#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2101994.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2101994_Fobs loop_ _publ_author_name 'Glidewell, Christopher' 'Ferguson, George' 'Gregson, Richard M.' 'Campana, Charles F.' _publ_section_title ; Supramolecular chemistry of amine--phenol adducts; novel three-dimensional framework structures in adducts of bis(2-aminoethyl)amine with 4,4'-sulfonyldiphenol, 1,1,1-tris(4-hydroxyphenyl)ethane and 3,5-dihydroxybenzoic acid, and in the methanol-solvated adduct of tris(2-aminoethyl)amine with 4,4'-biphenol ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 68 _journal_page_last 84 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.144 _cell_angle_gamma 90.000 _cell_length_a 8.2469 _cell_length_b 10.5267 _cell_length_c 23.0516 _exptl_crystal_F_000 872.00 _reflns_d_resolution_high 0.8346 _[local]_cod_data_source_file na00969828sup4.hkl _[local]_cod_data_source_block 9828 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 9828-CG8' _shelx_refln_list_code 4 _shelx_f_calc_maximum 168.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1755.93 1720.95 27.51 o 2 0 0 13918.90 14380.17 86.95 o 3 0 0 355.56 350.23 39.71 o 4 0 0 2566.13 2520.66 58.54 o 5 0 0 399.16 317.28 52.55 o 6 0 0 58.28 84.77 67.93 o 7 0 0 2765.12 2648.22 93.36 o 8 0 0 3.19 74.48 51.65 o 9 0 0 4.66 27.68 56.51 o 1 1 0 1526.01 1557.13 30.56 o 2 1 0 1571.91 1567.06 47.38 o 3 1 0 18.45 7.99 42.24 o 4 1 0 1216.48 1210.56 49.78 o 5 1 0 594.33 595.34 52.56 o 6 1 0 70.35 48.23 68.78 o 7 1 0 19.59 19.98 74.20 o 8 1 0 47.74 23.69 52.80 o 9 1 0 2.07 67.92 56.22 o 0 2 0 731.25 724.63 31.80 o 1 2 0 2864.55 2833.03 46.26 o 2 2 0 339.42 312.57 40.57 o 3 2 0 3269.89 3143.40 58.41 o 4 2 0 241.93 275.24 44.54 o 5 2 0 621.24 490.22 57.99 o 6 2 0 65.18 118.16 64.22 o 7 2 0 460.91 336.37 76.81 o 8 2 0 8.70 24.26 53.37 o 9 2 0 47.48 35.67 57.65 o 1 3 0 4287.93 4329.10 57.61 o 2 3 0 10.17 51.66 39.38 o 3 3 0 6682.10 6909.08 78.80 o 4 3 0 44.77 21.12 48.80 o 5 3 0 114.78 223.49 55.66 o 6 3 0 35.67 59.36 69.92 o 7 3 0 883.56 797.36 78.56 o 8 3 0 185.54 145.86 53.09 o 9 3 0 3.90 29.11 57.36 o 0 4 0 2445.31 2290.14 49.99 o 1 4 0 2039.91 2081.56 49.92 o 2 4 0 2.45 9.42 40.52 o 3 4 0 240.41 278.67 39.69 o 4 4 0 176.76 135.31 48.53 o 5 4 0 9.15 65.35 61.64 o 6 4 0 5.98 91.61 69.63 o 7 4 0 1094.86 1032.41 81.15 o 8 4 0 278.90 238.36 55.67 o 9 4 0 32.31 40.24 60.22 o 1 5 0 862.35 910.63 46.60 o 2 5 0 193.79 133.61 42.25 o 3 5 0 461.52 486.12 50.27 o 4 5 0 522.88 386.15 59.69 o 5 5 0 28.23 18.84 67.64 o 6 5 0 453.86 455.16 75.67 o 7 5 0 269.40 186.70 50.53 o 8 5 0 59.41 27.40 56.51 o 0 6 0 3514.72 3601.55 71.24 o 1 6 0 1124.50 1129.29 54.05 o 2 6 0 1158.65 1147.23 57.48 o 3 6 0 376.55 474.01 54.25 o 4 6 0 528.96 528.64 61.40 o 5 6 0 1.42 87.90 62.50 o 6 6 0 74.81 21.98 69.35 o 7 6 0 11.51 93.89 48.23 o 8 6 0 44.44 28.82 56.22 o 1 7 0 395.07 431.77 54.83 o 2 7 0 1.23 15.70 56.79 o 3 7 0 15.06 87.61 55.65 o 4 7 0 12.92 19.12 66.78 o 5 7 0 467.78 373.49 68.82 o 6 7 0 122.61 111.31 48.81 o 7 7 0 120.53 76.21 54.51 o 8 7 0 108.09 85.34 59.37 o 0 8 0 1326.29 1354.69 69.19 o 1 8 0 189.76 175.84 58.80 o 2 8 0 6.16 49.94 61.64 o 3 8 0 162.43 148.43 63.94 o 4 8 0 242.21 190.69 64.23 o 5 8 0 29.57 99.03 44.24 o 6 8 0 70.87 143.84 48.52 o 7 8 0 41.08 103.03 50.51 o 1 9 0 91.96 21.69 65.93 o 2 9 0 203.17 207.52 63.37 o 3 9 0 10.80 21.97 67.07 o 4 9 0 159.85 245.19 45.95 o 5 9 0 694.32 766.24 53.69 o 6 9 0 12.67 38.53 53.08 o 0 10 0 76.02 39.67 64.50 o 1 10 0 89.30 85.05 60.22 o 2 10 0 10.71 45.66 45.09 o 3 10 0 9.46 76.20 45.38 o 4 10 0 0.48 26.54 49.66 o 5 10 0 145.59 169.83 50.23 o 1 11 0 429.37 461.10 49.68 o 2 11 0 3.02 3.42 46.23 o 3 11 0 102.63 167.82 49.09 o 4 11 0 363.00 324.59 56.53 o 0 12 0 9.11 33.96 50.51 o 1 12 0 9.92 29.39 51.94 o 2 12 0 120.52 112.74 52.80 o 3 12 0 84.97 103.32 54.51 o -9 1 1 72.11 127.57 55.65 o -8 1 1 50.42 36.53 53.08 o -7 1 1 517.94 548.01 73.96 o -6 1 1 103.44 45.10 69.64 o -5 1 1 1.28 13.41 53.94 o -4 1 1 935.85 839.84 46.61 o -3 1 1 415.70 441.43 41.43 o -2 1 1 26576.50 27581.35 127.02 o -1 1 1 104.99 69.11 25.42 o 0 1 1 1340.29 1427.66 17.35 o 1 1 1 1576.70 1573.32 31.13 o 2 1 1 1629.67 1677.06 48.24 o 3 1 1 3850.59 3947.52 58.25 o 4 1 1 2790.18 2941.04 62.29 o 5 1 1 110.08 140.15 51.09 o 6 1 1 73.42 47.38 69.07 o 7 1 1 6.71 80.76 72.77 o 8 1 1 0.01 23.97 52.51 o 9 1 1 59.48 49.66 57.65 o -9 2 1 140.28 173.25 55.66 o -8 2 1 43.43 95.89 51.09 o -7 2 1 284.11 279.20 74.80 o -6 2 1 392.55 456.01 66.82 o -5 2 1 229.42 169.30 54.53 o -4 2 1 616.36 617.20 46.29 o -3 2 1 112.64 94.49 37.97 o -2 2 1 1438.76 1460.55 45.31 o -1 2 1 136.77 134.78 35.70 o 0 2 1 3855.04 3704.97 30.00 o 1 2 1 7326.36 7004.66 67.76 o 2 2 1 945.61 1006.82 43.80 o 3 2 1 5645.30 5635.27 69.74 o 4 2 1 323.30 434.34 44.26 o 5 2 1 96.50 18.84 56.51 o 6 2 1 398.63 325.23 66.25 o 7 2 1 477.67 488.86 75.67 o 8 2 1 19.09 24.54 53.65 o 9 2 1 37.86 28.54 57.36 o -9 3 1 122.22 84.77 58.22 o -8 3 1 3.06 67.64 52.22 o -7 3 1 424.26 362.62 77.66 o -6 3 1 59.59 17.70 68.50 o -5 3 1 334.98 257.84 57.39 o -4 3 1 766.63 789.08 51.16 o -3 3 1 2767.14 2701.53 56.86 o -2 3 1 443.57 449.18 39.15 o -1 3 1 457.93 496.19 39.73 o 0 3 1 3786.82 3727.47 38.48 o 1 3 1 2843.56 2725.42 51.85 o 2 3 1 377.41 315.67 39.14 o 3 3 1 93.80 87.92 37.68 o 4 3 1 433.63 428.99 49.41 o 5 3 1 137.16 148.14 55.95 o 6 3 1 62.48 57.08 71.64 o 7 3 1 1429.15 1308.16 83.48 o 8 3 1 25.32 25.11 55.65 o 9 3 1 1.03 29.39 59.64 o -9 4 1 22.50 45.09 58.22 o -8 4 1 272.61 260.06 55.95 o -7 4 1 131.05 200.65 68.22 o -6 4 1 165.67 94.20 73.36 o -5 4 1 1924.83 1898.69 73.27 o -4 4 1 734.68 770.37 53.15 o -3 4 1 2049.29 2154.93 55.88 o -2 4 1 49.08 48.81 40.24 o -1 4 1 2479.89 2437.25 51.13 o 0 4 1 138.85 121.90 25.12 o 1 4 1 189.13 199.87 35.69 o 2 4 1 4831.10 4727.91 67.52 o 3 4 1 5.39 11.42 43.95 o 4 4 1 177.73 194.97 49.67 o 5 4 1 14.66 87.90 57.36 o 6 4 1 149.67 176.40 67.36 o 7 4 1 83.60 57.94 72.49 o 8 4 1 22.20 27.40 53.94 o 9 4 1 68.63 30.25 60.22 o -9 5 1 42.58 77.06 61.93 o -8 5 1 199.35 107.04 56.80 o -7 5 1 6.43 23.40 49.94 o -6 5 1 53.36 47.09 72.21 o -5 5 1 198.93 269.47 59.66 o -4 5 1 869.51 938.48 61.73 o -3 5 1 605.05 612.52 52.28 o -2 5 1 868.84 905.65 45.74 o -1 5 1 918.60 1020.54 46.32 o 0 5 1 1886.23 1906.86 35.82 o 1 5 1 345.25 322.72 40.27 o 2 5 1 3.96 42.24 43.38 o 3 5 1 640.00 607.98 52.57 o 4 5 1 892.18 886.49 61.73 o 5 5 1 13.97 77.91 65.35 o 6 5 1 695.77 661.80 73.41 o 7 5 1 327.77 349.72 51.10 o 8 5 1 605.08 605.10 59.40 o -8 6 1 284.26 287.18 55.09 o -7 6 1 39.96 25.11 52.23 o -6 6 1 0.61 52.80 68.49 o -5 6 1 22.03 28.54 67.92 o -4 6 1 10.09 16.84 60.79 o -3 6 1 827.06 849.84 58.87 o -2 6 1 232.80 209.27 48.25 o -1 6 1 139.14 137.02 45.96 o 0 6 1 1.91 12.27 32.82 o 1 6 1 93.28 117.88 42.53 o 2 6 1 175.05 158.72 48.81 o 3 6 1 385.62 374.65 54.54 o 4 6 1 242.32 270.35 61.09 o 5 6 1 375.32 310.07 69.67 o 6 6 1 246.46 226.94 70.51 o 7 6 1 236.77 223.51 53.38 o 8 6 1 83.95 109.31 52.80 o -8 7 1 0.02 34.53 57.36 o -7 7 1 32.04 35.10 51.94 o -6 7 1 65.83 77.63 47.38 o -5 7 1 85.26 49.38 68.50 o -4 7 1 52.77 54.80 67.07 o -3 7 1 290.04 239.53 61.67 o -2 7 1 259.79 367.43 55.39 o -1 7 1 1588.28 1618.47 66.38 o 0 7 1 13.02 50.51 37.96 o 1 7 1 0.60 14.84 54.22 o 2 7 1 31.33 65.93 56.79 o 3 7 1 35.26 41.38 60.79 o 4 7 1 58.03 76.20 65.93 o 5 7 1 1.79 21.40 65.92 o 6 7 1 3.66 26.26 48.23 o 7 7 1 50.82 47.09 53.94 o 8 7 1 9.66 31.11 59.36 o -7 8 1 5.63 29.11 54.22 o -6 8 1 60.43 95.89 49.94 o -5 8 1 55.49 95.04 45.09 o -4 8 1 57.74 21.12 69.07 o -3 8 1 498.21 462.62 65.39 o -2 8 1 196.69 190.11 60.80 o -1 8 1 195.92 83.93 65.08 o 0 8 1 44.75 53.94 38.81 o 1 8 1 15.76 17.41 61.93 o 2 8 1 82.06 100.18 59.08 o 3 8 1 0.06 89.61 65.07 o 4 8 1 118.86 88.77 64.79 o 5 8 1 18.99 23.69 47.94 o 6 8 1 1.83 26.54 52.22 o 7 8 1 112.41 74.21 56.51 o -6 9 1 3.29 28.54 52.22 o -5 9 1 41.59 49.94 47.09 o -4 9 1 181.97 155.56 46.81 o -3 9 1 390.83 326.34 65.38 o -2 9 1 73.02 48.52 65.36 o -1 9 1 33.82 19.98 64.78 o 0 9 1 64.33 81.63 43.95 o 1 9 1 188.21 195.82 65.94 o 2 9 1 98.70 125.01 62.22 o 3 9 1 452.28 364.34 70.24 o 4 9 1 284.81 312.02 48.82 o 5 9 1 47.80 27.40 50.51 o 6 9 1 119.91 28.83 54.51 o -5 10 1 0.51 56.22 50.23 o -4 10 1 280.25 343.99 51.10 o -3 10 1 378.52 331.46 50.82 o -2 10 1 134.39 117.31 45.67 o -1 10 1 333.01 253.23 64.24 o 0 10 1 4.03 22.83 44.23 o 1 10 1 0.09 3.71 57.93 o 2 10 1 10.64 23.69 47.37 o 3 10 1 77.90 37.67 50.80 o 4 10 1 32.19 26.83 50.80 o 5 10 1 102.79 28.83 53.09 o -4 11 1 43.79 29.68 54.80 o -3 11 1 38.17 99.60 47.09 o -2 11 1 37.47 26.83 49.94 o -1 11 1 150.50 163.83 47.38 o 0 11 1 7.81 25.97 34.25 o 1 11 1 121.12 85.63 49.09 o 2 11 1 105.61 51.66 51.37 o 3 11 1 337.86 393.68 53.67 o 4 11 1 102.49 79.91 51.66 o -3 12 1 545.77 584.77 61.39 o -2 12 1 33.67 29.97 54.79 o -1 12 1 6.12 71.35 48.52 o 0 12 1 0.38 29.11 35.67 o 1 12 1 8.79 29.39 49.66 o 2 12 1 91.40 54.51 55.65 o -9 0 2 204.06 159.28 55.66 o -8 0 2 870.49 840.43 59.13 o -7 0 2 68.67 73.35 76.77 o -6 0 2 1744.55 1715.57 76.97 o -5 0 2 1139.23 1081.19 59.48 o -4 0 2 610.96 584.95 45.15 o -3 0 2 1201.76 1228.80 44.96 o -2 0 2 170.01 275.59 40.55 o -1 0 2 620.60 616.98 26.66 o 1 0 2 0.20 3.14 29.39 o 2 0 2 28368.65 26891.27 127.30 o 3 0 2 4917.37 4924.26 64.48 o 4 0 2 24.20 10.85 46.80 o 5 0 2 654.08 589.97 57.14 o 6 0 2 708.65 834.16 69.42 o 7 0 2 34.96 20.26 76.49 o 8 0 2 29.75 24.26 55.08 o 9 0 2 103.41 208.06 55.08 o -9 1 2 39.01 31.11 57.08 o -8 1 2 135.52 135.58 50.81 o -7 1 2 25.93 19.69 74.77 o -6 1 2 649.17 585.30 68.27 o -5 1 2 517.21 435.03 54.56 o -4 1 2 112.54 125.88 41.10 o -3 1 2 2808.99 2799.87 54.36 o -2 1 2 13909.89 14210.16 95.30 o -1 1 2 3371.91 3531.58 38.74 o 0 1 2 91.37 55.12 16.28 o 1 1 2 800.12 698.88 31.25 o 2 1 2 6002.97 5490.98 62.69 o 3 1 2 13.22 8.28 41.38 o 4 1 2 38.48 77.63 40.24 o 5 1 2 388.02 316.41 55.40 o 6 1 2 55.37 17.12 69.92 o 7 1 2 0.18 20.55 72.20 o 8 1 2 112.69 136.43 51.37 o 9 1 2 97.94 103.60 57.37 o -9 2 2 20.26 62.21 57.36 o -8 2 2 28.84 23.97 53.08 o -7 2 2 641.31 558.08 77.69 o -6 2 2 8.54 16.84 69.35 o -5 2 2 11.09 8.28 49.94 o -4 2 2 443.98 385.90 45.13 o -3 2 2 218.72 157.62 38.26 o -2 2 2 5468.97 5405.34 63.35 o -1 2 2 198.41 120.82 37.42 o 0 2 2 2066.21 2075.01 29.12 o 1 2 2 283.07 320.86 39.14 o 2 2 2 0.11 30.54 41.09 o 3 2 2 781.84 777.71 43.75 o 4 2 2 631.69 643.18 48.00 o 5 2 2 0.10 34.82 56.79 o 6 2 2 38.63 84.48 69.07 o 7 2 2 0.00 21.12 72.77 o 8 2 2 93.98 189.80 51.94 o 9 2 2 44.93 32.82 57.08 o -9 3 2 88.78 154.69 55.08 o -8 3 2 205.84 233.21 51.95 o -7 3 2 877.40 798.78 79.14 o -6 3 2 58.73 83.91 69.35 o -5 3 2 653.78 627.35 59.14 o -4 3 2 1046.91 1063.15 54.90 o -3 3 2 1999.58 1996.45 53.04 o -2 3 2 17.36 30.54 39.67 o -1 3 2 6312.16 6106.09 64.66 o 0 3 2 3917.38 3851.61 38.76 o 1 3 2 67.82 117.32 36.82 o 2 3 2 100.87 129.31 35.68 o 3 3 2 56.06 10.27 42.81 o 4 3 2 220.18 195.28 46.54 o 5 3 2 28.49 58.51 58.79 o 6 3 2 8.60 41.10 71.63 o 7 3 2 17.90 21.69 71.35 o 8 3 2 23.85 37.39 55.08 o 9 3 2 11.19 29.68 59.07 o -9 4 2 66.41 29.68 59.65 o -8 4 2 10.18 69.06 54.79 o -7 4 2 118.23 21.98 72.78 o -6 4 2 14.38 18.84 72.49 o -5 4 2 62.77 95.33 57.65 o -4 4 2 24.68 69.07 51.09 o -3 4 2 0.12 53.65 38.81 o -2 4 2 36.33 87.90 36.53 o -1 4 2 0.43 8.56 38.81 o 0 4 2 116.26 151.01 24.84 o 1 4 2 43.77 31.40 38.82 o 2 4 2 347.37 343.58 38.27 o 3 4 2 34.95 11.70 44.24 o 4 4 2 328.64 314.09 51.40 o 5 4 2 51.44 16.55 63.93 o 6 4 2 11.73 106.73 64.50 o 7 4 2 9.72 22.83 69.35 o 8 4 2 0.06 26.54 55.36 o 9 4 2 8.22 38.53 57.93 o -9 5 2 10.61 31.11 61.93 o -8 5 2 1.81 27.11 56.51 o -7 5 2 172.14 163.27 49.10 o -6 5 2 1.03 20.26 71.35 o -5 5 2 11.57 17.41 68.49 o -4 5 2 523.72 548.39 58.55 o -3 5 2 296.55 297.52 47.40 o -2 5 2 3.88 11.42 44.52 o -1 5 2 28.58 21.69 41.10 o 0 5 2 224.23 218.99 26.55 o 1 5 2 48.34 87.62 37.10 o 2 5 2 75.11 66.79 41.96 o 3 5 2 386.42 423.50 49.12 o 4 5 2 2.31 15.41 59.07 o 5 5 2 176.78 180.12 61.37 o 6 5 2 31.10 20.83 72.49 o 7 5 2 426.85 340.62 52.25 o 8 5 2 617.46 623.38 58.54 o -8 6 2 22.57 28.54 54.79 o -7 6 2 15.06 101.60 49.09 o -6 6 2 3.98 21.97 67.35 o -5 6 2 21.40 19.12 68.21 o -4 6 2 165.23 69.93 64.80 o -3 6 2 57.07 54.51 55.65 o -2 6 2 262.00 252.39 47.97 o -1 6 2 887.14 967.86 52.88 o 0 6 2 201.25 178.14 30.83 o 1 6 2 72.62 92.76 43.38 o 2 6 2 30.03 28.54 49.66 o 3 6 2 15.02 117.29 51.37 o 4 6 2 136.01 190.39 59.37 o 5 6 2 871.17 813.96 71.43 o 6 6 2 463.45 377.76 70.24 o 7 6 2 3.80 25.68 53.08 o 8 6 2 20.82 73.92 54.22 o -8 7 2 33.62 57.36 57.36 o -7 7 2 176.49 256.32 52.23 o -6 7 2 0.00 70.77 48.51 o -5 7 2 411.39 358.33 67.10 o -4 7 2 0.17 20.26 63.93 o -3 7 2 635.70 652.69 63.70 o -2 7 2 168.11 53.67 60.52 o -1 7 2 573.26 544.43 56.27 o 0 7 2 1336.11 1344.16 44.90 o 1 7 2 119.59 183.82 50.81 o 2 7 2 270.00 262.09 55.96 o 3 7 2 10.77 17.41 61.36 o 4 7 2 225.38 177.27 61.37 o 5 7 2 4.77 21.69 65.64 o 6 7 2 67.67 50.23 50.23 o 7 7 2 73.25 84.48 50.52 o 8 7 2 0.01 31.39 56.51 o -7 8 2 0.09 29.11 53.65 o -6 8 2 13.20 103.59 47.66 o -5 8 2 12.47 23.40 48.23 o -4 8 2 14.21 21.12 65.92 o -3 8 2 1023.00 1032.73 72.58 o -2 8 2 299.29 363.44 61.95 o -1 8 2 28.42 71.06 60.79 o 0 8 2 780.57 813.95 45.43 o 1 8 2 211.07 312.87 58.81 o 2 8 2 125.97 89.34 59.94 o 3 8 2 55.72 87.05 65.93 o 4 8 2 1835.63 1785.57 83.23 o 5 8 2 0.00 23.97 47.37 o 6 8 2 36.63 26.54 53.65 o 7 8 2 48.86 138.70 53.94 o -6 9 2 122.45 159.55 51.66 o -5 9 2 2.31 25.97 50.23 o -4 9 2 335.83 267.50 47.96 o -3 9 2 58.70 21.98 64.79 o -2 9 2 22.17 20.83 67.07 o -1 9 2 40.60 134.42 61.36 o 0 9 2 914.18 883.43 49.43 o 1 9 2 295.34 226.68 67.66 o 2 9 2 244.04 302.02 65.37 o 3 9 2 51.16 101.03 60.79 o 4 9 2 76.51 24.26 48.80 o 5 9 2 90.17 113.02 47.66 o 6 9 2 7.94 37.67 52.23 o -6 10 2 52.11 31.11 56.22 o 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