o 7 4 2 76.18 84.99 2.64 o 8 4 2 25.23 24.00 1.84 o 9 4 2 10.40 8.29 0.86 o 10 4 2 63.06 55.90 2.54 o 11 4 2 54.00 60.62 2.83 o 12 4 2 37.10 40.86 2.41 o 13 4 2 15.29 14.93 1.18 o 14 4 2 3.31 2.43 0.62 o 1 5 2 0.68 0.64 1.12 o 2 5 2 1.38 -2.47 1.18 o 3 5 2 173.84 177.70 3.33 o 4 5 2 343.78 317.45 4.56 o 5 5 2 176.46 178.55 3.53 o 6 5 2 0.11 3.45 0.65 o 7 5 2 44.69 47.60 2.23 o 8 5 2 128.22 133.59 3.34 o 9 5 2 38.16 40.42 2.18 o 10 5 2 17.07 19.75 1.98 o 11 5 2 0.74 1.28 1.70 o 12 5 2 1.82 2.12 0.75 o 13 5 2 5.14 5.52 0.77 o 0 6 2 21.50 24.20 1.59 o 1 6 2 215.76 214.21 3.75 o 2 6 2 148.86 162.73 3.31 o 3 6 2 163.92 199.47 3.74 o 4 6 2 349.69 337.28 4.99 o 5 6 2 60.38 66.52 2.51 o 6 6 2 76.29 69.91 2.54 o 7 6 2 132.70 144.63 3.63 o 8 6 2 231.29 232.00 4.48 o 9 6 2 18.44 22.49 2.04 o 10 6 2 113.62 102.21 3.22 o 11 6 2 1.60 -0.09 0.96 o 12 6 2 3.51 3.27 0.70 o 13 6 2 2.31 -0.05 1.68 o 1 7 2 86.58 84.86 2.73 o 2 7 2 116.26 124.82 3.16 o 3 7 2 21.74 18.08 1.69 o 4 7 2 590.65 587.30 7.13 o 5 7 2 102.24 95.20 3.15 o 6 7 2 52.96 44.99 2.58 o 7 7 2 53.29 47.32 2.53 o 8 7 2 295.13 288.92 5.12 o 9 7 2 80.39 81.50 2.88 o 10 7 2 9.14 6.44 0.84 o 11 7 2 0.28 -0.11 1.57 o 12 7 2 0.09 -0.97 1.52 o 0 8 2 86.78 77.65 2.80 o 1 8 2 0.58 -0.30 0.87 o 2 8 2 12.48 14.46 1.17 o 3 8 2 130.54 122.55 3.46 o 4 8 2 405.66 409.83 6.26 o 5 8 2 50.69 56.08 2.58 o 6 8 2 17.76 16.73 1.30 o 7 8 2 164.99 161.97 4.07 o 8 8 2 111.35 111.65 3.44 o 9 8 2 1.52 2.87 0.78 o 10 8 2 55.27 54.40 2.64 o 11 8 2 14.89 13.53 1.05 o 1 9 2 2.09 1.52 0.74 o 2 9 2 0.39 -2.64 1.66 o 3 9 2 52.51 58.87 2.60 o 4 9 2 200.53 201.77 4.43 o 5 9 2 114.23 117.06 3.68 o 6 9 2 6.73 6.17 0.83 o 7 9 2 5.29 5.35 0.82 o 8 9 2 136.91 153.87 3.85 o 9 9 2 5.76 6.76 0.78 o 10 9 2 4.95 4.28 0.69 o 0 10 2 7.94 7.49 0.85 o 1 10 2 0.25 1.30 1.52 o 2 10 2 0.30 1.15 1.64 o 3 10 2 98.54 91.83 3.28 o 4 10 2 60.20 69.07 2.94 o 5 10 2 89.67 80.86 3.22 o 1 11 2 59.10 54.84 2.73 o 2 11 2 16.51 16.50 1.25 o 0 12 2 3.10 1.22 0.68 o 1 12 2 5.46 6.31 0.70 o 2 12 2 51.05 53.25 2.09 o 1 1 3 512.32 539.75 5.00 o 2 1 3 191.08 172.18 2.77 o 3 1 3 148.56 129.90 2.48 o 4 1 3 210.79 201.93 3.18 o 5 1 3 371.57 337.10 4.26 o 6 1 3 546.64 619.31 6.14 o 7 1 3 69.48 80.22 2.50 o 8 1 3 2.38 2.89 0.70 o 9 1 3 48.89 50.93 2.37 o 10 1 3 17.21 17.60 1.25 o 11 1 3 115.40 97.75 3.34 o 12 1 3 40.21 48.08 2.56 o 13 1 3 14.08 15.14 1.19 o 0 2 3 3118.82 3203.35 17.59 o 1 2 3 745.76 722.48 6.20 o 2 2 3 192.84 180.71 2.98 o 3 2 3 6.39 6.55 0.62 o 4 2 3 3.94 4.47 0.60 o 5 2 3 119.05 120.97 2.63 o 6 2 3 231.04 269.02 4.03 o 7 2 3 81.92 77.21 2.44 o 8 2 3 28.19 27.12 1.93 o 9 2 3 21.14 20.51 1.88 o 10 2 3 54.11 51.83 2.66 o 11 2 3 142.97 139.50 3.76 o 12 2 3 8.50 9.78 0.97 o 13 2 3 26.90 22.80 2.06 o 1 3 3 1442.51 1533.45 10.55 o 2 3 3 109.66 107.42 2.49 o 3 3 3 0.34 0.01 1.11 o 4 3 3 330.70 344.60 4.52 o 5 3 3 138.88 139.92 2.94 o 6 3 3 25.13 31.87 1.80 o 7 3 3 222.13 253.62 4.21 o 8 3 3 5.46 3.50 0.73 o 9 3 3 0.35 1.36 0.70 o 10 3 3 36.07 44.75 2.42 o 11 3 3 15.58 15.53 1.29 o 12 3 3 21.62 21.67 1.39 o 13 3 3 38.84 35.06 2.15 o 14 3 3 1.22 1.95 0.58 o 0 4 3 30.60 25.80 1.67 o 1 4 3 2310.99 2383.68 14.98 o 2 4 3 4.49 3.97 0.64 o 3 4 3 13.02 8.93 0.71 o 4 4 3 36.30 32.76 1.76 o 5 4 3 19.22 23.95 1.80 o 6 4 3 80.22 86.79 2.74 o 7 4 3 612.18 588.69 6.94 o 8 4 3 0.17 1.13 1.48 o 9 4 3 43.60 37.57 2.38 o 10 4 3 0.57 -1.58 1.66 o 11 4 3 184.92 180.86 4.22 o 12 4 3 54.10 47.77 2.53 o 13 4 3 0.04 0.49 1.54 o 1 5 3 238.81 229.15 3.97 o 2 5 3 19.97 22.65 1.74 o 3 5 3 1.09 0.94 0.60 o 4 5 3 3.23 5.26 0.70 o 5 5 3 375.17 380.26 5.64 o 6 5 3 0.77 0.70 0.65 o 7 5 3 259.53 240.67 4.82 o 8 5 3 13.27 9.63 1.02 o 9 5 3 20.17 16.49 1.31 o 10 5 3 11.94 12.85 1.26 o 11 5 3 118.23 114.65 3.56 o 12 5 3 3.98 3.76 0.76 o 13 5 3 3.32 1.32 1.57 o 0 6 3 292.10 298.80 4.74 o 1 6 3 0.39 -0.29 0.77 o 2 6 3 2.23 3.27 0.66 o 3 6 3 23.00 18.28 1.79 o 4 6 3 0.02 0.68 1.37 o 5 6 3 202.54 200.50 4.30 o 6 6 3 44.68 47.59 2.45 o 7 6 3 88.40 86.02 3.13 o 8 6 3 40.05 38.74 2.56 o 9 6 3 30.15 28.79 2.20 o 10 6 3 3.80 5.60 0.86 o 11 6 3 44.08 41.52 2.45 o 12 6 3 0.43 0.10 1.45 o 1 7 3 99.05 91.13 2.96 o 2 7 3 9.50 12.81 1.08 o 3 7 3 14.72 14.48 1.15 o 4 7 3 21.70 19.46 1.32 o 5 7 3 35.45 38.13 2.38 o 6 7 3 36.56 32.09 2.32 o 7 7 3 2.05 3.03 0.77 o 8 7 3 17.29 18.37 1.38 o 9 7 3 41.95 39.28 2.35 o 10 7 3 0.03 -0.57 1.57 o 11 7 3 0.52 -0.66 1.52 o 0 8 3 20.24 20.02 1.32 o 1 8 3 17.97 20.50 2.00 o 2 8 3 166.50 160.22 4.15 o 3 8 3 307.21 292.28 5.46 o 4 8 3 90.68 90.19 3.30 o 5 8 3 17.27 16.45 1.28 o 6 8 3 2.68 0.09 1.68 o 7 8 3 0.21 -0.71 1.74 o 8 8 3 9.28 10.12 0.89 o 9 8 3 3.41 4.80 0.78 o 10 8 3 2.90 3.06 0.73 o 1 9 3 14.11 14.78 1.28 o 2 9 3 157.92 145.38 4.14 o 3 9 3 113.96 116.05 3.69 o 4 9 3 1.04 1.48 0.75 o 5 9 3 60.88 55.13 2.76 o 6 9 3 0.70 0.89 0.99 o 7 9 3 0.56 -0.63 1.60 o 8 9 3 78.46 82.69 2.82 o 9 9 3 5.92 4.62 0.73 o 0 10 3 12.27 10.02 0.92 o 1 10 3 6.49 7.06 0.92 o 2 10 3 30.62 35.52 2.31 o 3 10 3 117.78 109.42 3.56 o 4 10 3 116.98 106.10 3.54 o 0 12 3 2.97 3.94 0.67 o 1 12 3 8.47 7.99 0.72 o 2 12 3 1.16 0.60 0.50 o 0 0 4 562.85 552.81 5.76 o 1 0 4 216.16 255.85 3.83 o 2 0 4 165.00 165.05 3.15 o 3 0 4 0.39 -0.52 1.11 o 4 0 4 1.20 1.38 0.60 o 5 0 4 20.55 20.09 1.70 o 6 0 4 0.19 2.00 0.69 o 7 0 4 356.09 372.43 5.49 o 8 0 4 6.31 7.08 0.85 o 9 0 4 7.43 8.43 0.87 o 10 0 4 39.27 36.62 2.35 o 11 0 4 74.10 79.22 2.92 o 12 0 4 457.98 441.31 6.12 o 1 1 4 0.79 -0.12 1.15 o 2 1 4 446.89 446.61 5.19 o 3 1 4 150.66 158.72 3.21 o 4 1 4 33.94 38.12 1.81 o 5 1 4 324.80 376.47 5.09 o 6 1 4 33.31 34.97 2.09 o 7 1 4 11.65 14.62 1.12 o 8 1 4 3.22 4.24 0.75 o 9 1 4 1.95 4.00 0.78 o 10 1 4 50.27 54.69 2.57 o 11 1 4 5.94 7.43 0.91 o 12 1 4 56.10 49.22 2.55 o 0 2 4 7989.87 8014.10 39.95 o 1 2 4 141.97 152.33 3.20 o 2 2 4 158.59 169.36 3.34 o 3 2 4 2.09 2.23 0.59 o 4 2 4 27.44 28.35 1.69 o 5 2 4 242.03 231.13 4.01 o 6 2 4 79.88 80.29 2.65 o 7 2 4 0.92 0.49 1.56 o 8 2 4 1.31 1.40 0.75 o 9 2 4 4.12 3.65 0.80 o 10 2 4 8.86 8.54 0.90 o 11 2 4 4.74 4.94 0.84 o 12 2 4 50.45 50.48 2.50 o 13 2 4 0.06 0.22 1.47 o 1 3 4 132.87 125.81 3.01 o 2 3 4 8.84 11.53 0.95 o 3 3 4 43.10 52.05 2.17 o 4 3 4 72.28 58.97 2.38 o 5 3 4 79.26 83.07 2.67 o 6 3 4 17.71 18.91 1.87 o 7 3 4 57.47 61.93 2.59 o 8 3 4 29.31 25.40 2.08 o 9 3 4 2.84 4.33 0.82 o 10 3 4 52.58 56.90 2.56 o 11 3 4 8.65 11.00 0.95 o 12 3 4 3.99 4.22 0.74 o 13 3 4 8.13 7.65 0.79 o 0 4 4 14.77 10.00 0.91 o 1 4 4 315.33 317.69 4.92 o 2 4 4 539.93 509.34 6.33 o 3 4 4 6.75 5.12 0.73 o 4 4 4 11.68 12.46 1.05 o 5 4 4 1.43 -0.38 1.41 o 6 4 4 33.10 28.62 2.12 o 7 4 4 35.89 38.15 2.33 o 8 4 4 21.33 22.11 1.31 o 9 4 4 6.25 7.66 0.86 o 10 4 4 0.03 0.09 0.91 o 11 4 4 4.99 6.00 0.85 o 12 4 4 45.89 45.70 2.20 o 1 5 4 16.52 16.32 1.14 o 2 5 4 4.75 13.31 1.08 o 3 5 4 0.72 0.59 1.46 o 4 5 4 9.99 8.53 0.82 o 5 5 4 20.63 22.82 1.99 o 6 5 4 0.03 -0.78 1.61 o 7 5 4 0.06 -0.16 1.77 o 8 5 4 264.62 273.64 5.15 o 9 5 4 36.71 37.26 2.37 o 10 5 4 16.56 13.45 1.22 o 0 6 4 4.40 6.71 0.80 o 1 6 4 23.70 26.61 2.02 o 2 6 4 1.81 0.46 1.43 o 3 6 4 1.29 1.84 0.70 o 4 6 4 258.96 270.50 5.15 o 5 6 4 14.34 14.77 1.27 o 6 6 4 213.54 206.00 4.68 o 7 6 4 25.68 23.30 2.18 o 8 6 4 129.08 137.32 3.81 o 9 6 4 12.73 15.00 1.31 o 10 6 4 153.92 139.37 3.60 o 1 7 4 75.81 72.01 2.94 o 2 7 4 6.60 7.13 0.87 o 3 7 4 66.14 66.08 2.94 o 4 7 4 702.94 679.32 8.51 o 5 7 4 31.82 28.80 2.30 o 6 7 4 74.77 71.63 3.07 o 7 7 4 31.81 25.96 2.29 o 8 7 4 30.81 29.83 2.11 o 9 7 4 5.27 6.01 0.75 o 10 7 4 4.39 3.61 0.73 o 0 8 4 0.40 0.84 0.74 o 1 8 4 39.56 38.93 2.51 o 2 8 4 25.80 27.42 2.43 o 3 8 4 93.79 81.30 3.31 o 4 8 4 158.81 167.17 4.34 o 5 8 4 20.01 20.30 1.36 o 6 8 4 32.69 30.19 2.19 o 7 8 4 3.35 3.77 0.73 o 8 8 4 16.13 21.39 1.92 o 9 8 4 0.78 -0.01 1.48 o 1 9 4 4.22 4.15 0.82 o 2 9 4 2.83 1.27 1.74 o 3 9 4 14.80 13.86 1.25 o 4 9 4 19.99 17.03 1.32 o 5 9 4 18.19 20.08 1.70 o 6 9 4 1.84 2.19 0.68 o 7 9 4 7.86 7.28 0.77 o 8 9 4 86.44 87.13 2.70 o 1 1 5 86.01 84.95 2.79 o 2 1 5 2.14 0.83 1.35 o 3 1 5 27.98 25.21 1.81 o 4 1 5 19.79 18.78 1.27 o 5 1 5 262.14 265.02 4.57 o 6 1 5 229.84 233.44 4.51 o 7 1 5 59.31 66.77 2.76 o 8 1 5 0.02 0.60 1.60 o 9 1 5 14.63 13.37 1.27 o 10 1 5 1.50 1.95 0.72 o 11 1 5 75.03 69.65 2.76 o 0 2 5 173.89 181.80 3.93 o 1 2 5 13.56 17.68 1.72 o 2 2 5 50.14 44.02 2.31 o 3 2 5 16.21 14.66 1.04 o 4 2 5 0.05 1.03 1.35 o 5 2 5 61.33 68.54 2.68 o 6 2 5 0.16 0.86 0.75 o 7 2 5 0.11 -0.85 1.68 o 8 2 5 1.04 1.44 1.57 o 9 2 5 2.32 2.37 0.75 o 10 2 5 12.46 13.50 1.20 o 11 2 5 40.56 42.83 2.26 o 12 2 5 41.95 43.66 2.07 o 1 3 5 449.19 461.96 6.33 o 2 3 5 63.76 68.39 2.65 o 3 3 5 3.09 8.83 0.82 o 4 3 5 8.65 8.65 0.83 o 5 3 5 0.29 0.21 1.56 o 6 3 5 23.21 21.51 2.02 o 7 3 5 70.52 80.65 3.05 o 8 3 5 28.79 26.29 2.08 o 9 3 5 0.45 0.96 1.63 o 10 3 5 0.07 0.10 0.90 o 11 3 5 0.02 0.88 1.46 o 0 4 5 743.99 786.76 8.69 o 1 4 5 725.91 692.09 8.10 o 2 4 5 29.92 32.44 2.26 o 3 4 5 0.01 1.83 0.71 o 4 4 5 17.72 16.06 1.27 o 5 4 5 1.63 0.86 1.66 o 6 4 5 35.71 38.03 2.30 o 7 4 5 272.79 293.02 5.24 o 8 4 5 35.60 35.17 2.47 o 9 4 5 27.52 26.18 2.12 o 10 4 5 14.80 14.43 1.14 o 11 4 5 55.24 56.72 2.41 o 1 5 5 67.80 69.94 2.88 o 2 5 5 21.92 16.87 1.32 o 3 5 5 5.80 4.79 0.82 o 4 5 5 103.27 95.32 3.51 o 5 5 5 189.91 193.03 4.39 o 6 5 5 71.05 63.89 2.82 o 7 5 5 72.85 71.95 2.84 o 8 5 5 36.55 36.44 2.20 o 9 5 5 5.13 6.13 0.80 o 10 5 5 7.70 7.27 0.80 o 0 6 5 11.70 13.07 1.24 o 1 6 5 2.12 0.75 1.64 o 2 6 5 107.82 102.68 3.52 o 3 6 5 0.24 -0.26 1.66 o 4 6 5 76.89 79.21 3.14 o 5 6 5 92.99 96.34 3.34 o 6 6 5 1.04 1.64 0.77 o 7 6 5 3.43 4.46 0.83 o 8 6 5 3.81 4.27 0.80 o 9 6 5 27.77 21.84 1.96 o 1 7 5 25.02 26.44 2.06 o 2 7 5 43.77 42.53 2.49 o 3 7 5 22.98 25.01 2.22 o 4 7 5 30.25 30.12 2.31 o 5 7 5 0.00 1.20 1.56 o 6 7 5 14.90 14.95 1.16 o 7 7 5 0.43 -1.25 1.63 o 8 7 5 11.85 11.06 0.83 o 9 7 5 10.00 9.66 0.96 o 0 8 5 0.99 0.31 0.92 o 1 8 5 17.08 16.99 1.30 o 2 8 5 2.43 2.08 0.79 o 3 8 5 236.32 233.13 4.91 o 6 8 5 5.40 3.11 0.70 o 7 8 5 8.05 9.44 0.75 o 0 10 5 4.05 3.66 0.60 o 0 0 6 757.36 770.26 8.83 o 1 0 6 5.76 8.41 0.85 o 2 0 6 2.41 3.21 0.74 o 3 0 6 1.53 1.57 0.74 o 4 0 6 0.70 1.83 0.77 o 5 0 6 73.72 72.56 2.80 o 6 0 6 44.96 41.49 2.35 o 7 0 6 3.63 3.71 0.80 o 1 1 6 23.39 26.92 2.12 o 2 1 6 2.81 3.15 0.76 o 3 1 6 15.94 17.44 1.24 o 4 1 6 112.47 123.18 3.56 o 5 1 6 0.14 0.42 0.94 o 6 1 6 21.10 26.56 2.10 o 7 1 6 3.31 0.46 1.80 o 0 2 6 380.80 390.50 6.08 o 1 2 6 325.07 332.13 5.65 o 2 2 6 11.55 11.59 0.97 o 3 2 6 3.56 3.56 0.78 o 4 2 6 41.82 35.60 2.23 o 5 2 6 6.64 5.96 0.83 o 6 2 6 90.76 91.23 3.15 o 7 2 6 77.28 79.75 2.92 o 8 2 6 0.23 -2.92 1.55 o 9 2 6 0.72 1.25 0.59 o 1 3 6 57.68 50.91 2.72 o 2 3 6 58.97 62.92 2.79 o 3 3 6 0.72 0.28 1.63 o 4 3 6 0.05 1.08 1.54 o 5 3 6 128.47 145.21 3.70 o 6 3 6 2.03 3.24 0.76 o 7 3 6 76.72 77.49 2.89 o 8 3 6 12.72 12.65 1.15 o 9 3 6 10.79 11.00 1.04 o 10 3 6 1.08 1.79 0.55 o 0 4 6 312.29 295.23 5.34 o 1 4 6 182.58 173.49 4.38 o 2 4 6 0.16 1.36 0.74 o 3 4 6 69.86 69.19 2.87 o 4 4 6 6.47 6.44 0.87 o 5 4 6 21.37 21.35 2.02 o 6 4 6 13.58 14.41 1.22 o 7 4 6 12.28 14.10 1.19 o 8 4 6 46.27 46.48 2.35 o 9 4 6 3.45 3.60 0.70 o 1 5 6 82.48 82.99 3.18 o 2 5 6 21.79 22.53 2.14 o 3 5 6 1.29 0.26 1.74 o 4 5 6 120.92 127.69 3.67 o 5 5 6 64.09 64.36 2.78 o 6 5 6 17.20 19.85 1.90 o 7 5 6 8.84 8.47 0.78 o 8 5 6 16.09 15.39 1.14 o 0 6 6 15.37 14.94 1.28 o 1 6 6 62.07 68.39 2.94 o 2 6 6 15.91 13.44 1.26 o 3 6 6 59.00 63.46 2.88 o 6 6 6 0.42 -0.92 1.23 o 7 6 6 49.35 47.03 2.20 o 1 9 6 0.43 0.01 1.11 o 1 1 7 35.53 31.57 2.28 o 2 1 7 0.20 0.39 1.52 o 3 1 7 1.27 0.09 1.69 o 0 2 7 28.20 30.13 2.30 o 1 2 7 26.65 25.60 2.21 o 2 2 7 16.01 17.13 1.30 o 3 2 7 0.08 1.16 1.52 o 1 3 7 19.01 19.24 1.29 o 0 6 7 4.65 2.22 0.63 o 0 0 8 293.53 293.75 4.92 o 1 0 8 62.72 63.16 2.46 o 2 0 8 2.44 -0.52 1.49 o 3 0 8 3.47 2.14 0.60 o 1 1 8 2.23 0.61 1.59 o 2 1 8 4.44 3.39 0.63 o 3 1 8 9.74 8.82 0.88 o 0 2 8 5.38 7.87 0.72 o 1 2 8 4.71 3.40 0.68 o 2 2 8 11.22 12.31 0.96 o 3 2 8 0.01 1.33 0.53 o 1 3 8 2.55 2.94 0.62 o