#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103270.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103270_Fobs loop_ _publ_author_name 'Farrell, Dorcas M. M.' 'Ferguson, George' 'Lough, Alan J.' 'Glidewell, Christopher' _publ_section_title ; Chiral versus racemic building blocks in supramolecular chemistry: tartrate salts of organic diamines ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 272 _journal_page_last 288 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.405 _cell_angle_gamma 90.000 _cell_length_a 7.3240 _cell_length_b 15.9935 _cell_length_c 7.5149 _exptl_crystal_F_000 436.00 _reflns_d_resolution_high 0.7711 _[local]_cod_data_source_file na0130VIIsup8.hkl _[local]_cod_data_source_block VII #BEGIN Tags that were not found in dictionaries: _shelx_title ' 0121 DF107 (rac-tartaric acid):DABCO 2:1 in P21/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 65.46 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 30.58 30.37 1.38 o 6 0 0 11.07 7.66 0.95 o 8 0 0 277.25 268.56 13.33 o 1 1 0 160.37 155.96 4.22 o 2 1 0 952.53 936.17 18.84 o 3 1 0 549.65 547.78 10.75 o 4 1 0 39.03 40.60 1.12 o 5 1 0 41.36 33.63 1.03 o 6 1 0 71.98 77.59 1.98 o 7 1 0 46.59 33.55 1.46 o 8 1 0 52.10 52.56 2.41 o 9 1 0 31.01 40.86 2.49 o 1 2 0 1573.09 1453.75 36.56 o 2 2 0 855.17 796.30 15.74 o 3 2 0 638.47 627.95 13.51 o 4 2 0 61.64 60.47 1.81 o 5 2 0 224.05 240.77 5.59 o 6 2 0 64.52 71.05 1.98 o 7 2 0 154.24 161.03 3.87 o 8 2 0 7.40 8.43 0.95 o 9 2 0 9.89 9.46 3.27 o 3 3 0 190.96 204.64 4.39 o 4 3 0 416.24 411.95 7.66 o 5 3 0 233.13 238.97 4.73 o 6 3 0 71.41 76.56 2.15 o 7 3 0 109.46 110.45 2.58 o 8 3 0 57.78 57.46 2.32 o 9 3 0 0.09 -1.63 1.63 o 0 4 0 128.88 110.79 3.44 o 1 4 0 3004.17 2817.36 72.95 o 2 4 0 95.39 95.14 2.15 o 3 4 0 557.54 555.70 10.32 o 4 4 0 39.46 63.31 1.89 o 5 4 0 2.78 2.06 0.60 o 6 4 0 43.07 42.41 1.89 o 7 4 0 0.17 0.26 0.69 o 8 4 0 6.57 2.15 1.20 o 9 4 0 0.16 -0.52 1.63 o 1 5 0 61.41 37.33 0.95 o 2 5 0 15.89 17.98 0.77 o 3 5 0 548.25 564.38 11.53 o 4 5 0 0.29 0.26 0.43 o 5 5 0 141.60 154.67 3.61 o 6 5 0 628.24 620.04 17.12 o 7 5 0 1.73 -0.26 0.86 o 8 5 0 0.79 -0.26 0.95 o 9 5 0 35.17 32.09 2.06 o 0 6 0 4.06 2.49 0.43 o 1 6 0 102.54 103.14 2.24 o 2 6 0 587.09 576.08 13.94 o 3 6 0 2482.55 2632.84 59.18 o 4 6 0 177.75 193.38 4.39 o 5 6 0 104.94 100.64 2.58 o 6 6 0 185.97 221.59 5.33 o 7 6 0 61.98 59.01 2.58 o 8 6 0 8.11 7.83 1.29 o 9 6 0 9.02 13.85 3.35 o 1 7 0 376.17 367.22 7.31 o 2 7 0 477.11 482.49 9.72 o 3 7 0 154.43 174.11 4.04 o 4 7 0 144.96 137.03 3.27 o 5 7 0 1.04 0.86 0.69 o 6 7 0 37.62 34.84 1.89 o 7 7 0 76.86 78.28 3.70 o 8 7 0 2.70 1.20 1.29 o 0 8 0 2308.22 2307.34 64.60 o 1 8 0 106.88 98.24 2.41 o 2 8 0 931.38 967.05 18.92 o 3 8 0 9.22 10.58 0.69 o 4 8 0 415.91 414.45 9.63 o 5 8 0 58.45 53.16 1.72 o 6 8 0 33.33 33.55 1.55 o 7 8 0 150.88 160.95 5.85 o 8 8 0 16.10 12.73 1.55 o 1 9 0 0.00 0.09 0.52 o 2 9 0 51.21 61.76 1.63 o 3 9 0 471.20 524.38 11.78 o 4 9 0 0.16 -0.26 0.52 o 5 9 0 757.77 795.78 22.62 o 6 9 0 20.18 22.11 1.29 o 7 9 0 86.54 79.14 3.27 o 8 9 0 22.23 20.65 2.41 o 0 10 0 85.97 106.32 3.35 o 1 10 0 16.50 11.01 0.77 o 2 10 0 456.82 443.61 9.81 o 3 10 0 162.12 156.82 4.04 o 4 10 0 4.91 1.20 0.43 o 5 10 0 548.45 558.02 15.23 o 6 10 0 90.11 88.60 2.58 o 7 10 0 0.23 -0.17 0.77 o 8 10 0 15.72 16.00 2.24 o 1 11 0 201.63 214.19 4.99 o 2 11 0 281.97 304.00 6.28 o 3 11 0 588.78 577.89 13.42 o 4 11 0 33.95 39.14 1.20 o 5 11 0 93.85 86.88 2.75 o 6 11 0 79.72 81.20 3.10 o 7 11 0 3.49 3.53 0.95 o 8 11 0 24.13 25.38 3.01 o 0 12 0 51.18 46.11 2.24 o 1 12 0 237.34 252.99 6.28 o 2 12 0 11.41 12.99 1.12 o 3 12 0 1.80 0.86 0.77 o 4 12 0 1.71 1.63 0.52 o 5 12 0 60.36 48.00 1.98 o 6 12 0 0.04 0.09 0.95 o 7 12 0 46.74 47.91 2.49 o 1 13 0 349.03 342.36 7.83 o 2 13 0 0.21 0.77 0.86 o 3 13 0 177.00 196.90 5.76 o 4 13 0 242.29 251.70 8.34 o 5 13 0 2.10 -0.43 0.86 o 6 13 0 0.85 -1.03 1.29 o 7 13 0 0.53 -0.69 1.20 o 0 14 0 706.45 723.01 28.90 o 1 14 0 167.82 173.93 5.08 o 2 14 0 293.27 307.61 8.86 o 3 14 0 41.34 45.42 1.98 o 4 14 0 529.32 539.35 17.38 o 5 14 0 0.00 -0.34 1.03 o 6 14 0 1.27 0.69 1.20 o 1 15 0 93.95 96.77 3.18 o 2 15 0 0.81 2.24 0.86 o 3 15 0 1.27 1.63 0.77 o 4 15 0 38.10 40.52 2.06 o 5 15 0 21.22 14.37 1.46 o 6 15 0 0.27 0.00 1.12 o 0 16 0 143.89 142.19 8.43 o 1 16 0 1.57 1.81 0.77 o 2 16 0 123.41 119.31 4.39 o 3 16 0 78.98 78.37 3.78 o 4 16 0 7.67 5.08 1.12 o 5 16 0 7.88 7.57 0.69 o 6 16 0 0.05 0.34 1.29 o 1 17 0 36.60 40.17 2.06 o 2 17 0 13.53 13.08 1.29 o 3 17 0 8.90 8.77 1.46 o 4 17 0 0.15 -0.77 1.29 o 5 17 0 28.03 28.73 3.01 o 0 18 0 0.25 3.10 1.29 o 1 18 0 1.99 3.18 1.38 o 2 18 0 60.19 63.66 2.75 o 3 18 0 3.10 3.10 1.55 o 4 18 0 38.73 47.23 5.59 o 1 19 0 22.50 22.45 2.58 o 2 19 0 34.53 38.45 2.58 o 3 19 0 9.53 6.28 3.01 o 0 20 0 30.60 31.48 4.47 o 1 20 0 7.30 5.59 2.15 o 2 20 0 4.12 4.47 2.06 o -9 0 1 2.79 4.73 1.03 o -7 0 1 8.23 4.99 1.03 o -5 0 1 19.73 19.61 1.12 o -3 0 1 1822.48 1770.40 46.62 o -1 0 1 1869.28 1600.59 60.21 o 3 0 1 148.38 118.02 3.78 o 5 0 1 152.08 150.79 4.47 o 7 0 1 15.96 16.00 1.46 o 9 0 1 2.82 -3.70 3.70 o -9 1 1 0.53 1.89 0.86 o -8 1 1 4.21 6.71 0.77 o -7 1 1 51.13 56.00 1.63 o -6 1 1 8.62 4.82 0.60 o -5 1 1 204.60 207.40 4.90 o -4 1 1 574.53 583.82 12.04 o -2 1 1 1611.61 1502.44 31.40 o -1 1 1 3.40 3.27 0.09 o 0 1 1 367.08 277.33 9.72 o 1 1 1 608.00 610.15 11.44 o 2 1 1 74.36 66.75 1.46 o 3 1 1 182.20 169.63 3.78 o 4 1 1 763.50 832.60 17.12 o 5 1 1 543.81 562.32 11.27 o 6 1 1 0.01 0.86 0.60 o 7 1 1 25.44 25.98 1.55 o 8 1 1 16.30 11.96 1.38 o 9 1 1 3.85 5.42 1.46 o -9 2 1 10.72 10.24 1.20 o -8 2 1 3.26 0.69 0.60 o -7 2 1 117.24 123.87 3.44 o -6 2 1 709.12 747.61 16.52 o -5 2 1 177.47 183.57 5.59 o -4 2 1 994.54 1008.42 20.82 o -3 2 1 50.19 47.48 1.03 o 0 2 1 512.48 430.28 14.45 o 1 2 1 1073.15 1014.19 20.73 o 2 2 1 89.74 91.35 1.81 o 3 2 1 220.26 222.36 4.65 o 4 2 1 568.16 570.58 10.92 o 5 2 1 33.33 29.94 1.20 o 6 2 1 91.59 86.71 2.49 o 7 2 1 125.49 130.41 3.78 o 8 2 1 4.39 5.85 0.60 o 9 2 1 89.51 76.99 5.16 o -9 3 1 16.95 11.18 1.29 o -8 3 1 1.02 -0.52 0.52 o -7 3 1 27.10 29.68 1.12 o -6 3 1 280.40 301.76 5.76 o -5 3 1 12.51 10.32 0.52 o -4 3 1 1056.75 1070.96 19.87 o -3 3 1 696.41 743.56 13.76 o -2 3 1 98.28 103.40 2.15 o -1 3 1 505.35 496.43 9.98 o 1 3 1 519.42 509.24 11.96 o 2 3 1 167.54 182.19 4.22 o 3 3 1 85.97 77.93 1.72 o 4 3 1 369.96 407.91 10.24 o 5 3 1 271.12 259.18 5.33 o 6 3 1 196.50 192.26 3.61 o 7 3 1 25.60 19.78 1.29 o 8 3 1 10.42 9.46 1.29 o 9 3 1 0.03 0.00 1.29 o -9 4 1 21.78 20.65 2.32 o -8 4 1 10.19 3.78 0.86 o -7 4 1 6.47 8.17 0.60 o -6 4 1 123.23 117.59 2.58 o -5 4 1 151.90 155.61 3.27 o -4 4 1 28.23 32.00 0.95 o -3 4 1 4285.27 4276.10 177.63 o -2 4 1 2904.25 2740.37 83.87 o -1 4 1 909.94 882.14 17.81 o 0 4 1 0.77 -0.09 0.34 o 1 4 1 784.36 753.72 17.98 o 2 4 1 6.32 2.41 0.17 o 3 4 1 48.52 47.31 1.20 o 4 4 1 123.35 123.10 3.18 o 5 4 1 79.31 92.39 2.32 o 6 4 1 68.13 82.32 2.67 o 7 4 1 87.58 94.71 3.18 o 8 4 1 3.98 5.33 1.46 o 9 4 1 4.68 4.13 1.38 o -9 5 1 77.83 79.48 4.99 o -8 5 1 110.17 125.50 3.78 o -7 5 1 192.22 210.58 5.94 o -6 5 1 548.02 584.43 15.05 o -5 5 1 2.67 2.67 0.60 o -4 5 1 751.07 717.67 15.31 o -3 5 1 195.71 199.40 4.04 o -2 5 1 208.29 229.76 5.85 o -1 5 1 162.98 155.96 3.10 o 0 5 1 16.55 11.44 0.43 o 1 5 1 0.01 2.84 0.34 o 2 5 1 2015.89 2070.27 43.18 o 3 5 1 267.34 287.48 6.02 o 4 5 1 16.73 17.81 0.77 o 5 5 1 40.73 40.09 1.63 o 6 5 1 75.13 70.28 2.84 o 7 5 1 221.15 212.39 9.38 o 8 5 1 63.78 57.12 3.61 o 9 5 1 4.86 3.53 1.72 o -9 6 1 11.08 10.92 1.98 o -8 6 1 5.57 3.78 0.86 o -7 6 1 2.77 2.67 0.77 o -6 6 1 36.76 27.01 1.29 o -5 6 1 134.53 150.54 3.61 o -4 6 1 417.58 423.91 9.03 o -3 6 1 117.85 126.62 2.67 o -2 6 1 7.17 6.97 0.43 o -1 6 1 1575.86 1640.93 39.48 o 0 6 1 1013.40 1055.05 21.94 o 1 6 1 5.93 4.30 0.43 o 2 6 1 403.32 389.76 8.69 o 3 6 1 456.61 509.93 12.39 o 4 6 1 974.53 1038.96 24.09 o 5 6 1 12.78 17.81 1.03 o 6 6 1 4.55 5.59 0.95 o 7 6 1 112.06 107.01 4.39 o 8 6 1 0.29 0.17 0.95 o -8 7 1 40.18 39.48 2.24 o -7 7 1 17.01 14.11 1.20 o -6 7 1 135.26 135.05 3.70 o -5 7 1 145.00 143.57 3.18 o -4 7 1 81.39 82.75 1.98 o -3 7 1 106.38 112.26 2.24 o -2 7 1 15.18 9.63 0.52 o -1 7 1 228.82 233.80 4.65 o 0 7 1 34.25 28.73 0.86 o 1 7 1 29.94 39.23 1.12 o 2 7 1 402.21 387.27 9.38 o 3 7 1 256.04 268.64 5.59 o 4 7 1 11.77 8.60 0.77 o 5 7 1 134.01 136.86 3.70 o 6 7 1 87.34 83.35 2.75 o 7 7 1 32.90 24.86 1.72 o 8 7 1 11.24 10.92 1.63 o -8 8 1 46.46 55.57 2.75 o -7 8 1 34.10 37.16 1.89 o -6 8 1 5.79 5.76 0.69 o -5 8 1 3.17 1.72 0.52 o -4 8 1 1499.18 1572.46 31.74 o -3 8 1 22.71 29.08 0.86 o -2 8 1 140.60 149.50 3.10 o -1 8 1 167.27 180.64 4.04 o 0 8 1 258.42 240.43 5.33 o 1 8 1 8.67 13.94 0.77 o 2 8 1 354.00 330.32 8.17 o 3 8 1 25.51 29.51 1.12 o 4 8 1 239.67 253.42 5.68 o 5 8 1 347.51 347.44 8.34 o 6 8 1 179.25 191.31 6.02 o 7 8 1 23.95 20.65 1.63 o 8 8 1 29.19 23.74 2.06 o -8 9 1 92.88 99.44 5.33 o -7 9 1 5.61 5.94 0.86 o -6 9 1 12.85 14.80 0.95 o -5 9 1 8.60 5.76 0.60 o -4 9 1 170.79 182.19 3.78 o -3 9 1 22.68 21.85 0.86 o -2 9 1 1.31 3.18 0.52 o -1 9 1 130.82 124.39 3.10 o 0 9 1 313.01 308.82 5.68 o 1 9 1 701.68 718.70 16.34 o 2 9 1 76.67 68.82 1.89 o 3 9 1 610.19 630.45 15.23 o 4 9 1 524.20 562.06 13.25 o 5 9 1 13.22 13.59 1.03 o 6 9 1 0.11 0.00 1.12 o 7 9 1 5.73 3.87 1.03 o 8 9 1 24.50 27.78 3.44 o -8 10 1 87.76 80.69 4.22 o -7 10 1 70.51 70.19 3.18 o -6 10 1 71.90 80.69 2.75 o -5 10 1 28.56 25.72 1.12 o -4 10 1 41.72 39.48 1.20 o -3 10 1 84.53 91.27 2.15 o -2 10 1 0.38 -0.17 0.52 o -1 10 1 0.02 0.77 0.34 o 0 10 1 0.45 0.52 0.43 o 1 10 1 632.51 691.52 16.43 o 2 10 1 329.52 327.48 6.37 o 3 10 1 129.00 127.40 3.10 o 4 10 1 70.98 69.76 2.67 o 5 10 1 25.72 26.75 1.55 o 6 10 1 9.65 7.48 1.20 o 7 10 1 1.34 1.63 1.20 o 8 10 1 31.13 27.44 3.96 o -8 11 1 9.81 6.54 1.20 o -7 11 1 30.97 28.82 1.63 o -6 11 1 136.09 143.05 5.94 o -5 11 1 1.60 1.29 0.77 o -4 11 1 22.99 26.06 0.95 o -3 11 1 60.58 54.37 1.63 o -2 11 1 119.49 115.78 2.92 o -1 11 1 507.23 509.07 12.04 o 0 11 1 13.71 6.19 0.69 o 1 11 1 12.48 13.68 1.03 o 2 11 1 9.98 8.69 0.77 o 3 11 1 29.01 27.10 1.29 o 4 11 1 596.21 593.20 12.82 o 5 11 1 15.60 13.94 1.20 o 6 11 1 12.43 7.31 1.12 o 7 11 1 5.70 4.99 1.46 o -7 12 1 140.46 151.31 6.02 o -6 12 1 137.15 141.25 4.99 o -5 12 1 54.31 57.72 1.89 o -4 12 1 3.28 3.61 0.60 o -3 12 1 502.99 538.40 12.56 o -2 12 1 50.28 47.91 1.63 o -1 12 1 323.41 339.35 8.09 o 0 12 1 58.53 54.80 1.55 o 1 12 1 16.40 14.02 0.95 o 2 12 1 252.88 259.10 7.31 o 3 12 1 286.50 299.52 7.14 o 4 12 1 63.91 64.34 2.32 o 5 12 1 231.77 246.19 7.48 o 6 12 1 2.51 1.29 0.86 o 7 12 1 1.99 2.15 1.20 o -7 13 1 24.24 22.88 1.98 o -6 13 1 20.95 18.15 1.38 o -5 13 1 1.02 2.24 0.69 o -4 13 1 5.19 3.27 0.69 o -3 13 1 6.22 5.51 0.77 o -2 13 1 0.56 0.34 0.77 o -1 13 1 27.22 29.76 1.55 o 0 13 1 109.96 122.06 3.10 o 1 13 1 516.17 510.71 17.72 o 2 13 1 45.51 45.51 1.72 o 3 13 1 16.50 16.17 1.03 o 4 13 1 90.67 86.19 3.10 o 5 13 1 0.64 -0.34 0.95 o 6 13 1 17.78 15.05 1.38 o 7 13 1 31.91 32.09 2.24 o -6 14 1 1.08 0.43 0.86 o -5 14 1 22.19 20.65 1.12 o -4 14 1 69.62 73.89 2.32 o -3 14 1 8.02 8.60 1.03 o -2 14 1 137.63 128.86 4.30 o -1 14 1 2.09 0.95 0.86 o 0 14 1 29.32 28.82 1.55 o 1 14 1 57.24 53.33 1.98 o 2 14 1 542.71 545.20 15.14 o 3 14 1 19.31 16.95 1.38 o 4 14 1 32.59 33.12 1.72 o 5 14 1 0.38 -0.09 0.95 o 6 14 1 16.80 13.33 1.46 o -6 15 1 110.39 108.04 3.78 o -5 15 1 138.43 156.64 5.68 o -4 15 1 1.22 1.12 0.69 o -3 15 1 30.09 31.74 1.98 o -2 15 1 97.45 92.82 3.87 o -1 15 1 11.65 14.19 1.29 o 0 15 1 240.45 242.67 7.40 o 1 15 1 167.10 167.14 5.16 o 2 15 1 100.83 96.09 3.78 o 3 15 1 37.01 35.61 1.81 o 4 15 1 27.35 26.49 1.63 o 5 15 1 58.19 58.24 2.67 o 6 15 1 1.52 3.01 1.29 o -6 16 1 36.35 34.15 2.92 o -5 16 1 57.34 62.97 3.10 o -4 16 1 11.03 11.78 1.03 o -3 16 1 18.55 17.89 1.55 o -2 16 1 284.80 296.00 10.92 o -1 16 1 27.10 27.01 1.81 o 0 16 1 168.80 172.13 5.42 o 1 16 1 0.56 1.72 0.95 o 2 16 1 639.54 694.62 20.90 o 3 16 1 7.93 4.13 1.03 o 4 16 1 63.24 69.25 3.78 o 5 16 1 0.19 0.69 1.38 o -5 17 1 0.01 0.77 1.38 o -4 17 1 0.17 0.26 1.46 o -3 17 1 2.37 2.24 1.20 o -2 17 1 106.97 107.96 4.39 o -1 17 1 4.17 2.32 1.20 o 0 17 1 390.75 407.14 15.57 o 1 17 1 212.37 213.07 6.71 o 2 17 1 7.08 7.74 1.20 o 3 17 1 32.21 29.33 2.32 o 4 17 1 38.90 33.72 2.58 o 5 17 1 10.63 9.46 1.98 o -4 18 1 89.79 93.93 5.16 o -3 18 1 0.01 2.67 1.38 o -2 18 1 3.26 1.38 1.20 o -1 18 1 13.38 13.33 1.72 o 0 18 1 0.32 0.52 1.20 o 1 18 1 53.27 45.59 2.15 o 2 18 1 106.28 100.13 3.96 o 3 18 1 6.83 6.45 1.81 o 4 18 1 81.75 90.49 9.98 o -3 19 1 0.12 -0.43 2.06 o -2 19 1 52.01 45.76 3.44 o -1 19 1 33.64 33.98 2.49 o 0 19 1 8.22 5.94 1.63 o 1 19 1 22.85 21.51 1.63 o 2 19 1 0.58 0.26 1.63 o 3 19 1 14.95 8.17 2.32 o -2 20 1 0.14 1.81 2.67 o -1 20 1 31.52 28.82 3.01 o 0 20 1 61.83 59.35 3.96 o 1 20 1 54.50 52.73 3.44 o 2 20 1 4.31 4.73 2.49 o -8 0 2 90.71 94.54 4.04 o -6 0 2 289.18 294.62 9.81 o -4 0 2 24.21 18.41 0.77 o -2 0 2 2.56 3.70 0.26 o 0 0 2 76.26 53.68 1.81 o 4 0 2 866.27 887.39 22.19 o 6 0 2 24.00 22.97 1.46 o 8 0 2 72.33 73.98 4.04 o -9 1 2 15.21 11.61 0.95 o -8 1 2 6.38 4.39 0.60 o -7 1 2 5.31 6.37 0.69 o -6 1 2 296.86 297.29 5.85 o -5 1 2 33.77 34.67 0.86 o -4 1 2 924.10 929.03 21.68 o -3 1 2 454.13 461.76 8.86 o -2 1 2 2835.01 2742.95 139.44 o -1 1 2 742.47 724.55 14.71 o 0 1 2 424.61 411.44 8.52 o 1 1 2 454.43 434.92 8.09 o 3 1 2 341.32 322.84 6.88 o 4 1 2 7.69 8.34 0.77 o 5 1 2 217.21 236.47 4.82 o 6 1 2 1.13 1.29 0.60 o 7 1 2 21.46 20.47 1.29 o 8 1 2 0.70 2.32 1.12 o 9 1 2 0.55 3.18 2.32 o -9 2 2 13.77 7.23 1.29 o -8 2 2 14.36 10.84 1.03 o -7 2 2 81.49 75.53 2.06 o -6 2 2 129.83 125.85 3.53 o -5 2 2 1190.84 1183.22 22.37 o -4 2 2 65.17 90.92 2.06 o -3 2 2 90.61 86.54 1.89 o -2 2 2 546.33 543.91 12.90 o -1 2 2 184.82 184.26 3.87 o 0 2 2 44.99 38.62 0.77 o 1 2 2 66.80 64.52 1.46 o 2 2 2 94.63 69.85 1.55 o 3 2 2 307.83 308.56 5.94 o 4 2 2 149.96 132.21 2.92 o 5 2 2 21.91 25.12 0.86 o 6 2 2 6.56 7.40 0.69 o 7 2 2 103.69 113.81 3.78 o 8 2 2 10.82 4.99 0.60 o 9 2 2 2.66 3.01 1.89 o -9 3 2 7.96 6.62 2.67 o -8 3 2 8.32 12.21 0.77 o -7 3 2 12.60 11.10 0.86 o -6 3 2 0.01 -0.43 0.52 o -5 3 2 0.50 0.00 0.26 o -4 3 2 240.54 243.01 4.13 o -3 3 2 68.91 69.94 1.38 o -2 3 2 326.12 301.16 5.16 o -1 3 2 399.58 322.41 7.91 o 0 3 2 632.70 617.89 18.67 o 1 3 2 245.96 259.53 5.33 o 2 3 2 487.25 528.51 10.75 o 3 3 2 1766.16 1745.02 37.33 o 4 3 2 95.52 82.24 1.89 o 5 3 2 19.57 22.02 0.86 o 6 3 2 114.58 113.72 3.01 o 7 3 2 31.18 26.32 1.55 o 8 3 2 2.16 7.57 1.38 o 9 3 2 6.58 4.04 2.24 o -9 4 2 8.06 11.87 2.49 o -8 4 2 0.05 0.77 0.52 o -7 4 2 179.37 169.20 3.61 o -6 4 2 23.14 25.38 0.86 o -5 4 2 7.10 6.54 0.34 o -4 4 2 2.27 1.12 0.26 o -3 4 2 4.58 2.67 0.26 o -2 4 2 2131.81 2177.10 43.44 o -1 4 2 48.46 76.82 1.63 o 0 4 2 103.71 88.17 2.15 o 1 4 2 141.86 166.62 3.70 o 2 4 2 40.87 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