#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2102484.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102484_Fobs loop_ _publ_author_name 'Palatinus, Luk\'as' 'Amami, Mongi' 'van Smaalen, Sander' _publ_section_title ; Structure of incommensurate ammonium tetrafluoroberyllate studied by structure refinements and the maximum entropy method ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 127 _journal_page_last 137 _journal_volume 60 _journal_year 2004 _[local]_cod_data_source_file ck5001sup2.hkl _[local]_cod_data_source_block (I) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_intensity_meas _refln_intensity_calc _refln_intensity_sigma _refln_observed_status 4 0 0 0 4847.2 4376.3 32.8 o 6 0 0 0 5205.2 5415.7 40.2 o 8 0 0 0 9192.3 9204.2 84.2 o 10 0 0 0 14242.6 14012.7 113.1 o 12 0 0 0 148.8 121.1 16.5 o 1 1 0 -1 -3.4 0.2 5.0 < 1 1 0 1 223.0 271.3 14.3 o 2 1 0 0 2224.9 2297.0 19.0 o 3 1 0 -1 511.5 516.0 14.5 o 3 1 0 1 345.1 331.2 16.8 o 4 1 0 0 8115.1 8255.8 51.4 o 5 1 0 -1 10.2 19.1 6.3 < 5 1 0 1 406.9 351.5 18.0 o 6 1 0 0 267.2 405.1 15.6 o 7 1 0 -1 485.8 480.2 18.4 o 7 1 0 1 36.6 35.6 8.8 o 8 1 0 0 119.4 70.2 12.4 o 9 1 0 -1 13.0 12.4 14.6 < 9 1 0 1 43.0 39.3 7.8 o 10 1 0 0 4111.2 3953.2 57.5 o 11 1 0 -1 19.8 12.8 9.9 < 11 1 0 1 7.8 7.6 6.5 < 12 1 0 0 281.8 254.0 17.1 o 13 1 0 -1 30.1 37.8 8.6 o 13 1 0 1 3.3 2.9 7.7 < 0 2 0 0 206907.0 233888.1 525.9 o 1 2 0 -1 2683.1 2609.2 22.2 o 1 2 0 1 57.3 49.5 7.5 o 2 2 0 0 10617.2 11014.9 41.1 o 3 2 0 -1 2956.2 2743.1 46.1 o 3 2 0 1 450.3 408.8 15.3 o 4 2 0 0 141785.0 139752.0 274.7 o 5 2 0 -1 222.6 182.4 13.6 o 5 2 0 1 83.0 72.0 9.9 o 6 2 0 0 52513.4 52348.3 161.3 o 7 2 0 -1 88.4 87.4 10.9 o 7 2 0 1 -3.4 0.6 5.9 < 8 2 0 0 1492.3 1562.6 31.9 o 9 2 0 -1 30.7 38.5 9.6 o 9 2 0 1 -1.9 2.7 7.2 < 10 2 0 0 1092.6 1142.0 29.8 o 11 2 0 -1 6.7 7.6 11.4 < 11 2 0 1 11.2 0.5 4.6 < 12 2 0 0 1723.9 1653.0 42.7 o 13 2 0 -1 41.0 22.4 12.4 o 13 2 0 1 12.6 10.0 9.5 < 1 3 0 -1 7.4 1.7 6.9 < 1 3 0 1 1700.3 1671.9 26.9 o 2 3 0 0 63988.3 62071.8 160.9 o 3 3 0 -1 99.6 103.2 10.3 o 3 3 0 1 2.7 6.1 8.2 < 4 3 0 0 7821.0 7302.0 51.9 o 5 3 0 -1 33.4 15.4 13.8 < 5 3 0 1 3.5 4.4 7.2 < 6 3 0 0 103.4 117.1 11.4 o 7 3 0 -1 5.7 4.1 6.8 < 7 3 0 1 111.4 102.3 12.8 o 8 3 0 0 3862.5 3701.8 53.4 o 9 3 0 -1 93.7 115.0 16.0 o 9 3 0 1 72.2 66.8 16.7 o 10 3 0 0 5696.5 5903.4 56.9 o 11 3 0 -1 113.8 80.1 12.5 o 11 3 0 1 100.1 72.0 17.0 o 12 3 0 0 50.6 55.2 11.5 o 0 4 0 0 303458.0 308553.2 662.1 o 1 4 0 -1 1046.1 1062.9 25.9 o 1 4 0 1 88.2 101.8 11.9 o 2 4 0 0 10351.0 10048.6 61.5 o 3 4 0 -1 683.6 692.9 24.4 o 3 4 0 1 1303.1 1218.1 33.7 o 4 4 0 0 5463.7 5012.4 53.7 o 5 4 0 -1 20.5 43.3 9.1 < 5 4 0 1 13.7 1.7 7.0 < 6 4 0 0 406.8 390.1 18.6 o 7 4 0 -1 393.8 449.9 23.6 o 7 4 0 1 59.4 47.2 10.3 o 8 4 0 0 3206.6 3154.9 50.3 o 9 4 0 -1 163.1 139.9 16.7 o 9 4 0 1 -0.9 2.1 7.3 < 10 4 0 0 4964.9 4743.4 68.1 o 11 4 0 -1 35.2 35.2 11.8 < 11 4 0 1 39.4 53.5 12.2 o 12 4 0 0 4.5 1.7 10.4 < 1 5 0 -1 314.3 260.2 27.6 o 1 5 0 1 100.9 75.4 16.7 o 2 5 0 0 9007.2 9565.6 64.3 o 3 5 0 -1 351.8 347.9 16.5 o 3 5 0 1 47.5 44.9 8.8 o 4 5 0 0 4805.0 4766.7 46.3 o 5 5 0 -1 254.5 250.4 16.4 o 5 5 0 1 432.1 382.7 22.8 o 6 5 0 0 280.1 229.0 18.4 o 7 5 0 -1 85.2 92.5 10.9 o 7 5 0 1 269.9 260.5 15.5 o 8 5 0 0 2324.5 2350.3 47.8 o 9 5 0 -1 -5.6 3.2 6.8 < 9 5 0 1 -1.8 0.0 6.9 < 10 5 0 0 396.0 353.7 21.9 o 11 5 0 -1 66.1 79.8 16.3 o 11 5 0 1 3.8 2.9 7.3 < 0 6 0 0 22945.4 22434.1 124.5 o 1 6 0 -1 648.4 622.4 28.8 o 1 6 0 1 46.5 41.3 11.1 o 2 6 0 0 68.3 93.7 11.9 o 3 6 0 -1 1078.7 1069.0 34.9 o 3 6 0 1 501.4 555.6 27.2 o 4 6 0 0 7332.0 7061.5 64.3 o 5 6 0 -1 90.1 106.7 19.4 o 5 6 0 1 105.0 131.4 18.0 o 6 6 0 0 1436.8 1393.1 34.7 o 7 6 0 -1 211.6 195.4 20.5 o 7 6 0 1 6.5 18.9 6.6 < 8 6 0 0 790.4 798.6 25.2 o 9 6 0 -1 57.8 57.5 11.4 o 9 6 0 1 3.5 0.3 6.2 < 10 6 0 0 476.4 459.8 22.6 o 1 7 0 -1 45.3 39.3 10.0 o 1 7 0 1 528.5 593.9 19.6 o 2 7 0 0 8607.6 8544.2 78.1 o 3 7 0 -1 -0.9 12.4 9.0 < 3 7 0 1 -1.7 0.4 8.8 < 4 7 0 0 8650.3 8639.4 71.5 o 5 7 0 -1 2.9 12.9 8.9 < 5 7 0 1 -1.1 1.2 9.8 < 6 7 0 0 142.8 154.4 12.4 o 7 7 0 -1 176.8 148.2 16.4 o 7 7 0 1 10.2 7.3 12.6 < 8 7 0 0 918.7 906.1 26.8 o 9 7 0 -1 63.0 44.0 17.8 o 9 7 0 1 15.6 8.6 10.2 < 0 8 0 0 6026.8 6404.5 68.1 o 1 8 0 -1 271.4 284.3 25.9 o 1 8 0 1 0.7 0.6 8.6 < 2 8 0 0 65.5 69.4 13.8 o 3 8 0 -1 186.8 194.6 24.6 o 3 8 0 1 58.2 69.8 11.5 o 4 8 0 0 1471.3 1431.0 36.5 o 5 8 0 -1 -8.1 14.2 8.4 < 5 8 0 1 46.9 31.3 13.9 o 6 8 0 0 65.6 100.9 13.8 o 7 8 0 -1 30.2 42.8 14.3 < 7 8 0 1 20.9 24.4 9.2 < 8 8 0 0 261.8 297.7 19.9 o 1 9 0 -1 31.6 73.0 16.0 < 1 9 0 1 6.6 2.1 9.0 < 2 9 0 0 1204.2 1190.1 31.9 o 3 9 0 -1 -2.9 8.4 9.2 < 3 9 0 1 -3.7 13.3 7.8 < 4 9 0 0 19.5 0.1 11.2 < 5 9 0 -1 170.8 135.5 18.7 o 5 9 0 1 31.3 38.8 11.1 < 6 9 0 0 9.9 24.3 10.9 < 0 10 0 0 3979.9 4406.7 49.5 o 1 10 0 -1 23.5 18.6 11.2 < 1 10 0 1 13.4 4.8 8.7 < 2 10 0 0 218.7 242.8 16.2 o 3 10 0 -1 -7.3 8.1 8.3 < 3 10 0 1 181.0 136.5 17.7 o 1 0 1 0 1505.5 1530.6 16.8 o 2 0 1 0 54.3 256.5 7.0 o 3 0 1 0 333286.0 329866.2 2472.3 o 4 0 1 0 100023.0 97721.5 203.5 o 5 0 1 0 34497.7 35901.1 100.0 o 6 0 1 0 29634.0 34424.9 97.6 o 7 0 1 0 2941.2 2785.4 39.6 o 8 0 1 0 1022.3 1117.1 28.3 o 9 0 1 0 184.7 239.6 12.4 o 10 0 1 0 745.0 755.7 28.0 o 11 0 1 0 1217.6 1245.5 36.0 o 12 0 1 0 3.0 1.6 8.9 < 13 0 1 0 424.5 364.2 24.0 o 0 1 1 0 14351.8 13828.7 34.9 o 0 1 1 1 2.7 3.5 4.1 < 1 1 1 -1 -3.8 0.5 5.4 < 1 1 1 0 49588.5 48407.2 167.9 o 1 1 1 1 14.3 20.4 6.2 < 2 1 1 -1 78.0 91.0 11.4 o 2 1 1 0 10127.0 13620.1 35.1 o 2 1 1 1 841.5 867.1 14.2 o 3 1 1 -1 338.5 318.7 17.7 o 3 1 1 0 5521.1 5694.1 31.0 o 3 1 1 1 15.2 37.4 7.8 < 4 1 1 -1 372.7 378.3 14.8 o 4 1 1 0 8481.3 7716.2 53.4 o 4 1 1 1 151.6 137.9 10.2 o 5 1 1 -1 9.3 0.0 8.0 < 5 1 1 0 39853.5 37980.8 127.0 o 5 1 1 1 132.7 152.0 15.3 o 6 1 1 -1 189.2 234.0 16.7 o 6 1 1 0 792.6 812.9 24.8 o 6 1 1 1 37.3 37.7 11.4 o 7 1 1 -1 -5.7 8.2 6.7 < 7 1 1 0 5106.4 5126.1 55.2 o 7 1 1 1 28.4 64.8 10.4 < 8 1 1 -1 14.4 15.1 8.9 < 8 1 1 0 2031.6 2109.0 41.4 o 8 1 1 1 11.8 18.8 8.1 < 9 1 1 -1 75.6 99.0 13.2 o 9 1 1 0 3991.9 4136.2 54.4 o 9 1 1 1 1.3 2.0 6.1 < 10 1 1 -1 51.2 47.9 10.4 o 10 1 1 0 10.2 9.7 7.2 < 10 1 1 1 -2.7 0.8 8.7 < 11 1 1 -1 47.1 49.0 10.6 o 11 1 1 0 2535.4 2468.1 41.9 o 11 1 1 1 -0.2 7.8 8.0 < 12 1 1 -1 5.2 1.1 8.2 < 12 1 1 0 402.8 386.1 20.4 o 12 1 1 1 12.6 7.3 7.7 < 13 1 1 -1 7.1 6.8 7.9 < 13 1 1 0 60.8 58.3 17.1 o 13 1 1 1 7.2 9.4 7.7 < 0 2 1 1 385.9 368.8 9.1 o 1 2 1 -1 194.6 200.2 10.5 o 1 2 1 0 70307.0 67546.7 142.8 o 1 2 1 1 192.6 199.0 10.7 o 2 2 1 -1 74.3 73.9 15.1 o 2 2 1 0 206641.0 201545.8 413.8 o 2 2 1 1 990.8 974.1 21.1 o 3 2 1 -1 59.7 38.9 11.3 o 3 2 1 0 514.6 468.4 15.6 o 3 2 1 1 -4.5 1.2 7.2 < 4 2 1 -1 53.7 36.9 9.5 o 4 2 1 0 2677.3 2714.9 27.1 o 4 2 1 1 17.5 60.7 8.2 < 5 2 1 -1 166.6 183.6 13.8 o 5 2 1 0 4061.8 4055.9 42.6 o 5 2 1 1 112.0 103.4 15.0 o 6 2 1 -1 212.4 221.4 22.1 o 6 2 1 0 15454.9 16137.4 90.1 o 6 2 1 1 126.2 122.3 15.2 o 7 2 1 -1 67.4 70.4 11.0 o 7 2 1 0 3573.9 3754.1 45.3 o 7 2 1 1 17.1 2.7 13.6 < 8 2 1 -1 15.9 14.2 9.6 < 8 2 1 0 8596.4 8393.1 72.4 o 8 2 1 1 11.6 5.1 10.7 < 9 2 1 -1 17.4 8.3 12.4 < 9 2 1 0 8091.3 8242.5 81.3 o 9 2 1 1 27.6 41.5 9.0 o 10 2 1 -1 14.2 0.1 9.4 < 10 2 1 0 629.3 662.3 23.1 o 10 2 1 1 5.1 1.1 5.8 < 11 2 1 -1 8.5 2.7 9.0 < 11 2 1 0 835.7 836.7 27.1 o 11 2 1 1 1.2 0.0 5.0 < 12 2 1 -1 -7.7 0.7 5.5 < 12 2 1 0 221.1 161.7 17.6 o 12 2 1 1 -6.6 4.3 6.9 < 13 2 1 -1 -1.2 9.0 11.5 < 13 2 1 0 11.8 44.1 9.7 < 13 2 1 1 -1.1 0.6 5.6 < 0 3 1 0 16552.8 14913.0 59.0 o 0 3 1 1 124.1 115.3 7.8 o 1 3 1 -1 96.2 98.7 8.6 o 1 3 1 0 114.0 124.1 9.5 o 1 3 1 1 260.1 254.9 13.6 o 2 3 1 -1 2083.4 1925.8 27.5 o 2 3 1 0 658.8 582.1 15.6 o 2 3 1 1 156.3 190.9 12.1 o 3 3 1 -1 19.3 28.2 10.0 < 3 3 1 0 3588.1 3761.4 31.2 o 3 3 1 1 19.9 28.5 10.8 < 4 3 1 -1 187.6 194.5 11.7 o 4 3 1 0 415.8 396.5 14.7 o 4 3 1 1 18.6 6.2 11.4 < 5 3 1 -1 604.7 596.0 21.6 o 5 3 1 0 45552.8 43160.4 144.2 o 5 3 1 1 34.1 33.1 16.3 < 6 3 1 -1 0.8 4.1 9.3 < 6 3 1 0 4677.1 4411.8 48.8 o 6 3 1 1 61.9 31.6 15.0 o 7 3 1 -1 -10.6 2.2 6.5 < 7 3 1 0 9318.3 9503.9 74.0 o 7 3 1 1 56.4 48.5 14.2 o 8 3 1 -1 190.8 196.7 14.7 o 8 3 1 0 220.6 212.7 17.2 o 8 3 1 1 117.1 117.2 15.8 o 9 3 1 -1 19.5 8.0 8.2 < 9 3 1 0 1780.8 1764.4 39.7 o 9 3 1 1 21.2 6.1 11.7 < 10 3 1 -1 19.5 31.4 10.4 < 10 3 1 0 389.8 445.3 18.4 o 10 3 1 1 -1.9 0.7 6.1 < 11 3 1 -1 -9.2 1.2 6.4 < 11 3 1 0 503.6 512.9 21.9 o 11 3 1 1 10.9 5.4 10.8 < 12 3 1 -1 48.6 36.8 11.0 o 12 3 1 0 14.9 6.3 9.6 < 12 3 1 1 5.0 7.3 8.4 < 0 4 1 1 99.4 144.4 11.4 o 1 4 1 -1 1246.8 1253.8 29.8 o 1 4 1 0 332.3 14.2 14.1 o 1 4 1 1 130.5 91.9 13.6 o 2 4 1 -1 28.6 21.4 11.4 < 2 4 1 0 141.9 77.9 11.7 o 2 4 1 1 895.8 1000.5 27.5 o 3 4 1 -1 172.8 145.4 15.8 o 3 4 1 0 40024.2 40129.7 121.9 o 3 4 1 1 239.3 259.1 19.7 o 4 4 1 -1 75.2 70.7 18.5 o 4 4 1 0 12479.5 12367.5 71.8 o 4 4 1 1 29.4 10.1 10.4 < 5 4 1 -1 103.5 66.8 18.9 o 5 4 1 0 6285.0 6480.2 51.0 o 5 4 1 1 179.5 189.0 17.4 o 6 4 1 -1 37.0 20.1 15.2 < 6 4 1 0 10901.0 10969.1 74.9 o 6 4 1 1 185.8 182.3 18.3 o 7 4 1 -1 62.2 68.9 12.8 o 7 4 1 0 397.4 384.1 20.8 o 7 4 1 1 59.2 46.6 14.0 o 8 4 1 -1 28.1 35.6 9.1 o 8 4 1 0 18.4 3.0 14.6 < 8 4 1 1 42.4 50.2 8.0 o 9 4 1 -1 28.9 29.8 19.8 < 9 4 1 0 112.8 113.3 12.8 o 9 4 1 1 6.4 7.1 11.4 < 10 4 1 -1 19.0 4.3 16.5 < 10 4 1 0 146.6 137.8 15.2 o 10 4 1 1 3.2 6.3 6.7 < 11 4 1 -1 93.7 62.5 10.8 o 11 4 1 0 740.2 716.8 26.0 o 11 4 1 1 6.2 3.8 7.9 < 12 4 1 -1 52.0 50.3 15.2 o 12 4 1 0 -8.9 3.1 9.2 < 12 4 1 1 9.3 12.6 12.5 < 0 5 1 0 20048.0 19402.7 95.9 o 0 5 1 1 -11.5 0.9 6.4 < 1 5 1 -1 260.8 283.6 18.7 o 1 5 1 0 17634.6 16850.7 89.5 o 1 5 1 1 26.8 0.3 17.2 < 2 5 1 -1 158.0 194.7 16.3 o 2 5 1 0 8693.1 8623.4 64.0 o 2 5 1 1 813.6 814.2 25.4 o 3 5 1 -1 4.9 3.8 8.3 < 3 5 1 0 362.6 435.3 15.2 o 3 5 1 1 99.1 112.1 16.9 o 4 5 1 -1 82.6 106.2 10.9 o 4 5 1 0 4088.9 3879.2 44.1 o 4 5 1 1 201.4 218.1 19.9 o 5 5 1 -1 186.9 193.1 19.5 o 5 5 1 0 285.2 280.4 17.4 o 5 5 1 1 37.5 32.5 9.4 o 6 5 1 -1 141.0 180.1 13.4 o 6 5 1 0 3212.5 3134.7 41.7 o 6 5 1 1 9.0 0.0 8.1 < 7 5 1 -1 -1.8 8.1 10.0 < 7 5 1 0 537.3 541.1 26.6 o 7 5 1 1 5.2 14.0 8.9 < 8 5 1 -1 305.7 328.0 24.9 o 8 5 1 0 508.4 562.6 25.6 o 8 5 1 1 15.9 1.0 9.5 < 9 5 1 -1 3.9 1.7 6.3 < 9 5 1 0 2098.1 1987.1 37.3 o 9 5 1 1 12.4 11.6 7.2 < 10 5 1 -1 17.2 0.0 9.9 < 10 5 1 0 78.6 72.7 12.9 o 10 5 1 1 -7.0 12.0 7.7 < 11 5 1 -1 58.3 51.7 21.5 < 11 5 1 0 1807.8 1665.4 38.3 o 11 5 1 1 26.3 0.1 9.7 < 0 6 1 1 47.8 44.1 9.6 o 1 6 1 -1 189.4 167.9 17.0 o 1 6 1 0 1089.9 1083.5 26.8 o 1 6 1 1 10.5 9.7 8.7 < 2 6 1 -1 19.2 19.6 10.5 < 2 6 1 0 4955.6 5073.1 51.2 o 2 6 1 1 472.8 436.5 27.7 o 3 6 1 -1 99.2 91.9 16.6 o 3 6 1 0 1335.0 1279.2 31.5 o 3 6 1 1 10.6 12.4 8.8 < 4 6 1 -1 51.1 63.7 11.1 o 4 6 1 0 88.8 104.6 12.6 o 4 6 1 1 50.4 56.5 17.1 < 5 6 1 -1 75.8 58.7 16.5 o 5 6 1 0 826.7 853.9 26.9 o 5 6 1 1 71.7 76.6 13.9 o 6 6 1 -1 186.7 227.7 20.7 o 6 6 1 0 3122.9 2946.9 47.7 o 6 6 1 1 146.4 208.9 15.4 o 7 6 1 -1 53.3 50.3 16.8 o 7 6 1 0 240.6 219.4 19.3 o 7 6 1 1 11.1 3.7 10.9 < 8 6 1 -1 12.9 34.7 8.8 < 8 6 1 0 819.7 830.6 25.5 o 8 6 1 1 3.9 3.4 7.6 < 9 6 1 -1 19.5 4.2 13.7 < 9 6 1 0 453.5 474.1 23.8 o 9 6 1 1 135.0 88.2 16.5 o 10 6 1 -1 3.0 1.9 9.3 < 10 6 1 0 22.3 18.8 12.9 < 10 6 1 1 32.7 11.4 9.6 o 0 7 1 0 3557.5 3589.2 46.5 o 0 7 1 1 9.1 2.9 5.0 < 1 7 1 -1 -5.0 0.2 7.0 < 1 7 1 0 1874.4 1897.2 37.4 o 1 7 1 1 8.1 21.5 8.1 < 2 7 1 -1 362.1 436.8 19.3 o 2 7 1 0 166.2 137.5 16.7 o 2 7 1 1 13.5 25.1 11.0 < 3 7 1 -1 181.3 180.9 15.7 o 3 7 1 0 539.5 551.3 25.2 o 3 7 1 1 57.1 48.0 15.0 o 4 7 1 -1 129.1 162.5 14.1 o 4 7 1 0 764.1 791.0 26.5 o 4 7 1 1 19.2 0.5 10.6 < 5 7 1 -1 75.7 55.7 20.0 o 5 7 1 0 5179.9 5416.7 52.7 o 5 7 1 1 56.6 59.4 13.1 o 6 7 1 -1 -6.9 10.8 9.3 < 6 7 1 0 1505.1 1569.8 32.4 o 6 7 1 1 21.8 4.3 14.4 < 7 7 1 -1 57.4 27.7 13.5 o 7 7 1 0 3090.8 3221.4 46.2 o 7 7 1 1 4.7 9.1 9.3 < 8 7 1 -1 50.1 51.5 13.6 o 8 7 1 0 39.4 30.8 12.4 o 8 7 1 1 49.2 44.9 10.8 o 9 7 1 -1 40.6 23.0 16.4 < 9 7 1 0 242.7 225.1 21.4 o 9 7 1 1 19.4 4.5 13.2 < 0 8 1 1 39.3 36.4 10.0 o 1 8 1 -1 71.7 77.6 15.5 o 1 8 1 0 52.9 49.7 12.1 o 1 8 1 1 -17.9 0.2 8.5 < 2 8 1 -1 5.2 4.9 9.9 < 2 8 1 0 1335.5 1340.4 35.4 o 2 8 1 1 219.8 190.9 25.1 o 3 8 1 -1 -13.9 18.2 10.0 < 3 8 1 0 720.3 763.8 30.1 o 3 8 1 1 34.2 42.6 13.8 < 4 8 1 -1 19.0 2.0 10.2 < 4 8 1 0 18.0 8.8 10.2 < 4 8 1 1 -8.2 1.3 7.1 < 5 8 1 -1 -5.0 2.7 8.8 < 5 8 1 0 290.1 297.2 18.8 o 5 8 1 1 143.9 126.0 14.3 o 6 8 1 -1 26.3 36.5 10.4 < 6 8 1 0 960.9 1022.0 27.4 o 6 8 1 1 28.1 17.0 11.4 < 7 8 1 -1 23.6 20.6 17.5 < 7 8 1 0 13.0 21.6 10.2 < 7 8 1 1 12.4 8.3 13.9 < 8 8 1 -1 -1.7 12.3 7.2 < 8 8 1 0 336.0 348.8 20.2 o 8 8 1 1 0.1 5.4 7.3 < 0 9 1 0 1386.1 1424.3 33.3 o 0 9 1 1 -1.2 1.4 5.3 < 1 9 1 -1 47.5 51.1 16.5 < 1 9 1 0 533.2 583.2 26.8 o 1 9 1 1 25.3 14.0 10.1 < 2 9 1 -1 16.8 0.2 8.1 < 2 9 1 0 2272.8 2032.9 48.4 o 2 9 1 1 59.6 69.7 12.0 o 3 9 1 -1 -12.1 5.4 10.0 < 3 9 1 0 18.8 21.9 12.9 < 3 9 1 1 8.5 19.7 7.7 < 4 9 1 -1 9.5 0.7 13.2 < 4 9 1 0 316.0 342.5 25.0 o 4 9 1 1 19.7 20.2 11.6 < 5 9 1 -1 -0.4 48.9 9.1 < 5 9 1 0 97.8 93.3 15.3 o 5 9 1 1 18.5 0.0 14.8 < 6 9 1 -1 2.1 5.8 8.3 < 6 9 1 0 515.0 526.6 19.8 o 6 9 1 1 -2.7 3.5 6.5 < 0 10 1 1 4.0 7.9 6.3 < 1 10 1 -1 51.7 50.9 14.4 o 1 10 1 0 41.5 27.9 14.0 < 1 10 1 1 24.1 14.5 13.2 < 2 10 1 -1 -2.4 0.2 7.7 < 2 10 1 0 3.0 1.4 8.7 < 2 10 1 1 2.0 17.7 8.6 < 3 10 1 -1 36.1 29.5 14.1 < 3 10 1 0 611.6 727.0 22.9 o 3 10 1 1 14.4 1.1 10.9 < 0 0 2 0 4484.7 4226.1 21.4 o 1 0 2 0 59368.5 50952.9 109.7 o 2 0 2 0 118051.0 119404.9 243.5 o 3 0 2 0 153977.0 153248.4 491.7 o 4 0 2 0 8460.8 8576.0 48.7 o 5 0 2 0 994.0 1092.8 18.9 o 6 0 2 0 3676.8 4164.6 33.8 o 7 0 2 0 14357.6 15130.1 91.5 o 8 0 2 0 2097.7 2124.6 43.8 o 9 0 2 0 6311.1 6649.2 76.9 o 10 0 2 0 22.7 26.3 8.5 < 11 0 2 0 5931.2 5722.8 63.6 o 12 0 2 0 308.1 304.6 16.0 o 13 0 2 0 170.7 144.5 16.3 o 0 1 2 1 233.3 223.1 10.8 o 1 1 2 -1 44.3 47.9 8.5 o 1 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