#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/27/2102772.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102772_Fobs loop_ _publ_author_name 'Bartalucci, Giuditta' 'Coppin, Jennifer' 'Fisher, Stuart' 'Hall, Gillian' 'Helliwell, John R.' 'Helliwell, Madeleine' 'Liaaen-Jensen, Synn\/ove' _publ_section_title ; Unravelling the chemical basis of the bathochromic shift in the lobster carapace; new crystal structures of unbound astaxanthin, canthaxanthin and zeaxanthin ; _journal_coeditor_code BM5041 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 328 _journal_page_last 337 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.746 _cell_angle_gamma 90.000 _cell_length_a 18.5681 _cell_length_b 6.1926 _cell_length_c 19.8034 _exptl_crystal_F_000 816.00 _reflns_d_resolution_high 0.9001 _[local]_cod_data_source_file bm5041axt-PYsup3.hkl _[local]_cod_data_source_block axt-PY #BEGIN Tags that were not found in dictionaries: _shelx_title ' axtbm in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 170.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2320.16 2221.85 214.56 o 4 0 0 10085.90 9868.31 943.84 o 6 0 0 83.43 149.14 31.14 o 8 0 0 210.64 239.49 36.19 o 10 0 0 4173.16 4160.48 310.28 o 12 0 0 1504.18 1627.27 132.65 o 14 0 0 19.46 29.55 33.41 o 16 0 0 288.85 190.93 56.49 o 18 0 0 241.50 269.09 63.59 o 1 1 0 2082.58 1998.03 82.86 o 2 1 0 3548.60 3307.24 193.99 o 3 1 0 6280.96 5935.57 338.20 o 4 1 0 10824.02 10315.03 634.98 o 5 1 0 7.27 -1.85 11.28 o 6 1 0 3050.23 2764.27 176.92 o 7 1 0 484.82 530.29 68.04 o 8 1 0 321.43 376.77 36.85 o 9 1 0 226.34 312.13 31.22 o 10 1 0 653.76 566.42 38.83 o 11 1 0 27.33 41.09 20.91 o 12 1 0 37.48 43.99 22.67 o 13 1 0 34.73 40.63 24.52 o 14 1 0 25.69 -12.68 25.73 o 15 1 0 185.24 190.67 32.78 o 16 1 0 56.70 68.07 32.17 o 17 1 0 11.82 -8.69 37.19 o 18 1 0 24.00 49.51 41.12 o 19 1 0 56.99 61.74 50.61 o 0 2 0 485.54 477.08 31.50 o 1 2 0 272.52 279.34 15.95 o 2 2 0 837.67 829.44 25.71 o 3 2 0 131.92 154.71 16.95 o 4 2 0 165.73 163.63 19.32 o 5 2 0 92.56 66.47 19.35 o 6 2 0 149.94 172.01 23.75 o 7 2 0 1388.53 1277.44 78.57 o 8 2 0 10.35 18.08 19.68 o 9 2 0 27.75 43.00 20.78 o 10 2 0 638.51 611.98 58.06 o 11 2 0 0.27 -11.77 20.76 o 12 2 0 620.40 579.80 36.78 o 13 2 0 373.91 409.16 47.79 o 14 2 0 794.50 766.12 52.60 o 15 2 0 73.93 81.27 39.17 o 16 2 0 63.15 59.45 39.25 o 17 2 0 11.67 20.85 44.64 o 18 2 0 22.08 40.97 41.34 o 1 3 0 578.83 610.39 37.17 o 2 3 0 1062.33 1020.31 37.21 o 3 3 0 44.62 36.95 23.29 o 4 3 0 71.47 41.62 23.61 o 5 3 0 159.70 138.93 23.20 o 6 3 0 637.84 649.37 29.73 o 7 3 0 21.27 15.46 19.06 o 8 3 0 9.67 -0.67 29.17 o 9 3 0 63.36 63.22 29.80 o 10 3 0 251.98 313.70 45.74 o 11 3 0 2128.09 2050.71 78.58 o 12 3 0 832.46 731.68 53.00 o 13 3 0 295.19 359.32 47.92 o 14 3 0 4.66 27.23 38.80 o 15 3 0 64.97 72.28 41.37 o 16 3 0 0.00 -15.45 39.99 o 17 3 0 0.42 -6.38 41.44 o 0 4 0 430.23 392.14 47.02 o 1 4 0 66.50 63.70 20.60 o 2 4 0 247.59 245.92 24.67 o 3 4 0 234.29 249.85 27.93 o 4 4 0 3.73 -1.57 28.07 o 5 4 0 97.67 123.62 32.28 o 6 4 0 151.65 140.49 34.48 o 7 4 0 127.88 101.20 35.36 o 8 4 0 138.18 126.03 37.02 o 9 4 0 234.83 215.20 42.91 o 10 4 0 7.49 -4.40 36.14 o 11 4 0 34.15 23.88 36.81 o 12 4 0 138.83 157.85 43.29 o 13 4 0 36.56 22.71 40.17 o 14 4 0 49.47 65.31 42.28 o 15 4 0 2.88 6.86 39.99 o 1 5 0 431.06 445.14 37.61 o 2 5 0 44.91 63.07 35.87 o 3 5 0 9.01 -9.32 35.09 o 4 5 0 268.29 222.21 41.08 o 5 5 0 413.25 481.52 48.51 o 6 5 0 1.92 -16.71 34.29 o 7 5 0 5.83 -6.32 35.84 o 8 5 0 11.67 -33.24 36.33 o 9 5 0 14.91 27.94 39.23 o 10 5 0 1.71 -1.48 38.65 o 11 5 0 31.95 78.08 41.45 o 12 5 0 7.98 -17.02 40.83 o 13 5 0 42.07 38.59 43.33 o 0 6 0 0.28 8.44 93.99 o 1 6 0 2.07 13.10 49.55 o 2 6 0 3.37 17.14 58.62 o 3 6 0 6.00 17.32 48.44 o 4 6 0 54.31 83.61 41.82 o 5 6 0 39.94 26.69 40.18 o 6 6 0 20.55 32.37 40.67 o 7 6 0 20.13 62.61 42.17 o 8 6 0 63.40 48.85 41.79 o 9 6 0 11.92 7.01 40.60 o -19 0 1 144.34 171.19 87.14 o -17 0 1 247.95 180.91 58.21 o -15 0 1 96.83 106.14 40.29 o -13 0 1 178.10 184.67 34.95 o -11 0 1 441.08 538.57 54.60 o -9 0 1 264.42 235.44 34.16 o -7 0 1 117.57 137.61 23.29 o -5 0 1 812.43 703.75 74.83 o -3 0 1 1079.05 998.94 105.30 o 1 0 1 4000.40 4274.41 41.17 o 3 0 1 7060.47 7098.71 522.95 o 5 0 1 1409.11 1283.08 110.27 o 7 0 1 643.98 672.18 75.39 o 9 0 1 3.42 8.69 27.69 o 11 0 1 1071.52 1110.97 92.33 o 13 0 1 18.81 47.26 32.07 o 15 0 1 45.64 40.68 37.78 o 17 0 1 32.75 78.81 53.85 o 19 0 1 60.09 82.91 58.25 o -19 1 1 10.08 19.96 49.59 o -18 1 1 259.23 163.69 62.54 o -17 1 1 380.19 408.52 47.96 o -16 1 1 1140.43 1257.73 64.80 o -15 1 1 324.72 335.82 36.00 o -14 1 1 44.42 6.78 24.86 o -13 1 1 62.20 86.30 25.34 o -12 1 1 24.66 23.38 22.04 o -11 1 1 63.85 75.87 22.42 o -10 1 1 132.49 105.79 22.55 o -9 1 1 1046.16 1032.52 83.09 o -8 1 1 151.24 228.10 26.10 o -7 1 1 502.68 503.56 37.63 o -6 1 1 575.92 541.23 29.82 o -5 1 1 149.05 154.04 14.10 o -4 1 1 8896.15 8076.21 466.03 o -3 1 1 377.46 403.71 22.60 o -2 1 1 773.63 758.05 56.79 o -1 1 1 4462.32 4102.45 233.25 o 0 1 1 2803.87 2581.75 87.19 o 1 1 1 4.78 -9.66 9.66 o 2 1 1 3693.34 3444.35 214.89 o 3 1 1 10732.05 10558.74 701.25 o 4 1 1 3135.78 3118.76 195.31 o 5 1 1 233.31 248.29 26.43 o 6 1 1 346.43 397.76 36.02 o 7 1 1 1276.73 1200.68 73.88 o 8 1 1 971.38 991.55 71.23 o 9 1 1 1135.69 1076.06 63.51 o 10 1 1 147.84 171.58 22.81 o 11 1 1 0.02 -0.56 19.66 o 12 1 1 0.60 -1.54 20.71 o 13 1 1 39.28 40.63 26.53 o 14 1 1 105.30 109.30 30.41 o 15 1 1 272.10 277.40 35.75 o 16 1 1 7.12 -28.60 28.60 o 17 1 1 1.17 -8.83 36.76 o 18 1 1 2.32 -9.26 37.54 o 19 1 1 173.73 155.61 53.59 o -19 2 1 75.32 55.10 43.58 o -18 2 1 11.75 42.32 40.99 o -17 2 1 82.09 97.63 41.14 o -16 2 1 0.12 -2.46 37.65 o -15 2 1 0.01 -1.03 36.54 o -14 2 1 23.72 31.55 36.76 o -13 2 1 358.83 435.38 45.79 o -12 2 1 32.48 5.48 31.00 o -11 2 1 506.56 505.21 46.47 o -10 2 1 257.69 245.82 24.95 o -9 2 1 321.12 334.00 25.70 o -8 2 1 270.69 299.33 25.34 o -7 2 1 811.60 744.28 53.88 o -6 2 1 708.35 697.78 46.58 o -5 2 1 6163.18 5854.18 315.62 o -4 2 1 2495.13 2339.15 103.98 o -3 2 1 5035.67 4541.08 279.41 o -2 2 1 108.11 118.33 16.61 o -1 2 1 890.86 784.27 29.17 o 0 2 1 83.23 82.15 12.89 o 1 2 1 150.51 175.40 15.64 o 2 2 1 275.81 311.61 17.48 o 3 2 1 110.93 109.16 18.73 o 4 2 1 166.50 168.15 20.20 o 5 2 1 67.40 50.79 21.62 o 6 2 1 10.65 13.74 21.79 o 7 2 1 46.58 24.37 21.52 o 8 2 1 208.89 283.30 32.23 o 9 2 1 370.93 431.66 31.49 o 10 2 1 3.75 -4.70 21.53 o 11 2 1 716.00 606.51 48.69 o 12 2 1 268.75 282.89 32.03 o 13 2 1 1332.95 1368.06 72.36 o 14 2 1 441.70 473.83 48.25 o 15 2 1 476.92 480.15 59.62 o 16 2 1 10.57 10.75 37.58 o 17 2 1 0.97 14.51 39.18 o 18 2 1 88.85 59.91 42.31 o -17 3 1 10.53 14.31 40.44 o -16 3 1 52.28 53.16 42.30 o -15 3 1 0.01 16.41 38.32 o -14 3 1 98.49 80.83 48.15 o -13 3 1 51.57 55.72 38.96 o -12 3 1 114.11 100.43 39.72 o -11 3 1 63.05 86.28 35.73 o -10 3 1 99.50 96.58 32.32 o -9 3 1 27.32 39.43 29.77 o -8 3 1 111.30 99.39 30.91 o -7 3 1 494.04 549.18 47.81 o -6 3 1 388.18 409.17 26.64 o -5 3 1 25.12 5.37 19.73 o -4 3 1 372.60 467.69 40.96 o -3 3 1 907.52 808.59 32.74 o -2 3 1 21.54 20.13 20.97 o -1 3 1 26.91 16.22 21.31 o 0 3 1 1204.69 1217.66 48.82 o 1 3 1 1528.78 1481.91 57.31 o 2 3 1 37.97 59.12 26.13 o 3 3 1 764.12 726.08 33.20 o 4 3 1 44.04 26.34 21.83 o 5 3 1 259.20 305.90 35.93 o 6 3 1 15.24 -5.55 25.18 o 7 3 1 0.13 4.73 18.89 o 8 3 1 35.41 26.05 21.06 o 9 3 1 1.33 1.58 28.65 o 10 3 1 280.77 317.71 41.21 o 11 3 1 70.07 88.01 37.06 o 12 3 1 1615.07 1630.09 114.75 o 13 3 1 26.79 45.78 38.99 o 14 3 1 69.09 55.75 39.85 o 15 3 1 0.20 -11.20 39.48 o 16 3 1 1.03 1.83 39.57 o 17 3 1 0.50 -30.67 39.68 o -16 4 1 22.24 42.78 43.19 o -15 4 1 70.06 7.92 41.83 o -14 4 1 206.62 231.70 45.32 o -13 4 1 54.75 16.94 37.09 o -12 4 1 0.18 8.82 36.72 o -11 4 1 3.55 1.02 36.60 o -10 4 1 266.88 380.16 53.55 o -9 4 1 869.26 843.88 56.09 o -8 4 1 22.81 38.93 34.63 o -7 4 1 16.82 2.71 31.81 o -6 4 1 0.00 -10.80 29.44 o -5 4 1 26.55 25.29 29.19 o -4 4 1 491.38 514.36 40.14 o -3 4 1 117.15 115.99 24.49 o -2 4 1 56.80 58.25 19.84 o -1 4 1 0.68 6.08 18.61 o 0 4 1 20.44 7.51 18.92 o 1 4 1 59.21 94.91 21.75 o 2 4 1 329.27 367.49 27.65 o 3 4 1 926.81 861.14 31.23 o 4 4 1 27.33 26.55 22.75 o 5 4 1 182.52 200.59 34.38 o 6 4 1 8.89 5.79 29.98 o 7 4 1 3.40 2.01 32.26 o 8 4 1 1862.45 1820.29 107.50 o 9 4 1 230.53 191.33 41.88 o 10 4 1 7.40 1.89 37.36 o 11 4 1 6.42 19.30 36.63 o 12 4 1 23.02 9.50 38.78 o 13 4 1 11.00 26.63 40.89 o 14 4 1 39.19 69.16 42.42 o 15 4 1 3.37 15.37 40.27 o -13 5 1 1.99 12.98 39.90 o -12 5 1 31.71 49.19 40.87 o -11 5 1 3.78 15.01 41.04 o -10 5 1 3.79 -22.42 38.11 o -9 5 1 0.41 24.14 37.11 o -8 5 1 0.10 5.01 36.58 o -7 5 1 169.65 195.81 42.89 o -6 5 1 511.30 544.97 50.11 o -5 5 1 54.18 59.84 38.46 o -4 5 1 10.56 7.96 35.59 o -3 5 1 24.91 -6.35 35.11 o -2 5 1 117.96 109.08 41.00 o -1 5 1 81.93 57.13 28.97 o 0 5 1 453.26 441.11 32.84 o 1 5 1 0.11 -1.44 23.98 o 2 5 1 34.56 49.75 35.25 o 3 5 1 6.65 -4.84 32.90 o 4 5 1 8.94 -6.84 34.75 o 5 5 1 493.01 487.16 65.11 o 6 5 1 2.33 20.64 36.74 o 7 5 1 12.30 15.83 37.40 o 8 5 1 13.40 30.21 38.58 o 9 5 1 1.39 -4.76 38.36 o 10 5 1 1.52 17.62 40.26 o 11 5 1 4.79 14.68 42.18 o 12 5 1 40.07 35.25 43.01 o 13 5 1 1.59 -40.92 41.01 o -9 6 1 6.45 4.30 41.00 o -8 6 1 14.72 0.11 40.84 o -7 6 1 1.01 3.81 39.30 o -6 6 1 79.35 79.59 42.01 o -5 6 1 19.32 31.68 40.12 o -4 6 1 9.74 -10.24 38.12 o -3 6 1 0.19 0.20 38.05 o -2 6 1 171.10 223.77 67.41 o -1 6 1 0.01 -10.96 50.32 o 0 6 1 13.69 69.31 67.86 o 1 6 1 352.18 320.32 59.67 o 2 6 1 250.66 254.62 69.05 o 3 6 1 11.19 -7.66 47.60 o 4 6 1 13.52 24.96 37.94 o 5 6 1 9.98 -8.24 38.00 o 6 6 1 0.00 -11.52 38.23 o 7 6 1 16.27 16.14 41.31 o 8 6 1 7.59 -6.73 40.75 o 9 6 1 181.58 201.93 48.76 o -20 0 2 74.37 24.55 98.19 o -18 0 2 7.28 -29.03 51.28 o -16 0 2 454.99 462.76 66.50 o -14 0 2 20.45 51.62 33.85 o -12 0 2 547.45 561.36 41.20 o -10 0 2 166.55 210.69 40.52 o -8 0 2 1128.89 1095.53 102.59 o -6 0 2 4170.77 4008.60 335.66 o -4 0 2 547.29 468.37 42.63 o -2 0 2 109.80 143.46 18.58 o 0 0 2 2319.96 2611.04 124.50 o 2 0 2 3456.64 3318.16 49.80 o 4 0 2 28501.43 30632.40 1970.22 o 6 0 2 607.86 556.33 30.56 o 8 0 2 568.42 586.87 39.69 o 10 0 2 22.47 21.08 26.11 o 12 0 2 133.61 195.51 35.96 o 14 0 2 244.20 208.50 53.01 o 16 0 2 18.39 -15.44 47.59 o 18 0 2 27.94 31.89 53.60 o -19 1 2 95.15 26.45 51.70 o -18 1 2 39.04 22.33 46.01 o -17 1 2 217.25 241.08 45.06 o -16 1 2 33.19 21.87 36.96 o -15 1 2 70.75 34.64 28.68 o -14 1 2 370.03 364.09 50.49 o -13 1 2 2.48 -21.94 21.94 o -12 1 2 44.96 70.16 23.11 o -11 1 2 37.28 40.66 21.13 o -10 1 2 187.16 230.44 26.30 o -9 1 2 1800.29 1739.92 100.48 o -8 1 2 356.60 399.17 32.12 o -7 1 2 0.29 2.18 17.05 o -6 1 2 69.48 72.73 14.45 o -5 1 2 254.05 262.41 26.29 o -4 1 2 6427.46 6211.93 325.05 o -3 1 2 17550.42 17260.51 1272.61 o -2 1 2 6186.12 6026.40 598.06 o -1 1 2 719.62 646.81 33.08 o 0 1 2 2055.13 1981.93 65.08 o 1 1 2 231.48 231.02 14.04 o 2 1 2 2576.09 2397.86 127.01 o 3 1 2 3958.28 3843.77 206.31 o 4 1 2 176.81 204.52 14.88 o 5 1 2 1362.86 1226.81 57.74 o 6 1 2 106.62 123.39 19.98 o 7 1 2 6.37 0.27 20.63 o 8 1 2 339.05 308.33 26.17 o 9 1 2 160.45 198.42 23.64 o 10 1 2 207.72 235.58 24.42 o 11 1 2 0.01 8.20 20.27 o 12 1 2 85.50 90.50 23.83 o 13 1 2 116.50 97.76 28.07 o 14 1 2 57.00 61.80 28.74 o 15 1 2 268.34 233.13 35.86 o 16 1 2 7.31 9.63 29.84 o 17 1 2 133.84 110.87 41.00 o 18 1 2 10.82 -33.83 43.21 o -19 2 2 324.29 451.34 53.84 o -18 2 2 252.46 269.36 48.54 o -17 2 2 46.66 35.53 39.85 o -16 2 2 77.91 85.56 40.55 o -15 2 2 231.90 212.69 43.38 o -14 2 2 72.85 26.70 37.18 o -13 2 2 29.10 -8.22 32.06 o -12 2 2 11.74 1.06 30.09 o -11 2 2 71.33 58.44 29.43 o -10 2 2 5.25 8.25 17.19 o -9 2 2 317.80 350.47 25.92 o -8 2 2 2005.91 1759.73 134.09 o -7 2 2 205.96 286.05 35.53 o -6 2 2 818.65 780.72 48.51 o -5 2 2 28.04 36.38 26.26 o -4 2 2 222.12 267.13 26.43 o -3 2 2 381.97 386.94 32.47 o -2 2 2 518.00 471.21 27.43 o -1 2 2 1148.92 1098.50 43.44 o 0 2 2 3.26 17.14 12.96 o 1 2 2 372.55 394.97 19.34 o 2 2 2 9.80 8.96 13.34 o 3 2 2 586.78 577.53 23.44 o 4 2 2 1712.61 1548.60 100.14 o 5 2 2 696.91 736.23 50.46 o 6 2 2 2105.96 2029.28 145.79 o 7 2 2 6.34 8.37 21.37 o 8 2 2 261.67 259.56 26.53 o 9 2 2 7.69 7.52 20.61 o 10 2 2 16.39 26.36 22.24 o 11 2 2 153.82 124.80 27.32 o 12 2 2 307.19 349.68 34.63 o 13 2 2 1.26 5.01 27.11 o 14 2 2 397.09 425.02 47.20 o 15 2 2 569.92 664.04 75.28 o 16 2 2 48.22 58.97 38.90 o 17 2 2 1.21 -13.39 44.54 o 18 2 2 60.20 72.31 46.84 o -18 3 2 2.83 -9.61 39.49 o -17 3 2 15.81 0.76 41.89 o -16 3 2 22.05 16.73 39.69 o -15 3 2 3.41 -22.01 37.83 o -14 3 2 302.36 316.52 47.01 o -13 3 2 129.96 127.63 40.60 o -12 3 2 0.62 -30.89 35.05 o -11 3 2 325.10 399.59 43.52 o -10 3 2 36.26 52.62 31.47 o -9 3 2 107.94 119.05 32.88 o -8 3 2 267.45 266.35 40.63 o -7 3 2 198.90 229.09 33.15 o -6 3 2 384.82 460.24 37.42 o -5 3 2 1048.17 1028.34 83.59 o -4 3 2 1625.58 1540.11 127.11 o -3 3 2 520.70 539.10 49.94 o -2 3 2 56.76 68.62 21.57 o -1 3 2 0.03 9.23 20.81 o 0 3 2 1541.37 1564.42 65.17 o 1 3 2 142.34 140.71 24.24 o 2 3 2 1641.12 1578.24 68.01 o 3 3 2 26.47 -0.74 20.16 o 4 3 2 45.97 48.04 22.80 o 5 3 2 196.22 192.73 25.12 o 6 3 2 5.47 8.33 20.51 o 7 3 2 22.58 22.14 21.71 o 8 3 2 288.12 289.27 29.61 o 9 3 2 6.97 14.29 30.67 o 10 3 2 1.59 -21.06 32.30 o 11 3 2 573.58 700.58 59.20 o 12 3 2 343.58 451.00 55.91 o 13 3 2 11.33 17.13 38.76 o 14 3 2 51.14 90.39 41.61 o 15 3 2 61.68 84.75 42.60 o 16 3 2 14.84 26.86 41.94 o 17 3 2 29.97 75.12 50.45 o -16 4 2 92.76 116.68 45.95 o -15 4 2 14.39 2.76 40.58 o -14 4 2 137.29 194.66 45.00 o -13 4 2 0.04 -9.19 36.22 o -12 4 2 1.08 14.61 37.67 o -11 4 2 10.10 18.42 35.90 o -10 4 2 681.36 722.91 63.56 o -9 4 2 29.89 23.30 35.85 o -8 4 2 289.10 273.35 41.79 o -7 4 2 153.73 150.58 36.09 o -6 4 2 29.39 1.06 29.83 o -5 4 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