#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:59:25 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180888 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/28/2102897.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102897_Fobs loop_ _publ_author_name 'Gelbrich, Thomas' 'Hursthouse, Michael B.' 'Threlfall, Terence L.' _publ_section_title ; Structural systematics of 4,4'-disubstituted benzenesulfonamidobenzenes. 1. Overview and dimer-based isostructures ; _journal_coeditor_code BM5045 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 621 _journal_page_last 632 _journal_volume 63 _journal_year 2007 _space_group_IT_number 148 _symmetry_space_group_name_Hall '-R 3' _symmetry_space_group_name_H-M 'R -3 :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 27.4403 _cell_length_b 27.4403 _cell_length_c 9.5034 _exptl_crystal_F_000 2916.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file bm5045F~CF3sup16.hkl _cod_data_source_block F~CF3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' s92 in R-3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 544.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -2 4 0 316.85 267.88 26.03 o -1 5 0 2946.03 2508.33 178.39 o -3 6 0 65744.11 61534.47 2106.81 o 0 6 0 76925.49 75394.83 879.14 o -5 7 0 32395.43 31462.32 325.56 o -2 7 0 1879.82 1531.60 19.06 o -7 8 0 9456.91 8344.16 107.15 o -4 8 0 25152.44 23048.46 203.35 o -1 8 0 8419.63 8062.26 386.60 o -6 9 0 4011.37 3570.79 38.68 o -3 9 0 9972.95 10145.74 100.90 o -8 10 0 1021.09 1081.92 18.40 o -5 10 0 44109.83 41380.89 363.47 o -2 10 0 8742.07 9288.03 128.28 o -10 11 0 350.19 300.03 9.15 o -7 11 0 2572.70 2232.50 30.65 o -4 11 0 443.94 346.01 11.22 o -1 11 0 91.62 66.16 11.46 o -9 12 0 26540.11 28868.30 309.70 o -6 12 0 7067.84 6513.75 82.34 o -3 12 0 224.91 291.87 11.93 o 0 12 0 13501.52 12547.62 152.45 o -11 13 0 923.20 1040.73 26.87 o -8 13 0 17.56 0.00 10.85 o -5 13 0 5865.26 5383.87 60.03 o -2 13 0 3126.76 3200.92 77.48 o -13 14 0 383.46 374.14 17.48 o -10 14 0 7083.89 7866.19 76.66 o -7 14 0 10304.41 10209.30 110.60 o -4 14 0 1040.59 949.32 23.28 o -1 14 0 2067.09 2072.64 42.29 o -12 15 0 8340.97 8303.71 78.89 o -9 15 0 742.86 545.16 15.46 o -6 15 0 1.37 19.38 8.55 o -3 15 0 13.62 6.09 20.24 o 0 15 0 95.34 103.54 12.36 o -14 16 0 14489.66 15589.07 209.22 o -11 16 0 4095.00 4336.98 62.00 o -8 16 0 7894.37 8109.25 126.10 o -5 16 0 4.70 22.10 29.33 o -2 16 0 1832.14 1824.56 58.87 o -16 17 0 5954.78 6546.35 111.97 o -13 17 0 7385.42 8004.59 95.40 o -10 17 0 1168.03 941.02 18.08 o -7 17 0 2890.61 3113.93 53.10 o -4 17 0 1350.80 1370.68 45.99 o -1 17 0 582.95 538.89 21.82 o -15 18 0 445.68 418.38 19.84 o -12 18 0 280.83 211.80 11.83 o -9 18 0 186.00 238.26 16.65 o -6 18 0 188.53 145.87 23.47 o -3 18 0 142.49 129.97 29.31 o 0 18 0 1382.92 1411.83 43.23 o -17 19 0 1241.69 1545.73 41.77 o -14 19 0 2062.41 1774.67 34.39 o -11 19 0 7088.91 7236.63 102.00 o -8 19 0 901.04 894.30 37.83 o -5 19 0 702.21 630.29 36.99 o -2 19 0 1625.27 1716.30 65.92 o -19 20 0 451.67 381.72 21.06 o -16 20 0 5.33 0.00 12.63 o -13 20 0 1252.60 1325.34 22.52 o -10 20 0 710.08 640.43 37.10 o -7 20 0 8153.00 8818.34 190.76 o -4 20 0 1706.37 1797.72 59.31 o -1 20 0 56.85 56.94 15.17 o -18 21 0 37.69 26.81 21.89 o -15 21 0 2072.63 2454.31 46.43 o -12 21 0 39.12 34.86 14.03 o -9 21 0 3337.50 3863.90 87.97 o -6 21 0 1000.46 1085.64 49.34 o -3 21 0 87.96 107.75 32.00 o 0 21 0 5403.90 5823.76 127.77 o -20 22 0 665.18 728.80 33.96 o -17 22 0 153.32 226.96 23.71 o -14 22 0 1570.65 1352.98 26.63 o -11 22 0 1538.28 1369.57 49.87 o -8 22 0 2759.90 2945.87 88.27 o -5 22 0 2491.84 2922.69 96.66 o -2 22 0 428.27 628.45 46.33 o -22 23 0 2174.75 2388.67 76.16 o -19 23 0 6.49 23.92 15.79 o -16 23 0 916.23 872.24 22.73 o -13 23 0 360.57 394.71 24.19 o -10 23 0 1626.62 1533.41 52.01 o -7 23 0 1777.59 1783.22 79.90 o -4 23 0 1037.48 1197.30 58.02 o -1 23 0 299.33 226.22 32.90 o -21 24 0 6365.25 6939.33 162.92 o -18 24 0 5.35 1.35 13.32 o -15 24 0 1148.01 965.18 34.82 o -12 24 0 1466.17 1648.27 66.71 o -9 24 0 160.27 142.54 33.40 o -6 24 0 527.70 296.29 44.90 o -3 24 0 2503.34 2404.06 80.65 o 0 24 0 127.75 139.58 22.89 o -23 25 0 0.80 0.00 24.69 o -20 25 0 503.03 541.87 42.67 o -17 25 0 2464.03 2281.79 48.13 o -14 25 0 1229.02 1123.95 39.33 o -11 25 0 545.34 512.71 28.76 o -8 25 0 140.10 171.58 43.34 o -5 25 0 480.82 421.83 48.46 o -2 25 0 141.99 162.28 41.12 o -25 26 0 0.20 0.00 20.63 o -22 26 0 787.57 820.30 65.68 o -19 26 0 2.24 1.85 13.34 o -16 26 0 2059.60 1987.28 71.05 o -13 26 0 225.49 264.08 25.33 o -10 26 0 392.00 270.74 48.96 o -7 26 0 54.79 54.60 40.49 o -4 26 0 1505.30 1691.97 75.29 o -1 26 0 4.83 48.93 46.33 o -24 27 0 29.43 0.50 23.91 o -21 27 0 156.59 176.34 20.67 o -18 27 0 983.47 956.89 42.61 o -15 27 0 23.23 23.32 42.74 o -12 27 0 1048.00 936.53 56.97 o -9 27 0 19.19 0.00 49.33 o -6 27 0 36.65 37.60 38.43 o -3 27 0 947.57 966.90 69.16 o 0 27 0 627.50 564.60 54.13 o -26 28 0 253.11 192.90 50.39 o -23 28 0 1463.87 1567.18 53.17 o -20 28 0 99.19 111.86 11.75 o -17 28 0 340.33 368.42 25.22 o -14 28 0 924.28 892.91 54.23 o -11 28 0 3119.84 3446.75 133.34 o -8 28 0 1388.86 1461.81 80.18 o -5 28 0 2.58 41.12 64.43 o -2 28 0 159.86 140.66 42.41 o -28 29 0 281.31 375.31 137.77 o -25 29 0 6.57 0.00 47.78 o -22 29 0 7.81 13.97 19.40 o -19 29 0 167.00 150.95 26.58 o -16 29 0 118.98 84.53 24.44 o -13 29 0 459.79 513.26 48.57 o -10 29 0 48.63 62.59 36.54 o -7 29 0 21.12 53.76 54.61 o -4 29 0 416.48 377.00 133.38 o -27 30 0 117.80 114.56 93.97 o -24 30 0 36.66 129.95 64.17 o -21 30 0 8.52 20.47 39.21 o -18 30 0 146.24 178.21 38.02 o -15 30 0 247.46 273.26 28.65 o -12 30 0 13.99 0.00 49.92 o -9 30 0 201.70 160.52 49.56 o -6 30 0 34.46 0.00 58.70 o -3 30 0 10.77 2.40 72.17 o -26 31 0 832.02 941.48 118.21 o -23 31 0 24.97 99.56 60.58 o -20 31 0 109.73 137.47 46.67 o -17 31 0 5.78 18.68 40.91 o -14 31 0 987.76 996.01 71.18 o -11 31 0 235.19 330.67 68.43 o -8 31 0 7.62 3.38 52.20 o -5 31 0 1.02 32.59 76.37 o -25 32 0 124.00 0.00 73.57 o -22 32 0 154.00 165.95 68.18 o -19 32 0 9.41 137.54 60.17 o -16 32 0 21.01 48.78 68.77 o -10 32 0 147.37 139.75 61.78 o -7 32 0 212.57 328.62 61.43 o -18 33 0 113.00 224.92 104.76 o -3 2 1 29012.04 22832.83 989.70 o -5 3 1 227690.33 62595.51 77446.77 o 1 3 1 93345.89 89322.75 5316.24 o -7 4 1 5045.19 4962.24 48.53 o -4 4 1 2267.97 2317.11 141.39 o -1 4 1 28.80 0.00 16.22 o 2 4 1 16780.98 15893.75 144.12 o -9 5 1 14136.62 14335.41 136.08 o -6 5 1 18802.29 17007.75 143.29 o -3 5 1 231078.72 237832.81 5738.64 o 0 5 1 159375.39 157409.23 2977.68 o 3 5 1 2884.10 2902.38 30.32 o -11 6 1 6657.55 7415.60 67.06 o -8 6 1 2509.59 2574.81 37.74 o -5 6 1 41311.66 40315.30 434.91 o -2 6 1 3399.70 3072.08 34.71 o 1 6 1 2757.49 2833.68 36.39 o 4 6 1 1479.97 1451.63 20.81 o -13 7 1 1358.27 1050.62 17.48 o -10 7 1 14084.94 12532.16 125.47 o -7 7 1 12154.83 11187.47 108.34 o -4 7 1 35093.96 32971.39 330.96 o 2 7 1 74510.13 73566.75 1167.69 o 5 7 1 4636.52 4450.38 42.13 o -15 8 1 389.05 466.20 12.47 o -12 8 1 3414.94 3823.31 39.11 o -9 8 1 3948.50 3935.97 43.10 o -6 8 1 73652.99 73367.60 875.85 o -3 8 1 2460.72 2000.81 20.15 o 0 8 1 1371.84 1459.20 23.11 o 3 8 1 30182.82 27997.01 252.85 o 6 8 1 11453.82 11422.55 97.77 o -17 9 1 668.29 639.72 14.88 o -14 9 1 3628.57 3712.82 41.28 o -11 9 1 13994.25 14088.34 122.32 o -8 9 1 364.16 423.60 13.75 o -5 9 1 4644.18 5125.27 50.49 o -2 9 1 3633.22 3097.72 30.98 o 1 9 1 54.77 50.16 12.44 o 4 9 1 23542.29 26428.80 253.51 o 7 9 1 3503.34 3577.63 73.44 o -19 10 1 133.73 123.90 15.70 o -16 10 1 31.24 28.18 13.59 o -13 10 1 4813.42 4579.02 45.24 o -10 10 1 38.15 0.00 12.37 o -7 10 1 2246.50 2791.69 35.04 o -1 10 1 4069.23 3356.67 43.46 o 2 10 1 2278.07 2357.54 48.95 o 5 10 1 5151.05 5509.29 84.45 o 8 10 1 3913.44 3838.68 65.31 o -21 11 1 3782.32 3978.75 83.23 o -18 11 1 1260.27 1301.90 38.95 o -15 11 1 8133.03 8735.04 120.53 o -12 11 1 6046.53 6435.70 74.90 o -9 11 1 1086.48 1219.87 35.32 o -6 11 1 12839.18 13272.36 153.05 o -3 11 1 3346.32 3388.89 37.14 o 0 11 1 1590.62 1596.58 40.51 o 3 11 1 1407.11 1482.05 27.71 o 6 11 1 9172.36 10079.51 117.60 o 9 11 1 161.14 210.01 7.52 o -23 12 1 785.16 715.45 25.71 o -20 12 1 535.21 521.91 24.27 o -17 12 1 941.84 853.73 21.92 o -14 12 1 4454.39 4436.36 52.87 o -11 12 1 7020.78 7429.96 81.58 o -8 12 1 16374.22 17638.58 194.99 o -5 12 1 530.00 490.16 24.19 o -2 12 1 701.84 564.98 20.88 o 1 12 1 600.37 627.26 28.97 o 4 12 1 427.18 553.04 21.97 o 7 12 1 626.59 598.29 16.68 o 10 12 1 105.06 104.11 13.74 o -25 13 1 5035.82 5509.49 118.67 o -22 13 1 714.35 622.09 27.63 o -19 13 1 56.32 60.76 22.45 o -16 13 1 1119.28 1016.23 33.84 o -13 13 1 19.55 21.31 9.43 o -10 13 1 15074.75 16287.77 204.62 o -7 13 1 12848.09 13318.11 124.37 o -4 13 1 23204.99 24083.72 290.87 o -1 13 1 4123.00 4797.42 57.63 o 2 13 1 5308.55 5751.02 98.16 o 5 13 1 160.24 183.88 12.07 o 8 13 1 197.23 238.26 13.09 o 11 13 1 178.29 217.84 19.99 o -27 14 1 420.78 377.80 38.69 o -24 14 1 45.69 44.69 19.22 o -21 14 1 1816.04 1851.61 46.99 o -18 14 1 2083.13 2024.34 41.36 o -15 14 1 142.84 106.18 9.62 o -12 14 1 1251.33 1134.49 27.41 o -9 14 1 940.95 735.42 19.83 o -6 14 1 1628.51 1722.88 30.62 o -3 14 1 4743.84 5440.41 65.68 o 0 14 1 5283.41 5819.03 95.03 o 3 14 1 8480.42 9054.06 165.86 o 6 14 1 4.76 6.27 10.40 o 9 14 1 1.83 4.70 6.20 o 12 14 1 808.87 809.91 46.23 o -29 15 1 28.47 67.28 30.12 o -26 15 1 439.56 383.40 41.43 o -23 15 1 5034.38 5349.92 135.23 o -20 15 1 1142.79 910.89 32.91 o -17 15 1 505.10 479.58 13.26 o -14 15 1 3630.36 3354.34 41.78 o -11 15 1 5060.64 4994.46 68.26 o -8 15 1 18927.75 18873.37 282.19 o -5 15 1 3600.97 3676.51 53.90 o -2 15 1 11835.24 11923.05 238.09 o 1 15 1 1126.11 1016.80 39.83 o 4 15 1 470.88 381.08 42.25 o 7 15 1 76.04 47.10 13.59 o 10 15 1 269.71 257.61 18.65 o 13 15 1 205.62 279.22 26.88 o -31 16 1 207.27 224.54 76.98 o -28 16 1 159.98 125.64 39.30 o -25 16 1 1904.69 2111.84 199.62 o -22 16 1 3038.42 3011.19 76.31 o -19 16 1 2307.13 2336.02 40.44 o -16 16 1 2049.63 2169.26 35.38 o -13 16 1 2720.01 3107.13 51.28 o -10 16 1 45.09 42.16 11.82 o -7 16 1 3363.42 3444.66 53.33 o -4 16 1 317.85 326.50 24.15 o -1 16 1 5542.72 5686.48 94.84 o 2 16 1 43.08 30.75 25.91 o 5 16 1 4595.63 4547.14 99.56 o 8 16 1 2508.28 2255.02 49.55 o 11 16 1 92.07 59.44 17.44 o 14 16 1 97.96 117.82 40.13 o -33 17 1 316.43 369.92 97.58 o -30 17 1 6.03 46.01 33.49 o -27 17 1 754.94 853.08 56.62 o -24 17 1 158.91 217.96 33.74 o -21 17 1 7708.71 8304.43 282.11 o -18 17 1 1990.28 2015.42 37.45 o -15 17 1 3932.12 4175.84 54.55 o -12 17 1 17789.62 17976.87 204.94 o -9 17 1 4587.26 5216.86 75.67 o -6 17 1 3075.63 2864.47 43.95 o -3 17 1 1208.23 1223.55 55.90 o 0 17 1 0.18 0.00 11.67 o 3 17 1 1021.73 978.02 45.13 o 6 17 1 5010.72 5193.54 114.17 o 9 17 1 182.33 182.81 18.23 o 12 17 1 309.20 311.42 28.23 o 15 17 1 202.34 342.30 109.97 o -32 18 1 270.84 251.34 86.58 o -29 18 1 42.77 87.15 40.01 o -26 18 1 1479.99 1556.47 73.11 o -23 18 1 1561.27 1561.56 65.08 o -20 18 1 387.23 374.36 19.68 o -17 18 1 177.53 248.91 17.27 o -14 18 1 208.59 190.64 13.80 o -11 18 1 137.66 104.76 10.83 o -8 18 1 7389.88 7992.64 142.14 o -5 18 1 21.48 29.33 38.84 o -2 18 1 460.88 508.76 17.10 o 1 18 1 668.15 680.04 27.62 o 4 18 1 32.59 45.48 15.67 o 7 18 1 28.43 22.88 13.33 o 10 18 1 85.48 84.07 15.30 o 13 18 1 423.02 448.39 106.18 o -31 19 1 46.15 49.58 65.17 o -28 19 1 1428.40 1397.88 66.75 o -25 19 1 1274.70 1386.23 67.32 o -22 19 1 1454.23 1564.42 59.44 o -19 19 1 15500.56 16126.73 314.52 o -16 19 1 5308.26 5345.90 106.38 o -13 19 1 512.22 418.50 21.35 o -10 19 1 2928.07 3450.34 69.94 o -7 19 1 1727.47 1500.13 34.54 o -4 19 1 284.29 289.63 25.66 o -1 19 1 1196.27 1207.39 28.97 o 2 19 1 521.20 495.11 33.98 o 5 19 1 0.72 0.00 15.13 o 8 19 1 28.60 16.10 16.52 o 11 19 1 397.48 395.42 47.01 o -30 20 1 342.55 331.95 56.76 o -27 20 1 16.22 2.82 60.70 o -24 20 1 526.57 531.70 51.21 o -21 20 1 87.77 29.69 15.54 o -18 20 1 3492.38 3610.01 56.59 o -15 20 1 45.25 62.01 12.34 o -12 20 1 1985.92 1793.98 34.03 o -9 20 1 1843.41 2049.04 42.42 o -6 20 1 87.92 136.68 31.78 o -3 20 1 10.12 0.00 32.20 o 0 20 1 1528.67 1586.83 34.44 o 3 20 1 3815.54 4447.40 104.64 o 6 20 1 66.28 40.85 20.23 o 9 20 1 64.21 36.74 32.61 o 12 20 1 13.25 12.99 51.78 o -29 21 1 129.44 194.80 124.36 o -26 21 1 145.94 147.02 39.18 o -23 21 1 196.91 100.35 31.72 o -20 21 1 619.83 689.11 29.07 o -17 21 1 274.89 272.21 14.42 o -14 21 1 1913.31 2020.16 53.83 o -11 21 1 1217.32 1070.19 33.40 o -8 21 1 9.40 4.09 9.88 o -5 21 1 12.62 52.07 28.54 o -2 21 1 681.85 643.42 48.71 o 1 21 1 999.90 1066.47 32.13 o 4 21 1 15.33 10.00 20.88 o 7 21 1 344.22 333.51 27.31 o 10 21 1 172.18 268.28 71.31 o -31 22 1 8.19 0.00 52.97 o -28 22 1 181.84 142.45 48.06 o -25 22 1 1907.47 2139.80 85.71 o -22 22 1 63.52 85.88 16.90 o -19 22 1 4063.18 4301.81 104.99 o -16 22 1 285.33 360.59 16.52 o -13 22 1 7824.44 8386.89 169.28 o -10 22 1 4.45 12.57 18.67 o -7 22 1 1.13 26.97 24.84 o -4 22 1 1412.30 1541.97 57.57 o -1 22 1 1193.70 1242.27 32.94 o 2 22 1 603.71 690.27 29.09 o 5 22 1 63.55 96.15 21.33 o 8 22 1 859.43 780.50 84.81 o -30 23 1 16.30 5.86 46.58 o -27 23 1 1.38 0.00 40.87 o -24 23 1 154.80 153.98 21.19 o -21 23 1 536.33 495.51 26.04 o -18 23 1 35.13 4.18 19.67 o -15 23 1 53.65 45.71 9.88 o -12 23 1 133.59 85.35 17.80 o -9 23 1 2377.90 2303.23 75.20 o -6 23 1 461.17 386.19 36.39 o -3 23 1 2124.19 2297.50 83.90 o 0 23 1 166.70 212.60 15.92 o 3 23 1 630.04 582.74 31.37 o 6 23 1 559.17 564.78 36.44 o 9 23 1 4.28 0.00 56.58 o -32 24 1 69.03 70.50 52.31 o -29 24 1 5.09 0.00 44.10 o -26 24 1 825.70 871.50 60.06 o -23 24 1 401.39 435.63 52.93 o -20 24 1 885.74 855.54 31.31 o -17 24 1 373.97 407.68 29.46 o -14 24 1 3924.82 4425.64 100.58 o -11 24 1 717.41 626.06 27.00 o -8 24 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407.38 32.07 o -20 27 1 921.60 785.48 32.80 o -17 27 1 146.33 89.20 22.08 o -14 27 1 0.06 28.08 27.58 o -11 27 1 0.42 0.00 53.76 o -8 27 1 1412.20 1422.91 67.36 o -5 27 1 1116.49 1220.05 60.28 o -2 27 1 0.15 7.97 35.79 o 1 27 1 416.56 527.50 125.68 o 4 27 1 101.63 50.58 113.56 o -28 28 1 85.21 116.31 44.43 o -25 28 1 15.96 15.63 34.36 o -22 28 1 316.99 266.61 28.44 o -19 28 1 36.23 34.53 18.29 o -16 28 1 1.33 6.05 23.72 o -13 28 1 609.61 705.11 33.29 o -10 28 1 311.28 333.70 40.76 o -7 28 1 899.91 937.31 57.03 o -4 28 1 803.05 1013.73 74.68 o -1 28 1 17.06 53.58 43.83 o -27 29 1 351.12 280.54 94.38 o -24 29 1 4.51 89.36 72.37 o -21 29 1 12.53 29.39 13.50 o -18 29 1 402.52 522.30 38.60 o -15 29 1 929.72 1035.09 46.58 o -12 29 1 167.65 261.98 49.64 o -9 29 1 59.07 63.07 44.77 o -6 29 1 415.83 496.99 65.21 o -3 29 1 271.63 171.76 73.58 o -26 30 1 0.86 58.18 79.17 o -23 30 1 3.25 59.37 84.16 o -20 30 1 26.40 3.77 35.98 o -17 30 1 57.93 25.07 22.56 o -14 30 1 488.94 563.63 49.62 o -11 30 1 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