#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/27/2102768.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102768_Fobs loop_ _publ_author_name 'Luthe, G.' 'Swenson, D. C.' 'Robertson, L. W.' _publ_section_title ; Influence of fluoro-substitution on the planarity of 4-chlorobiphenyl (PCB 3) ; _journal_coeditor_code BK5043 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 319 _journal_page_last 327 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.701 _cell_angle_gamma 90.000 _cell_length_a 17.9426 _cell_length_b 6.0863 _cell_length_c 18.3206 _exptl_crystal_F_000 848.00 _reflns_d_resolution_high 0.7704 _[local]_cod_data_source_file bk50432primeF-PCB3sup4.hkl _[local]_cod_data_source_block 2'F-PCB3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' Rob05_4 C2/c sample #05161 2'F-PCB' _shelx_refln_list_code 4 _shelx_f_calc_maximum 192.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2899.14 2651.16 41.26 o 6 0 0 7177.20 6857.20 98.12 o 8 0 0 2289.00 2179.54 31.42 o 10 0 0 12364.11 12642.59 181.45 o 12 0 0 55.01 68.34 4.56 o 14 0 0 2341.04 2441.70 54.80 o 16 0 0 1003.82 989.28 28.17 o 18 0 0 65.25 67.55 11.66 o 20 0 0 202.02 190.23 15.48 o 22 0 0 102.61 93.98 16.33 o 1 1 0 7.52 8.01 0.73 o 3 1 0 5934.29 5750.75 60.52 o 5 1 0 10164.67 9337.93 89.37 o 7 1 0 1124.78 1092.71 11.16 o 9 1 0 1016.11 935.33 9.98 o 11 1 0 2241.01 2249.86 27.16 o 13 1 0 565.96 536.42 8.97 o 15 1 0 2297.91 2365.11 33.56 o 17 1 0 12.17 6.58 5.84 o 19 1 0 118.10 129.79 12.72 o 21 1 0 4.95 11.99 8.39 o 0 2 0 15.41 28.38 1.61 o 2 2 0 762.90 809.14 8.58 o 4 2 0 9444.80 9490.22 103.62 o 6 2 0 1939.43 2231.04 45.47 o 8 2 0 228.71 212.18 5.04 o 10 2 0 2567.79 2801.40 29.88 o 12 2 0 474.11 521.34 8.22 o 14 2 0 383.21 402.26 8.53 o 16 2 0 333.63 322.29 15.63 o 18 2 0 252.02 278.48 12.38 o 20 2 0 51.84 49.23 8.95 o 1 3 0 200.71 217.69 3.39 o 3 3 0 186.95 235.81 3.34 o 5 3 0 838.28 939.34 15.57 o 7 3 0 273.40 292.45 6.87 o 9 3 0 2.16 2.03 1.25 o 11 3 0 4.60 7.24 2.75 o 13 3 0 71.72 86.94 7.45 o 15 3 0 316.61 318.13 9.95 o 17 3 0 45.35 53.45 9.30 o 19 3 0 205.46 214.86 11.77 o 0 4 0 0.01 4.45 3.14 o 2 4 0 258.77 249.41 4.48 o 4 4 0 566.07 488.46 15.30 o 6 4 0 1309.88 1361.58 20.39 o 8 4 0 1.67 1.01 2.70 o 10 4 0 2.65 15.00 3.35 o 12 4 0 5.21 6.87 4.65 o 14 4 0 15.05 5.52 5.41 o 16 4 0 2.13 -5.51 8.67 o 18 4 0 197.23 188.65 15.02 o 1 5 0 1243.44 1285.63 18.52 o 3 5 0 241.51 229.79 6.20 o 5 5 0 137.94 127.82 9.51 o 7 5 0 7.70 9.44 5.35 o 9 5 0 389.27 365.43 10.55 o 11 5 0 78.28 49.27 6.99 o 13 5 0 106.75 104.63 8.48 o 15 5 0 142.45 148.99 14.33 o 17 5 0 99.95 98.51 20.09 o 0 6 0 992.80 1019.74 31.22 o 2 6 0 531.98 544.18 15.45 o 4 6 0 18.05 14.87 3.54 o 6 6 0 7.20 19.18 6.99 o 8 6 0 184.35 211.01 10.86 o 10 6 0 32.38 11.57 11.41 o 12 6 0 1.73 5.31 8.09 o 14 6 0 4.55 7.87 12.80 o 1 7 0 0.87 -3.07 7.11 o 3 7 0 176.64 189.55 14.01 o 5 7 0 34.15 46.22 10.40 o 7 7 0 27.71 24.63 10.50 o 9 7 0 36.69 24.83 11.74 o -21 1 1 94.62 92.73 9.97 o -19 1 1 159.75 178.36 10.23 o -17 1 1 67.38 65.08 6.59 o -15 1 1 1997.49 2056.91 28.43 o -13 1 1 1816.62 1878.56 25.66 o -11 1 1 257.98 271.28 7.39 o -9 1 1 1484.62 1373.10 15.02 o -7 1 1 174.40 172.29 4.43 o -5 1 1 16766.30 15539.17 215.05 o -3 1 1 4168.23 3703.63 68.70 o -1 1 1 2.46 4.90 0.56 o 1 1 1 2862.77 2547.12 49.86 o 3 1 1 826.50 758.19 9.01 o 5 1 1 1649.90 1692.52 16.18 o 7 1 1 1793.83 1834.20 18.66 o 9 1 1 111.33 111.25 3.16 o 11 1 1 762.97 763.62 10.45 o 13 1 1 1811.82 1932.45 24.63 o 15 1 1 0.82 -1.45 3.83 o 17 1 1 1923.50 2077.47 35.12 o 19 1 1 78.39 69.57 8.71 o 21 1 1 10.71 4.80 9.14 o -22 2 1 47.38 43.29 11.77 o -20 2 1 109.11 107.94 10.09 o -18 2 1 725.89 756.06 23.87 o -16 2 1 4.11 3.63 4.34 o -14 2 1 41.85 42.79 2.69 o -12 2 1 534.58 520.11 8.06 o -10 2 1 2301.23 2279.24 25.67 o -8 2 1 7509.71 7603.94 79.13 o -6 2 1 0.10 3.04 1.94 o -4 2 1 4776.59 4458.08 52.75 o -2 2 1 3495.78 3358.23 35.31 o 0 2 1 4060.36 3926.42 36.13 o 2 2 1 8438.99 8169.31 81.58 o 4 2 1 173.61 165.02 2.38 o 6 2 1 590.70 487.92 6.97 o 8 2 1 38.84 49.25 2.12 o 10 2 1 1154.11 1113.77 12.65 o 12 2 1 183.38 174.48 4.55 o 14 2 1 890.59 955.22 26.08 o 16 2 1 299.22 324.52 11.18 o 18 2 1 10.35 6.64 7.20 o 20 2 1 13.12 22.37 8.92 o -21 3 1 67.03 80.94 17.93 o -19 3 1 163.47 156.85 11.29 o -17 3 1 75.92 95.86 7.57 o -15 3 1 52.44 52.68 6.47 o -13 3 1 1355.70 1386.51 17.31 o -11 3 1 9.17 6.38 1.39 o -9 3 1 1022.36 948.99 15.84 o -7 3 1 472.94 442.40 8.18 o -5 3 1 900.50 876.30 13.11 o -3 3 1 1960.20 1802.75 18.02 o -1 3 1 1101.68 1061.08 10.78 o 1 3 1 5016.03 5075.42 46.29 o 3 3 1 1276.62 1483.31 15.16 o 5 3 1 4356.06 4500.63 55.60 o 7 3 1 720.83 662.79 8.49 o 9 3 1 196.01 194.25 3.84 o 11 3 1 472.09 445.21 9.11 o 13 3 1 1244.92 1303.93 22.95 o 15 3 1 63.13 57.15 5.06 o 17 3 1 3.89 3.72 5.53 o 19 3 1 60.24 52.98 12.39 o -18 4 1 54.12 64.17 12.26 o -16 4 1 398.61 389.51 20.04 o -14 4 1 2409.70 2473.98 44.76 o -12 4 1 33.95 24.71 4.01 o -10 4 1 859.95 824.45 17.58 o -8 4 1 278.51 233.77 7.06 o -6 4 1 9.69 4.14 2.67 o -4 4 1 3035.70 3187.42 35.29 o -2 4 1 380.01 354.73 7.08 o 0 4 1 2388.38 2417.62 27.35 o 2 4 1 5.00 7.94 2.44 o 4 4 1 78.98 72.48 3.06 o 6 4 1 71.84 63.53 1.96 o 8 4 1 339.05 399.74 9.16 o 10 4 1 473.88 500.62 14.26 o 12 4 1 102.07 91.95 5.90 o 14 4 1 0.14 -5.21 5.21 o 16 4 1 55.77 64.91 8.74 o 18 4 1 138.33 151.28 18.98 o -17 5 1 0.42 -0.71 17.95 o -15 5 1 0.25 -6.65 6.65 o -13 5 1 61.98 53.69 7.06 o -11 5 1 17.53 14.57 5.12 o -9 5 1 22.78 11.58 5.60 o -7 5 1 206.00 192.19 6.98 o -5 5 1 8.05 3.70 5.09 o -3 5 1 1977.34 2052.57 26.24 o -1 5 1 42.98 49.18 3.67 o 1 5 1 31.00 29.42 2.85 o 3 5 1 259.98 250.71 8.45 o 5 5 1 162.33 146.30 8.44 o 7 5 1 9.36 8.05 4.90 o 9 5 1 702.94 710.99 18.00 o 11 5 1 808.85 777.73 20.52 o 13 5 1 975.02 970.70 23.11 o 15 5 1 56.26 64.07 10.54 o 17 5 1 1.42 29.14 16.55 o -14 6 1 0.32 -15.89 15.89 o -12 6 1 8.83 -4.59 12.45 o -10 6 1 170.08 160.60 11.57 o -8 6 1 30.38 26.02 7.21 o -6 6 1 10.41 5.38 6.18 o -4 6 1 416.07 407.05 10.99 o -2 6 1 947.60 1006.76 23.44 o 0 6 1 1079.13 1054.98 25.46 o 2 6 1 930.78 958.94 22.98 o 4 6 1 242.96 252.37 11.61 o 6 6 1 0.84 7.01 6.61 o 8 6 1 63.71 72.50 16.19 o 10 6 1 97.66 113.42 10.97 o 12 6 1 38.41 9.26 9.92 o 14 6 1 188.12 212.19 19.05 o -9 7 1 50.27 58.37 13.34 o -7 7 1 13.02 10.25 11.21 o -5 7 1 58.04 55.30 10.26 o -3 7 1 5.98 3.06 7.84 o -1 7 1 15.76 4.51 7.36 o 1 7 1 14.32 6.20 6.21 o 3 7 1 11.08 11.56 15.21 o 5 7 1 6.13 8.53 11.05 o 7 7 1 25.32 18.30 12.43 o 9 7 1 57.60 39.90 23.28 o -22 0 2 8.39 9.92 13.55 o -20 0 2 205.37 235.08 20.04 o -18 0 2 3584.39 3769.09 88.22 o -16 0 2 17.98 17.20 7.95 o -14 0 2 1181.90 1178.55 26.94 o -12 0 2 821.87 788.85 18.55 o -10 0 2 591.82 606.91 13.33 o -8 0 2 6294.07 6233.43 194.71 o -6 0 2 6439.01 6105.24 99.24 o -4 0 2 2230.29 2162.37 40.50 o 2 0 2 5975.24 5349.73 79.29 o 4 0 2 589.96 802.21 21.78 o 6 0 2 1182.13 1278.36 18.55 o 8 0 2 2438.97 2771.61 45.62 o 10 0 2 66.24 54.74 3.74 o 12 0 2 161.04 151.32 8.72 o 14 0 2 1677.75 1714.11 40.42 o 16 0 2 4.15 11.20 13.34 o 18 0 2 89.58 84.97 10.55 o 20 0 2 41.82 33.45 18.84 o 22 0 2 132.37 122.47 19.89 o -21 1 2 60.47 50.85 9.25 o -19 1 2 493.99 465.09 14.25 o -17 1 2 1717.69 1822.92 33.00 o -15 1 2 38.92 34.13 4.19 o -13 1 2 4279.13 4575.19 62.42 o -11 1 2 6.51 4.34 1.62 o -9 1 2 569.04 484.54 7.17 o -7 1 2 4295.84 4229.34 50.47 o -5 1 2 3299.93 3139.97 34.61 o -1 1 2 28959.56 25419.38 577.85 o 1 1 2 5034.82 4778.90 44.94 o 3 1 2 127.08 127.97 1.62 o 5 1 2 453.52 440.23 4.67 o 7 1 2 950.08 1039.57 10.89 o 9 1 2 6144.61 6589.13 65.20 o 11 1 2 163.68 149.54 4.20 o 13 1 2 1828.98 1849.81 24.05 o 15 1 2 145.66 147.39 9.72 o 17 1 2 35.89 36.78 8.15 o 19 1 2 356.60 366.43 14.02 o 21 1 2 49.88 40.66 10.03 o -22 2 2 149.22 165.23 15.09 o -20 2 2 32.52 30.27 8.55 o -18 2 2 98.56 89.00 8.17 o -16 2 2 55.01 55.86 5.09 o -14 2 2 600.02 589.75 9.37 o -12 2 2 104.93 129.89 5.05 o -10 2 2 639.57 614.15 9.43 o -8 2 2 73.27 62.84 3.07 o -6 2 2 1414.44 1499.12 15.93 o -4 2 2 3013.27 2978.32 37.73 o -2 2 2 234.71 233.98 3.40 o 0 2 2 6218.64 5935.75 59.29 o 2 2 2 7548.68 7596.36 67.22 o 4 2 2 314.32 312.33 3.80 o 6 2 2 1342.33 1298.40 14.34 o 8 2 2 0.37 1.23 1.53 o 10 2 2 2304.61 2255.07 23.86 o 12 2 2 634.10 623.93 10.29 o 14 2 2 796.04 806.37 14.13 o 16 2 2 345.16 376.53 12.44 o 18 2 2 100.77 94.72 9.12 o 20 2 2 0.30 -4.48 8.21 o -21 3 2 3.99 4.92 13.06 o -19 3 2 99.95 123.12 10.22 o -17 3 2 62.25 61.93 6.31 o -15 3 2 53.31 51.01 5.44 o -13 3 2 227.87 199.34 4.73 o -11 3 2 361.79 352.06 11.73 o -9 3 2 8.27 14.01 3.32 o -7 3 2 446.18 590.27 9.86 o -5 3 2 1254.16 1304.06 15.58 o -3 3 2 837.61 885.85 9.14 o -1 3 2 152.47 126.48 2.19 o 1 3 2 1738.38 1809.49 17.34 o 3 3 2 9823.94 10718.92 164.20 o 5 3 2 115.79 73.37 3.08 o 7 3 2 170.24 166.93 3.61 o 9 3 2 338.32 345.91 6.36 o 11 3 2 388.09 420.71 7.94 o 13 3 2 118.80 121.15 6.00 o 15 3 2 2.21 2.27 5.23 o 17 3 2 0.00 -5.28 5.28 o 19 3 2 22.24 25.79 8.99 o -18 4 2 191.93 170.34 15.04 o -16 4 2 120.11 127.77 9.22 o -14 4 2 132.34 117.52 7.99 o -12 4 2 530.41 494.23 14.74 o -10 4 2 403.13 421.71 10.37 o -8 4 2 1.49 2.35 3.25 o -6 4 2 1707.22 1808.37 24.64 o -4 4 2 0.61 -0.93 1.59 o -2 4 2 19.96 15.19 3.66 o 0 4 2 148.20 135.39 3.59 o 2 4 2 182.03 210.34 4.09 o 4 4 2 486.77 483.30 8.34 o 6 4 2 471.23 485.67 11.74 o 8 4 2 17.68 10.80 2.17 o 10 4 2 17.62 20.98 3.97 o 12 4 2 339.94 347.51 9.34 o 14 4 2 1332.45 1420.88 34.65 o 16 4 2 244.26 241.73 12.08 o 18 4 2 20.27 12.31 10.94 o -17 5 2 27.15 6.35 13.99 o -15 5 2 140.74 130.34 12.87 o -13 5 2 10.56 14.65 7.48 o -11 5 2 206.24 211.19 8.45 o -9 5 2 51.58 55.32 5.45 o -7 5 2 552.14 553.05 12.57 o -5 5 2 76.26 66.10 4.13 o -3 5 2 716.05 767.44 11.25 o -1 5 2 3760.15 3980.80 48.84 o 1 5 2 169.31 176.41 4.70 o 3 5 2 99.91 90.35 6.24 o 5 5 2 41.13 28.78 5.12 o 7 5 2 116.07 82.93 8.20 o 9 5 2 154.16 132.40 8.29 o 11 5 2 48.66 46.62 7.16 o 13 5 2 174.30 134.52 10.46 o 15 5 2 174.11 187.64 14.11 o -14 6 2 0.11 9.99 12.57 o -12 6 2 59.38 57.50 12.66 o -10 6 2 39.38 31.12 10.09 o -8 6 2 143.84 155.85 9.82 o -6 6 2 2.45 2.97 10.86 o -4 6 2 515.58 539.81 14.66 o -2 6 2 21.84 24.87 5.72 o 0 6 2 710.51 766.08 20.15 o 2 6 2 1.05 1.29 5.32 o 4 6 2 139.15 134.80 8.18 o 6 6 2 378.02 375.75 15.24 o 8 6 2 189.39 182.45 10.13 o 10 6 2 26.74 27.56 9.16 o 12 6 2 52.59 39.59 12.36 o 14 6 2 67.55 64.73 15.68 o -9 7 2 72.20 69.76 21.53 o -7 7 2 329.89 357.89 19.82 o -5 7 2 18.60 24.14 10.89 o -3 7 2 74.22 58.34 10.35 o -1 7 2 107.26 112.29 9.67 o 1 7 2 65.66 41.05 7.90 o 3 7 2 10.67 17.90 8.10 o 5 7 2 279.49 330.27 18.25 o 7 7 2 7.47 6.03 11.00 o 9 7 2 15.54 22.58 14.07 o -21 1 3 443.06 454.03 21.68 o -19 1 3 47.59 50.34 10.14 o -17 1 3 130.50 130.83 8.65 o -15 1 3 773.06 789.51 17.21 o -13 1 3 102.03 94.24 4.48 o -11 1 3 242.12 244.08 5.73 o -9 1 3 30.43 38.76 3.30 o -7 1 3 0.15 2.75 1.36 o -5 1 3 24533.99 22268.28 386.18 o -3 1 3 714.77 616.55 7.11 o -1 1 3 5021.63 4807.83 57.27 o 1 1 3 247.72 227.06 2.61 o 3 1 3 370.08 364.00 5.33 o 5 1 3 145.43 152.94 2.38 o 7 1 3 1128.27 1150.30 17.78 o 9 1 3 1810.91 1826.32 22.38 o 11 1 3 1290.19 1293.20 16.92 o 13 1 3 337.37 350.08 7.43 o 15 1 3 223.42 212.90 7.53 o 17 1 3 93.47 85.49 6.96 o 19 1 3 20.54 15.73 7.91 o 21 1 3 0.82 11.46 9.68 o -22 2 3 72.81 64.07 14.55 o -20 2 3 0.09 7.56 8.50 o -18 2 3 479.45 501.01 15.67 o -16 2 3 420.75 399.39 11.76 o -14 2 3 24.41 23.52 4.67 o -12 2 3 517.86 463.89 8.92 o -10 2 3 240.38 244.62 5.27 o -8 2 3 542.95 532.69 7.31 o -6 2 3 2050.10 2249.57 25.03 o -4 2 3 711.59 718.81 7.39 o -2 2 3 1272.53 1360.37 14.38 o 0 2 3 3378.98 3487.91 34.68 o 2 2 3 5.13 10.09 0.99 o 4 2 3 2476.53 2527.62 23.59 o 6 2 3 82.68 77.57 2.14 o 8 2 3 1337.21 1265.82 13.21 o 10 2 3 89.84 83.49 3.35 o 12 2 3 453.39 423.84 8.69 o 14 2 3 3405.70 3435.76 45.57 o 16 2 3 768.06 762.84 19.83 o 18 2 3 264.34 275.01 12.43 o 20 2 3 53.39 32.22 11.20 o -21 3 3 21.78 3.47 11.42 o -19 3 3 0.14 10.53 6.74 o -17 3 3 355.04 378.92 18.88 o -15 3 3 25.26 15.08 4.05 o -13 3 3 431.17 414.46 7.96 o -11 3 3 26.56 34.05 7.47 o -9 3 3 353.25 346.75 9.18 o -7 3 3 1686.10 1799.84 26.12 o -5 3 3 1305.92 1290.29 16.66 o -3 3 3 481.92 448.22 6.08 o -1 3 3 65.29 81.13 2.92 o 1 3 3 321.90 299.88 4.17 o 3 3 3 625.71 641.85 7.82 o 5 3 3 138.84 108.33 2.38 o 7 3 3 1.62 -0.83 2.05 o 9 3 3 1214.27 1175.18 15.23 o 11 3 3 314.96 327.20 10.73 o 13 3 3 37.30 28.04 7.49 o 15 3 3 25.12 20.77 5.10 o 17 3 3 264.45 302.14 11.78 o 19 3 3 273.18 259.79 15.08 o -18 4 3 1.00 -9.70 9.70 o -16 4 3 174.08 165.14 10.44 o -14 4 3 96.82 112.90 7.94 o -12 4 3 95.36 125.33 6.88 o -10 4 3 41.54 46.09 4.66 o -8 4 3 2.60 1.18 3.21 o -6 4 3 1050.65 1073.53 15.96 o -4 4 3 2177.69 2178.81 33.76 o -2 4 3 5.62 6.45 0.91 o 0 4 3 1201.10 1302.88 15.24 o 2 4 3 175.72 172.32 3.69 o 4 4 3 500.72 498.28 7.79 o 6 4 3 1562.55 1604.88 19.49 o 8 4 3 110.53 99.00 6.40 o 10 4 3 3539.41 3612.97 63.19 o 12 4 3 544.78 524.77 11.32 o 14 4 3 66.78 61.55 8.05 o 16 4 3 1079.88 1165.12 31.88 o 18 4 3 26.22 9.30 11.12 o -17 5 3 536.11 533.37 25.93 o -15 5 3 587.84 554.00 19.83 o -13 5 3 241.82 230.08 12.53 o -11 5 3 157.99 145.45 14.40 o -9 5 3 659.14 703.18 15.53 o -7 5 3 160.75 154.18 10.17 o -5 5 3 1595.74 1640.61 31.99 o -3 5 3 451.91 484.08 6.85 o -1 5 3 2678.86 2774.72 35.37 o 1 5 3 1143.92 1189.25 17.15 o 3 5 3 372.64 395.45 8.60 o 5 5 3 289.46 328.24 7.84 o 7 5 3 120.87 115.80 5.37 o 9 5 3 251.07 249.85 12.16 o 11 5 3 71.81 102.40 11.38 o 13 5 3 3.89 4.31 7.67 o 15 5 3 0.18 16.89 14.05 o -14 6 3 162.24 193.19 18.19 o -12 6 3 4.54 11.59 9.09 o -10 6 3 45.06 49.07 8.41 o -8 6 3 275.67 275.51 17.18 o -6 6 3 13.02 13.31 6.72 o -4 6 3 992.72 1027.86 28.70 o -2 6 3 930.27 1009.76 26.19 o 0 6 3 7.14 4.64 6.80 o 2 6 3 70.09 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