#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/29/2102902.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102902_Fobs loop_ _publ_author_name 'Gelbrich, Thomas' 'Hursthouse, Michael B.' 'Threlfall, Terence L.' _publ_section_title ; Structural systematics of 4,4'-disubstituted benzenesulfonamidobenzenes. 1. Overview and dimer-based isostructures ; _journal_coeditor_code BM5045 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 621 _journal_page_last 632 _journal_volume 63 _journal_year 2007 _space_group_IT_number 148 _symmetry_space_group_name_Hall '-R 3' _symmetry_space_group_name_H-M 'R -3 :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 27.7243 _cell_length_b 27.7243 _cell_length_c 9.8101 _exptl_crystal_F_000 2916.00 _reflns_d_resolution_high 0.8394 _[local]_cod_data_source_file bm5045Me~CF3sup21.hkl _[local]_cod_data_source_block Me~CF3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' s92 in R-3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 367.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 5 0 5623.23 4187.55 972.54 o -3 6 0 64183.93 53395.92 1329.41 o 0 6 0 78358.02 1034.22 34757.91 o -5 7 0 33591.15 29724.94 491.15 o -2 7 0 1525.68 975.16 29.13 o -7 8 0 11945.59 10557.35 307.44 o -4 8 0 21238.93 20087.00 331.21 o -1 8 0 3660.85 3788.35 80.12 o -6 9 0 7348.08 6801.49 111.65 o -3 9 0 7459.25 6973.64 131.84 o 0 9 0 1980.23 1654.49 50.52 o -8 10 0 1855.66 1949.29 55.06 o -5 10 0 33349.82 31011.17 479.23 o -2 10 0 10878.94 10516.60 218.29 o -10 11 0 16.33 19.43 8.95 o -7 11 0 4248.97 4085.63 93.76 o -4 11 0 143.72 142.01 15.64 o -1 11 0 475.67 419.78 32.60 o -9 12 0 27611.72 23354.45 7401.09 o -6 12 0 4836.06 4174.70 78.87 o -3 12 0 3.95 6.78 11.69 o 0 12 0 9238.87 9008.33 215.60 o -11 13 0 16.13 3.79 12.29 o -8 13 0 1483.42 1684.45 55.75 o -5 13 0 6295.35 5838.64 139.77 o -2 13 0 2377.65 2390.68 70.92 o -13 14 0 352.68 309.63 31.21 o -10 14 0 5821.08 6708.39 182.84 o -7 14 0 13430.35 9349.58 5909.71 o -4 14 0 917.43 898.78 23.88 o -1 14 0 1288.39 1693.86 63.61 o -12 15 0 7941.47 8587.08 159.43 o -9 15 0 701.15 523.49 43.33 o -6 15 0 1.90 6.06 26.60 o -3 15 0 14.75 30.47 21.35 o 0 15 0 366.07 311.71 27.63 o -14 16 0 14329.28 15965.12 311.66 o -11 16 0 4851.08 5165.90 168.99 o -8 16 0 11123.14 12704.36 345.43 o -5 16 0 15.50 12.82 15.37 o -2 16 0 1055.70 1125.23 55.74 o -16 17 0 5948.97 6635.58 132.01 o -13 17 0 9913.46 9946.56 298.40 o -10 17 0 4953.89 3286.76 1175.42 o -7 17 0 5112.15 5180.65 117.69 o -4 17 0 3941.88 3658.12 83.36 o -1 17 0 2266.70 1844.01 97.99 o -15 18 0 634.11 615.77 28.30 o -12 18 0 3.68 3.25 26.26 o -9 18 0 254.46 126.23 34.07 o -6 18 0 657.82 672.93 27.45 o -3 18 0 1.31 0.00 24.87 o 0 18 0 630.04 680.54 41.14 o -17 19 0 1350.94 1705.03 58.78 o -14 19 0 2448.84 2497.94 70.84 o -11 19 0 4073.08 4333.92 132.88 o -8 19 0 386.43 370.79 62.35 o -5 19 0 1218.53 1698.86 78.03 o -2 19 0 985.46 1145.53 56.32 o -19 20 0 50.66 65.67 33.64 o -16 20 0 154.66 197.90 19.16 o -13 20 0 1834.58 1892.21 76.04 o -10 20 0 1590.13 1815.26 102.94 o -7 20 0 11551.95 11720.14 331.29 o -4 20 0 541.20 538.80 35.04 o -1 20 0 195.08 178.86 32.54 o -18 21 0 629.21 579.13 37.47 o -15 21 0 4065.67 4084.90 97.25 o -12 21 0 55.94 40.63 38.06 o -9 21 0 8296.08 9454.30 305.72 o -6 21 0 56.54 23.36 35.85 o -3 21 0 10.07 2.26 32.08 o 0 21 0 10181.41 10923.26 338.10 o -20 22 0 1462.50 1643.03 67.03 o -17 22 0 82.61 96.16 15.91 o -14 22 0 316.56 318.04 33.69 o -11 22 0 2527.81 2387.30 97.35 o -8 22 0 955.80 915.11 37.63 o -5 22 0 3924.95 4258.27 149.30 o -2 22 0 6.74 67.27 36.91 o -22 23 0 5171.96 5267.34 207.03 o -19 23 0 10.05 0.00 29.79 o -16 23 0 1382.66 1402.08 49.55 o -13 23 0 410.82 439.98 40.98 o -10 23 0 1809.55 1687.43 65.61 o -7 23 0 1673.69 1440.84 104.04 o -4 23 0 2753.67 2541.47 118.83 o -1 23 0 459.04 489.62 62.29 o -21 24 0 7026.98 7066.01 261.28 o -18 24 0 0.03 16.96 19.70 o -15 24 0 1321.65 1215.58 57.62 o -12 24 0 2162.96 2507.01 90.87 o -9 24 0 12.47 6.54 18.95 o -6 24 0 2068.84 2299.04 115.19 o -3 24 0 2463.50 2463.06 126.56 o 0 24 0 592.07 698.34 72.29 o -23 25 0 0.02 25.15 45.59 o -20 25 0 537.65 521.80 45.52 o -17 25 0 3898.89 3888.67 115.46 o -14 25 0 1920.74 1731.63 71.06 o -11 25 0 110.53 74.91 23.09 o -8 25 0 91.88 112.50 34.68 o -5 25 0 31.05 0.00 51.18 o -2 25 0 12.49 63.45 61.88 o -22 26 0 731.95 686.49 62.93 o -19 26 0 502.51 555.24 34.15 o -16 26 0 2447.79 2602.72 88.51 o -13 26 0 47.05 41.23 37.90 o -10 26 0 364.99 425.23 28.52 o -7 26 0 72.38 84.95 47.36 o -4 26 0 1413.85 1062.03 409.98 o -1 26 0 53.86 0.00 101.10 o -24 27 0 665.65 555.00 122.42 o -21 27 0 469.72 523.24 55.03 o -18 27 0 749.65 775.93 47.34 o -15 27 0 149.23 160.96 39.75 o -12 27 0 1948.65 2180.53 82.46 o -9 27 0 191.86 132.57 46.23 o -6 27 0 3.91 64.28 52.03 o -3 27 0 1081.10 707.97 342.58 o -23 28 0 3052.76 3575.71 271.14 o -20 28 0 3.82 4.17 35.70 o -17 28 0 507.79 536.43 47.60 o -14 28 0 2586.59 2676.64 101.68 o -11 28 0 3855.51 3568.28 150.31 o -8 28 0 1612.29 1936.76 99.08 o -5 28 0 106.71 112.96 58.07 o -2 28 0 737.72 830.29 109.14 o -28 29 0 274.12 197.94 88.24 o -25 29 0 261.39 321.52 134.80 o -22 29 0 1.03 13.24 97.66 o -19 29 0 303.83 210.18 39.83 o -16 29 0 56.10 77.44 49.53 o -13 29 0 991.12 1132.96 69.75 o -10 29 0 23.73 0.00 49.35 o -7 29 0 62.74 13.63 75.71 o -4 29 0 364.15 114.34 100.93 o -1 29 0 455.55 651.48 121.90 o -24 30 0 14.86 0.00 110.90 o -21 30 0 235.06 111.77 30.76 o -18 30 0 77.84 185.79 64.25 o -15 30 0 437.60 375.00 41.98 o -12 30 0 44.56 72.46 65.82 o -9 30 0 846.06 764.29 81.27 o -6 30 0 46.35 5.29 61.43 o -23 31 0 5.25 0.00 78.32 o -20 31 0 94.23 87.01 76.59 o -17 31 0 108.98 112.32 47.76 o -14 31 0 1044.96 1147.54 123.02 o -11 31 0 7.47 61.91 78.23 o -8 31 0 40.71 0.00 65.35 o -22 32 0 211.25 312.45 88.65 o -19 32 0 59.84 0.00 82.17 o -16 32 0 160.31 143.80 82.27 o -13 32 0 197.76 170.84 62.91 o -10 32 0 306.21 460.57 91.60 o 1 3 1 99356.04 81269.99 2595.46 o -7 4 1 457.38 511.94 16.38 o -4 4 1 5518.48 4592.57 543.71 o -1 4 1 627.69 455.63 22.70 o 2 4 1 20955.42 18911.41 367.11 o -9 5 1 15460.17 14948.58 235.59 o -6 5 1 26007.75 22331.94 378.49 o 0 5 1 135268.88 77242.46 34092.18 o 3 5 1 2544.41 2701.22 51.66 o -11 6 1 12026.68 13804.23 281.67 o -8 6 1 861.67 924.81 26.47 o -5 6 1 30085.56 27704.62 585.51 o -2 6 1 11673.50 11039.81 188.71 o 1 6 1 2616.94 3231.12 94.55 o 4 6 1 855.81 975.40 29.23 o -13 7 1 694.80 517.10 30.94 o -10 7 1 7750.17 7267.21 114.93 o -7 7 1 17290.38 15916.50 282.05 o -4 7 1 42645.86 39217.23 666.89 o -1 7 1 1.94 0.00 9.32 o 2 7 1 81366.20 77120.05 1779.60 o 5 7 1 4107.35 3679.35 83.95 o -15 8 1 34.18 73.45 22.71 o -12 8 1 6540.84 6643.92 125.62 o -9 8 1 573.71 431.77 19.59 o -6 8 1 78081.83 68699.12 1152.23 o -3 8 1 4827.05 5144.40 93.88 o 0 8 1 1004.91 946.91 32.08 o 3 8 1 27451.51 26173.96 522.59 o 6 8 1 11507.06 6872.53 5330.64 o -17 9 1 22.72 23.41 31.52 o -14 9 1 6822.13 6841.93 107.49 o -11 9 1 15732.41 15505.20 513.46 o -8 9 1 21.87 30.35 12.35 o -5 9 1 3210.87 3958.05 66.56 o 1 9 1 1016.46 866.99 28.09 o 4 9 1 33650.88 37450.94 744.88 o 7 9 1 4504.66 4282.95 111.00 o -19 10 1 55.27 117.48 30.10 o -16 10 1 80.02 78.73 15.09 o -13 10 1 8666.24 8053.83 119.74 o -10 10 1 449.40 425.56 20.10 o -7 10 1 1295.47 1538.09 34.63 o -1 10 1 3344.40 3023.37 93.83 o 2 10 1 4102.86 3834.10 87.79 o 5 10 1 8197.86 7594.41 1834.60 o 8 10 1 4783.17 4954.63 170.72 o -21 11 1 2129.59 2412.12 102.82 o -18 11 1 915.06 1083.76 37.55 o -15 11 1 11527.77 12394.23 233.33 o -12 11 1 3467.85 4108.43 106.19 o -9 11 1 19.70 41.17 20.42 o -6 11 1 8010.39 8700.53 142.80 o -3 11 1 5839.63 5431.80 105.77 o 0 11 1 3789.08 4244.23 102.18 o 3 11 1 150.37 60.00 46.93 o 6 11 1 10968.53 7445.94 4000.65 o 9 11 1 864.85 641.46 111.28 o -23 12 1 1917.91 1901.32 64.10 o -20 12 1 1022.55 975.05 41.26 o -17 12 1 416.50 307.52 20.22 o -14 12 1 3189.51 2810.47 63.68 o -11 12 1 4681.67 5310.33 105.34 o -8 12 1 10717.43 11214.96 197.65 o -5 12 1 1149.82 924.41 40.57 o -2 12 1 1459.73 1148.55 42.00 o 1 12 1 134.04 143.38 26.10 o 4 12 1 578.22 603.26 32.18 o 7 12 1 1623.82 1278.65 76.47 o 10 12 1 166.61 98.12 31.92 o -25 13 1 6069.38 6228.52 199.97 o -22 13 1 1163.10 1117.69 59.15 o -19 13 1 205.06 234.94 28.72 o -16 13 1 1092.82 1075.46 29.61 o -13 13 1 306.39 360.81 27.82 o -10 13 1 22426.83 24025.79 418.10 o -7 13 1 12055.18 12662.55 318.80 o -4 13 1 20951.40 21145.98 572.42 o -1 13 1 2998.10 3150.50 87.94 o 2 13 1 4054.76 4130.94 141.49 o 5 13 1 450.81 536.84 69.57 o 8 13 1 301.87 396.97 39.71 o 11 13 1 293.51 394.64 50.30 o -27 14 1 1098.07 1242.33 56.88 o -24 14 1 183.89 220.18 30.26 o -21 14 1 3731.46 3902.33 111.36 o -18 14 1 531.35 545.06 28.39 o -15 14 1 443.68 414.84 35.10 o -12 14 1 1014.66 921.20 35.63 o -9 14 1 1233.72 1049.65 41.06 o -6 14 1 2029.79 2064.68 52.52 o -3 14 1 6223.82 7333.41 149.74 o 0 14 1 5452.85 6016.86 142.37 o 3 14 1 6352.63 5912.95 136.49 o 6 14 1 428.50 506.22 34.24 o 9 14 1 349.55 240.92 31.54 o 12 14 1 2401.61 2430.92 97.19 o -29 15 1 26.07 9.74 32.95 o -26 15 1 442.89 550.36 36.06 o -23 15 1 6191.64 6325.34 188.77 o -20 15 1 3170.92 2868.35 70.46 o -17 15 1 2.55 0.26 22.75 o -14 15 1 1789.75 1553.11 42.25 o -11 15 1 6973.29 6710.83 152.78 o -8 15 1 9466.30 9524.17 202.05 o -5 15 1 1350.90 1419.05 36.27 o -2 15 1 17372.78 17598.07 346.73 o 1 15 1 1847.71 1722.21 54.14 o 4 15 1 556.07 604.05 20.96 o 7 15 1 58.29 71.93 30.08 o 10 15 1 1180.67 1065.77 56.75 o 13 15 1 77.23 95.34 33.91 o -31 16 1 601.51 674.26 55.18 o -28 16 1 53.81 28.38 31.33 o -25 16 1 1337.29 1232.87 66.56 o -22 16 1 6997.00 7320.20 204.50 o -19 16 1 4931.76 5205.27 173.23 o -16 16 1 4045.50 4355.08 104.61 o -13 16 1 6686.71 7358.01 133.31 o -10 16 1 200.55 180.27 41.56 o -7 16 1 2877.00 3296.78 87.20 o -4 16 1 715.08 751.98 31.34 o -1 16 1 5012.67 5419.84 118.82 o 2 16 1 17.95 5.82 19.52 o 5 16 1 4702.63 4557.82 105.35 o 8 16 1 1079.91 990.83 48.62 o 11 16 1 885.91 652.27 50.89 o 14 16 1 235.54 350.81 82.34 o -30 17 1 2.98 18.78 38.39 o -27 17 1 1889.36 2407.82 89.78 o -24 17 1 261.57 341.10 28.74 o -21 17 1 6779.78 7058.80 261.62 o -18 17 1 3964.25 3541.66 345.76 o -15 17 1 3040.74 3095.44 78.87 o -12 17 1 22023.90 23219.47 460.90 o -9 17 1 3302.06 3823.77 104.21 o -6 17 1 4432.05 3952.09 95.01 o -3 17 1 2076.64 1961.80 63.38 o 0 17 1 20.89 57.43 25.16 o 3 17 1 2318.10 2501.28 72.99 o 6 17 1 6715.24 7135.67 200.24 o 9 17 1 1230.69 1307.81 54.28 o 12 17 1 259.69 278.09 56.20 o 15 17 1 930.58 885.72 66.23 o -32 18 1 508.70 484.75 79.27 o -29 18 1 15.64 0.00 35.72 o -26 18 1 1394.78 1060.01 342.75 o -23 18 1 1984.21 2272.33 132.46 o -20 18 1 1837.02 2063.62 77.87 o -17 18 1 137.50 163.37 38.34 o -14 18 1 4.88 0.00 15.72 o -11 18 1 37.69 63.77 46.37 o -8 18 1 11125.64 11383.84 273.65 o -5 18 1 260.46 270.92 31.96 o -2 18 1 419.55 348.70 30.56 o 1 18 1 753.19 680.41 55.07 o 4 18 1 0.70 4.98 30.72 o 7 18 1 2.09 34.72 18.10 o 10 18 1 131.02 127.69 47.19 o 13 18 1 360.11 392.59 45.87 o -31 19 1 123.69 236.99 77.26 o -28 19 1 1750.81 1481.13 118.60 o -25 19 1 1954.68 1708.24 104.70 o -22 19 1 450.13 523.48 48.77 o -19 19 1 21592.19 22307.21 580.90 o -16 19 1 5045.81 5289.18 109.71 o -13 19 1 1156.35 938.12 37.99 o -10 19 1 3724.74 4160.95 146.68 o -7 19 1 1799.83 1762.81 73.88 o -4 19 1 27.59 17.10 33.65 o -1 19 1 1453.36 1604.99 52.87 o 2 19 1 123.96 88.22 35.06 o 5 19 1 41.81 42.64 35.79 o 8 19 1 385.79 415.65 28.34 o 11 19 1 808.63 698.63 58.16 o -30 20 1 784.36 960.87 96.47 o -27 20 1 39.05 0.00 106.30 o -24 20 1 1120.04 923.42 74.69 o -21 20 1 1145.37 1233.33 73.71 o -18 20 1 4834.04 4975.40 153.36 o -15 20 1 55.66 45.12 19.22 o -12 20 1 1890.49 1982.86 160.41 o -9 20 1 2402.72 2453.47 121.89 o -6 20 1 13.25 27.50 31.55 o -3 20 1 3.79 24.42 29.85 o 0 20 1 1287.65 1471.76 60.84 o 3 20 1 3231.21 3409.31 111.55 o 6 20 1 122.65 59.99 59.93 o 9 20 1 31.20 18.03 55.16 o 12 20 1 144.08 145.74 72.54 o -32 21 1 437.47 392.85 78.91 o -29 21 1 214.84 149.08 61.60 o -26 21 1 0.34 29.11 49.07 o -23 21 1 59.09 32.71 33.78 o -20 21 1 483.34 458.85 82.58 o -17 21 1 294.34 309.49 35.14 o -14 21 1 3631.77 4309.95 111.32 o -11 21 1 1914.76 1929.59 75.58 o -8 21 1 300.86 304.80 31.54 o -5 21 1 2.99 9.71 29.68 o -2 21 1 1623.08 1581.78 88.83 o 1 21 1 673.08 781.21 61.76 o 4 21 1 19.22 12.94 41.32 o 7 21 1 890.30 966.78 84.97 o 10 21 1 221.57 338.11 71.60 o -31 22 1 2.00 102.15 74.42 o -28 22 1 30.59 14.75 52.17 o -25 22 1 2208.98 2185.99 193.75 o -22 22 1 33.63 97.45 34.97 o -19 22 1 1554.68 1841.70 73.90 o -16 22 1 4.89 5.18 19.96 o -13 22 1 8493.31 8693.12 303.44 o -10 22 1 479.35 364.75 37.18 o -7 22 1 67.77 139.19 36.40 o -4 22 1 3506.44 3874.73 129.76 o -1 22 1 451.75 444.50 43.26 o 2 22 1 338.95 355.53 81.17 o 5 22 1 293.84 404.59 54.97 o 8 22 1 663.95 620.17 138.92 o -30 23 1 4.22 0.00 58.06 o -27 23 1 60.04 7.23 59.69 o -24 23 1 61.57 53.60 47.35 o -21 23 1 790.19 904.18 55.52 o -18 23 1 164.97 214.41 26.48 o -15 23 1 103.44 49.08 24.27 o -12 23 1 14.60 25.06 31.22 o -9 23 1 5500.97 5570.38 156.58 o -6 23 1 1745.31 1623.71 84.15 o -3 23 1 1474.60 1674.57 114.14 o 0 23 1 322.78 512.84 59.69 o 3 23 1 1056.83 1033.11 179.24 o 6 23 1 348.57 225.75 97.49 o -29 24 1 2.53 0.00 75.69 o -26 24 1 1330.68 1309.96 156.12 o -23 24 1 388.77 354.63 50.72 o -20 24 1 937.52 790.80 52.21 o -17 24 1 725.52 774.06 39.70 o -14 24 1 3906.68 4540.09 154.00 o -11 24 1 4705.53 4754.77 152.53 o -8 24 1 4119.81 4481.96 140.70 o -5 24 1 891.22 904.23 67.30 o -2 24 1 1721.43 2080.26 118.62 o 1 24 1 1520.08 1417.05 125.35 o 4 24 1 173.64 165.23 103.85 o 7 24 1 202.55 325.47 134.97 o -31 25 1 336.12 429.60 74.62 o -28 25 1 1610.58 1609.59 176.32 o -25 25 1 914.18 1152.69 214.92 o -22 25 1 98.77 69.25 38.35 o -19 25 1 35.35 70.14 26.21 o -16 25 1 1339.49 1200.17 48.75 o -13 25 1 612.99 512.27 48.17 o -10 25 1 8908.40 9553.79 384.05 o -7 25 1 8.84 19.92 46.36 o -4 25 1 93.43 167.30 53.67 o -1 25 1 295.20 225.46 68.86 o 2 25 1 42.69 0.00 138.75 o 5 25 1 8.28 0.00 78.60 o -30 26 1 208.82 172.15 95.57 o -27 26 1 77.99 63.10 110.04 o -24 26 1 25.29 8.65 63.91 o -21 26 1 3232.90 3398.17 158.36 o -18 26 1 7.52 0.00 27.42 o -15 26 1 1575.70 1459.66 61.51 o -12 26 1 0.41 9.67 37.07 o -9 26 1 2205.70 2390.20 97.89 o -6 26 1 2180.22 2112.83 209.13 o -3 26 1 590.32 446.46 81.75 o 0 26 1 372.50 292.49 133.51 o 3 26 1 683.69 825.63 126.54 o -29 27 1 1.08 0.00 82.43 o -26 27 1 109.56 182.42 108.32 o -23 27 1 735.04 697.71 166.78 o -20 27 1 503.28 525.74 41.24 o -17 27 1 32.89 76.59 30.28 o -14 27 1 623.41 563.51 46.74 o -11 27 1 20.60 9.50 22.44 o -8 27 1 872.59 919.56 112.65 o -5 27 1 1179.29 1137.26 96.79 o -2 27 1 68.42 133.25 121.82 o 1 27 1 266.66 387.20 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