#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2102168.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102168_Fobs loop_ _publ_author_name 'Chohan, Zahid H.' 'Harrison, William T. A.' 'Howie, R. Alan' 'Milne, Bruce F.' 'Wardell, James L.' _publ_section_title ; Crystallographic and molecular mechanics investigation of an order--disorder transition and dimorphism in 5H,10H-dithiolo[2,3-b]-2,5-benzodithiocine-2-thione ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 1011 _journal_page_last 1017 _journal_volume 56 _journal_year 2000 _space_group_IT_number 12 _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.800 _cell_angle_gamma 90.000 _cell_length_a 12.0750 _cell_length_b 11.8250 _cell_length_c 9.0630 _exptl_crystal_F_000 616.00 _reflns_d_resolution_high 0.7088 _[local]_cod_data_source_file bm0027alphaprime-2sup3.hkl _[local]_cod_data_source_block alphaprime-2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' C11H8S5 room temp. alphaprime form (Z=4,C2/m)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 207.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z' '-x, -y, -z' '-x, y, -z' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5375.63 5268.49 91.96 o 4 0 0 25883.64 22999.54 274.98 o 6 0 0 17816.06 17513.91 302.51 o 8 0 0 124.50 139.32 12.47 o 10 0 0 1406.09 1429.67 36.83 o 12 0 0 42.04 79.30 13.78 o 14 0 0 118.67 146.47 19.94 o 16 0 0 61.26 67.90 18.90 o 1 1 0 1384.58 1438.53 34.79 o 3 1 0 43024.70 37208.39 1129.65 o 5 1 0 7.38 21.04 4.15 o 7 1 0 6620.98 6501.59 102.18 o 9 1 0 1212.29 1308.49 23.40 o 11 1 0 1.05 -7.60 7.60 o 13 1 0 665.87 660.22 22.71 o 15 1 0 1.11 -1.37 9.77 o 0 2 0 19475.27 16976.26 115.87 o 2 2 0 796.95 790.47 50.81 o 4 2 0 4556.69 4761.98 66.90 o 6 2 0 0.52 4.58 5.96 o 8 2 0 783.77 794.65 37.45 o 10 2 0 153.86 169.37 19.61 o 12 2 0 68.75 63.35 10.30 o 14 2 0 2.19 -9.21 9.21 o 16 2 0 7.67 4.47 10.51 o 1 3 0 333.18 262.68 9.78 o 3 3 0 4208.38 3937.78 59.17 o 5 3 0 681.84 708.82 13.26 o 7 3 0 167.90 118.84 7.89 o 9 3 0 1084.50 1033.67 21.67 o 11 3 0 123.79 127.47 11.10 o 13 3 0 59.94 61.38 11.14 o 15 3 0 35.11 20.45 15.18 o 0 4 0 25058.58 22533.54 272.05 o 2 4 0 2392.56 2472.92 36.59 o 4 4 0 791.69 646.80 12.46 o 6 4 0 6894.07 6992.07 106.23 o 8 4 0 768.69 870.34 19.15 o 10 4 0 658.31 620.29 30.47 o 12 4 0 342.39 367.80 17.30 o 14 4 0 15.67 0.47 10.31 o 16 4 0 57.26 37.08 12.93 o 1 5 0 50.06 69.32 4.86 o 3 5 0 2259.04 2243.40 37.37 o 5 5 0 5.92 -0.42 5.66 o 7 5 0 1235.17 1135.80 21.14 o 9 5 0 775.28 841.52 54.11 o 11 5 0 3.15 -6.46 7.16 o 13 5 0 487.12 557.00 59.48 o 15 5 0 20.78 41.06 10.62 o 0 6 0 68.88 59.55 7.15 o 2 6 0 529.65 632.44 20.33 o 4 6 0 2.37 3.18 4.68 o 6 6 0 64.75 44.55 6.64 o 8 6 0 110.63 128.86 14.65 o 10 6 0 53.49 77.22 9.92 o 12 6 0 5.19 2.52 13.18 o 14 6 0 0.06 -9.72 9.72 o 1 7 0 1429.05 1443.22 25.26 o 3 7 0 1377.03 1307.04 23.05 o 5 7 0 41.40 35.72 6.74 o 7 7 0 478.27 386.13 14.49 o 9 7 0 107.94 95.54 9.47 o 11 7 0 1.97 9.85 8.70 o 13 7 0 6.24 21.03 10.30 o 15 7 0 17.04 10.56 10.52 o 0 8 0 1316.58 987.81 26.99 o 2 8 0 237.34 237.61 10.42 o 4 8 0 337.86 272.47 11.92 o 6 8 0 1096.74 1101.17 30.25 o 8 8 0 0.50 10.03 9.03 o 10 8 0 384.81 427.58 18.63 o 12 8 0 57.62 29.90 10.67 o 14 8 0 31.75 36.37 15.59 o 1 9 0 126.47 67.72 8.09 o 3 9 0 220.25 127.57 9.42 o 5 9 0 420.30 466.51 39.18 o 7 9 0 263.13 337.05 15.58 o 9 9 0 0.06 11.70 11.67 o 11 9 0 90.12 117.73 13.03 o 13 9 0 44.14 71.81 12.51 o 0 10 0 147.86 260.63 17.66 o 2 10 0 20.88 30.78 7.86 o 4 10 0 78.32 107.17 10.25 o 6 10 0 11.17 0.51 7.85 o 8 10 0 37.85 46.20 37.54 o 10 10 0 0.59 4.43 14.17 o 12 10 0 16.90 -9.68 9.93 o 1 11 0 7.40 12.50 17.91 o 3 11 0 146.09 124.44 10.61 o 5 11 0 7.71 9.70 8.08 o 7 11 0 157.27 200.80 26.36 o 9 11 0 73.19 49.93 10.86 o 11 11 0 0.03 -2.63 10.43 o 0 12 0 497.12 436.25 24.23 o 2 12 0 2.38 -8.14 17.21 o 4 12 0 86.30 126.72 11.74 o 6 12 0 104.73 79.79 10.78 o 8 12 0 0.55 1.44 10.29 o 10 12 0 78.77 96.32 13.39 o 1 13 0 0.01 -8.88 8.88 o 3 13 0 72.68 81.74 21.30 o 5 13 0 10.63 30.15 9.19 o 7 13 0 34.30 51.29 11.61 o 9 13 0 1.61 17.82 9.87 o 0 14 0 1.00 31.65 13.93 o 2 14 0 1.61 3.90 9.22 o 4 14 0 7.05 9.48 22.10 o 6 14 0 0.72 -10.15 10.15 o 8 14 0 0.03 3.11 10.40 o 1 15 0 0.00 20.25 9.46 o 3 15 0 2.69 -9.93 9.93 o 5 15 0 1.06 12.03 10.00 o 7 15 0 9.61 12.71 10.54 o 0 16 0 68.97 81.29 19.94 o 2 16 0 0.01 0.64 10.52 o 4 16 0 10.77 3.57 10.90 o -16 0 1 180.00 143.42 23.63 o -14 0 1 251.61 246.26 23.40 o -12 0 1 135.10 120.53 15.75 o -10 0 1 6292.66 6583.16 146.28 o -8 0 1 512.80 559.82 20.59 o -6 0 1 9394.79 9330.06 218.19 o -4 0 1 8636.84 9027.49 169.72 o -2 0 1 1142.94 1147.02 26.12 o 0 0 1 1780.97 1972.15 45.99 o 2 0 1 114.56 171.33 6.74 o 4 0 1 526.74 618.90 15.12 o 6 0 1 16.03 12.61 5.94 o 8 0 1 665.45 671.30 22.76 o 10 0 1 4.44 5.97 9.45 o 12 0 1 371.41 374.12 23.27 o 14 0 1 3.64 0.00 13.84 o 16 0 1 11.33 -9.55 14.76 o -15 1 1 15.25 -13.78 14.59 o -13 1 1 718.32 750.56 33.44 o -11 1 1 3.42 8.10 10.84 o -9 1 1 1451.93 1477.00 36.43 o -7 1 1 3333.10 3680.07 75.64 o -5 1 1 63.05 40.49 6.35 o -3 1 1 16532.35 15958.26 201.55 o -1 1 1 10645.35 8899.74 112.38 o 1 1 1 10.34 36.28 3.77 o 3 1 1 3951.90 4011.60 77.58 o 5 1 1 1819.69 1869.57 42.57 o 7 1 1 40.07 33.36 8.13 o 9 1 1 25.72 31.06 9.18 o 11 1 1 26.34 37.58 11.92 o 13 1 1 35.31 2.39 13.65 o 15 1 1 10.40 2.91 13.20 o -16 2 1 13.18 6.11 16.02 o -14 2 1 34.77 16.41 15.41 o -12 2 1 2.90 11.26 12.24 o -10 2 1 394.70 387.79 21.40 o -8 2 1 1.47 -7.99 7.99 o -6 2 1 3084.99 3740.63 82.07 o -4 2 1 1075.95 920.58 22.63 o -2 2 1 4394.37 4386.03 102.14 o 0 2 1 71.14 88.31 5.15 o 2 2 1 1999.35 2098.41 43.89 o 4 2 1 97.60 104.32 7.73 o 6 2 1 132.98 157.23 10.85 o 8 2 1 771.94 768.13 24.98 o 10 2 1 2.08 0.87 9.35 o 12 2 1 247.23 230.13 20.66 o 14 2 1 10.94 1.34 14.34 o 16 2 1 1.67 -13.56 13.56 o -15 3 1 16.63 26.87 15.17 o -13 3 1 14.88 31.39 12.89 o -11 3 1 17.65 20.66 11.27 o -9 3 1 31.51 9.67 9.61 o -7 3 1 2981.34 3111.95 65.51 o -5 3 1 186.39 167.07 10.41 o -3 3 1 630.67 591.99 14.94 o -1 3 1 15901.86 14357.53 197.38 o 1 3 1 2464.51 2902.87 64.70 o 3 3 1 2715.64 2732.94 60.16 o 5 3 1 524.43 589.57 17.90 o 7 3 1 456.05 481.13 19.17 o 9 3 1 34.70 49.49 10.03 o 11 3 1 64.50 66.12 13.59 o 13 3 1 0.43 18.50 12.15 o 15 3 1 37.44 49.26 15.73 o -16 4 1 25.11 52.11 16.18 o -14 4 1 36.14 36.87 13.30 o -12 4 1 6.86 2.16 10.25 o -10 4 1 629.76 611.00 26.01 o -8 4 1 401.11 387.58 18.75 o -6 4 1 205.49 217.32 12.72 o -4 4 1 5375.31 5689.35 116.93 o -2 4 1 1112.49 1312.05 29.47 o 0 4 1 1475.93 1535.91 33.24 o 2 4 1 1438.71 1716.12 37.87 o 4 4 1 193.70 149.29 10.45 o 6 4 1 2373.57 2293.03 52.25 o 8 4 1 102.36 146.40 13.68 o 10 4 1 63.25 69.80 13.19 o 12 4 1 54.60 37.84 13.42 o 14 4 1 1.98 6.96 12.68 o -15 5 1 0.06 -7.42 15.22 o -13 5 1 3.93 -1.24 13.26 o -11 5 1 3.01 -2.03 10.16 o -9 5 1 35.26 34.66 10.63 o -7 5 1 99.42 126.07 12.34 o -5 5 1 6.77 -5.99 5.99 o -3 5 1 557.97 592.80 17.19 o -1 5 1 2113.20 2446.27 52.27 o 1 5 1 181.47 190.12 9.82 o 3 5 1 4247.74 4470.76 89.23 o 5 5 1 347.98 362.78 16.01 o 7 5 1 270.85 288.81 16.54 o 9 5 1 639.42 612.89 26.69 o 11 5 1 0.01 2.15 10.45 o 13 5 1 8.04 2.61 13.83 o 15 5 1 19.08 23.43 16.31 o -14 6 1 13.50 5.63 13.35 o -12 6 1 47.83 57.51 14.80 o -10 6 1 86.66 60.15 12.80 o -8 6 1 42.13 13.55 9.73 o -6 6 1 0.89 7.21 8.10 o -4 6 1 429.70 365.21 15.75 o -2 6 1 268.50 379.03 14.78 o 0 6 1 124.26 149.88 10.38 o 2 6 1 27.46 52.34 8.05 o 4 6 1 466.79 541.31 19.42 o 6 6 1 469.04 535.36 21.44 o 8 6 1 113.11 114.88 13.72 o 10 6 1 156.25 128.32 16.46 o 12 6 1 269.83 286.19 23.60 o 14 6 1 5.98 -5.92 13.73 o -15 7 1 0.01 15.89 14.22 o -13 7 1 67.69 33.64 15.87 o -11 7 1 188.27 146.78 16.97 o -9 7 1 62.81 50.94 14.31 o -7 7 1 1475.12 1252.17 34.58 o -5 7 1 54.30 70.23 11.21 o -3 7 1 246.79 270.95 15.32 o -1 7 1 331.57 409.51 16.91 o 1 7 1 3.00 7.17 8.05 o 3 7 1 4.46 13.32 7.32 o 5 7 1 1.18 0.00 7.67 o 7 7 1 414.94 383.13 21.04 o 9 7 1 1.95 1.99 11.07 o 11 7 1 0.75 5.95 13.19 o 13 7 1 5.71 -4.24 14.49 o -14 8 1 53.57 45.91 17.04 o -12 8 1 1.24 2.60 14.50 o -10 8 1 79.32 30.89 13.51 o -8 8 1 4.07 17.78 10.79 o -6 8 1 286.34 373.78 20.29 o -4 8 1 385.07 278.71 17.47 o -2 8 1 109.27 72.21 10.35 o 0 8 1 242.71 290.54 16.23 o 2 8 1 27.83 20.39 8.45 o 4 8 1 461.39 601.82 23.13 o 6 8 1 767.79 912.11 30.97 o 8 8 1 378.46 453.33 24.67 o 10 8 1 20.23 20.84 14.55 o 12 8 1 4.97 9.56 12.29 o 14 8 1 0.08 1.60 14.05 o -13 9 1 18.66 29.77 16.57 o -11 9 1 0.04 -8.94 13.21 o -9 9 1 18.54 53.69 13.82 o -7 9 1 40.88 -12.03 12.03 o -5 9 1 998.73 792.20 29.05 o -3 9 1 57.10 17.45 10.15 o -1 9 1 89.86 93.27 10.94 o 1 9 1 607.00 753.22 25.23 o 3 9 1 216.65 372.95 19.90 o 5 9 1 156.58 125.28 14.53 o 7 9 1 1.03 21.72 11.60 o 9 9 1 292.11 340.08 24.10 o 11 9 1 13.48 1.33 12.60 o 13 9 1 38.50 45.09 16.23 o -12 10 1 0.02 -2.93 14.04 o -10 10 1 127.22 129.49 19.58 o -8 10 1 282.15 239.14 20.59 o -6 10 1 100.03 166.43 17.18 o -4 10 1 60.40 52.32 12.19 o -2 10 1 191.37 128.24 13.78 o 0 10 1 7.13 13.91 9.08 o 2 10 1 88.90 52.35 10.88 o 4 10 1 151.86 209.26 17.83 o 6 10 1 108.94 209.62 17.45 o 8 10 1 185.92 195.65 19.53 o 10 10 1 21.70 5.29 14.85 o 12 10 1 3.05 12.20 13.81 o -11 11 1 37.04 34.96 16.35 o -9 11 1 0.02 -1.28 13.00 o -7 11 1 97.55 56.87 14.39 o -5 11 1 112.65 58.66 13.92 o -3 11 1 59.99 63.20 13.61 o -1 11 1 279.94 127.53 14.67 o 1 11 1 5.30 2.79 10.23 o 3 11 1 168.79 164.68 16.74 o 5 11 1 63.99 52.84 13.37 o 7 11 1 4.02 -12.55 12.55 o 9 11 1 3.48 15.94 13.55 o 11 11 1 7.33 -10.59 14.90 o -10 12 1 39.59 13.20 15.46 o -8 12 1 6.48 5.24 13.23 o -6 12 1 0.24 26.09 12.32 o -4 12 1 51.28 25.24 11.87 o -2 12 1 33.49 82.64 14.15 o 0 12 1 65.27 60.92 13.34 o 2 12 1 0.29 14.80 11.48 o 4 12 1 41.09 70.52 15.63 o 6 12 1 121.30 201.02 20.42 o 8 12 1 0.75 -6.76 13.45 o 10 12 1 12.50 19.74 16.70 o -9 13 1 1.43 -11.96 15.40 o -7 13 1 9.97 21.71 13.16 o -5 13 1 69.53 98.95 17.04 o -3 13 1 24.22 9.47 14.60 o -1 13 1 6.94 6.91 10.56 o 1 13 1 40.98 47.45 14.50 o 3 13 1 81.90 48.00 13.58 o 5 13 1 5.57 19.19 12.60 o 7 13 1 4.20 -4.18 14.42 o 9 13 1 40.95 64.74 17.57 o -8 14 1 33.02 35.44 16.38 o -6 14 1 2.30 1.42 12.96 o -4 14 1 0.07 -5.35 14.27 o -2 14 1 10.15 -7.72 13.25 o 0 14 1 3.54 -12.16 12.16 o 2 14 1 0.92 -9.08 12.52 o 4 14 1 4.73 1.36 13.23 o 6 14 1 15.13 4.36 14.31 o 8 14 1 13.12 17.39 13.69 o -7 15 1 1.55 -14.95 14.95 o -5 15 1 7.99 13.53 14.66 o -3 15 1 4.29 18.69 14.73 o -1 15 1 24.09 14.07 13.78 o 1 15 1 0.06 -14.19 14.19 o 3 15 1 18.52 30.52 15.17 o 5 15 1 3.34 1.53 14.26 o -4 16 1 7.59 4.80 14.93 o -2 16 1 8.33 9.32 15.69 o 0 16 1 4.83 37.00 15.10 o 2 16 1 0.30 -14.08 15.24 o 4 16 1 0.13 3.24 15.55 o -16 0 2 79.28 73.08 16.81 o -14 0 2 27.91 17.22 12.90 o -12 0 2 920.73 953.13 34.25 o -10 0 2 99.58 102.66 13.72 o -8 0 2 320.28 333.51 16.08 o -6 0 2 62.55 44.54 6.72 o -4 0 2 699.14 738.42 18.81 o -2 0 2 46.73 38.43 4.61 o 0 0 2 12011.02 11981.19 159.36 o 2 0 2 9101.92 9192.98 165.77 o 4 0 2 2695.92 2451.08 52.53 o 6 0 2 14.53 33.52 7.34 o 8 0 2 1708.93 1623.77 39.91 o 10 0 2 655.11 522.93 25.26 o 12 0 2 57.49 68.95 15.29 o 14 0 2 577.32 588.34 34.50 o -15 1 2 40.01 68.11 16.12 o -13 1 2 0.73 14.48 10.86 o -11 1 2 55.40 58.14 11.28 o -9 1 2 113.04 131.19 12.65 o -7 1 2 490.59 460.23 16.96 o -5 1 2 7.54 1.55 4.95 o -3 1 2 1164.75 1346.99 28.85 o -1 1 2 108.17 111.76 5.79 o 1 1 2 11507.98 10601.11 165.61 o 3 1 2 2990.17 3261.33 64.17 o 5 1 2 271.87 289.79 12.77 o 7 1 2 874.77 842.00 25.00 o 9 1 2 11.73 -2.44 8.48 o 11 1 2 277.02 336.70 21.60 o 13 1 2 0.23 3.77 12.25 o 15 1 2 12.18 7.60 14.02 o -16 2 2 32.19 15.09 14.63 o -14 2 2 4.16 1.25 13.04 o -12 2 2 281.50 269.00 20.73 o -10 2 2 182.87 243.00 17.18 o -8 2 2 532.27 515.62 20.13 o -6 2 2 0.01 -3.81 5.80 o -4 2 2 1191.94 1214.96 26.57 o -2 2 2 611.46 744.35 17.18 o 0 2 2 1119.29 1156.17 25.51 o 2 2 2 7417.53 7378.52 159.06 o 4 2 2 110.47 112.98 8.51 o 6 2 2 627.94 639.05 20.70 o 8 2 2 207.20 164.26 13.60 o 10 2 2 0.87 0.00 8.50 o 12 2 2 0.20 14.94 11.55 o 14 2 2 1.89 -1.40 15.13 o -15 3 2 4.24 -12.66 12.66 o -13 3 2 1.58 11.52 12.51 o -11 3 2 162.42 182.96 16.70 o -9 3 2 60.44 51.31 11.54 o -7 3 2 11.92 32.50 7.91 o -5 3 2 288.85 253.81 12.47 o -3 3 2 288.35 345.18 12.10 o -1 3 2 3492.40 3496.85 76.41 o 1 3 2 7092.62 6931.83 156.70 o 3 3 2 264.92 321.12 12.59 o 5 3 2 4501.23 4657.47 97.56 o 7 3 2 1946.12 1883.55 44.34 o 9 3 2 76.63 98.82 13.52 o 11 3 2 634.03 646.51 29.27 o 13 3 2 137.54 134.50 18.10 o 15 3 2 2.56 20.21 12.73 o -16 4 2 16.57 23.42 15.69 o -14 4 2 6.65 5.21 12.36 o -12 4 2 29.01 33.23 12.55 o -10 4 2 0.02 0.00 9.04 o -8 4 2 88.04 81.49 11.12 o -6 4 2 930.25 1013.28 25.82 o -4 4 2 161.17 277.45 12.80 o -2 4 2 5990.51 5374.97 105.97 o 0 4 2 224.74 237.49 10.64 o 2 4 2 775.32 892.49 22.13 o 4 4 2 3078.66 3118.10 68.20 o 6 4 2 513.06 557.13 21.15 o 8 4 2 1286.39 1354.61 35.01 o 10 4 2 140.78 131.01 15.91 o 12 4 2 55.01 91.53 15.80 o 14 4 2 230.70 235.25 23.95 o -15 5 2 11.34 -1.47 13.71 o -13 5 2 36.58 35.54 13.81 o -11 5 2 0.89 9.09 11.02 o -9 5 2 199.93 212.92 16.71 o -7 5 2 0.04 -2.01 7.95 o -5 5 2 1436.60 1369.76 34.11 o -3 5 2 1178.31 1212.01 29.10 o -1 5 2 62.69 31.47 6.96 o 1 5 2 7886.56 7820.85 140.30 o 3 5 2 23.12 40.39 7.00 o 5 5 2 258.05 271.70 15.06 o 7 5 2 418.59 430.26 20.91 o 9 5 2 0.02 0.93 9.44 o 11 5 2 32.31 54.39 13.88 o 13 5 2 2.32 -8.19 12.81 o 15 5 2 1.82 17.86 12.68 o -14 6 2 8.74 2.79 16.72 o -12 6 2 158.35 158.50 18.57 o -10 6 2 16.15 23.22 12.08 o -8 6 2 363.99 468.17 21.87 o -6 6 2 643.13 603.10 21.78 o -4 6 2 15.73 18.06 7.27 o -2 6 2 620.49 643.04 19.29 o 0 6 2 270.20 317.02 14.41 o 2 6 2 1249.19 1504.89 37.24 o 4 6 2 69.88 67.45 9.57 o 6 6 2 147.40 156.96 14.09 o 8 6 2 189.69 159.23 15.90 o 10 6 2 21.68 27.00 12.36 o 12 6 2 10.64 20.73 13.09 o 14 6 2 5.41 6.16 14.11 o -15 7 2 4.80 -16.05 16.05 o -13 7 2 0.00 17.35 13.68 o -11 7 2 7.04 -12.46 12.46 o -9 7 2 60.01 20.75 11.08 o -7 7 2 359.54 228.32 17.01 o -5 7 2 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