#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/18/2101897.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2101897_Fobs loop_ _publ_author_name 'Harada, J.' 'Ogawa, K.' 'Tomoda, S.' _publ_section_title ; Molecular Motion and Conformational Interconversion of Azobenzenes in Crystals as Studied by X-ray Diffraction ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 662 _journal_page_last 672 _journal_volume 53 _journal_year 1997 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _exptl_crystal_F_000 224.00 _[local]_cod_data_source_file oa0007490sup12.hkl _[local]_cod_data_source_block 490 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 4,4'-Dimethylazobenzene 90 K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 77.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1899.28 1270.48 8.97 o 4 0 0 57.95 42.34 0.72 o 6 0 0 816.88 943.57 28.43 o 8 0 0 4.20 6.78 0.42 o 10 0 0 6.18 9.35 0.61 o 12 0 0 14.46 13.15 0.62 o 14 0 0 5.74 3.75 0.47 o 16 0 0 25.65 27.66 1.36 o 18 0 0 7.80 7.36 0.64 o 1 1 0 458.10 479.61 3.55 o 2 1 0 186.22 192.63 2.94 o 3 1 0 1.64 1.83 0.20 o 4 1 0 35.51 39.83 0.58 o 5 1 0 307.51 354.19 2.73 o 6 1 0 106.68 133.47 1.36 o 7 1 0 29.82 46.90 0.79 o 8 1 0 0.05 0.31 0.33 o 9 1 0 154.17 145.20 1.93 o 10 1 0 75.96 82.08 1.12 o 11 1 0 155.61 156.47 3.26 o 12 1 0 42.01 37.15 0.97 o 13 1 0 5.20 4.93 0.83 o 14 1 0 0.90 -0.05 0.79 o 15 1 0 34.81 36.54 1.15 o 16 1 0 0.07 -1.36 0.90 o 17 1 0 30.31 29.32 1.25 o 18 1 0 4.15 1.63 1.28 o 0 2 0 34.74 40.37 1.93 o 1 2 0 9.54 8.90 0.43 o 2 2 0 0.85 1.05 0.23 o 3 2 0 52.24 58.13 0.87 o 4 2 0 189.22 205.23 4.21 o 5 2 0 277.69 315.56 7.12 o 6 2 0 95.16 117.15 2.08 o 7 2 0 12.64 6.76 0.37 o 8 2 0 19.81 26.31 0.82 o 9 2 0 3.10 3.30 0.30 o 10 2 0 2.84 4.16 0.44 o 11 2 0 212.98 193.62 2.53 o 12 2 0 0.00 0.25 0.68 o 13 2 0 1.35 1.59 0.61 o 14 2 0 1.74 2.07 0.40 o 15 2 0 23.88 28.50 1.08 o 16 2 0 0.04 0.60 0.62 o 17 2 0 2.95 2.75 0.63 o 18 2 0 0.28 0.66 0.61 o 1 3 0 347.43 368.82 3.91 o 2 3 0 153.75 172.97 1.34 o 3 3 0 27.60 25.06 0.70 o 4 3 0 0.08 1.60 0.90 o 5 3 0 35.29 43.73 0.80 o 6 3 0 105.73 112.36 1.22 o 7 3 0 5.70 4.68 0.68 o 8 3 0 43.10 47.43 0.95 o 9 3 0 6.87 7.69 0.57 o 10 3 0 16.41 14.09 0.59 o 11 3 0 25.70 29.33 1.16 o 12 3 0 12.70 11.66 0.57 o 13 3 0 57.05 56.29 1.70 o 14 3 0 7.53 7.72 0.49 o 15 3 0 1.16 0.84 0.53 o 16 3 0 39.98 45.40 1.50 o 17 3 0 10.71 10.80 0.60 o 0 4 0 220.79 216.38 2.12 o 1 4 0 26.30 27.71 0.75 o 2 4 0 20.24 22.18 0.73 o 3 4 0 7.87 8.30 0.39 o 4 4 0 54.40 55.97 0.99 o 5 4 0 16.59 13.85 0.62 o 6 4 0 97.64 99.80 2.16 o 7 4 0 85.21 83.92 1.27 o 8 4 0 38.06 34.68 1.08 o 9 4 0 16.22 16.75 0.87 o 10 4 0 2.44 2.99 0.70 o 11 4 0 6.80 7.94 1.17 o 12 4 0 0.07 -0.20 0.64 o 13 4 0 10.24 9.82 0.50 o 14 4 0 2.40 2.87 0.46 o 15 4 0 0.25 0.77 0.64 o 16 4 0 1.85 1.29 0.72 o 1 5 0 3.98 1.48 0.75 o 2 5 0 29.24 27.22 0.90 o 3 5 0 23.55 24.53 0.93 o 4 5 0 142.48 146.90 1.68 o 5 5 0 34.94 34.72 1.02 o 6 5 0 5.36 4.72 0.38 o 7 5 0 9.64 11.13 0.76 o 8 5 0 2.38 2.58 0.70 o 9 5 0 0.37 0.39 0.85 o 10 5 0 14.29 13.61 0.65 o 11 5 0 11.48 13.69 0.72 o 12 5 0 11.57 12.92 0.63 o 13 5 0 0.93 -0.29 0.94 o 14 5 0 1.44 1.37 0.68 o 0 6 0 20.89 21.63 1.26 o 1 6 0 57.57 59.30 1.29 o 2 6 0 21.08 22.47 1.68 o 3 6 0 3.67 2.36 0.48 o 4 6 0 87.44 85.45 1.56 o 5 6 0 70.75 69.98 1.71 o 6 6 0 4.51 5.12 0.57 o 7 6 0 11.72 12.25 0.62 o 8 6 0 48.19 47.29 1.46 o 9 6 0 5.02 4.78 0.49 o 10 6 0 1.73 1.35 0.80 o 11 6 0 17.84 18.71 0.85 o 1 7 0 3.34 4.40 1.16 o 2 7 0 3.87 4.83 0.47 o 3 7 0 0.04 -0.28 0.72 o 4 7 0 1.53 1.71 0.66 o 5 7 0 13.78 12.10 0.60 o 6 7 0 0.98 1.03 0.98 o 7 7 0 1.43 2.12 1.34 o 8 7 0 5.09 5.39 0.53 o -18 0 1 49.93 44.48 2.59 o -16 0 1 0.30 -1.18 1.45 o -14 0 1 0.89 0.00 1.25 o -12 0 1 78.18 64.20 1.96 o -10 0 1 10.98 7.00 0.66 o -8 0 1 210.81 243.18 2.90 o -6 0 1 38.86 45.10 1.15 o -4 0 1 2251.26 1975.87 13.25 o -2 0 1 781.57 756.19 5.22 o 0 0 1 784.43 639.33 4.26 o 2 0 1 5505.78 2275.27 14.76 o 4 0 1 38.19 47.66 1.01 o 6 0 1 140.03 145.10 1.89 o 8 0 1 285.65 240.98 2.86 o 10 0 1 56.05 56.12 1.66 o 12 0 1 5.19 5.86 0.61 o 14 0 1 68.51 64.92 2.23 o 16 0 1 3.96 2.75 0.76 o 18 0 1 7.90 6.84 0.90 o -18 1 1 1.39 0.87 1.63 o -17 1 1 24.25 24.48 2.00 o -16 1 1 8.79 9.35 0.88 o -15 1 1 10.20 9.26 0.79 o -14 1 1 0.37 -0.33 1.33 o -13 1 1 9.52 8.52 0.72 o -12 1 1 7.42 8.15 0.80 o -11 1 1 7.58 5.35 0.59 o -10 1 1 64.93 47.08 1.57 o -9 1 1 17.81 19.19 1.12 o -8 1 1 3.49 2.11 0.44 o -7 1 1 20.06 19.56 1.02 o -6 1 1 1.83 2.29 0.39 o -5 1 1 37.90 58.03 1.20 o -4 1 1 53.79 74.27 1.25 o -3 1 1 804.53 904.93 6.48 o -2 1 1 2488.18 2013.70 13.33 o -1 1 1 958.53 992.44 6.82 o 0 1 1 0.35 1.86 0.28 o 1 1 1 86.07 99.56 2.34 o 2 1 1 190.57 202.72 1.37 o 3 1 1 1808.47 1689.37 8.07 o 4 1 1 171.64 198.14 2.19 o 5 1 1 36.12 45.53 0.92 o 6 1 1 8.48 12.17 0.62 o 7 1 1 38.49 50.76 0.93 o 8 1 1 152.79 150.68 1.59 o 9 1 1 70.52 68.38 2.32 o 10 1 1 23.81 21.78 0.92 o 11 1 1 95.21 87.89 1.49 o 12 1 1 23.67 27.70 1.13 o 13 1 1 33.29 34.42 1.18 o 14 1 1 0.05 -1.16 0.93 o 15 1 1 8.50 8.24 0.57 o 16 1 1 1.98 2.76 0.55 o 17 1 1 5.50 5.31 0.66 o 18 1 1 25.04 24.83 1.53 o -18 2 1 0.34 0.56 1.81 o -17 2 1 1.38 2.28 0.83 o -16 2 1 14.38 12.30 1.18 o -15 2 1 51.75 51.63 2.25 o -14 2 1 41.67 42.48 2.10 o -13 2 1 37.19 34.24 1.90 o -12 2 1 69.36 66.56 2.19 o -11 2 1 0.65 0.55 1.19 o -10 2 1 0.23 -0.43 1.07 o -9 2 1 171.27 152.75 2.56 o -8 2 1 5.42 4.34 0.51 o -7 2 1 4.26 2.80 0.44 o -6 2 1 32.27 31.00 1.15 o -5 2 1 0.18 -0.05 0.73 o -4 2 1 144.70 157.73 2.03 o -3 2 1 0.78 0.88 0.34 o -2 2 1 13.64 12.39 0.82 o -1 2 1 11.39 13.16 0.79 o 0 2 1 0.17 0.22 0.48 o 1 2 1 9.10 7.59 0.53 o 2 2 1 6.40 9.50 0.54 o 3 2 1 1.50 1.12 0.25 o 4 2 1 137.53 176.83 1.54 o 5 2 1 17.50 21.80 0.70 o 6 2 1 9.53 14.90 0.68 o 7 2 1 28.71 33.75 0.88 o 8 2 1 15.71 15.46 1.33 o 9 2 1 128.23 105.39 1.55 o 10 2 1 20.88 27.21 1.60 o 11 2 1 93.13 90.60 2.04 o 12 2 1 2.31 2.29 0.68 o 13 2 1 2.70 1.13 0.92 o 14 2 1 10.40 10.59 0.73 o 15 2 1 7.15 10.24 0.68 o 16 2 1 0.51 0.03 0.70 o 17 2 1 33.51 36.19 4.01 o 18 2 1 0.34 0.27 1.15 o -17 3 1 0.03 1.05 1.58 o -16 3 1 43.53 44.19 2.36 o -15 3 1 19.79 20.61 1.27 o -14 3 1 26.77 24.02 2.05 o -13 3 1 32.68 33.62 1.85 o -12 3 1 47.71 49.78 2.15 o -11 3 1 9.52 9.54 0.76 o -10 3 1 82.01 76.52 2.15 o -9 3 1 30.29 32.83 1.53 o -8 3 1 3.58 4.11 0.58 o -7 3 1 208.55 215.75 3.08 o -6 3 1 126.05 124.17 2.22 o -5 3 1 155.96 152.95 2.35 o -4 3 1 137.99 134.31 2.16 o -3 3 1 23.30 26.46 1.12 o -2 3 1 10.91 7.66 0.59 o -1 3 1 80.41 82.00 1.59 o 0 3 1 289.64 309.80 4.75 o 1 3 1 238.00 253.21 2.03 o 2 3 1 15.55 18.83 0.72 o 3 3 1 9.33 10.10 0.52 o 4 3 1 1.37 1.94 0.44 o 5 3 1 2.17 2.41 0.32 o 6 3 1 0.48 1.11 0.41 o 7 3 1 51.17 49.29 1.49 o 8 3 1 15.36 12.73 0.81 o 9 3 1 47.85 42.67 2.06 o 10 3 1 14.90 13.14 0.65 o 11 3 1 3.36 3.21 0.77 o 12 3 1 0.03 0.03 0.67 o 13 3 1 1.02 -1.27 2.52 o 14 3 1 32.48 33.82 1.46 o 15 3 1 35.67 40.99 1.57 o 16 3 1 0.32 -1.26 1.85 o 17 3 1 4.87 5.73 1.66 o -16 4 1 7.82 8.58 0.94 o -15 4 1 0.14 -0.62 1.63 o -14 4 1 0.49 1.43 1.47 o -13 4 1 0.72 1.45 0.73 o -12 4 1 3.11 1.95 0.72 o -11 4 1 16.90 17.95 1.67 o -10 4 1 27.85 25.07 1.70 o -9 4 1 0.33 -0.27 1.23 o -8 4 1 6.43 5.95 0.66 o -7 4 1 3.28 2.89 0.58 o -6 4 1 130.79 121.69 2.48 o -5 4 1 199.64 184.23 2.94 o -4 4 1 130.26 126.36 2.38 o -3 4 1 61.90 61.47 1.70 o -2 4 1 71.39 72.33 1.79 o -1 4 1 172.97 175.08 2.67 o 0 4 1 81.98 81.72 1.32 o 1 4 1 5.60 6.33 0.97 o 2 4 1 0.58 0.85 0.42 o 3 4 1 1.31 1.34 1.07 o 4 4 1 63.31 63.17 1.74 o 5 4 1 227.84 246.36 2.43 o 6 4 1 101.08 102.65 1.65 o 7 4 1 2.60 4.34 0.44 o 8 4 1 3.89 2.13 0.78 o 9 4 1 3.65 2.78 0.44 o 10 4 1 2.80 2.86 0.92 o 11 4 1 54.08 49.94 1.56 o 12 4 1 2.27 3.50 0.53 o 13 4 1 51.97 52.27 1.68 o 14 4 1 14.04 16.35 0.89 o 15 4 1 60.57 59.58 1.82 o 16 4 1 3.22 4.73 0.70 o -14 5 1 6.18 4.92 0.89 o -13 5 1 0.06 -3.78 1.68 o -12 5 1 26.20 24.40 2.12 o -11 5 1 0.05 0.65 1.49 o -10 5 1 25.65 23.17 1.90 o -9 5 1 4.73 3.94 0.73 o -8 5 1 0.98 0.01 1.37 o -7 5 1 3.99 3.27 0.65 o -6 5 1 4.59 4.51 0.66 o -5 5 1 0.13 -1.08 1.24 o -4 5 1 0.57 1.10 1.16 o -3 5 1 2.62 3.06 0.59 o -2 5 1 13.07 13.35 0.93 o -1 5 1 4.55 4.86 0.63 o 0 5 1 13.59 14.47 0.92 o 1 5 1 4.12 1.71 0.53 o 2 5 1 26.68 24.66 1.11 o 3 5 1 164.21 155.83 2.11 o 4 5 1 297.54 292.44 2.97 o 5 5 1 0.38 -1.12 0.95 o 6 5 1 242.24 244.21 2.78 o 7 5 1 4.99 6.36 0.72 o 8 5 1 7.36 8.45 1.09 o 9 5 1 42.56 41.88 1.78 o 10 5 1 13.23 14.11 2.39 o 11 5 1 0.01 -1.76 2.54 o 12 5 1 3.88 4.24 1.19 o 13 5 1 1.90 1.89 0.93 o 14 5 1 0.57 0.84 0.58 o -11 6 1 1.57 -0.02 1.72 o -10 6 1 1.46 0.85 1.04 o -9 6 1 31.88 33.75 2.13 o -8 6 1 19.60 19.44 1.88 o -7 6 1 6.04 1.49 1.70 o -6 6 1 122.15 118.76 3.19 o -5 6 1 50.53 53.36 2.31 o -4 6 1 1.89 1.22 0.72 o -3 6 1 15.70 15.07 1.08 o -2 6 1 28.57 30.20 1.79 o -1 6 1 33.18 40.36 1.92 o 0 6 1 12.83 13.34 2.36 o 1 6 1 50.06 51.67 1.54 o 2 6 1 0.83 0.82 1.08 o 3 6 1 1.28 1.21 0.49 o 4 6 1 0.03 0.33 0.73 o 5 6 1 37.32 33.52 1.45 o 6 6 1 19.75 20.31 1.29 o 7 6 1 11.30 11.47 0.69 o 8 6 1 1.92 2.26 1.21 o 9 6 1 3.65 3.39 0.57 o 10 6 1 9.21 9.67 0.65 o 11 6 1 4.99 5.07 1.23 o -7 7 1 67.44 55.13 2.75 o -6 7 1 0.09 0.37 1.62 o -5 7 1 44.15 38.95 2.40 o -4 7 1 4.42 4.20 0.84 o -3 7 1 0.44 -1.99 1.72 o -2 7 1 18.08 22.95 1.94 o -1 7 1 21.46 22.63 1.99 o 0 7 1 33.49 36.13 1.55 o 1 7 1 9.40 11.08 0.66 o 2 7 1 0.00 -2.61 1.13 o 3 7 1 0.99 -0.89 1.17 o 4 7 1 2.43 1.69 1.71 o 5 7 1 2.25 1.86 0.57 o 6 7 1 5.26 5.54 0.63 o 7 7 1 5.82 5.96 0.63 o -18 0 2 15.48 13.93 1.32 o -16 0 2 38.07 38.68 2.18 o -14 0 2 16.72 12.32 1.02 o -12 0 2 2.45 2.66 0.56 o -10 0 2 45.38 39.81 1.46 o -8 0 2 59.94 58.54 1.44 o -6 0 2 509.60 595.63 4.96 o -4 0 2 21.52 23.68 0.87 o -2 0 2 0.49 0.22 0.32 o 0 0 2 651.54 645.14 4.54 o 2 0 2 35.74 48.45 0.94 o 4 0 2 154.40 172.09 1.91 o 6 0 2 32.93 11.53 0.84 o 8 0 2 157.64 162.16 2.33 o 10 0 2 790.96 769.34 6.91 o 12 0 2 3.16 3.85 0.59 o 14 0 2 15.50 15.56 1.45 o 16 0 2 25.92 24.71 1.90 o 18 0 2 5.01 3.68 0.86 o -18 1 2 15.83 11.77 1.06 o -17 1 2 0.12 -0.32 1.57 o -16 1 2 0.68 -0.40 1.57 o -15 1 2 0.75 0.38 1.47 o -14 1 2 10.22 8.08 0.76 o -13 1 2 29.50 22.55 1.61 o -12 1 2 33.17 23.93 1.58 o -11 1 2 46.09 41.75 1.68 o -10 1 2 0.59 -1.21 1.03 o -9 1 2 0.36 1.32 0.48 o -8 1 2 14.95 24.07 1.12 o -7 1 2 158.95 191.59 2.47 o -6 1 2 197.64 205.38 2.44 o -5 1 2 40.51 36.28 1.05 o -4 1 2 9.03 8.00 0.73 o -3 1 2 34.35 35.93 0.95 o -2 1 2 1205.16 1282.63 8.85 o -1 1 2 5994.28 3346.64 21.75 o 0 1 2 4073.84 2592.72 20.35 o 1 1 2 703.01 804.87 4.08 o 2 1 2 4.37 6.02 0.33 o 3 1 2 166.23 183.03 1.39 o 4 1 2 186.68 223.40 6.06 o 5 1 2 687.99 805.57 4.40 o 6 1 2 28.89 30.69 1.13 o 7 1 2 36.51 27.92 0.79 o 8 1 2 20.86 22.55 0.80 o 9 1 2 0.01 -0.51 0.68 o 10 1 2 60.04 61.49 1.23 o 11 1 2 20.17 22.53 0.96 o 12 1 2 10.60 10.31 0.66 o 13 1 2 23.14 22.52 1.13 o 14 1 2 18.56 22.29 1.17 o 15 1 2 2.02 0.97 0.63 o 16 1 2 8.64 9.17 0.61 o 17 1 2 5.11 6.24 0.61 o 18 1 2 1.69 -0.48 1.98 o -18 2 2 5.41 4.83 0.92 o -17 2 2 63.88 67.07 2.78 o -16 2 2 0.15 0.49 1.52 o -15 2 2 7.46 6.37 0.83 o -14 2 2 1.93 2.24 0.68 o -13 2 2 0.90 -0.96 0.82 o -12 2 2 56.45 61.06 2.04 o -11 2 2 114.37 106.31 2.42 o -10 2 2 25.98 30.52 1.47 o -9 2 2 147.74 159.27 2.62 o -8 2 2 62.90 52.02 1.65 o -7 2 2 98.42 100.82 1.89 o -6 2 2 0.31 -0.16 0.78 o -5 2 2 7.21 10.27 0.88 o -4 2 2 34.31 42.42 1.16 o -3 2 2 175.87 185.43 2.20 o -2 2 2 238.80 259.80 2.65 o -1 2 2 1610.84 1792.23 12.37 o 0 2 2 0.48 0.31 0.83 o 1 2 2 31.88 35.83 0.73 o 2 2 2 33.14 33.42 0.71 o 3 2 2 0.60 0.37 0.38 o 4 2 2 200.46 256.89 1.97 o 5 2 2 7.54 9.90 0.63 o 6 2 2 151.28 194.50 1.80 o 7 2 2 1.30 -0.11 0.82 o 8 2 2 20.08 16.91 0.81 o 9 2 2 3.35 1.39 0.36 o 10 2 2 53.83 54.47 1.23 o 11 2 2 24.06 25.23 1.22 o 12 2 2 6.31 6.78 0.49 o 13 2 2 27.85 25.91 1.20 o 14 2 2 35.18 38.71 1.43 o 15 2 2 0.75 0.49 1.08 o 16 2 2 31.11 31.28 1.54 o 17 2 2 12.35 10.83 0.70 o 18 2 2 1.15 1.74 0.60 o -17 3 2 0.14 -1.30 1.67 o -16 3 2 5.40 5.51 0.85 o -15 3 2 3.64 4.61 0.81 o -14 3 2 16.00 18.35 1.69 o -13 3 2 2.42 2.64 0.72 o -12 3 2 56.89 53.65 2.14 o -11 3 2 78.69 83.68 2.40 o -10 3 2 0.17 -0.14 1.18 o -9 3 2 38.11 34.73 1.58 o -8 3 2 53.17 47.48 1.67 o -7 3 2 122.53 102.45 2.13 o -6 3 2 403.24 403.40 4.34 o -5 3 2 139.08 151.74 2.41 o -4 3 2 0.36 0.40 0.88 o -3 3 2 32.72 37.07 1.23 o -2 3 2 28.04 31.24 1.14 o -1 3 2 72.55 65.66 1.47 o 0 3 2 41.50 35.26 0.84 o 1 3 2 1.50 0.78 0.47 o 2 3 2 9.83 12.02 1.25 o 3 3 2 1.26 1.17 0.37 o 4 3 2 0.93 1.58 0.31 o 5 3 2 3.75 3.35 0.41 o 6 3 2 2.43 1.10 0.72 o 7 3 2 0.14 -0.22 0.70 o 8 3 2 27.78 24.62 1.23 o 9 3 2 13.45 12.15 0.66 o 10 3 2 4.39 3.76 0.44 o 11 3 2 39.46 33.62 1.82 o 12 3 2 0.61 0.56 0.98 o 13 3 2 0.00 -2.90 1.01 o 14 3 2 13.44 13.37 0.80 o 15 3 2 13.34 11.71 0.78 o 16 3 2 1.13 1.67 0.74 o 17 3 2 0.02 0.51 1.16 o -16 4 2 0.24 -0.17 1.76 o -15 4 2 13.19 14.83 1.30 o -14 4 2 8.43 8.54 0.88 o -13 4 2 52.05 53.65 2.45 o -12 4 2 7.40 6.12 0.82 o -11 4 2 20.06 19.96 1.72 o -10 4 2 2.95 3.22 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