#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/32/2103273.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103273_Fobs loop_ _publ_author_name 'Farrell, Dorcas M. M.' 'Glidewell, Christopher' 'Low, John N.' 'Skakle, Janet M. S.' 'Zakaria, Choudhury M.' _publ_section_title ; Polymorphs and pseudopolymorphs of N,N'-dithiobisphthalimide ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 289 _journal_page_last 299 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.964 _cell_angle_gamma 90.000 _cell_length_a 13.5052 _cell_length_b 7.8740 _cell_length_c 29.2050 _exptl_crystal_F_000 1456.00 _reflns_d_resolution_high 0.7710 _[local]_cod_data_source_file na01325sup3.hkl _[local]_cod_data_source_block 5 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 426 - SHELXL' _shelx_refln_list_code 4 _shelx_F_calc_maximum 413.86 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 915.11 535.90 190.13 o 3 0 0 7631.26 7340.28 995.74 o 4 0 0 31363.08 30865.79 1399.69 o 5 0 0 17209.49 16388.60 659.70 o 6 0 0 378.08 386.24 25.39 o 7 0 0 4516.46 4450.67 184.09 o 8 0 0 9577.53 10769.84 385.15 o 9 0 0 2927.29 2633.94 113.07 o 10 0 0 468.52 492.37 44.14 o 11 0 0 3262.25 3370.51 163.86 o 13 0 0 111.74 116.84 36.10 o 16 0 0 1497.80 1692.15 144.32 o 17 0 0 0.02 -21.62 77.57 o 1 1 0 16039.56 14533.28 1911.28 o 2 1 0 425.04 410.35 10.81 o 3 1 0 7752.03 8368.49 191.81 o 4 1 0 52665.40 51816.16 7941.49 o 5 1 0 3141.72 3414.14 63.68 o 6 1 0 991.23 1221.36 35.28 o 7 1 0 1078.42 1023.08 24.18 o 8 1 0 2879.67 2459.80 256.85 o 9 1 0 532.37 548.93 42.55 o 10 1 0 4111.37 3900.28 127.02 o 12 1 0 7.71 -17.46 22.52 o 13 1 0 2521.32 2750.98 149.08 o 14 1 0 558.15 601.87 64.97 o 15 1 0 2206.76 2525.82 168.12 o 16 1 0 125.99 165.35 57.33 o 17 1 0 14.82 3.97 57.03 o 1 2 0 76.81 72.03 3.63 o 2 2 0 27556.64 30428.26 1078.74 o 3 2 0 1322.31 1380.94 43.07 o 4 2 0 2532.91 2734.60 76.94 o 5 2 0 3724.62 3569.40 117.07 o 6 2 0 102.75 117.69 4.17 o 7 2 0 909.60 890.43 86.22 o 8 2 0 54.61 57.52 4.29 o 9 2 0 334.17 293.40 13.12 o 10 2 0 240.84 216.27 12.96 o 11 2 0 124.41 120.32 31.34 o 12 2 0 2258.71 2158.54 346.46 o 15 2 0 157.65 110.50 49.30 o 1 3 0 24.18 27.04 3.56 o 2 3 0 1335.39 1591.21 48.02 o 3 3 0 814.57 911.52 28.57 o 4 3 0 7472.08 8013.08 247.68 o 5 3 0 587.54 630.10 23.19 o 6 3 0 48.34 82.53 5.52 o 7 3 0 2708.28 2892.23 107.91 o 8 3 0 233.96 244.06 12.32 o 9 3 0 495.04 393.71 43.18 o 10 3 0 0.46 -7.26 7.26 o 11 3 0 241.94 199.57 25.00 o 12 3 0 0.09 -5.85 11.80 o 14 3 0 13.07 -9.52 37.99 o 15 3 0 271.28 269.00 67.25 o 16 3 0 27.43 34.82 73.80 o 0 4 0 154.34 159.04 27.77 o 1 4 0 37.41 36.79 5.83 o 2 4 0 898.62 1100.01 43.58 o 3 4 0 447.68 418.57 22.49 o 4 4 0 848.97 1006.96 42.64 o 5 4 0 203.34 242.16 11.80 o 6 4 0 15.38 15.36 5.25 o 7 4 0 3002.62 3388.13 120.65 o 8 4 0 160.60 164.45 11.42 o 9 4 0 90.69 122.23 9.77 o 10 4 0 778.03 794.88 37.38 o 11 4 0 53.19 84.85 33.82 o 12 4 0 123.33 124.62 21.16 o 14 4 0 414.50 390.01 80.54 o 15 4 0 185.47 238.25 63.08 o 1 5 0 757.91 728.03 40.74 o 2 5 0 2961.81 3256.43 137.65 o 3 5 0 936.92 915.24 35.30 o 4 5 0 95.85 106.02 11.45 o 5 5 0 442.67 429.67 27.15 o 6 5 0 90.56 76.54 9.76 o 7 5 0 154.91 147.25 12.98 o 8 5 0 1162.27 1209.25 63.42 o 9 5 0 2548.28 2855.73 161.02 o 10 5 0 174.41 170.43 15.21 o 11 5 0 273.84 284.22 21.19 o 12 5 0 46.38 100.33 29.10 o 13 5 0 32.87 5.14 22.54 o 14 5 0 4.42 -40.77 46.42 o 15 5 0 290.82 305.30 79.55 o 0 6 0 0.02 -3.74 11.15 o 1 6 0 241.90 251.87 18.54 o 2 6 0 456.35 453.95 29.13 o 3 6 0 785.79 718.07 30.02 o 4 6 0 3617.51 3869.99 102.93 o 5 6 0 10.97 7.33 10.19 o 6 6 0 2066.56 2206.62 61.17 o 7 6 0 3.48 17.24 11.83 o 8 6 0 350.74 373.00 22.27 o 9 6 0 36.17 43.91 15.18 o 10 6 0 207.63 243.85 24.77 o 11 6 0 83.79 85.68 20.07 o 12 6 0 439.65 423.26 42.73 o 13 6 0 26.76 36.51 56.09 o 14 6 0 2.95 -17.52 71.66 o 1 7 0 474.71 498.49 25.70 o 2 7 0 636.30 687.67 37.24 o 3 7 0 70.29 72.54 13.13 o 4 7 0 126.52 155.19 17.29 o 5 7 0 1492.74 1484.50 73.76 o 6 7 0 116.19 119.37 15.78 o 7 7 0 422.04 448.06 29.62 o 8 7 0 408.18 438.71 32.68 o 9 7 0 1506.51 1389.83 56.55 o 10 7 0 434.34 418.61 35.76 o 11 7 0 73.60 55.51 26.72 o 12 7 0 903.94 771.76 125.13 o 0 8 0 862.34 959.80 63.23 o 1 8 0 398.05 390.27 24.04 o 2 8 0 1432.09 1557.99 58.67 o 3 8 0 9.57 3.46 17.19 o 4 8 0 68.34 53.43 18.46 o 5 8 0 240.16 235.93 24.29 o 6 8 0 727.00 808.14 47.57 o 7 8 0 0.08 3.73 19.14 o 8 8 0 376.13 324.99 31.19 o 9 8 0 1.35 -3.34 18.97 o 10 8 0 2.67 -0.39 26.88 o 1 9 0 1657.82 1802.40 66.29 o 2 9 0 48.88 73.70 20.46 o 3 9 0 27.75 47.03 26.37 o 4 9 0 113.60 99.09 26.28 o 5 9 0 276.34 276.98 33.01 o 6 9 0 142.25 93.74 29.27 o 7 9 0 1162.61 1010.01 67.59 o 8 9 0 106.78 92.65 45.72 o 0 10 0 19.62 39.20 42.85 o 1 10 0 42.05 19.15 30.52 o 2 10 0 892.78 834.93 72.86 o 3 10 0 0.89 2.67 31.13 o -14 1 1 443.54 431.96 48.11 o -13 1 1 635.06 631.83 60.21 o -12 1 1 17.06 11.21 28.57 o -10 1 1 149.17 140.38 10.34 o -9 1 1 3539.40 3329.87 147.31 o -8 1 1 138.41 141.01 15.90 o -7 1 1 11941.75 12250.39 1192.77 o -6 1 1 3792.68 3991.45 159.60 o -5 1 1 4357.12 4120.71 90.01 o -4 1 1 11.30 18.49 2.91 o -3 1 1 0.17 3.23 1.28 o -2 1 1 21781.87 21802.13 398.08 o -1 1 1 6558.37 6069.88 413.71 o 1 1 1 2441.98 2110.12 158.66 o 2 1 1 28740.34 27846.46 1969.93 o 3 1 1 12914.62 13143.33 245.19 o 4 1 1 10184.42 10839.78 265.62 o 5 1 1 2300.62 2398.62 104.32 o 6 1 1 648.35 902.87 17.07 o 7 1 1 3184.04 2992.69 576.24 o 8 1 1 1310.55 1027.65 203.22 o 9 1 1 747.92 758.05 25.82 o 10 1 1 2522.27 2535.42 94.76 o 12 1 1 185.99 250.15 36.50 o 13 1 1 6.08 35.41 31.54 o 14 1 1 4.30 25.49 33.13 o 17 1 1 60.35 162.77 84.11 o -17 2 1 7.43 12.30 76.57 o -15 2 1 836.64 844.59 82.62 o -12 2 1 1135.68 978.40 142.19 o -11 2 1 603.20 526.27 58.37 o -10 2 1 9.41 11.04 6.31 o -9 2 1 1606.87 1673.62 42.84 o -8 2 1 1208.16 1139.23 46.51 o -7 2 1 381.06 296.00 25.39 o -6 2 1 2108.67 2107.24 33.11 o -5 2 1 960.40 928.74 19.71 o -4 2 1 10.87 6.42 2.31 o -3 2 1 557.81 568.98 10.93 o -2 2 1 39529.55 38944.29 2697.11 o -1 2 1 1769.79 1984.23 73.14 o 0 2 1 7188.62 7649.68 240.70 o 1 2 1 776.09 679.87 21.53 o 2 2 1 21450.89 22950.33 656.50 o 3 2 1 3430.13 3465.24 79.96 o 4 2 1 987.90 1194.07 19.31 o 5 2 1 57.48 73.46 4.50 o 6 2 1 5253.75 5689.94 163.63 o 7 2 1 3454.75 2841.09 389.68 o 8 2 1 1727.54 1724.73 42.89 o 9 2 1 1434.37 1386.33 37.88 o 10 2 1 12.02 10.77 21.08 o 11 2 1 637.43 601.48 32.48 o 12 2 1 56.14 70.30 23.66 o 14 2 1 2.76 22.52 38.39 o 15 2 1 809.76 773.37 87.48 o -16 3 1 116.08 97.01 49.89 o -15 3 1 465.09 467.08 73.90 o -14 3 1 17.79 5.46 40.57 o -12 3 1 8.02 18.85 12.89 o -11 3 1 1369.00 1226.36 66.06 o -10 3 1 207.91 190.13 15.38 o -9 3 1 324.34 327.16 44.42 o -8 3 1 486.39 509.66 22.14 o -7 3 1 1975.36 2008.93 44.18 o -6 3 1 264.19 221.82 9.29 o -5 3 1 400.38 443.18 11.63 o -4 3 1 81.92 79.99 4.90 o -3 3 1 6.41 11.01 3.55 o -2 3 1 3402.07 3342.11 99.15 o -1 3 1 10663.46 11187.80 506.32 o 0 3 1 2100.58 2314.82 55.80 o 1 3 1 1344.41 1708.38 42.03 o 2 3 1 252.95 310.89 9.42 o 3 3 1 2728.29 2680.76 79.29 o 4 3 1 2183.92 2615.01 85.18 o 5 3 1 1252.09 1434.25 33.57 o 6 3 1 279.87 376.96 12.95 o 7 3 1 12165.52 13055.65 355.49 o 8 3 1 1093.64 1111.54 39.35 o 9 3 1 344.55 309.28 42.79 o 10 3 1 1423.71 1364.33 48.05 o 11 3 1 48.96 33.23 16.66 o 12 3 1 1255.09 954.39 56.04 o 14 3 1 0.05 -61.30 61.30 o 15 3 1 414.60 371.86 63.48 o 16 3 1 16.09 39.18 47.51 o -15 4 1 423.27 482.05 74.19 o -14 4 1 103.59 102.36 55.35 o -13 4 1 54.95 28.29 18.81 o -12 4 1 291.28 278.82 46.92 o -11 4 1 80.13 60.41 12.52 o -10 4 1 479.38 482.70 19.37 o -9 4 1 0.12 0.04 7.13 o -8 4 1 349.00 319.03 27.33 o -7 4 1 60.32 49.60 6.61 o -6 4 1 296.44 254.23 11.22 o -5 4 1 1275.68 1458.31 51.38 o -4 4 1 8.56 5.75 4.38 o -3 4 1 5907.86 5329.34 408.87 o -2 4 1 3081.95 3531.65 166.23 o -1 4 1 5632.10 5694.79 202.69 o 0 4 1 1041.60 1382.13 53.40 o 1 4 1 1325.25 1467.35 50.96 o 2 4 1 5518.61 5509.01 519.10 o 3 4 1 674.53 695.06 28.63 o 4 4 1 933.97 1238.81 47.06 o 5 4 1 244.23 270.53 16.66 o 6 4 1 277.93 272.31 15.08 o 7 4 1 1966.01 2025.00 72.02 o 8 4 1 392.07 406.91 17.48 o 9 4 1 12.22 7.15 7.44 o 10 4 1 1818.40 1666.33 72.77 o 11 4 1 1519.49 1676.02 89.57 o 12 4 1 2558.75 2444.09 174.47 o 13 4 1 707.24 505.46 41.16 o 14 4 1 61.57 -11.11 66.75 o 15 4 1 0.59 5.65 75.88 o -15 5 1 86.09 72.31 56.74 o -14 5 1 62.55 43.54 53.36 o -13 5 1 346.40 357.83 43.54 o -12 5 1 30.52 37.52 42.01 o -11 5 1 1376.98 1370.14 65.71 o -10 5 1 2.15 11.09 12.93 o -9 5 1 26.96 30.97 11.17 o -8 5 1 123.74 116.24 14.56 o -7 5 1 1193.56 1158.90 43.58 o -6 5 1 2035.67 2050.45 114.36 o -5 5 1 419.81 473.90 39.00 o -4 5 1 1390.60 1497.44 52.57 o -3 5 1 232.42 232.30 13.35 o -2 5 1 249.72 181.65 12.11 o -1 5 1 2527.32 2826.10 135.23 o 0 5 1 348.33 362.70 18.27 o 1 5 1 275.27 248.24 14.69 o 2 5 1 67.57 99.87 10.82 o 3 5 1 6.04 15.64 9.80 o 4 5 1 1082.46 1255.33 43.79 o 5 5 1 0.08 0.44 7.17 o 6 5 1 184.70 183.40 11.60 o 7 5 1 671.95 700.31 26.32 o 8 5 1 15.21 13.94 8.68 o 9 5 1 195.30 207.19 18.41 o 10 5 1 621.69 692.16 75.97 o 11 5 1 1619.01 1507.36 93.98 o 12 5 1 924.43 885.51 59.49 o 13 5 1 458.19 432.14 38.82 o 14 5 1 49.95 119.62 77.37 o 15 5 1 44.68 106.53 90.96 o -14 6 1 141.86 162.94 41.51 o -13 6 1 34.27 23.05 41.36 o -12 6 1 0.82 16.96 32.63 o -11 6 1 392.40 361.49 27.16 o -10 6 1 143.77 144.67 21.16 o -9 6 1 0.15 15.20 12.77 o -8 6 1 588.92 567.58 29.71 o -7 6 1 264.63 282.46 16.27 o -6 6 1 1329.23 1546.46 70.95 o -5 6 1 3480.58 3796.68 140.79 o -4 6 1 2557.97 2667.07 118.50 o -3 6 1 892.50 942.21 36.74 o -2 6 1 2959.59 3115.21 114.75 o -1 6 1 170.37 167.72 12.94 o 0 6 1 615.06 685.27 34.95 o 1 6 1 36.86 56.82 11.30 o 2 6 1 2.85 -1.04 10.08 o 3 6 1 1.72 -6.56 8.58 o 4 6 1 208.33 231.33 17.63 o 5 6 1 341.97 355.58 29.32 o 6 6 1 1132.85 1172.25 36.63 o 7 6 1 1104.80 1141.92 51.89 o 8 6 1 0.64 20.21 14.32 o 9 6 1 205.00 236.92 19.74 o 10 6 1 133.82 152.35 22.98 o 11 6 1 26.48 32.22 16.06 o 12 6 1 732.37 792.33 51.25 o 13 6 1 20.76 -22.04 75.23 o -12 7 1 646.75 599.59 76.47 o -11 7 1 339.84 330.74 34.89 o -10 7 1 1330.20 1309.13 62.35 o -9 7 1 1560.48 1509.52 78.65 o -8 7 1 288.40 292.17 23.09 o -7 7 1 351.25 329.92 28.75 o -6 7 1 756.03 795.93 45.68 o -5 7 1 386.66 429.88 44.09 o -4 7 1 71.79 58.17 15.24 o -3 7 1 2679.60 2950.40 166.06 o -2 7 1 1.08 3.84 13.19 o -1 7 1 1517.28 1590.92 50.28 o 0 7 1 245.13 265.34 19.81 o 1 7 1 507.28 469.70 24.11 o 2 7 1 10.45 19.96 12.79 o 3 7 1 6.80 5.69 13.21 o 4 7 1 13.73 22.48 11.47 o 5 7 1 282.75 296.00 26.64 o 6 7 1 3590.48 3943.68 102.30 o 7 7 1 710.01 645.37 33.38 o 8 7 1 3217.95 3037.71 169.48 o 9 7 1 239.27 246.44 26.32 o 10 7 1 3.64 11.50 17.10 o 11 7 1 48.89 64.14 21.03 o 12 7 1 93.11 105.23 35.97 o -10 8 1 42.04 56.85 32.17 o -9 8 1 161.56 172.08 26.86 o -8 8 1 216.04 213.61 26.65 o -7 8 1 284.98 288.08 34.58 o -6 8 1 278.99 299.56 25.24 o -5 8 1 147.36 164.65 22.88 o -4 8 1 2273.09 2334.68 79.01 o -3 8 1 70.40 103.51 17.94 o -2 8 1 438.73 508.61 27.79 o -1 8 1 26.38 9.88 13.61 o 0 8 1 14.58 17.29 16.93 o 1 8 1 51.91 34.27 14.91 o 2 8 1 260.86 309.71 22.56 o 3 8 1 62.89 62.60 20.19 o 4 8 1 80.99 86.30 19.29 o 5 8 1 612.46 630.64 45.23 o 6 8 1 738.80 699.22 38.42 o 7 8 1 73.14 71.80 21.83 o 8 8 1 22.28 49.77 20.91 o 9 8 1 204.12 168.61 29.28 o 10 8 1 962.76 983.66 74.79 o -8 9 1 53.28 98.03 37.93 o -7 9 1 171.49 199.85 30.72 o -6 9 1 9.97 0.98 42.36 o -5 9 1 0.10 9.11 23.37 o -4 9 1 549.11 554.19 36.20 o -3 9 1 652.90 604.28 57.95 o -2 9 1 1.06 18.14 20.86 o -1 9 1 48.18 93.15 22.63 o 0 9 1 3.47 12.53 18.59 o 1 9 1 8.11 23.59 31.60 o 2 9 1 41.45 79.98 32.46 o 3 9 1 85.97 80.60 20.07 o 4 9 1 5.16 3.85 19.24 o 5 9 1 70.54 91.94 24.32 o 6 9 1 63.12 48.27 27.62 o 7 9 1 2.19 22.92 21.04 o 8 9 1 0.89 9.35 27.65 o -3 10 1 109.50 78.55 40.78 o -2 10 1 2.21 -23.40 25.25 o -1 10 1 1.05 -10.70 21.99 o 0 10 1 479.89 517.28 38.93 o 1 10 1 275.47 230.92 30.90 o 2 10 1 23.00 17.65 28.92 o 3 10 1 545.88 525.14 69.96 o -15 0 2 5.54 12.20 36.60 o -13 0 2 4060.71 4504.63 209.98 o -11 0 2 1184.46 1271.39 74.99 o -10 0 2 59.22 56.64 17.66 o -9 0 2 3396.21 3597.15 144.42 o -8 0 2 5346.77 4861.50 184.29 o -7 0 2 21118.61 20839.91 749.66 o -6 0 2 159.45 98.59 16.66 o -5 0 2 33711.78 33357.48 5000.86 o -4 0 2 171280.67 -2.58 2.58 o -3 0 2 5514.90 5519.33 555.95 o -2 0 2 6451.04 5843.47 420.52 o 2 0 2 18379.54 16404.49 748.74 o 3 0 2 10337.41 9154.96 503.10 o 4 0 2 158.13 88.61 14.75 o 5 0 2 1394.78 1367.20 144.95 o 6 0 2 839.58 805.21 46.14 o 7 0 2 735.05 827.02 56.36 o 8 0 2 13.21 -1.19 13.29 o 9 0 2 2639.96 2768.34 123.89 o 10 0 2 1074.87 884.76 65.07 o 14 0 2 190.12 228.23 50.39 o 15 0 2 4957.12 5892.37 310.76 o 16 0 2 12.35 108.51 68.14 o 17 0 2 537.19 699.28 108.61 o -14 1 2 2614.27 2874.87 193.62 o -13 1 2 4527.52 4700.62 252.73 o -12 1 2 3845.28 4027.04 188.85 o -11 1 2 864.97 855.27 39.21 o -10 1 2 3542.29 3306.69 185.40 o -9 1 2 953.28 1077.14 64.22 o -8 1 2 10880.68 5263.95 2876.92 o -7 1 2 5182.66 4938.30 584.16 o -6 1 2 1901.32 1933.16 72.68 o -5 1 2 32.97 43.78 3.20 o -4 1 2 9000.97 9336.04 191.39 o -3 1 2 7000.68 6894.21 171.22 o -2 1 2 880.64 849.22 20.24 o -1 1 2 1755.25 1796.03 61.29 o 0 1 2 10310.14 9615.71 654.48 o 1 1 2 3108.42 3088.60 69.73 o 2 1 2 22908.11 23004.71 592.07 o 3 1 2 36.57 40.82 1.98 o 4 1 2 1.61 1.36 1.85 o 5 1 2 671.81 648.55 10.37 o 6 1 2 2564.64 2937.86 75.20 o 7 1 2 2481.40 2466.21 92.10 o 8 1 2 2039.53 1515.46 418.54 o 9 1 2 1244.87 1303.93 59.76 o 10 1 2 2022.62 2184.08 70.16 o 12 1 2 1000.80 1100.29 68.84 o 13 1 2 270.46 293.20 39.48 o 14 1 2 3069.12 3862.58 205.42 o 16 1 2 1018.08 1080.26 127.26 o 17 1 2 38.99 -54.08 54.08 o -17 2 2 50.15 47.51 51.68 o -16 2 2 426.68 269.49 61.50 o -15 2 2 21.99 44.73 34.22 o -13 2 2 866.22 871.76 73.99 o -12 2 2 309.20 283.48 53.36 o -11 2 2 798.44 834.73 41.51 o -10 2 2 3205.51 2784.07 209.93 o -9 2 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107.57 o -6 3 2 127.57 131.46 6.57 o -5 3 2 275.82 302.63 13.31 o -4 3 2 7.04 11.58 3.35 o -3 3 2 41.89 49.42 3.98 o -2 3 2 334.47 409.05 11.38 o -1 3 2 12538.35 13698.64 331.44 o 0 3 2 646.70 638.29 12.80 o 1 3 2 14148.19 15808.77 419.94 o 2 3 2 0.11 -0.05 3.32 o 3 3 2 4918.43 4418.93 289.52 o 4 3 2 4268.24 4453.35 197.16 o 5 3 2 2848.39 2961.79 61.41 o 6 3 2 1625.69 1852.33 37.46 o 7 3 2 3953.20 4200.70 97.86 o 8 3 2 1691.95 1813.83 43.33 o 9 3 2 1575.74 1328.12 231.86 o 10 3 2 209.82 193.45 15.79 o 11 3 2 1462.69 1274.77 79.15 o 12 3 2 818.16 638.42 98.69 o 14 3 2 261.59 318.39 58.82 o 15 3 2 0.16 8.33 67.65 o 16 3 2 75.60 58.92 63.08 o -16 4 2 3.20 95.91 76.18 o -15 4 2 8.08 19.44 51.48 o -14 4 2 23.09 -45.43 45.43 o -13 4 2 121.07 113.87 41.16 o -12 4 2 230.46 265.25 26.03 o -11 4 2 507.14 555.10 27.80 o -10 4 2 3096.35 3171.37 86.44 o -9 4 2 931.06 999.81 43.33 o -8 4 2 272.38 237.76 14.34 o -7 4 2 55.95 62.29 6.71 o -6 4 2 1713.50 1810.66 97.03 o -5 4 2 2612.48 2694.36 139.20 o 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