#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/26/2102680.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102680_Fobs loop_ _publ_author_name 'Guzei, Ilia A.' 'Spencer, Lara C.' 'Su, Joe W.' 'Burnette, Ronald R.' _publ_section_title ; Low-temperature enantiotropic k2 phase transition in the ionic 222-cryptand complex with LiClO~4~ ; _journal_coeditor_code AV5077 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 93 _journal_page_last 100 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.0273 _cell_length_b 13.3313 _cell_length_c 16.8827 _exptl_crystal_F_000 1032.00 _reflns_d_resolution_high 0.7997 _[local]_cod_data_source_file av5077burnette07sup2.hkl _[local]_cod_data_source_block burnette07 #BEGIN Tags that were not found in dictionaries: _shelx_title ' BURNETTE07 IN P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 278.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1467.57 1739.17 41.78 o 4 0 0 16183.46 16176.22 384.73 o 6 0 0 10172.67 10657.17 253.01 o 8 0 0 73.93 84.02 3.65 o 10 0 0 4077.44 4009.57 107.41 o 12 0 0 144.27 132.59 15.69 o 1 1 0 1978.29 1908.06 30.21 o 2 1 0 3923.00 3956.95 65.24 o 3 1 0 1101.99 1058.25 18.01 o 4 1 0 71.69 75.26 1.65 o 5 1 0 316.43 392.30 8.12 o 6 1 0 1892.44 1971.56 33.60 o 7 1 0 2686.97 2563.36 43.56 o 8 1 0 531.56 483.53 9.01 o 9 1 0 693.01 686.53 13.28 o 10 1 0 377.84 381.18 10.35 o 11 1 0 100.00 107.45 4.44 o 12 1 0 171.85 187.56 6.85 o 0 2 0 19731.46 18811.95 605.04 o 1 2 0 4635.28 4470.51 79.70 o 2 2 0 10165.49 9901.09 173.60 o 3 2 0 20.42 16.46 0.71 o 4 2 0 4370.66 4323.13 67.48 o 5 2 0 1755.36 1803.27 26.94 o 6 2 0 8511.29 8543.50 134.16 o 7 2 0 405.85 414.10 8.32 o 8 2 0 1120.19 1005.01 19.16 o 9 2 0 372.98 345.31 7.88 o 10 2 0 564.82 566.78 13.10 o 11 2 0 97.58 89.49 3.70 o 12 2 0 768.95 796.07 20.11 o 1 3 0 54168.80 46468.31 1376.56 o 2 3 0 7148.03 7075.15 103.73 o 3 3 0 115.23 227.14 5.24 o 4 3 0 9699.27 10212.23 188.46 o 5 3 0 10406.20 10961.98 161.36 o 6 3 0 111.45 91.83 2.13 o 7 3 0 44.14 39.77 2.06 o 8 3 0 659.13 638.26 27.89 o 9 3 0 2150.74 2132.41 41.68 o 10 3 0 555.71 541.59 12.62 o 11 3 0 30.36 24.24 2.25 o 12 3 0 268.86 266.30 8.29 o 0 4 0 2223.47 2575.68 68.41 o 1 4 0 14407.30 13917.54 213.58 o 2 4 0 593.88 481.58 8.54 o 3 4 0 8922.91 9268.69 153.10 o 4 4 0 77.80 124.38 2.31 o 5 4 0 416.40 426.32 6.78 o 6 4 0 63.26 50.06 1.49 o 7 4 0 3.86 4.57 0.85 o 8 4 0 883.18 865.79 17.67 o 9 4 0 1181.00 1116.42 22.59 o 10 4 0 176.90 166.88 5.08 o 11 4 0 36.76 39.02 2.59 o 12 4 0 270.32 288.38 8.15 o 1 5 0 1029.71 966.07 16.14 o 2 5 0 2135.30 2237.63 50.50 o 3 5 0 7121.80 7477.28 109.68 o 4 5 0 4548.64 4815.62 75.57 o 5 5 0 10155.95 10373.75 152.70 o 6 5 0 229.11 263.97 5.21 o 7 5 0 2334.65 2393.34 43.70 o 8 5 0 458.71 384.30 8.58 o 9 5 0 166.39 173.89 4.75 o 10 5 0 0.49 0.18 2.40 o 11 5 0 91.97 113.50 4.27 o 0 6 0 1146.12 1411.96 34.05 o 1 6 0 146.89 160.74 2.97 o 2 6 0 8.39 3.56 0.54 o 3 6 0 1370.65 1564.71 27.76 o 4 6 0 583.62 540.89 9.23 o 5 6 0 6.49 16.37 1.07 o 6 6 0 728.97 723.67 13.89 o 7 6 0 89.53 112.84 3.09 o 8 6 0 1124.48 1117.92 22.51 o 9 6 0 1.11 1.17 1.26 o 10 6 0 476.75 478.72 11.88 o 11 6 0 3.61 2.31 2.12 o 1 7 0 155.81 130.86 2.59 o 2 7 0 121.44 124.88 2.37 o 3 7 0 85.03 84.46 1.86 o 4 7 0 3410.12 3716.63 55.12 o 5 7 0 702.06 778.93 13.70 o 6 7 0 365.90 372.35 7.68 o 7 7 0 159.98 157.45 4.20 o 8 7 0 864.62 879.10 19.94 o 9 7 0 0.19 -0.86 1.43 o 10 7 0 0.02 1.97 1.76 o 11 7 0 156.74 158.51 6.67 o 0 8 0 1163.67 1264.77 30.82 o 1 8 0 290.25 289.08 5.51 o 2 8 0 1275.19 1279.69 20.54 o 3 8 0 1.34 2.07 0.64 o 4 8 0 4706.61 4675.66 82.90 o 5 8 0 511.67 490.68 9.73 o 6 8 0 204.57 205.13 5.16 o 7 8 0 74.02 60.74 2.60 o 8 8 0 620.52 659.07 17.29 o 9 8 0 0.90 3.89 1.70 o 10 8 0 244.80 258.49 8.27 o 11 8 0 6.99 -4.65 4.65 o 1 9 0 86.22 87.09 2.22 o 2 9 0 363.45 340.42 6.46 o 3 9 0 0.19 0.56 0.84 o 4 9 0 2592.23 2669.96 51.36 o 5 9 0 110.65 87.33 3.17 o 6 9 0 374.63 343.30 8.82 o 7 9 0 161.64 134.69 4.80 o 8 9 0 26.54 30.37 2.37 o 9 9 0 79.19 76.10 4.92 o 10 9 0 284.70 303.23 9.41 o 0 10 0 569.36 551.98 20.56 o 1 10 0 24.01 17.13 1.09 o 2 10 0 1444.69 1438.88 24.95 o 3 10 0 389.15 383.82 8.59 o 4 10 0 188.00 198.01 5.39 o 5 10 0 12.16 14.68 1.45 o 6 10 0 80.24 85.73 3.30 o 7 10 0 8.21 6.34 1.75 o 8 10 0 64.44 59.98 3.23 o 9 10 0 67.10 84.89 4.09 o 10 10 0 237.72 264.74 8.62 o 1 11 0 27.55 33.49 1.61 o 2 11 0 816.38 871.15 18.85 o 3 11 0 833.47 834.60 17.53 o 4 11 0 45.99 33.23 1.93 o 5 11 0 686.74 632.44 15.21 o 6 11 0 317.10 293.39 8.72 o 7 11 0 231.90 226.11 7.21 o 8 11 0 19.17 23.32 2.60 o 9 11 0 126.11 137.05 5.47 o 0 12 0 501.90 537.54 16.78 o 1 12 0 250.85 234.68 5.92 o 2 12 0 303.62 308.77 7.29 o 3 12 0 331.78 306.30 7.35 o 4 12 0 47.15 40.43 2.28 o 5 12 0 6.75 9.76 1.62 o 6 12 0 466.81 503.01 13.79 o 7 12 0 111.65 111.48 5.92 o 8 12 0 13.47 8.77 2.09 o 1 13 0 727.14 706.10 16.85 o 2 13 0 40.52 45.53 2.60 o 3 13 0 737.90 755.86 17.94 o 4 13 0 32.89 34.19 2.57 o 5 13 0 4.60 2.14 1.55 o 6 13 0 14.82 20.74 2.55 o 7 13 0 184.31 199.73 6.85 o 0 14 0 563.10 576.56 22.94 o 1 14 0 61.89 61.17 3.15 o 2 14 0 184.55 210.50 7.16 o 3 14 0 8.69 12.01 1.99 o 4 14 0 419.98 434.95 11.30 o 5 14 0 18.16 21.95 2.78 o 6 14 0 1545.44 1689.06 49.50 o 1 15 0 151.13 168.87 9.97 o 2 15 0 60.66 57.09 3.22 o 3 15 0 193.89 198.92 7.42 o 4 15 0 34.05 43.52 4.19 o 5 15 0 3.65 3.25 2.43 o 0 16 0 603.26 588.45 23.54 o 1 16 0 60.00 64.44 4.03 o 2 16 0 643.62 695.43 17.16 o 3 16 0 55.89 57.64 3.99 o 1 0 1 14.91 -0.75 0.75 o 2 0 1 242.14 239.12 4.00 o 3 0 1 1354.77 1425.08 27.04 o 4 0 1 476.93 462.27 9.79 o 5 0 1 2137.93 2347.74 37.09 o 6 0 1 1.65 2.07 0.66 o 7 0 1 16.19 24.40 1.23 o 8 0 1 37.00 43.04 1.71 o 9 0 1 47.09 42.82 1.96 o 10 0 1 74.71 62.58 3.20 o 11 0 1 7.52 17.06 2.45 o 12 0 1 32.30 25.98 3.87 o -12 1 1 53.80 66.44 5.01 o -11 1 1 148.42 140.65 5.18 o -10 1 1 6.73 2.29 1.35 o -9 1 1 583.11 572.86 10.55 o -8 1 1 98.32 89.53 2.65 o -7 1 1 1037.53 1148.83 20.07 o -6 1 1 96.44 91.01 2.42 o -5 1 1 1244.01 1351.35 21.60 o -4 1 1 242.28 259.42 4.47 o -3 1 1 2708.28 2800.68 44.09 o -2 1 1 795.65 774.72 11.67 o -1 1 1 262.93 235.73 3.87 o 0 1 1 88.71 29.98 1.75 o 1 1 1 262.73 240.65 7.79 o 2 1 1 795.38 806.28 14.60 o 3 1 1 2707.79 2772.00 49.39 o 4 1 1 242.50 263.50 5.06 o 5 1 1 1243.28 1277.46 20.38 o 6 1 1 96.53 95.54 2.15 o 7 1 1 1036.68 1096.23 20.48 o 8 1 1 97.54 89.52 2.68 o 9 1 1 582.45 571.49 17.94 o 10 1 1 6.57 1.54 1.55 o 11 1 1 148.33 140.16 5.12 o 12 1 1 53.92 68.66 3.49 o -12 2 1 25.80 25.14 2.61 o -11 2 1 0.04 -1.59 1.59 o -10 2 1 288.16 272.30 8.13 o -9 2 1 37.84 34.16 1.72 o -8 2 1 1025.27 1028.02 23.91 o -7 2 1 43.55 45.12 1.53 o -6 2 1 30.39 28.01 1.14 o -5 2 1 2701.44 2895.19 57.13 o -4 2 1 470.98 459.54 7.19 o -3 2 1 2121.30 2178.99 30.79 o -2 2 1 289.23 273.27 4.28 o -1 2 1 84.96 76.02 1.34 o 0 2 1 100.41 116.86 1.99 o 1 2 1 84.69 73.43 1.75 o 2 2 1 290.84 265.01 5.59 o 3 2 1 2121.91 2178.90 35.72 o 4 2 1 471.22 449.48 7.39 o 5 2 1 2703.00 2927.77 62.24 o 6 2 1 30.88 29.15 1.33 o 7 2 1 43.91 48.29 1.81 o 8 2 1 1024.20 1015.11 19.30 o 9 2 1 38.13 31.32 2.19 o 10 2 1 288.13 284.15 8.66 o 11 2 1 0.03 -1.43 1.43 o 12 2 1 25.33 21.21 2.55 o -12 3 1 35.78 36.88 3.05 o -11 3 1 14.56 16.63 2.24 o -10 3 1 137.99 132.67 4.39 o -9 3 1 514.14 488.70 10.66 o -8 3 1 43.54 43.50 1.88 o -7 3 1 429.77 455.24 10.82 o -6 3 1 116.25 115.09 2.69 o -5 3 1 2258.63 2353.38 35.15 o -4 3 1 484.41 498.23 7.74 o -3 3 1 4712.27 4802.35 70.74 o -2 3 1 234.77 235.44 4.68 o -1 3 1 381.77 405.62 6.22 o 0 3 1 0.90 0.34 0.29 o 1 3 1 380.36 401.48 6.52 o 2 3 1 234.14 233.81 4.87 o 3 3 1 4713.04 4837.13 79.28 o 4 3 1 484.16 503.82 7.84 o 5 3 1 2258.60 2362.34 35.08 o 6 3 1 116.38 117.88 2.49 o 7 3 1 429.42 455.96 8.49 o 8 3 1 43.93 44.52 1.89 o 9 3 1 515.97 471.26 11.79 o 10 3 1 138.86 139.21 4.49 o 11 3 1 14.46 21.28 2.30 o 12 3 1 36.10 48.82 3.00 o -12 4 1 159.22 169.52 8.92 o -11 4 1 8.13 15.68 4.09 o -10 4 1 97.18 87.00 3.27 o -9 4 1 216.32 204.19 5.34 o -8 4 1 116.29 117.38 3.53 o -7 4 1 58.22 68.42 3.34 o -6 4 1 459.79 453.99 8.32 o -5 4 1 34.27 33.79 1.08 o -4 4 1 1133.13 1115.62 16.86 o -3 4 1 547.75 567.85 8.95 o -2 4 1 761.71 755.73 11.51 o -1 4 1 507.61 507.46 9.60 o 0 4 1 319.07 310.71 5.19 o 1 4 1 504.81 517.08 8.38 o 2 4 1 763.20 773.40 14.83 o 3 4 1 545.13 563.70 9.54 o 4 4 1 1131.06 1121.61 17.77 o 5 4 1 33.88 33.21 1.05 o 6 4 1 457.01 462.66 7.89 o 7 4 1 57.22 62.40 2.30 o 8 4 1 114.01 114.50 3.18 o 9 4 1 215.19 207.62 5.37 o 10 4 1 95.64 97.47 3.67 o 11 4 1 8.07 12.44 1.94 o 12 4 1 158.54 162.32 5.45 o -11 5 1 114.20 117.97 4.32 o -10 5 1 156.67 147.44 4.43 o -9 5 1 426.39 377.75 8.62 o -8 5 1 134.99 130.60 3.80 o -7 5 1 204.56 189.30 4.36 o -6 5 1 216.42 214.73 4.40 o -5 5 1 344.57 327.80 5.43 o -4 5 1 547.37 549.36 9.17 o -3 5 1 438.66 438.60 6.68 o -2 5 1 368.99 376.03 5.93 o -1 5 1 4.50 2.31 0.52 o 0 5 1 1.92 0.52 0.38 o 1 5 1 4.64 3.17 0.44 o 2 5 1 368.16 387.62 6.10 o 3 5 1 440.67 439.27 8.29 o 4 5 1 547.67 554.30 9.07 o 5 5 1 348.10 340.07 5.57 o 6 5 1 217.38 219.43 5.14 o 7 5 1 207.70 186.08 4.34 o 8 5 1 136.14 131.21 3.76 o 9 5 1 427.94 409.02 9.19 o 10 5 1 157.73 129.66 4.37 o 11 5 1 116.46 128.56 5.04 o -11 6 1 105.87 101.06 4.54 o -10 6 1 135.05 130.88 4.21 o -9 6 1 205.00 198.93 5.30 o -8 6 1 164.16 163.26 4.45 o -7 6 1 126.21 117.38 3.43 o -6 6 1 109.07 130.01 3.08 o -5 6 1 977.60 993.05 16.20 o -4 6 1 2095.71 2302.00 34.44 o -3 6 1 689.97 712.08 10.58 o -2 6 1 594.20 612.68 9.60 o -1 6 1 398.18 439.56 6.88 o 0 6 1 225.60 255.13 4.44 o 1 6 1 399.05 442.30 7.34 o 2 6 1 597.71 612.52 9.43 o 3 6 1 684.98 708.18 11.27 o 4 6 1 2099.02 2272.51 43.01 o 5 6 1 972.83 1046.65 16.86 o 6 6 1 107.57 129.45 3.27 o 7 6 1 126.70 114.06 3.13 o 8 6 1 161.30 157.71 4.31 o 9 6 1 202.97 208.22 5.40 o 10 6 1 134.51 124.92 5.24 o 11 6 1 106.19 107.57 5.26 o -11 7 1 49.84 51.89 3.79 o -10 7 1 65.64 66.88 3.29 o -9 7 1 46.17 38.60 2.46 o -8 7 1 62.50 65.53 3.93 o -7 7 1 63.34 56.96 2.36 o -6 7 1 710.74 669.84 15.73 o -5 7 1 80.40 71.47 2.08 o -4 7 1 70.19 73.25 1.70 o -3 7 1 2.66 6.53 0.62 o -2 7 1 823.31 859.00 13.12 o -1 7 1 115.56 115.22 3.47 o 0 7 1 298.66 331.23 5.72 o 1 7 1 111.92 112.06 2.29 o 2 7 1 820.48 849.03 13.03 o 3 7 1 2.87 5.73 0.64 o 4 7 1 70.21 71.31 1.73 o 5 7 1 79.26 67.85 1.67 o 6 7 1 711.80 702.61 13.52 o 7 7 1 65.23 56.81 2.29 o 8 7 1 62.02 61.90 2.74 o 9 7 1 48.08 44.59 2.85 o 10 7 1 66.54 66.58 3.92 o 11 7 1 50.51 49.31 6.16 o -10 8 1 4.00 7.64 1.99 o -9 8 1 12.97 15.55 2.42 o -8 8 1 242.07 212.02 6.00 o -7 8 1 109.97 113.28 3.83 o -6 8 1 66.41 59.33 3.05 o -5 8 1 26.96 23.55 1.46 o -4 8 1 238.48 221.36 5.01 o -3 8 1 50.99 51.43 1.64 o -2 8 1 25.53 24.70 1.09 o -1 8 1 61.55 71.93 1.92 o 0 8 1 140.29 153.92 3.23 o 1 8 1 61.82 65.02 1.66 o 2 8 1 23.45 19.63 0.90 o 3 8 1 50.48 52.74 2.13 o 4 8 1 239.08 220.21 4.59 o 5 8 1 26.06 23.05 1.30 o 6 8 1 65.18 57.68 2.46 o 7 8 1 108.74 102.02 3.55 o 8 8 1 244.20 210.70 6.68 o 9 8 1 12.40 13.18 1.91 o 10 8 1 4.35 8.47 3.31 o -10 9 1 65.27 61.76 3.71 o -9 9 1 65.40 69.77 3.68 o -8 9 1 49.21 47.51 2.92 o -7 9 1 258.23 254.49 7.70 o -6 9 1 604.27 574.71 13.39 o -5 9 1 574.50 585.65 11.55 o -4 9 1 191.92 193.28 4.27 o -3 9 1 37.96 37.84 1.44 o -2 9 1 155.39 160.80 3.45 o -1 9 1 16.59 14.39 0.92 o 0 9 1 100.51 104.19 2.50 o 1 9 1 18.07 16.65 0.97 o 2 9 1 155.20 155.40 3.37 o 3 9 1 40.42 42.47 1.51 o 4 9 1 189.01 195.83 5.11 o 5 9 1 583.90 601.76 12.85 o 6 9 1 602.00 585.27 15.34 o 7 9 1 256.45 252.62 7.58 o 8 9 1 50.04 45.88 2.80 o 9 9 1 64.33 68.84 3.49 o 10 9 1 64.32 61.89 4.41 o -10 10 1 2.76 -0.97 2.37 o -9 10 1 30.85 29.92 2.68 o -8 10 1 86.43 83.83 4.70 o -7 10 1 70.95 58.72 3.12 o -6 10 1 630.41 601.00 15.90 o -5 10 1 216.96 213.97 5.49 o -4 10 1 712.78 665.51 12.34 o -3 10 1 185.26 175.40 4.17 o -2 10 1 485.03 463.32 8.64 o -1 10 1 332.30 338.38 6.48 o 0 10 1 206.06 208.65 4.34 o 1 10 1 333.81 331.42 6.37 o 2 10 1 478.08 425.16 10.41 o 3 10 1 186.73 174.17 4.15 o 4 10 1 717.97 703.92 17.33 o 5 10 1 219.28 230.68 6.38 o 6 10 1 623.47 597.11 14.45 o 7 10 1 70.00 68.10 3.26 o 8 10 1 90.57 86.94 3.89 o 9 10 1 30.08 30.70 4.76 o 10 10 1 3.27 -0.08 2.12 o -9 11 1 33.95 28.63 6.66 o -8 11 1 72.29 83.11 3.97 o -7 11 1 107.58 107.38 4.42 o -6 11 1 212.37 211.14 6.76 o -5 11 1 164.16 160.17 4.54 o -4 11 1 292.38 299.36 7.73 o -3 11 1 411.76 402.63 9.01 o -2 11 1 103.43 101.00 3.46 o -1 11 1 170.30 163.44 3.68 o 0 11 1 408.46 404.34 10.46 o 1 11 1 165.03 163.28 4.00 o 2 11 1 103.26 106.74 3.04 o 3 11 1 411.08 407.72 9.20 o 4 11 1 292.80 286.96 7.34 o 5 11 1 160.94 149.34 4.75 o 6 11 1 210.34 196.67 9.04 o 7 11 1 110.85 104.39 4.30 o 8 11 1 70.50 77.29 3.74 o 9 11 1 34.49 31.81 2.75 o -8 12 1 286.21 285.45 9.03 o -7 12 1 24.14 30.47 2.65 o -6 12 1 287.84 282.83 8.64 o -5 12 1 140.78 140.08 4.67 o -4 12 1 57.34 55.09 2.41 o -3 12 1 100.35 92.04 3.57 o -2 12 1 38.00 45.71 2.49 o -1 12 1 24.44 26.02 2.33 o 0 12 1 38.69 45.12 2.18 o 1 12 1 24.54 26.95 1.58 o 2 12 1 39.68 44.06 2.17 o 3 12 1 102.29 96.21 3.25 o 4 12 1 61.06 60.55 2.77 o 5 12 1 138.34 137.70 4.64 o 6 12 1 295.19 287.26 8.62 o 7 12 1 23.27 30.66 5.13 o 8 12 1 282.39 285.14 8.88 o -7 13 1 59.74 52.75 4.51 o -6 13 1 143.40 155.12 6.78 o -5 13 1 250.68 236.76 8.87 o -4 13 1 38.12 51.06 2.91 o -3 13 1 560.74 588.17 14.40 o -2 13 1 115.09 120.42 4.32 o -1 13 1 1188.53 1154.84 26.47 o 0 13 1 219.54 203.60 5.45 o 1 13 1 1181.23 1208.66 25.60 o 2 13 1 116.70 122.60 4.33 o 3 13 1 564.98 570.65 12.57 o 4 13 1 39.22 55.19 3.00 o 5 13 1 247.13 236.96 7.17 o 6 13 1 144.92 154.88 5.64 o 7 13 1 58.54 55.47 3.32 o -6 14 1 31.47 29.80 4.85 o -5 14 1 228.32 212.95 8.47 o -4 14 1 80.54 86.31 3.89 o -3 14 1 28.56 27.75 2.70 o -2 14 1 12.91 12.83 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534.12 13.73 o 6 9 9 48.01 42.93 3.76 o 7 9 9 408.98 419.69 21.35 o 8 9 9 17.70 13.18 2.87 o 9 9 9 40.79 40.16 4.30 o -8 10 9 46.69 44.68 3.53 o -7 10 9 10.67 7.91 2.27 o -6 10 9 81.20 87.61 3.98 o -5 10 9 302.85 292.09 7.42 o -4 10 9 309.42 325.04 8.02 o -3 10 9 43.10 36.71 2.19 o -2 10 9 164.82 148.70 4.42 o -1 10 9 1284.88 1226.39 25.25 o 0 10 9 117.04 121.10 3.78 o 1 10 9 1287.89 1294.89 30.70 o 2 10 9 162.41 154.74 4.74 o 3 10 9 44.39 43.33 2.38 o 4 10 9 303.65 313.04 11.20 o 5 10 9 305.35 290.65 7.67 o 6 10 9 82.81 88.53 4.44 o 7 10 9 10.99 9.33 2.67 o 8 10 9 45.43 42.41 5.47 o -7 11 9 43.80 50.98 3.61 o -6 11 9 75.16 70.16 3.71 o -5 11 9 18.77 17.37 1.87 o -4 11 9 67.93 74.49 3.23 o -3 11 9 60.36 57.43 3.02 o -2 11 9 544.40 520.16 13.40 o -1 11 9 56.78 52.87 2.57 o 0 11 9 858.00 854.45 18.12 o 1 11 9 58.05 54.87 2.53 o 2 11 9 546.11 523.04 12.64 o 3 11 9 58.18 55.02 3.95 o 4 11 9 68.82 74.94 3.07 o 5 11 9 17.43 14.11 1.56 o 6 11 9 74.76 69.08 2.93 o 7 11 9 42.80 43.74 4.09 o -6 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