#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:58:53 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180881 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/21/2102167.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102167_Fobs loop_ _publ_author_name 'Chohan, Zahid H.' 'Harrison, William T. A.' 'Howie, R. Alan' 'Milne, Bruce F.' 'Wardell, James L.' _publ_section_title ; Crystallographic and molecular mechanics investigation of an order--disorder transition and dimorphism in 5H,10H-dithiolo[2,3-b]-2,5-benzodithiocine-2-thione ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 1011 _journal_page_last 1017 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.950 _cell_angle_gamma 90.000 _cell_length_a 11.9290 _cell_length_b 11.7639 _cell_length_c 9.0612 _exptl_crystal_F_000 616.00 _reflns_d_resolution_high 0.7706 _cod_data_source_file bm0027alpha-2sup2.hkl _cod_data_source_block alpha-2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' C11H8S5 low temp. alpha form (Z=4, P2(1)/a)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 179.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4538.31 4414.83 103.28 o 4 0 0 32315.98 31650.96 1273.24 o 6 0 0 20385.93 21099.06 470.12 o 8 0 0 37.55 39.85 2.92 o 10 0 0 3492.18 3693.34 94.27 o 12 0 0 23.76 20.82 3.97 o 14 0 0 73.42 68.48 7.77 o 1 1 0 1865.91 1724.15 105.55 o 2 1 0 759.54 737.08 12.21 o 4 1 0 838.23 804.45 13.94 o 5 1 0 112.42 105.59 2.67 o 6 1 0 3314.48 3197.31 47.74 o 7 1 0 10476.47 10996.60 162.07 o 8 1 0 112.52 112.91 3.22 o 9 1 0 1513.25 1548.95 33.13 o 10 1 0 1573.72 1613.08 26.44 o 11 1 0 65.58 67.38 3.29 o 12 1 0 1184.26 1209.89 24.69 o 13 1 0 2027.41 2074.31 41.04 o 14 1 0 2.61 1.26 4.79 o 0 2 0 18658.50 17579.21 491.85 o 1 2 0 771.47 753.29 11.09 o 2 2 0 673.48 674.48 9.86 o 3 2 0 4615.11 4461.64 66.55 o 4 2 0 4497.88 4807.97 71.12 o 5 2 0 1847.87 1877.91 29.52 o 6 2 0 4.47 5.38 1.19 o 7 2 0 2690.75 2722.86 39.87 o 8 2 0 1178.84 1262.34 18.59 o 9 2 0 3456.57 3518.71 55.04 o 10 2 0 264.70 263.34 7.51 o 11 2 0 9.31 9.88 2.40 o 12 2 0 261.06 262.50 7.58 o 13 2 0 1517.78 1567.81 35.14 o 14 2 0 4.65 5.73 5.21 o 1 3 0 676.68 662.29 10.84 o 2 3 0 4269.62 4170.28 60.03 o 3 3 0 5015.61 4795.35 66.24 o 4 3 0 21.04 19.76 1.05 o 5 3 0 174.34 142.68 3.24 o 6 3 0 1743.37 1726.25 24.05 o 7 3 0 908.21 885.97 14.04 o 8 3 0 19.43 27.50 2.30 o 9 3 0 1579.14 1613.00 26.09 o 10 3 0 1346.27 1412.34 23.93 o 11 3 0 25.63 25.81 3.41 o 12 3 0 222.20 202.86 6.20 o 13 3 0 272.21 288.56 9.89 o 14 3 0 199.41 174.82 9.69 o 0 4 0 31376.64 30555.29 667.31 o 1 4 0 765.16 752.76 11.81 o 2 4 0 2301.11 2367.59 30.77 o 3 4 0 465.95 437.14 6.76 o 4 4 0 1919.93 1768.62 25.44 o 5 4 0 421.93 433.64 7.20 o 6 4 0 7563.01 7846.35 107.23 o 7 4 0 278.51 298.82 5.56 o 8 4 0 341.06 371.10 6.94 o 9 4 0 16.84 15.38 2.13 o 10 4 0 1437.14 1521.73 27.03 o 11 4 0 315.21 300.84 7.17 o 12 4 0 224.53 232.12 6.88 o 13 4 0 10.43 8.32 5.33 o 14 4 0 23.04 19.72 6.97 o 1 5 0 3.92 0.24 0.96 o 2 5 0 437.68 468.09 7.18 o 3 5 0 3235.59 3379.73 44.55 o 4 5 0 16.93 19.91 1.45 o 5 5 0 148.06 133.93 2.91 o 6 5 0 175.41 163.71 3.68 o 7 5 0 2472.94 2612.58 36.61 o 8 5 0 500.93 484.81 8.86 o 9 5 0 749.50 818.48 15.54 o 10 5 0 0.53 -1.00 2.33 o 11 5 0 106.68 101.73 4.24 o 12 5 0 1089.48 1115.58 24.44 o 13 5 0 1560.17 1649.50 51.04 o 14 5 0 243.67 217.98 12.85 o 0 6 0 591.74 754.14 16.80 o 1 6 0 46.92 41.16 1.85 o 2 6 0 681.11 704.91 10.31 o 3 6 0 26.76 24.15 1.51 o 4 6 0 123.28 124.40 2.90 o 5 6 0 196.23 186.39 4.10 o 6 6 0 102.97 91.18 2.93 o 7 6 0 105.70 107.50 3.32 o 8 6 0 310.01 302.77 6.26 o 9 6 0 149.92 159.17 5.38 o 10 6 0 164.41 179.89 5.96 o 11 6 0 215.05 202.52 9.06 o 12 6 0 18.13 14.35 4.49 o 13 6 0 32.87 42.75 7.55 o 1 7 0 832.75 946.95 14.62 o 2 7 0 101.97 112.03 3.95 o 3 7 0 554.11 549.36 9.21 o 4 7 0 247.94 258.51 4.70 o 5 7 0 50.87 49.17 2.24 o 6 7 0 1333.65 1363.00 21.59 o 7 7 0 527.70 519.07 9.75 o 8 7 0 29.65 30.05 3.01 o 9 7 0 167.50 165.46 5.31 o 10 7 0 211.36 200.38 6.23 o 11 7 0 161.04 155.71 6.04 o 12 7 0 24.70 20.96 5.69 o 13 7 0 35.84 34.09 7.54 o 0 8 0 60.90 59.33 3.49 o 1 8 0 968.36 977.34 16.41 o 2 8 0 178.65 201.54 4.53 o 3 8 0 462.94 447.54 8.17 o 4 8 0 1.15 0.95 1.79 o 5 8 0 484.17 473.70 8.63 o 6 8 0 850.13 844.22 14.06 o 7 8 0 29.57 29.92 2.57 o 8 8 0 0.02 -1.35 2.82 o 9 8 0 935.53 950.04 22.13 o 10 8 0 623.41 661.64 18.77 o 11 8 0 71.48 61.64 6.10 o 12 8 0 61.52 46.27 9.52 o 1 9 0 33.99 36.40 3.33 o 2 9 0 3236.43 3268.61 49.19 o 3 9 0 83.34 84.94 3.08 o 4 9 0 959.92 980.66 17.15 o 5 9 0 317.72 348.48 7.61 o 6 9 0 2155.97 2249.04 38.65 o 7 9 0 125.28 132.04 4.47 o 8 9 0 592.78 612.37 16.43 o 9 9 0 28.13 33.27 3.78 o 10 9 0 15.92 17.25 4.29 o 11 9 0 229.18 229.13 11.98 o 12 9 0 385.54 383.48 23.19 o 0 10 0 1703.58 1621.29 44.35 o 1 10 0 2073.71 2139.54 40.84 o 2 10 0 13.66 12.66 2.18 o 3 10 0 56.27 54.62 3.11 o 4 10 0 904.57 938.00 18.84 o 5 10 0 1183.69 1205.90 23.58 o 6 10 0 5.85 5.12 4.12 o 7 10 0 899.34 938.94 23.01 o 8 10 0 138.51 131.91 5.29 o 9 10 0 236.47 237.93 8.57 o 10 10 0 0.47 -4.40 4.40 o 11 10 0 270.72 259.35 15.93 o 1 11 0 92.65 104.15 4.76 o 2 11 0 368.05 334.15 8.19 o 3 11 0 252.64 258.24 7.88 o 4 11 0 433.36 421.37 14.49 o 5 11 0 551.01 546.15 15.06 o 6 11 0 21.43 25.75 3.38 o 7 11 0 906.39 929.51 23.85 o 8 11 0 18.37 16.03 4.22 o 9 11 0 38.44 44.35 6.22 o 10 11 0 32.47 26.66 8.07 o 0 12 0 775.04 685.12 35.85 o 1 12 0 1100.10 1099.44 26.36 o 2 12 0 66.81 56.65 3.98 o 3 12 0 74.53 77.78 6.53 o 4 12 0 399.93 383.20 12.70 o 5 12 0 447.76 436.93 15.16 o 6 12 0 7.32 1.44 4.66 o 7 12 0 131.91 114.19 7.74 o 8 12 0 458.03 449.82 28.98 o 9 12 0 59.76 59.67 11.29 o 1 13 0 3.91 1.98 6.63 o 2 13 0 1864.25 2087.40 72.54 o 3 13 0 114.13 104.58 10.96 o 4 13 0 1015.47 1051.33 58.34 o 5 13 0 133.39 130.81 13.59 o 6 13 0 398.93 425.75 20.94 o 7 13 0 137.35 149.45 14.93 o 0 14 0 97.08 52.09 14.48 o 1 14 0 917.21 956.78 47.85 o 2 14 0 25.85 24.83 6.91 o 3 14 0 66.16 74.06 9.54 o 4 14 0 0.94 2.00 6.24 o 5 14 0 541.55 563.14 30.13 o 1 15 0 68.02 47.66 10.52 o 2 15 0 175.17 212.26 14.95 o -14 0 1 785.02 750.61 42.73 o -12 0 1 187.44 174.23 7.57 o -10 0 1 10392.50 10694.58 325.17 o -8 0 1 791.05 821.01 17.97 o -6 0 1 9163.44 9550.15 207.31 o -4 0 1 8080.69 8011.76 201.82 o -2 0 1 1224.94 1184.27 25.79 o 0 0 1 1946.39 1147.93 265.53 o 2 0 1 106.30 118.39 3.86 o 4 0 1 73.60 89.73 3.73 o 6 0 1 360.54 376.21 8.83 o 8 0 1 1367.75 1408.96 32.62 o 10 0 1 0.05 -0.32 3.10 o 12 0 1 1671.85 1730.40 49.89 o 14 0 1 2.47 4.14 6.87 o -15 1 1 0.08 4.70 6.75 o -14 1 1 505.35 509.81 15.37 o -13 1 1 1076.88 1084.39 24.64 o -12 1 1 98.54 81.87 3.70 o -11 1 1 6.40 6.82 2.40 o -10 1 1 1217.43 1212.44 22.42 o -9 1 1 1593.27 1703.78 27.75 o -8 1 1 295.95 279.49 6.66 o -7 1 1 3477.58 3458.53 51.90 o -6 1 1 54.90 54.66 1.64 o -5 1 1 117.42 103.08 3.05 o -4 1 1 198.92 203.14 3.65 o -3 1 1 16554.86 15316.00 306.28 o -2 1 1 360.07 345.54 6.95 o -1 1 1 10381.43 9603.19 146.40 o 0 1 1 207.88 203.93 3.76 o 1 1 1 40.41 36.65 0.89 o 2 1 1 181.81 189.02 3.06 o 3 1 1 4468.11 4614.62 71.51 o 4 1 1 4.30 4.20 1.12 o 5 1 1 2491.87 2683.32 42.00 o 6 1 1 74.04 74.56 4.06 o 7 1 1 11.07 9.90 1.69 o 8 1 1 154.52 149.04 3.99 o 9 1 1 214.83 225.44 5.63 o 10 1 1 105.56 102.49 4.25 o 11 1 1 39.55 43.13 3.48 o 12 1 1 11.50 14.67 3.50 o 13 1 1 0.55 -0.08 3.77 o 14 1 1 56.50 60.77 6.56 o -15 2 1 88.25 66.82 9.82 o -14 2 1 97.81 92.29 6.40 o -13 2 1 2306.48 2373.51 46.13 o -12 2 1 0.01 1.66 2.41 o -11 2 1 643.15 665.83 12.43 o -10 2 1 500.53 531.65 9.89 o -9 2 1 627.79 599.96 10.00 o -8 2 1 91.70 79.58 2.33 o -7 2 1 1552.71 1486.86 24.96 o -6 2 1 4173.39 4582.18 65.74 o -5 2 1 305.02 284.86 4.75 o -4 2 1 1629.91 1548.98 24.35 o -3 2 1 18.00 17.14 0.68 o -2 2 1 4679.15 4582.66 62.08 o -1 2 1 168.81 154.31 2.26 o 0 2 1 34.12 40.08 1.53 o 1 2 1 1220.29 1223.74 20.37 o 2 2 1 2052.04 2084.59 30.71 o 3 2 1 17.91 18.46 1.07 o 4 2 1 147.22 156.16 3.33 o 5 2 1 115.18 103.97 2.66 o 6 2 1 216.76 242.31 4.45 o 7 2 1 22.92 22.85 1.77 o 8 2 1 1047.72 1117.58 17.40 o 9 2 1 16.01 11.50 2.35 o 10 2 1 27.82 28.33 2.73 o 11 2 1 85.15 94.18 4.13 o 12 2 1 817.01 827.10 16.94 o 13 2 1 138.96 120.06 9.33 o 14 2 1 36.66 41.15 5.66 o -14 3 1 268.48 272.42 12.56 o -13 3 1 0.60 1.96 3.07 o -12 3 1 437.78 418.88 9.40 o -11 3 1 41.06 42.51 2.66 o -10 3 1 1042.88 1083.72 18.27 o -9 3 1 0.10 0.18 1.91 o -8 3 1 0.34 -0.08 1.32 o -7 3 1 3829.00 3790.40 58.16 o -6 3 1 571.38 560.89 9.05 o -5 3 1 162.14 104.98 2.98 o -4 3 1 1037.46 991.09 14.75 o -3 3 1 770.68 698.65 9.63 o -2 3 1 791.87 720.77 10.19 o -1 3 1 16591.40 16194.47 220.29 o 0 3 1 54.33 55.61 1.48 o 1 3 1 2344.61 2495.51 40.21 o 2 3 1 3257.11 3179.88 46.07 o 3 3 1 3306.98 3292.16 44.24 o 4 3 1 408.76 404.01 6.38 o 5 3 1 750.91 799.60 13.35 o 6 3 1 887.95 858.69 12.91 o 7 3 1 795.47 910.95 14.53 o 8 3 1 564.24 563.21 10.63 o 9 3 1 49.42 56.65 2.99 o 10 3 1 122.19 125.35 4.11 o 11 3 1 143.88 130.02 4.57 o 12 3 1 189.70 176.48 5.90 o 13 3 1 20.45 16.96 3.97 o 14 3 1 0.08 3.69 5.93 o -14 4 1 53.74 47.03 6.33 o -13 4 1 12.28 5.03 3.57 o -12 4 1 5.28 8.31 2.85 o -11 4 1 132.08 125.45 4.19 o -10 4 1 921.33 907.48 16.16 o -9 4 1 236.53 237.57 5.08 o -8 4 1 611.76 609.13 10.38 o -7 4 1 74.64 65.42 2.05 o -6 4 1 371.35 455.88 7.28 o -5 4 1 156.37 157.93 3.05 o -4 4 1 5619.03 5807.88 75.77 o -3 4 1 0.96 2.30 0.79 o -2 4 1 973.19 1036.91 14.60 o -1 4 1 1912.40 1834.43 26.36 o 0 4 1 1217.76 1205.35 19.41 o 1 4 1 859.31 841.78 13.93 o 2 4 1 1228.72 1221.03 17.68 o 3 4 1 2349.07 2274.09 33.00 o 4 4 1 228.97 235.26 4.30 o 5 4 1 6958.56 7050.72 94.52 o 6 4 1 3458.20 3766.71 61.90 o 7 4 1 52.83 50.82 2.52 o 8 4 1 92.97 105.06 3.52 o 9 4 1 2188.12 2262.83 36.91 o 10 4 1 228.21 229.54 6.05 o 11 4 1 659.15 624.31 15.47 o 12 4 1 377.55 361.91 9.85 o 13 4 1 1.96 8.84 4.64 o 14 4 1 2.93 2.28 5.41 o -14 5 1 216.32 202.12 13.57 o -13 5 1 38.82 39.17 4.46 o -12 5 1 122.46 115.75 4.80 o -11 5 1 67.43 60.68 3.06 o -10 5 1 598.98 592.77 12.07 o -9 5 1 82.86 91.88 3.01 o -8 5 1 752.46 762.91 12.30 o -7 5 1 16.39 25.87 1.80 o -6 5 1 180.06 172.39 3.61 o -5 5 1 214.36 211.12 3.84 o -4 5 1 372.86 356.04 5.28 o -3 5 1 623.17 628.68 9.01 o -2 5 1 801.03 783.83 25.42 o -1 5 1 1010.12 1170.73 17.41 o 0 5 1 879.44 888.36 14.07 o 1 5 1 264.81 248.61 4.78 o 2 5 1 4068.31 4183.30 63.23 o 3 5 1 3195.02 3450.37 48.69 o 4 5 1 1492.71 1552.30 20.79 o 5 5 1 332.28 352.79 6.80 o 6 5 1 1199.27 1230.04 17.23 o 7 5 1 386.85 397.61 8.64 o 8 5 1 1610.59 1638.30 27.76 o 9 5 1 1445.25 1555.96 28.22 o 10 5 1 6.32 5.58 2.68 o 11 5 1 0.82 -3.15 3.15 o 12 5 1 367.83 348.20 11.11 o 13 5 1 229.05 226.41 11.10 o -14 6 1 42.91 46.33 8.26 o -13 6 1 382.09 385.96 16.29 o -12 6 1 40.66 50.88 4.17 o -11 6 1 512.47 522.22 11.48 o -10 6 1 125.22 132.59 4.43 o -9 6 1 168.90 147.66 4.19 o -8 6 1 420.10 410.30 7.43 o -7 6 1 2497.42 2588.81 37.81 o -6 6 1 130.87 122.63 3.16 o -5 6 1 13.38 14.34 1.50 o -4 6 1 1645.71 1498.01 24.29 o -3 6 1 4321.20 4213.74 54.56 o -2 6 1 1420.53 1437.92 20.22 o -1 6 1 795.35 697.29 9.91 o 0 6 1 4.73 6.74 1.32 o 1 6 1 1247.99 1174.28 16.96 o 2 6 1 532.22 558.13 8.98 o 3 6 1 1480.58 1517.04 22.67 o 4 6 1 504.27 517.69 8.14 o 5 6 1 142.76 162.51 3.72 o 6 6 1 335.96 382.20 7.59 o 7 6 1 204.89 216.34 5.86 o 8 6 1 367.82 383.65 8.25 o 9 6 1 17.07 22.63 3.25 o 10 6 1 404.11 397.20 10.02 o 11 6 1 2.44 4.33 3.62 o 12 6 1 1307.55 1350.11 37.91 o 13 6 1 1.76 2.07 6.09 o -13 7 1 1.67 10.86 8.25 o -12 7 1 21.47 25.15 6.20 o -11 7 1 274.27 265.17 8.29 o -10 7 1 890.59 913.41 20.34 o -9 7 1 66.28 64.89 3.43 o -8 7 1 597.79 628.41 10.88 o -7 7 1 1444.58 1469.19 21.28 o -6 7 1 2014.11 2046.82 29.62 o -5 7 1 46.06 43.17 2.17 o -4 7 1 6453.08 6482.96 83.07 o -3 7 1 35.62 38.54 1.95 o -2 7 1 56.96 54.96 2.57 o -1 7 1 1941.64 1796.90 27.77 o 0 7 1 8202.58 8421.91 117.61 o 1 7 1 196.88 199.60 4.22 o 2 7 1 1596.68 1586.68 23.02 o 3 7 1 278.13 227.32 4.52 o 4 7 1 643.77 657.43 12.28 o 5 7 1 0.80 2.61 1.71 o 6 7 1 1071.71 1067.29 18.16 o 7 7 1 468.01 486.58 9.57 o 8 7 1 372.09 371.70 8.83 o 9 7 1 10.89 9.87 3.24 o 10 7 1 0.02 -1.31 3.51 o 11 7 1 107.61 102.38 6.85 o 12 7 1 184.83 173.94 10.06 o -13 8 1 0.10 4.02 5.58 o -12 8 1 221.23 221.33 14.42 o -11 8 1 272.18 278.06 14.04 o -10 8 1 120.05 114.72 5.06 o -9 8 1 10.15 8.31 2.56 o -8 8 1 81.13 77.49 3.57 o -7 8 1 1003.49 1042.91 21.17 o -6 8 1 3165.74 3271.97 48.93 o -5 8 1 242.84 227.59 7.08 o -4 8 1 540.12 555.73 9.78 o -3 8 1 1523.23 1538.23 22.10 o -2 8 1 132.01 129.51 3.22 o -1 8 1 3799.21 3805.85 58.32 o 0 8 1 165.35 155.07 5.18 o 1 8 1 1.12 0.49 1.75 o 2 8 1 30.56 29.38 1.87 o 3 8 1 4233.23 4325.23 67.72 o 4 8 1 844.65 877.01 14.62 o 5 8 1 3029.18 3108.53 54.37 o 6 8 1 2360.76 2556.96 41.90 o 7 8 1 68.11 66.41 3.63 o 8 8 1 1202.26 1269.88 24.67 o 9 8 1 1370.22 1457.31 37.01 o 10 8 1 275.71 259.61 9.92 o 11 8 1 604.00 610.87 25.74 o 12 8 1 37.96 39.60 8.61 o -12 9 1 246.61 245.52 13.05 o -11 9 1 139.05 118.60 9.50 o -10 9 1 29.56 30.08 3.74 o -9 9 1 797.82 850.77 22.10 o -8 9 1 1019.75 1022.39 20.80 o -7 9 1 198.35 200.07 5.88 o -6 9 1 140.08 128.79 4.03 o -5 9 1 726.80 752.71 14.83 o -4 9 1 1795.72 1885.28 33.45 o -3 9 1 379.00 363.59 7.33 o -2 9 1 972.35 960.58 15.96 o -1 9 1 8.56 2.85 2.44 o 0 9 1 155.70 137.47 4.20 o 1 9 1 296.73 300.79 6.91 o 2 9 1 882.75 922.79 16.22 o 3 9 1 791.85 884.03 14.96 o 4 9 1 32.85 39.43 2.82 o 5 9 1 186.63 180.79 5.35 o 6 9 1 54.40 57.91 3.28 o 7 9 1 68.24 66.69 5.15 o 8 9 1 121.65 135.40 6.70 o 9 9 1 1056.89 1106.68 27.41 o 10 9 1 0.58 8.61 4.75 o 11 9 1 55.33 50.58 6.35 o -11 10 1 51.83 48.97 9.58 o -10 10 1 1178.46 1234.19 46.65 o -9 10 1 350.16 342.77 11.66 o -8 10 1 735.24 728.05 20.37 o -7 10 1 44.56 43.37 3.49 o -6 10 1 1194.56 1237.31 27.02 o -5 10 1 376.54 368.56 8.49 o -4 10 1 138.28 135.02 4.76 o -3 10 1 1458.10 1544.93 24.87 o -2 10 1 8.62 11.79 2.94 o -1 10 1 85.33 79.45 3.62 o 0 10 1 5.15 6.16 2.02 o 1 10 1 690.35 688.63 15.48 o 2 10 1 7.37 3.54 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