#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/21/2102158.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102158_Fobs loop_ _publ_author_name 'Glidewell, Christopher' 'Low, John N.' 'Wardell, James L.' _publ_section_title ; Conformational preferences and supramolecular aggregation in 2-nitrophenylthiolates: disulfides and thiosulfonates ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 893 _journal_page_last 905 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 101.057 _cell_angle_beta 91.966 _cell_angle_gamma 91.073 _cell_length_a 8.8211 _cell_length_b 11.0422 _cell_length_c 21.2576 _exptl_crystal_F_000 1044.00 _reflns_d_resolution_high 0.7176 _[local]_cod_data_source_file na01077sup8.hkl _[local]_cod_data_source_block 7 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 081' _shelx_refln_list_code 4 _shelx_f_calc_maximum 327.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k 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13.50 -234.98 234.98 o -10 2 0 909.29 1358.05 243.28 o -9 2 0 493.37 639.29 123.15 o -8 2 0 1122.60 1211.53 131.89 o -7 2 0 0.50 6.60 37.36 o -6 2 0 452.13 421.44 50.74 o -5 2 0 0.90 44.24 37.26 o -4 2 0 6963.34 7254.57 596.78 o -3 2 0 22.81 40.92 27.33 o -2 2 0 1665.22 1744.77 112.13 o -1 2 0 21.46 0.00 31.28 o 0 2 0 876.69 762.37 46.31 o 1 2 0 4.64 55.18 35.48 o 2 2 0 875.96 848.00 71.51 o 3 2 0 406.43 592.77 183.15 o 4 2 0 16.54 100.73 39.05 o 5 2 0 7.55 -28.39 31.04 o 6 2 0 740.81 873.81 65.41 o 7 2 0 181.64 170.51 51.28 o 8 2 0 3.39 -53.04 53.04 o 9 2 0 5.33 88.14 61.67 o 10 2 0 564.21 593.77 158.96 o -10 3 0 0.58 32.88 110.51 o -9 3 0 13.50 42.94 93.94 o -8 3 0 19.61 -75.79 75.79 o -7 3 0 106.18 167.08 63.90 o -6 3 0 0.10 26.12 50.98 o -5 3 0 8.16 -48.98 48.98 o -4 3 0 4400.38 4608.92 266.94 o -3 3 0 89.54 55.94 42.10 o -2 3 0 12287.38 13375.52 799.64 o -1 3 0 1510.03 1599.74 165.87 o 0 3 0 5621.36 5150.93 443.01 o 1 3 0 15224.34 12889.02 673.16 o 2 3 0 8892.86 8048.34 418.79 o 3 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61.57 o -4 5 0 261.20 286.90 60.08 o -3 5 0 2900.40 3230.63 322.07 o -2 5 0 1361.96 1399.21 261.25 o -1 5 0 2149.82 2137.53 162.91 o 0 5 0 1212.32 1353.36 92.99 o 1 5 0 154.82 41.55 46.50 o 2 5 0 187.47 250.19 56.42 o 3 5 0 1052.76 961.92 72.27 o 4 5 0 175.10 151.39 59.31 o 5 5 0 1.45 -24.29 61.68 o 6 5 0 449.52 573.72 94.32 o 7 5 0 65.84 -56.47 66.44 o 8 5 0 120.88 159.80 89.69 o 9 5 0 181.99 186.66 121.86 o 10 5 0 24.73 222.54 356.62 o -10 6 0 0.12 -90.78 124.47 o -9 6 0 27.34 -59.54 168.79 o -8 6 0 1.92 3.32 127.76 o -7 6 0 4.55 -47.72 139.29 o -6 6 0 4.26 80.25 63.80 o -5 6 0 178.24 10.71 60.37 o -4 6 0 431.99 258.57 78.72 o -3 6 0 3430.46 3912.40 219.27 o -2 6 0 1598.24 1254.34 124.34 o -1 6 0 53.75 261.21 1167.32 o 0 6 0 352.29 364.28 92.66 o 1 6 0 7.14 11.25 133.39 o 2 6 0 0.72 -58.91 96.07 o 3 6 0 1146.52 1683.80 144.45 o 4 6 0 73.06 50.61 60.40 o 5 6 0 89.81 -4.50 59.32 o 6 6 0 207.25 146.20 99.37 o 7 6 0 69.96 167.80 113.37 o 8 6 0 70.77 174.43 108.06 o 9 6 0 189.82 346.85 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94.77 o 4 8 0 569.91 579.71 124.91 o 5 8 0 698.83 710.73 115.51 o 6 8 0 16.51 59.75 107.75 o 7 8 0 4.30 142.58 136.48 o 8 8 0 1.04 -125.79 346.95 o 9 8 0 73.26 15.20 298.57 o -9 9 0 2.40 152.58 277.94 o -8 9 0 38.74 181.65 178.45 o -7 9 0 99.46 -127.79 153.90 o -6 9 0 647.43 603.97 172.70 o -5 9 0 217.49 283.22 95.22 o -4 9 0 879.42 900.37 168.64 o -3 9 0 0.04 89.15 119.37 o -2 9 0 5534.40 5453.91 388.21 o -1 9 0 1491.04 1443.43 223.93 o 0 9 0 91.78 -40.15 100.89 o 1 9 0 1255.11 1079.12 246.73 o 2 9 0 51.37 29.00 154.12 o 3 9 0 817.02 781.70 223.93 o 4 9 0 1256.48 1377.49 145.40 o 5 9 0 430.79 294.62 113.98 o 6 9 0 62.28 -58.90 133.32 o -8 10 0 55.26 -34.74 169.86 o -7 10 0 7.87 -11.54 223.98 o -6 10 0 141.33 166.37 150.69 o -5 10 0 1070.74 1002.83 243.23 o -4 10 0 77.27 111.65 133.60 o -3 10 0 399.03 217.79 133.22 o -2 10 0 200.94 206.06 119.92 o -1 10 0 19.46 74.55 127.52 o 0 10 0 502.58 378.91 161.05 o 1 10 0 58.24 215.28 171.37 o 2 10 0 22.71 60.61 123.71 o 3 10 0 22.78 273.10 149.20 o 4 10 0 352.95 531.39 162.11 o 5 10 0 6.60 161.38 183.21 o 6 10 0 2.37 -21.56 290.27 o 7 10 0 161.60 58.05 316.54 o -8 11 0 26.17 87.08 276.45 o -7 11 0 57.23 -46.24 199.53 o -6 11 0 213.83 333.81 206.89 o -5 11 0 82.02 134.59 172.37 o -4 11 0 75.41 -102.29 219.78 o -3 11 0 22.05 59.44 190.75 o -2 11 0 56.45 9.37 138.16 o -1 11 0 251.18 411.04 190.06 o 0 11 0 95.99 214.34 160.95 o 1 11 0 195.08 140.11 137.05 o 2 11 0 174.75 280.64 169.98 o 3 11 0 68.79 213.03 184.20 o 4 11 0 40.74 224.82 194.99 o 5 11 0 200.25 134.95 158.65 o 6 11 0 80.30 235.91 523.18 o -7 12 0 3.62 510.05 335.89 o -6 12 0 32.97 -233.60 262.63 o -5 12 0 56.92 288.72 287.52 o -4 12 0 35.79 58.05 351.09 o -3 12 0 0.04 15.20 308.24 o -2 12 0 183.77 -15.20 381.50 o -1 12 0 144.40 250.19 367.68 o 0 12 0 1505.84 1778.97 338.65 o 1 12 0 230.58 73.26 234.98 o 2 12 0 196.87 -160.34 160.34 o 3 12 0 29.36 378.74 335.89 o 4 12 0 116.10 320.68 247.42 o 5 12 0 1339.44 829.36 465.82 o -5 13 0 1.30 -306.86 306.86 o -3 13 0 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2224.72 328.98 o 4 -6 1 259.98 310.71 78.93 o 5 -6 1 20.87 19.64 60.66 o 6 -6 1 69.06 225.77 97.47 o 7 -6 1 85.19 45.14 90.22 o 8 -6 1 79.77 181.42 125.52 o 9 -6 1 55.34 -24.45 142.17 o 10 -6 1 7.53 -198.68 198.68 o -10 -5 1 2.54 -15.20 163.11 o -9 -5 1 75.51 182.95 108.72 o -8 -5 1 564.65 656.71 122.87 o -7 -5 1 335.85 233.29 93.34 o -6 -5 1 20.32 -11.05 56.42 o -5 -5 1 4.10 15.20 69.96 o -4 -5 1 241.85 217.74 72.48 o -3 -5 1 1271.22 1292.96 116.80 o -2 -5 1 172.52 300.68 67.29 o -1 -5 1 2375.04 2943.68 253.64 o 0 -5 1 17.48 32.57 49.34 o 1 -5 1 1875.21 1939.32 163.80 o 2 -5 1 18.87 42.93 59.83 o 3 -5 1 706.08 648.96 81.69 o 4 -5 1 135.41 97.76 46.68 o 5 -5 1 118.68 95.55 72.43 o 6 -5 1 5.07 16.00 64.83 o 7 -5 1 324.55 464.36 133.60 o 8 -5 1 23.95 9.78 85.88 o 9 -5 1 230.52 148.31 157.58 o 10 -5 1 0.17 12.75 138.14 o -10 -4 1 94.23 178.31 295.80 o -9 -4 1 9.85 -44.86 86.86 o -8 -4 1 364.61 318.88 95.89 o -7 -4 1 32.63 15.80 71.78 o -6 -4 1 469.33 507.53 102.29 o -5 -4 1 377.95 457.18 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