#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/21/2102171.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102171_Fobs loop_ _publ_author_name 'Chisholm, Greig' 'Kennedy, Alan R.' 'Wilson, Sharon' 'Teat, Simon J.' _publ_section_title ; Comparison of the structural motifs of acetoacetanilides and related azo pigments ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 1046 _journal_page_last 1053 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.967 _cell_angle_gamma 90.000 _cell_length_a 14.1109 _cell_length_b 7.5667 _cell_length_c 15.3382 _exptl_crystal_F_000 712.00 _reflns_d_resolution_high 0.8818 _[local]_cod_data_source_file bm00319sup2.hkl _[local]_cod_data_source_block 9 #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 106.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1163.53 1057.10 49.32 o 6 0 0 1655.64 2122.74 89.34 o 8 0 0 14.69 30.95 18.46 o 10 0 0 576.31 594.63 40.34 o 12 0 0 351.90 320.48 33.77 o 14 0 0 24.54 52.11 32.40 o 1 1 0 1018.41 709.19 34.28 o 2 1 0 4110.16 4352.59 151.12 o 3 1 0 742.38 904.59 46.69 o 4 1 0 1352.93 1496.91 60.70 o 5 1 0 641.28 675.72 25.40 o 6 1 0 221.92 220.95 29.25 o 7 1 0 523.47 681.46 26.09 o 8 1 0 14.54 33.03 12.77 o 9 1 0 589.83 563.41 21.82 o 10 1 0 839.71 791.80 28.52 o 11 1 0 1187.79 1243.71 40.70 o 12 1 0 945.35 974.39 45.51 o 13 1 0 469.67 385.22 22.90 o 14 1 0 602.45 578.11 29.98 o 15 1 0 55.23 36.16 16.50 o 0 2 0 341.19 307.07 36.34 o 1 2 0 2897.87 2824.37 105.15 o 2 2 0 255.64 223.50 14.51 o 3 2 0 24.08 37.19 7.05 o 4 2 0 37.75 71.56 18.02 o 5 2 0 86.43 115.76 27.41 o 6 2 0 47.75 66.91 26.71 o 7 2 0 309.54 354.31 16.67 o 8 2 0 233.79 252.53 13.78 o 9 2 0 103.02 111.99 21.00 o 10 2 0 625.14 664.34 33.02 o 11 2 0 1081.71 1040.90 48.65 o 12 2 0 657.44 674.48 40.53 o 13 2 0 315.11 295.76 19.61 o 14 2 0 78.87 69.58 16.35 o 15 2 0 112.07 93.91 25.98 o 1 3 0 1057.59 914.93 40.96 o 2 3 0 83.38 56.06 28.50 o 3 3 0 506.79 442.15 46.65 o 4 3 0 371.24 372.39 39.56 o 5 3 0 61.95 79.89 13.99 o 6 3 0 347.48 332.90 22.95 o 7 3 0 903.23 813.81 32.45 o 8 3 0 438.85 474.84 25.97 o 9 3 0 798.16 780.33 37.98 o 10 3 0 29.86 39.69 15.57 o 11 3 0 21.55 28.12 21.61 o 12 3 0 0.00 -3.79 23.10 o 13 3 0 0.56 -0.99 36.35 o 14 3 0 196.99 212.53 28.31 o 0 4 0 773.38 835.77 54.68 o 1 4 0 331.80 270.95 17.73 o 2 4 0 41.82 48.33 10.06 o 3 4 0 691.82 699.15 57.42 o 4 4 0 215.02 214.57 15.72 o 5 4 0 58.63 67.39 19.04 o 6 4 0 90.37 76.74 11.77 o 7 4 0 414.65 495.19 39.39 o 8 4 0 505.17 566.87 29.83 o 9 4 0 75.48 99.88 15.51 o 10 4 0 1787.24 1837.23 102.42 o 11 4 0 6.92 33.78 36.33 o 12 4 0 1.74 -6.72 35.71 o 13 4 0 3.48 -24.19 38.29 o 1 5 0 20.14 32.26 18.03 o 2 5 0 240.25 228.23 15.73 o 3 5 0 1100.25 997.17 68.74 o 4 5 0 736.68 779.08 34.27 o 5 5 0 246.22 300.33 29.94 o 6 5 0 106.37 127.94 14.54 o 7 5 0 3.64 7.75 21.79 o 8 5 0 96.42 151.15 16.40 o 9 5 0 639.51 701.60 51.85 o 10 5 0 17.98 24.50 36.00 o 11 5 0 214.20 179.01 24.34 o 12 5 0 52.85 65.35 38.75 o 0 6 0 259.31 268.65 25.60 o 1 6 0 119.79 149.24 14.93 o 2 6 0 0.32 -4.30 21.97 o 3 6 0 94.48 110.88 18.25 o 4 6 0 16.05 -0.82 20.81 o 5 6 0 54.10 44.79 24.29 o 6 6 0 52.20 44.77 32.84 o 7 6 0 7.58 9.07 34.58 o 8 6 0 37.14 42.36 35.99 o 9 6 0 31.22 50.45 23.26 o 10 6 0 304.40 303.91 29.77 o 1 7 0 2.72 17.11 26.09 o 2 7 0 29.90 44.78 26.72 o 3 7 0 10.53 35.46 21.89 o 4 7 0 5.26 20.84 31.36 o 5 7 0 13.42 6.73 32.57 o 6 7 0 6.82 26.56 31.11 o 8 7 0 10.74 17.85 37.78 o 9 7 0 168.90 116.61 23.13 o 0 8 0 8.32 16.18 46.92 o 1 8 0 37.89 68.51 31.04 o 3 8 0 40.48 28.22 19.47 o 4 8 0 85.21 80.80 20.32 o 5 8 0 55.61 47.68 22.24 o -15 0 1 41.77 66.79 23.92 o -13 0 1 723.88 636.80 45.89 o -11 0 1 4978.68 5419.66 283.47 o -9 0 1 18.52 32.25 19.21 o -7 0 1 3716.65 4422.21 169.09 o -5 0 1 14.59 11.30 18.79 o -3 0 1 30.12 61.39 67.31 o 3 0 1 463.25 472.12 47.59 o 5 0 1 4476.90 5698.11 208.42 o 7 0 1 0.61 15.85 19.28 o 9 0 1 0.78 -5.95 20.54 o 11 0 1 1.22 11.84 25.00 o 13 0 1 92.94 74.37 20.11 o 15 0 1 82.93 63.64 24.40 o -15 1 1 35.73 38.91 24.31 o -14 1 1 171.01 159.15 15.88 o -13 1 1 416.84 370.15 22.67 o -12 1 1 181.98 208.53 16.70 o -11 1 1 2.44 9.80 19.97 o -10 1 1 79.73 77.16 11.16 o -9 1 1 103.15 121.57 10.86 o -8 1 1 370.72 436.12 20.33 o -7 1 1 1056.90 1051.92 41.42 o -6 1 1 58.95 50.55 27.04 o -5 1 1 7.47 23.69 15.07 o -4 1 1 84.90 89.50 10.13 o -3 1 1 4869.78 5632.95 197.33 o -2 1 1 1160.84 868.56 76.90 o -1 1 1 38.17 37.24 32.32 o 0 1 1 1179.04 980.44 44.23 o 1 1 1 281.48 234.78 22.07 o 2 1 1 6019.14 8305.59 442.35 o 3 1 1 3242.58 4089.90 107.23 o 4 1 1 2755.72 3299.65 97.92 o 5 1 1 1354.44 1610.25 48.54 o 6 1 1 1455.36 1860.43 56.64 o 7 1 1 759.49 859.62 34.09 o 8 1 1 1327.35 1394.31 43.40 o 9 1 1 186.39 182.34 11.36 o 10 1 1 183.10 191.26 12.04 o 11 1 1 2.39 9.60 17.42 o 12 1 1 336.84 246.29 16.05 o 13 1 1 9.70 20.81 21.27 o 14 1 1 16.23 24.18 23.03 o 15 1 1 10.37 8.81 26.44 o -15 2 1 0.01 -8.81 25.28 o -14 2 1 18.57 19.59 24.67 o -13 2 1 37.14 24.74 16.70 o -12 2 1 4.97 8.22 21.78 o -11 2 1 216.89 237.36 26.92 o -10 2 1 150.92 163.08 14.77 o -9 2 1 59.78 71.44 16.38 o -8 2 1 73.65 88.42 9.22 o -7 2 1 285.66 349.81 25.11 o -6 2 1 175.23 176.05 29.46 o -5 2 1 180.11 197.34 40.59 o -4 2 1 118.27 151.56 49.02 o -3 2 1 3595.99 3493.50 104.71 o -2 2 1 459.20 390.87 27.41 o -1 2 1 56.52 67.38 33.50 o 0 2 1 101.71 140.31 39.77 o 1 2 1 436.36 379.35 29.83 o 2 2 1 96.87 103.07 9.95 o 3 2 1 2.19 0.90 10.12 o 4 2 1 214.26 205.29 14.76 o 5 2 1 586.73 691.60 51.83 o 6 2 1 93.70 129.47 16.90 o 7 2 1 1517.46 1640.96 48.88 o 8 2 1 272.95 282.37 13.24 o 9 2 1 1186.74 1309.66 41.59 o 10 2 1 666.67 625.68 23.98 o 11 2 1 1694.86 1690.47 60.63 o 12 2 1 208.04 202.38 14.73 o 13 2 1 8.21 4.65 25.17 o 14 2 1 8.73 4.68 38.43 o 15 2 1 8.17 -14.60 41.75 o -14 3 1 16.61 36.05 39.79 o -13 3 1 64.64 59.53 25.25 o -12 3 1 23.31 20.57 30.56 o -11 3 1 0.08 3.64 21.11 o -10 3 1 107.68 123.48 14.12 o -9 3 1 26.31 51.22 12.97 o -8 3 1 551.22 621.25 31.46 o -7 3 1 1394.15 1367.42 58.50 o -6 3 1 71.40 94.56 8.07 o -5 3 1 1227.36 1345.09 148.47 o -4 3 1 118.08 188.89 32.48 o -3 3 1 124.80 119.15 48.01 o -2 3 1 2646.52 2054.57 114.70 o -1 3 1 71.07 77.27 20.08 o 0 3 1 0.35 0.20 12.09 o 1 3 1 8.12 8.31 11.80 o 2 3 1 120.16 121.42 14.51 o 3 3 1 296.15 308.55 50.86 o 4 3 1 2.73 17.40 13.27 o 5 3 1 0.47 9.15 12.72 o 6 3 1 191.99 194.42 14.94 o 7 3 1 494.41 577.48 38.68 o 8 3 1 19.20 31.03 17.03 o 9 3 1 3.67 10.06 21.27 o 10 3 1 390.88 410.30 46.98 o 11 3 1 375.78 388.06 33.77 o 12 3 1 67.70 68.00 22.27 o 13 3 1 27.11 28.60 35.39 o 14 3 1 7.84 -23.91 41.02 o -14 4 1 142.30 135.46 26.76 o -13 4 1 80.19 96.45 23.77 o -12 4 1 212.95 257.87 27.41 o -11 4 1 218.89 223.98 21.42 o -10 4 1 65.42 99.85 16.08 o -9 4 1 228.20 281.40 20.28 o -8 4 1 27.79 45.34 17.14 o -7 4 1 137.86 173.12 21.93 o -6 4 1 0.36 8.94 19.32 o -5 4 1 32.00 40.83 20.81 o -4 4 1 488.71 520.21 21.51 o -3 4 1 369.52 407.15 22.38 o -2 4 1 44.77 55.56 19.56 o -1 4 1 230.79 253.34 17.28 o 0 4 1 11.56 9.11 14.89 o 1 4 1 767.00 650.39 31.49 o 2 4 1 2.94 -4.42 12.87 o 3 4 1 1340.81 1371.46 55.92 o 4 4 1 19.61 16.03 13.91 o 5 4 1 0.01 4.78 13.98 o 6 4 1 22.50 37.29 10.60 o 7 4 1 171.34 195.47 16.67 o 8 4 1 208.37 208.60 17.47 o 9 4 1 4.11 27.55 37.72 o 10 4 1 59.71 108.06 23.82 o 11 4 1 122.87 99.97 23.14 o 12 4 1 81.89 129.94 25.40 o 13 4 1 35.77 50.80 37.99 o -12 5 1 23.84 18.19 36.92 o -11 5 1 1.18 8.65 36.48 o -10 5 1 10.16 13.44 34.46 o -9 5 1 57.29 60.17 19.04 o -8 5 1 160.36 182.07 16.70 o -7 5 1 2.47 27.45 21.76 o -6 5 1 375.61 396.66 22.57 o -5 5 1 2.58 23.94 20.29 o -4 5 1 95.05 133.93 15.27 o -3 5 1 172.59 172.67 13.79 o -2 5 1 254.35 247.53 17.10 o -1 5 1 1.25 -4.47 17.48 o 0 5 1 456.38 439.35 23.38 o 1 5 1 661.64 561.02 28.55 o 2 5 1 7.74 13.34 14.83 o 3 5 1 1526.03 1414.10 49.09 o 4 5 1 1.17 7.09 22.26 o 5 5 1 11.60 18.11 17.91 o 6 5 1 0.12 -4.69 23.37 o 7 5 1 25.28 45.09 31.83 o 8 5 1 20.65 46.33 36.57 o 9 5 1 114.94 132.48 22.62 o 10 5 1 2.99 0.29 38.05 o 11 5 1 12.56 16.40 37.58 o 12 5 1 0.60 -18.71 38.97 o -11 6 1 2.32 -19.80 35.09 o -10 6 1 64.01 58.26 23.73 o -9 6 1 127.33 126.34 23.51 o -8 6 1 11.47 2.93 32.12 o -7 6 1 81.50 83.63 24.92 o -6 6 1 8.60 9.80 24.73 o -5 6 1 112.65 123.11 15.93 o -4 6 1 0.04 14.83 21.59 o -3 6 1 424.81 422.35 22.82 o -2 6 1 0.18 4.81 28.24 o -1 6 1 0.04 4.96 22.77 o 0 6 1 1.48 -3.10 21.72 o 1 6 1 277.79 306.41 29.21 o 2 6 1 19.76 23.24 18.05 o 3 6 1 612.64 695.91 35.37 o 4 6 1 2.63 17.52 20.39 o 5 6 1 6.90 44.97 30.29 o 6 6 1 16.89 51.29 34.08 o 7 6 1 0.09 7.18 32.98 o 8 6 1 5.53 16.05 37.73 o 9 6 1 134.19 106.17 23.34 o 10 6 1 2.07 -9.96 39.75 o 11 6 1 179.08 170.60 27.06 o -9 7 1 0.66 -10.58 40.66 o -8 7 1 23.40 18.86 32.48 o -7 7 1 5.26 16.97 34.93 o -6 7 1 5.55 -21.34 33.19 o -5 7 1 2.39 1.47 24.69 o -4 7 1 273.55 250.74 17.57 o -3 7 1 41.25 43.89 23.59 o -2 7 1 77.77 53.08 24.35 o -1 7 1 16.28 14.91 25.28 o 0 7 1 1.15 13.01 25.62 o 1 7 1 56.23 72.71 16.74 o 2 7 1 18.71 34.07 20.82 o 3 7 1 195.53 230.03 27.00 o 4 7 1 210.16 207.76 22.20 o 5 7 1 3.33 20.18 30.95 o 6 7 1 16.92 34.96 34.84 o 7 7 1 16.37 37.01 34.07 o 8 7 1 46.68 44.31 24.20 o -5 8 1 39.36 24.15 33.60 o -4 8 1 45.61 29.60 23.79 o -3 8 1 101.94 99.35 21.76 o -2 8 1 13.04 27.83 26.46 o -1 8 1 24.88 55.08 42.77 o 0 8 1 0.66 -2.66 44.52 o 1 8 1 36.55 67.18 40.91 o 2 8 1 2.51 -14.15 41.54 o 4 8 1 1.14 -3.90 30.01 o 5 8 1 27.31 42.00 31.63 o -14 0 2 1188.14 1135.08 73.49 o -12 0 2 5305.97 5163.69 274.77 o -10 0 2 286.85 330.55 28.87 o -8 0 2 13.79 30.15 24.04 o -6 0 2 57.03 59.61 71.48 o -4 0 2 269.00 219.70 42.40 o -2 0 2 1747.75 1756.73 100.48 o 2 0 2 128.54 185.78 28.72 o 4 0 2 745.09 816.84 39.02 o 6 0 2 569.00 722.30 87.34 o 8 0 2 0.12 4.50 18.47 o 10 0 2 1.12 0.12 21.90 o 12 0 2 5.77 16.00 26.67 o 14 0 2 44.27 30.12 34.76 o -15 1 2 268.04 231.84 17.68 o -14 1 2 721.63 681.22 34.15 o -13 1 2 593.08 552.41 30.69 o -12 1 2 741.52 763.22 47.22 o -11 1 2 370.28 357.74 42.19 o -10 1 2 811.59 784.97 38.34 o -9 1 2 0.01 7.21 17.59 o -8 1 2 26.43 57.20 18.05 o -7 1 2 366.83 427.68 33.30 o -6 1 2 853.84 945.39 54.22 o -5 1 2 22.58 49.90 37.51 o -4 1 2 10.32 16.54 32.96 o -3 1 2 3905.23 3416.73 279.46 o -2 1 2 7405.82 6995.08 241.21 o -1 1 2 677.00 547.05 32.55 o 0 1 2 0.92 -4.99 33.68 o 1 1 2 459.20 427.13 28.77 o 2 1 2 0.36 6.74 36.61 o 3 1 2 606.50 771.09 31.13 o 4 1 2 2.09 5.69 13.03 o 5 1 2 52.06 100.47 16.14 o 6 1 2 4599.89 5370.76 141.58 o 7 1 2 1545.24 1706.47 50.87 o 8 1 2 654.67 738.67 26.38 o 9 1 2 96.21 102.96 9.79 o 10 1 2 59.43 68.94 11.42 o 11 1 2 0.04 8.24 17.84 o 12 1 2 253.11 256.23 17.37 o 13 1 2 68.57 56.81 18.47 o 14 1 2 131.06 137.16 20.32 o 15 1 2 0.01 12.89 33.62 o -15 2 2 68.91 50.46 19.17 o -14 2 2 114.61 89.98 15.14 o -13 2 2 58.28 64.20 14.59 o -12 2 2 3.74 26.94 21.77 o -11 2 2 1750.57 1662.15 73.82 o -10 2 2 308.91 296.78 19.85 o -9 2 2 99.82 115.73 12.65 o -8 2 2 11.61 14.65 16.40 o -7 2 2 441.12 516.26 29.07 o -6 2 2 441.65 390.74 36.89 o -5 2 2 1753.15 1869.60 80.38 o -4 2 2 1055.69 1010.83 128.88 o -3 2 2 10759.01 12553.28 428.53 o 1 2 2 1404.08 1444.94 55.23 o 2 2 2 583.31 482.70 18.15 o 3 2 2 74.53 72.30 10.48 o 4 2 2 700.73 590.87 32.82 o 5 2 2 157.44 185.11 20.04 o 6 2 2 855.00 970.53 32.93 o 7 2 2 827.93 978.97 32.03 o 8 2 2 158.53 177.90 10.92 o 9 2 2 1044.18 1041.99 34.59 o 10 2 2 105.34 133.13 11.77 o 11 2 2 43.29 64.81 12.29 o 12 2 2 41.61 64.47 19.13 o 13 2 2 5.30 -4.60 31.29 o 14 2 2 144.44 150.18 20.44 o -14 3 2 56.00 87.92 16.73 o -13 3 2 12.11 33.64 24.29 o -12 3 2 74.18 109.30 15.33 o -11 3 2 331.62 342.65 36.33 o -10 3 2 324.87 358.05 40.42 o -9 3 2 697.56 707.95 35.59 o -8 3 2 59.87 64.57 11.82 o -7 3 2 575.50 697.41 55.68 o -6 3 2 373.70 419.83 23.56 o -5 3 2 2514.19 2620.55 180.05 o -4 3 2 2980.63 3304.83 150.36 o -3 3 2 587.95 511.89 95.59 o -2 3 2 0.01 8.25 19.24 o -1 3 2 92.18 33.06 20.43 o 0 3 2 1621.23 1380.27 57.67 o 1 3 2 88.53 88.36 9.82 o 2 3 2 89.19 80.75 26.71 o 3 3 2 620.45 553.75 41.85 o 4 3 2 234.21 209.09 43.20 o 5 3 2 57.81 53.55 8.89 o 6 3 2 14.84 23.18 12.84 o 7 3 2 6.60 20.26 14.54 o 8 3 2 27.91 56.48 13.03 o 9 3 2 1687.06 1812.41 63.74 o 10 3 2 443.43 528.38 31.08 o 11 3 2 646.82 662.78 38.05 o 12 3 2 986.15 970.91 64.06 o 13 3 2 19.55 52.65 37.04 o 14 3 2 224.38 180.15 26.94 o -14 4 2 17.96 30.40 43.23 o -13 4 2 5.62 31.88 29.98 o -12 4 2 57.50 81.23 16.92 o -11 4 2 132.98 149.94 18.32 o -10 4 2 254.59 270.02 19.29 o -9 4 2 0.16 13.55 22.81 o -8 4 2 252.28 251.51 18.43 o -7 4 2 44.60 69.72 13.04 o -6 4 2 8.99 27.77 18.76 o -5 4 2 28.78 39.68 10.13 o -4 4 2 14.62 9.91 12.98 o -3 4 2 773.64 738.05 49.85 o -2 4 2 608.89 551.10 36.42 o -1 4 2 421.04 334.48 20.25 o 0 4 2 24.32 26.10 14.99 o 1 4 2 674.74 611.52 29.73 o 2 4 2 2.66 14.87 12.71 o 3 4 2 73.04 91.53 9.11 o 4 4 2 39.76 51.24 10.39 o 5 4 2 233.89 227.02 20.91 o 6 4 2 5.19 3.49 17.36 o 7 4 2 13.43 33.84 22.84 o 8 4 2 7.42 22.16 35.39 o 9 4 2 554.00 497.91 41.47 o 10 4 2 245.21 224.71 27.90 o 11 4 2 445.01 400.45 36.18 o 12 4 2 189.29 211.14 27.08 o 13 4 2 24.43 10.18 39.29 o -11 5 2 2.30 22.32 28.03 o -10 5 2 274.10 282.74 20.52 o -9 5 2 187.29 175.27 17.49 o -8 5 2 245.08 229.15 17.54 o -7 5 2 51.87 39.76 14.53 o -6 5 2 0.80 12.67 20.43 o -5 5 2 1.83 12.50 19.53 o -4 5 2 106.12 105.27 12.15 o -3 5 2 300.15 264.66 17.30 o -2 5 2 64.84 62.82 11.76 o -1 5 2 174.41 146.59 13.53 o 0 5 2 95.56 79.08 12.88 o 1 5 2 13.87 6.53 18.44 o 2 5 2 91.25 80.57 9.67 o 3 5 2 1.34 7.51 15.83 o 4 5 2 36.38 49.08 15.82 o 5 5 2 2.88 -3.20 23.54 o 6 5 2 23.88 6.46 31.32 o 7 5 2 12.40 12.52 33.98 o 8 5 2 336.65 347.40 32.78 o 9 5 2 41.41 78.43 26.26 o 10 5 2 50.46 44.54 39.61 o 11 5 2 78.61 26.61 25.94 o 12 5 2 210.45 190.13 27.54 o -11 6 2 2.98 -2.75 36.38 o -10 6 2 232.99 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