#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/23/2102303.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102303_Fobs loop_ _publ_author_name 'Parkin, Andrew' 'Oswald, Iain D. H.' 'Parsons, Simon' _publ_section_title ; Structures of piperazine, piperidine and morpholine ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 219 _journal_page_last 227 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90 _cell_angle_beta 108.254(4) _cell_angle_gamma 90 _cell_length_a 6.0079(15) _cell_length_b 5.1920(13) _cell_length_c 8.407(2) _[local]_cod_data_source_file av5005c4h10n2sup2.hkl _[local]_cod_data_source_block c4h10n2 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 481.32 430.58 4.63 o 4 0 0 536.40 497.75 6.56 o 6 0 0 28.45 26.19 2.68 o 1 1 0 1544.57 1493.65 8.71 o 2 1 0 405.20 412.34 4.32 o 3 1 0 539.33 521.98 5.57 o 4 1 0 105.95 115.49 3.50 o 5 1 0 8.28 8.85 1.53 o 6 1 0 1.44 1.32 1.19 o 7 1 0 6.14 4.15 1.62 o 0 2 0 47.72 55.02 1.84 o 1 2 0 464.65 470.02 4.99 o 2 2 0 62.13 62.36 2.32 o 3 2 0 15.73 18.40 1.60 o 4 2 0 5.92 5.69 1.26 o 5 2 0 54.62 56.51 3.01 o 6 2 0 8.45 7.97 1.69 o 1 3 0 98.07 104.91 2.94 o 2 3 0 1.83 1.48 0.85 o 3 3 0 180.00 186.01 4.84 o 4 3 0 25.31 22.96 2.24 o 5 3 0 14.51 12.97 1.88 o 6 3 0 1.65 0.71 1.24 o 0 4 0 374.75 392.93 6.20 o 1 4 0 121.66 130.72 3.67 o 2 4 0 11.54 13.51 1.58 o 3 4 0 13.95 13.80 1.78 o 4 4 0 64.10 62.78 3.52 o 5 4 0 12.70 11.75 1.86 o 1 5 0 43.73 46.28 2.61 o 2 5 0 159.65 159.40 5.14 o 3 5 0 13.47 15.19 1.93 o 4 5 0 22.58 20.81 2.43 o 0 6 0 0.70 0.30 1.43 o 1 6 0 33.92 35.11 2.74 o 2 6 0 15.12 11.75 2.06 o -7 0 1 7.39 4.47 1.66 o -5 0 1 11.32 9.48 1.67 o -3 0 1 1114.19 1082.72 7.98 o -1 0 1 2611.07 2620.88 13.55 o 1 0 1 1330.07 1423.68 7.50 o 3 0 1 640.87 593.56 6.49 o 5 0 1 20.97 20.72 2.21 o -7 1 1 3.95 4.86 1.48 o -6 1 1 4.01 3.25 1.29 o -5 1 1 9.47 7.59 1.45 o -4 1 1 192.78 175.80 4.52 o -3 1 1 134.15 124.34 3.13 o -2 1 1 81.58 80.55 2.25 o -1 1 1 62.39 65.20 1.72 o 0 1 1 2255.53 2383.89 10.08 o 1 1 1 1810.05 1828.08 9.45 o 2 1 1 51.67 47.44 2.00 o 3 1 1 106.76 120.50 2.98 o 4 1 1 40.62 41.70 2.39 o 5 1 1 65.50 67.88 3.35 o 6 1 1 9.64 7.67 1.80 o -6 2 1 5.81 6.06 1.45 o -5 2 1 10.61 11.89 1.54 o -4 2 1 0.39 0.38 0.98 o -3 2 1 1.37 0.07 0.90 o -2 2 1 91.67 87.68 2.67 o -1 2 1 24.56 34.46 1.47 o 0 2 1 1127.98 1046.61 7.67 o 1 2 1 36.03 39.62 1.64 o 2 2 1 83.07 81.43 2.76 o 3 2 1 35.63 36.24 2.05 o 4 2 1 422.64 418.73 7.25 o 5 2 1 20.34 20.53 2.11 o 6 2 1 6.12 5.02 1.58 o -6 3 1 4.86 5.18 1.30 o -5 3 1 14.30 12.78 1.86 o -4 3 1 17.15 18.54 1.88 o -3 3 1 5.03 7.66 1.17 o -2 3 1 1.28 1.31 0.83 o -1 3 1 139.19 142.74 3.45 o 0 3 1 438.04 420.36 5.76 o 1 3 1 165.89 151.37 3.77 o 2 3 1 264.01 251.56 4.95 o 3 3 1 104.45 112.36 3.80 o 4 3 1 10.97 11.54 1.67 o 5 3 1 22.98 23.84 2.31 o 6 3 1 46.55 43.32 3.47 o -5 4 1 5.75 5.87 1.41 o -4 4 1 32.60 36.87 2.58 o -3 4 1 48.47 50.73 2.85 o -2 4 1 80.15 81.26 3.39 o -1 4 1 160.73 162.23 4.21 o 0 4 1 31.59 34.93 2.12 o 1 4 1 15.69 15.09 1.63 o 2 4 1 60.56 67.80 3.14 o 3 4 1 103.84 107.35 4.12 o 4 4 1 0.71 0.43 1.53 o 5 4 1 12.35 10.49 1.88 o -4 5 1 27.90 30.46 2.58 o -3 5 1 8.27 7.97 1.54 o -2 5 1 4.41 5.29 1.33 o -1 5 1 94.03 90.29 3.72 o 0 5 1 20.65 22.58 1.96 o 1 5 1 124.22 115.00 4.43 o 2 5 1 1.09 0.23 0.99 o 3 5 1 0.50 0.01 1.30 o 4 5 1 2.75 2.10 1.35 o -2 6 1 22.46 24.22 2.33 o -1 6 1 4.03 1.65 1.33 o 0 6 1 18.13 17.76 2.00 o 1 6 1 5.11 3.75 1.39 o 2 6 1 11.72 12.62 1.91 o -6 0 2 11.09 8.82 1.76 o -4 0 2 24.45 22.91 1.70 o -2 0 2 233.63 225.49 3.35 o 0 0 2 506.89 528.34 4.78 o 2 0 2 109.27 106.81 2.89 o 4 0 2 24.31 25.42 2.02 o 6 0 2 21.08 22.57 2.42 o -7 1 2 1.29 0.19 1.10 o -6 1 2 9.23 12.09 1.66 o -5 1 2 3.46 2.85 1.06 o -4 1 2 25.14 26.74 1.83 o -3 1 2 51.78 46.12 2.19 o -2 1 2 38.51 38.02 1.76 o -1 1 2 0.89 1.17 1.06 o 0 1 2 950.11 994.71 6.27 o 1 1 2 2.21 1.13 0.77 o 2 1 2 0.76 0.49 1.30 o 3 1 2 1.01 0.50 1.12 o 4 1 2 163.52 171.95 4.44 o 5 1 2 28.56 30.67 2.42 o 6 1 2 10.94 10.32 1.94 o -7 2 2 0.25 0.80 0.85 o -6 2 2 0.71 0.00 1.48 o -5 2 2 34.34 38.86 2.41 o -4 2 2 1.32 0.34 1.15 o -3 2 2 82.86 74.97 3.08 o -2 2 2 2.35 3.22 0.83 o -1 2 2 216.34 217.03 3.66 o 0 2 2 141.62 121.92 3.06 o 1 2 2 1036.84 950.17 7.79 o 2 2 2 81.12 71.96 2.89 o 3 2 2 264.49 263.39 5.49 o 4 2 2 4.40 4.92 1.20 o 5 2 2 45.28 51.26 3.07 o 6 2 2 11.44 9.50 2.04 o -6 3 2 5.84 5.31 1.38 o -5 3 2 4.93 6.97 1.29 o -4 3 2 88.03 89.42 3.80 o -3 3 2 0.65 1.70 1.34 o -2 3 2 4.24 4.62 1.00 o -1 3 2 85.72 84.28 2.82 o 0 3 2 430.62 431.05 5.74 o 1 3 2 21.10 20.87 1.62 o 2 3 2 0.58 0.04 1.23 o 3 3 2 101.42 102.66 3.89 o 4 3 2 94.55 97.68 4.01 o 5 3 2 59.88 56.60 3.52 o -5 4 2 23.63 23.77 2.38 o -4 4 2 0.95 0.87 1.30 o -3 4 2 19.06 22.61 1.95 o -2 4 2 4.03 4.38 1.16 o -1 4 2 131.59 132.80 3.96 o 0 4 2 9.74 7.86 1.41 o 1 4 2 1.12 1.12 0.92 o 2 4 2 62.12 60.15 3.29 o 3 4 2 1.68 2.86 1.17 o 4 4 2 9.47 8.38 1.75 o 5 4 2 -0.06 0.14 0.51 o -4 5 2 9.26 10.17 1.70 o -3 5 2 0.60 0.26 1.33 o -2 5 2 12.95 12.55 1.78 o -1 5 2 0.71 0.21 1.56 o 0 5 2 2.10 0.90 1.07 o 1 5 2 4.39 5.16 1.27 o 2 5 2 4.81 5.47 1.37 o 3 5 2 16.14 12.82 2.16 o -2 6 2 1.71 0.72 1.09 o -1 6 2 11.82 10.98 1.75 o 0 6 2 21.28 19.45 2.17 o 1 6 2 8.32 7.79 1.65 o -7 0 3 9.76 9.19 1.77 o -5 0 3 155.56 155.52 4.42 o -3 0 3 5.91 4.08 1.03 o -1 0 3 1114.99 1055.92 7.47 o 1 0 3 64.59 71.04 2.16 o 3 0 3 50.20 52.08 2.50 o 5 0 3 79.69 85.37 4.01 o -7 1 3 3.39 3.93 1.31 o -6 1 3 12.79 11.34 1.79 o -5 1 3 12.74 15.07 1.59 o -4 1 3 76.70 75.20 2.93 o -3 1 3 1.51 0.72 0.81 o -2 1 3 114.66 118.54 2.78 o -1 1 3 0.27 0.30 0.69 o 0 1 3 264.87 255.65 3.92 o 1 1 3 59.41 61.34 2.13 o 2 1 3 0.29 0.53 0.76 o 3 1 3 30.64 30.79 2.04 o 4 1 3 67.01 71.77 3.21 o 5 1 3 2.41 2.50 1.27 o 6 1 3 0.91 0.82 1.15 o -7 2 3 4.74 3.51 1.38 o -6 2 3 37.72 40.59 2.87 o -5 2 3 0.18 0.09 0.64 o -4 2 3 21.85 22.52 1.84 o -3 2 3 0.69 1.10 1.31 o -2 2 3 8.96 10.59 1.16 o -1 2 3 14.80 14.89 1.35 o 0 2 3 255.25 219.89 4.34 o 1 2 3 25.11 28.11 1.63 o 2 2 3 0.16 0.06 0.75 o 3 2 3 38.93 38.09 2.38 o 4 2 3 58.49 60.29 3.03 o 5 2 3 1.32 0.86 1.42 o -6 3 3 0.61 1.17 1.49 o -5 3 3 39.66 43.40 2.79 o -4 3 3 22.84 23.60 2.10 o -3 3 3 24.61 24.18 2.02 o -2 3 3 9.94 11.37 1.30 o -1 3 3 72.82 79.01 2.76 o 0 3 3 7.28 5.49 1.20 o 1 3 3 44.25 38.66 2.24 o 2 3 3 49.21 41.89 2.61 o 3 3 3 16.43 16.10 1.92 o 4 3 3 7.35 5.51 1.50 o 5 3 3 0.30 0.18 1.06 o -5 4 3 19.75 20.72 2.19 o -4 4 3 64.01 70.02 3.40 o -3 4 3 4.32 4.34 1.23 o -2 4 3 0.29 0.12 0.81 o -1 4 3 20.18 22.95 1.86 o 0 4 3 16.33 21.69 1.70 o 1 4 3 35.43 33.28 2.38 o 2 4 3 0.20 0.04 0.73 o 3 4 3 7.93 7.13 1.57 o 4 4 3 4.63 4.78 1.63 o -4 5 3 9.05 10.44 1.69 o -3 5 3 34.90 33.42 2.76 o -2 5 3 0.87 0.23 1.11 o -1 5 3 1.21 1.26 0.98 o 0 5 3 94.07 89.01 3.90 o 1 5 3 0.15 0.38 0.64 o 2 5 3 7.87 7.32 1.70 o 3 5 3 23.74 17.54 2.51 o -2 6 3 17.28 16.13 2.18 o -1 6 3 28.62 24.90 2.58 o 0 6 3 3.46 1.98 1.37 o 1 6 3 4.11 2.90 1.47 o -6 0 4 44.62 48.53 2.83 o -4 0 4 376.40 354.52 5.70 o -2 0 4 945.98 897.40 7.39 o 0 0 4 213.38 198.02 3.49 o 2 0 4 32.92 35.17 1.98 o 4 0 4 40.42 38.86 2.65 o -7 1 4 8.14 6.59 1.62 o -6 1 4 27.14 27.87 2.41 o -5 1 4 156.94 152.46 4.61 o -4 1 4 53.73 51.42 2.59 o -3 1 4 9.61 10.18 1.24 o -2 1 4 0.47 0.17 0.96 o -1 1 4 480.46 458.21 5.81 o 0 1 4 113.00 109.61 3.03 o 1 1 4 17.56 19.34 1.45 o 2 1 4 5.79 4.34 1.13 o 3 1 4 34.80 36.47 2.28 o 4 1 4 0.24 0.08 0.80 o 5 1 4 9.33 9.90 1.65 o -7 2 4 5.17 5.68 1.34 o -6 2 4 0.21 0.00 0.75 o -5 2 4 2.93 3.09 1.09 o -4 2 4 3.29 3.24 1.04 o -3 2 4 42.77 43.01 2.31 o -2 2 4 30.74 32.15 1.93 o -1 2 4 92.29 91.29 2.97 o 0 2 4 105.87 108.30 3.12 o 1 2 4 0.04 0.18 0.30 o 2 2 4 0.16 0.03 0.55 o 3 2 4 10.16 10.84 1.51 o 4 2 4 9.55 8.85 1.63 o 5 2 4 2.53 1.29 1.26 o -6 3 4 0.25 0.03 0.80 o -5 3 4 62.81 62.91 3.38 o -4 3 4 4.34 4.03 1.21 o -3 3 4 4.00 4.07 1.11 o -2 3 4 1.58 1.47 0.91 o -1 3 4 44.67 49.22 2.38 o 0 3 4 9.06 9.38 1.32 o 1 3 4 8.34 9.25 1.42 o 2 3 4 4.17 4.10 1.18 o 3 3 4 0.18 0.00 0.67 o 4 3 4 11.34 10.38 1.75 o -5 4 4 0.03 0.23 0.63 o -4 4 4 59.91 59.56 3.42 o -3 4 4 55.16 52.73 3.14 o -2 4 4 48.87 50.44 2.87 o -1 4 4 2.97 2.97 1.13 o 0 4 4 47.75 46.44 2.67 o 1 4 4 0.54 0.01 1.32 o 2 4 4 9.19 9.81 1.57 o 3 4 4 11.65 8.93 1.93 o 4 4 4 16.09 14.89 2.12 o -4 5 4 30.60 31.15 2.76 o -3 5 4 12.85 13.64 1.87 o -2 5 4 21.03 20.29 2.20 o -1 5 4 68.64 68.23 3.50 o 0 5 4 14.07 16.86 1.89 o 1 5 4 18.05 12.60 2.09 o 2 5 4 5.13 3.97 1.59 o -1 6 4 1.57 0.79 1.23 o -7 0 5 21.30 18.26 2.30 o -5 0 5 274.88 279.41 5.95 o -3 0 5 16.29 13.35 1.49 o -1 0 5 434.33 395.08 6.02 o 1 0 5 55.66 61.68 2.66 o 3 0 5 0.50 0.19 1.15 o -7 1 5 14.52 13.24 1.99 o -6 1 5 12.93 13.26 1.78 o -5 1 5 25.35 27.32 2.13 o -4 1 5 108.01 104.71 3.60 o -3 1 5 99.10 92.50 3.09 o -2 1 5 133.85 124.42 3.54 o -1 1 5 481.15 478.81 6.43 o 0 1 5 8.72 7.64 1.24 o 1 1 5 0.39 0.10 0.86 o 2 1 5 5.88 7.08 1.16 o 3 1 5 42.30 45.60 2.63 o 4 1 5 0.01 0.29 0.15 o 5 1 5 0.41 0.10 1.04 o -7 2 5 0.47 0.05 1.26 o -6 2 5 4.81 4.59 1.27 o -5 2 5 1.13 0.73 1.05 o -4 2 5 151.09 148.32 4.43 o -3 2 5 33.38 37.00 2.24 o -2 2 5 53.54 50.87 2.59 o -1 2 5 0.10 0.00 0.53 o 0 2 5 335.97 315.07 5.67 o 1 2 5 34.88 34.13 2.34 o 2 2 5 77.33 80.57 3.28 o 3 2 5 3.36 2.73 1.19 o 4 2 5 24.01 21.39 2.45 o -6 3 5 17.50 15.75 2.06 o -5 3 5 13.84 13.12 1.82 o -4 3 5 11.92 11.36 1.69 o -3 3 5 2.19 2.76 1.08 o -2 3 5 153.28 153.44 4.21 o -1 3 5 103.55 114.56 3.57 o 0 3 5 31.08 32.05 2.16 o 1 3 5 14.82 11.57 1.77 o 2 3 5 16.52 17.69 1.88 o 3 3 5 57.50 56.11 3.45 o 4 3 5 7.96 5.89 1.73 o -5 4 5 56.96 53.45 3.51 o -4 4 5 9.11 7.86 1.60 o -3 4 5 6.12 6.45 1.40 o -2 4 5 8.78 11.73 1.52 o -1 4 5 52.51 52.31 2.86 o 0 4 5 1.62 0.86 1.05 o 1 4 5 19.48 22.65 2.08 o 2 4 5 0.09 0.00 0.51 o 3 4 5 2.77 1.44 1.34 o -4 5 5 18.92 16.66 2.33 o -3 5 5 52.14 50.83 3.42 o -2 5 5 0.52 1.10 1.36 o -1 5 5 16.01 15.78 2.03 o 0 5 5 28.09 22.77 2.49 o 1 5 5 0.62 1.41 1.48 o -6 0 6 5.54 7.08 1.31 o -4 0 6 19.04 16.27 1.76 o -2 0 6 90.83 86.96 3.24 o 0 0 6 131.20 139.50 3.86 o 2 0 6 2.08 1.23 1.10 o 4 0 6 53.82 52.42 3.29 o -7 1 6 10.83 8.91 1.73 o -6 1 6 1.65 0.95 1.02 o -5 1 6 15.77 17.02 1.85 o -4 1 6 152.06 153.09 4.54 o -3 1 6 1.27 0.75 1.15 o -2 1 6 84.68 83.31 3.19 o -1 1 6 1.80 2.19 0.96 o 0 1 6 123.78 117.62 3.79 o 1 1 6 25.12 25.53 2.09 o 2 1 6 75.97 75.19 3.49 o 3 1 6 34.16 33.18 2.62 o 4 1 6 0.57 0.38 1.25 o -6 2 6 7.80 7.37 1.56 o -5 2 6 75.55 76.10 3.56 o -4 2 6 2.69 2.77 1.17 o -3 2 6 38.78 44.81 2.52 o -2 2 6 42.51 45.91 2.49 o -1 2 6 519.53 519.10 7.45 o 0 2 6 10.53 11.72 1.44 o 1 2 6 3.02 3.90 1.29 o 2 2 6 4.51 4.88 1.25 o 3 2 6 89.61 84.51 4.14 o 4 2 6 1.05 0.50 1.01 o -6 3 6 9.47 8.21 1.79 o -5 3 6 29.09 29.31 2.54 o -4 3 6 51.55 55.97 3.17 o -3 3 6 69.12 64.26 3.44 o -2 3 6 38.58 38.37 2.64 o -1 3 6 1.02 1.56 1.51 o 0 3 6 99.67 100.37 3.86 o 1 3 6 96.95 93.23 4.01 o 2 3 6 24.06 28.27 2.32 o 3 3 6 18.72 16.96 2.29 o -5 4 6 7.93 9.02 1.60 o -4 4 6 0.69 0.62 1.53 o -3 4 6 3.09 3.12 1.29 o -2 4 6 31.54 32.19 2.55 o -1 4 6 0.53 0.00 1.18 o 0 4 6 39.08 41.65 2.78 o 1 4 6 19.29 13.35 2.17 o 2 4 6 1.59 1.39 1.14 o -3 5 6 3.68 2.05 1.39 o -2 5 6 6.37 3.32 1.47 o -1 5 6 1.40 1.66 1.14 o 0 5 6 7.72 7.94 1.58 o -5 0 7 2.19 1.91 1.16 o -3 0 7 7.03 9.46 1.34 o -1 0 7 119.85 126.59 3.92 o 1 0 7 43.33 39.49 2.71 o 3 0 7 142.81 136.49 5.20 o -6 1 7 8.20 6.03 1.57 o -5 1 7 20.28 21.89 2.17 o -4 1 7 6.62 7.50 1.38 o -3 1 7 12.47 13.57 1.58 o -2 1 7 11.42 10.36 1.56 o -1 1 7 110.32 119.82 3.80 o 0 1 7 110.45 116.74 3.87 o 1 1 7 21.53 22.38 2.16 o 2 1 7 19.93 23.07 2.13 o 3 1 7 7.38 6.70 1.53 o -6 2 7 0.26 0.04 0.80 o -5 2 7 13.72 12.50 1.83 o -4 2 7 89.39 93.46 3.94 o -3 2 7 9.72 8.83 1.57 o -2 2 7 58.48 56.23 3.04 o -1 2 7 14.92 16.10 1.72 o 0 2 7 34.11 34.65 2.50 o 1 2 7 5.12 5.42 1.40 o 2 2 7 59.55 64.05 3.45 o 3 2 7 0.16 0.10 0.67 o -5 3 7 23.05 21.87 2.41 o -4 3 7 2.07 1.47 1.15 o -3 3 7 5.50 6.82 1.35 o -2 3 7 23.35 28.10 2.21 o -1 3 7 33.25 35.13 2.44 o 0 3 7 83.25 79.15 3.92 o 1 3 7 -0.03 0.02 0.49 o 2 3 7 2.70 1.60 1.34 o -4 4 7 0.92 1.01 1.31 o -3 4 7 13.67 13.63 2.00 o -2 4 7 7.78 5.24 1.58 o -1 4 7 34.71 30.23 2.75 o 0 4 7 1.80 1.73 1.23 o 1 4 7 19.94 17.80 2.46 o -6 0 8 17.27 13.49 2.17 o -4 0 8 18.87 24.36 2.08 o -2 0 8 19.14 15.76 1.99 o 0 0 8 124.05 129.63 4.34 o 2 0 8 41.37 42.25 3.02 o -6 1 8 8.16 6.68 1.65 o -5 1 8 22.29 21.78 2.34 o -4 1 8 7.75 8.83 1.47 o -3 1 8 2.09 2.82 1.11 o -2 1 8 0.42 0.33 1.01 o -1 1 8 80.56 82.40 3.58 o 0 1 8 0.85 1.04 1.24 o 1 1 8 3.28 2.84 1.34 o 2 1 8 9.40 7.13 1.74 o -5 2 8 0.06 0.13 0.54 o -4 2 8 9.43 8.36 1.64 o -3 2 8 9.59 8.01 1.65 o -2 2 8 12.16 12.52 1.68 o -1 2 8 2.87 3.15 1.21 o 0 2 8 1.13 0.68 1.59 o 1 2 8 20.71 18.87 2.36 o 2 2 8 0.03 0.17 0.26 o -5 3 8 1.43 1.51 1.09 o -4 3 8 2.20 2.61 1.16 o -3 3 8 2.96 3.95 1.16 o -2 3 8 3.91 3.68 1.28 o -1 3 8 10.48 8.82 1.76 o 0 3 8 4.09 2.34 1.49 o 1 3 8 2.12 2.50 1.26 o -3 4 8 3.07 3.37 1.37 o -2 4 8 7.20 5.68 1.54 o -1 4 8 18.20 16.57 2.30 o -5 0 9 4.19 4.70 1.61 o -3 0 9 1.75 2.85 1.10 o -1 0 9 10.02 13.67 1.61 o 1 0 9 0.58 0.28 1.42 o -5 1 9 13.30 10.22 1.93 o -4 1 9 6.96 8.40 1.50 o -3 1 9 9.54 7.74 1.62 o -2 1 9 0.83 0.48 1.36 o -1 1 9 5.40 4.76 1.41 o 0 1 9 8.49 9.36 1.64 o 1 1 9 4.09 3.51 1.40 o -4 2 9 0.78 0.90 1.31 o -3 2 9 1.95 1.86 1.13 o -2 2 9 24.78 21.83 2.32 o -1 2 9 2.03 1.69 1.18 o 0 2 9 13.10 14.97 1.96 o -3 3 9 2.74 2.39 1.18 o -2 3 9 0.05 0.03 0.67 o -1 3 9 37.17 35.09 2.95 o -4 0 10 4.58 1.43 1.61 o -2 0 10 19.66 18.41 2.19 o -4 1 10 0.35 0.43 0.94 o -3 1 10 2.51 3.22 1.24 o -2 1 10 16.57 14.19 2.06 o -1 1 10 8.51 7.24 1.77 o