#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/32/2103277.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103277_Fobs loop_ _publ_author_name 'Farrell, Dorcas M. M.' 'Glidewell, Christopher' 'Low, John N.' 'Skakle, Janet M. S.' 'Zakaria, Choudhury M.' _publ_section_title ; Polymorphs and pseudopolymorphs of N,N'-dithiobisphthalimide ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 289 _journal_page_last 299 _journal_volume 58 _journal_year 2002 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.369 _cell_angle_gamma 90.000 _cell_length_a 14.4180 _cell_length_b 16.0502 _cell_length_c 7.6616 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file na01329sup7.hkl _[local]_cod_data_source_block 9 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 01src585' _shelx_refln_list_code 4 _shelx_F_calc_maximum 172.07 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 626.37 2117.87 75.52 o 6 0 0 6816.27 8482.32 402.23 o 8 0 0 103.96 44.92 9.09 o 10 0 0 8032.84 9878.32 351.15 o 12 0 0 5269.67 6298.54 277.13 o 14 0 0 4.10 -0.35 8.46 o 16 0 0 21.58 -3.69 10.97 o 18 0 0 690.49 570.10 65.00 o 3 1 0 326.41 3495.11 85.08 o 5 1 0 1049.24 938.63 22.80 o 7 1 0 1597.16 1027.74 25.12 o 9 1 0 377.79 156.53 7.93 o 11 1 0 4663.17 4544.30 129.75 o 13 1 0 888.95 865.07 40.41 o 15 1 0 75.87 65.93 9.63 o 17 1 0 127.98 158.23 20.14 o 2 2 0 4049.54 13226.64 314.00 o 4 2 0 9627.88 11931.50 425.33 o 6 2 0 154.58 93.56 4.33 o 8 2 0 1627.56 2735.02 81.63 o 10 2 0 172.54 245.96 10.77 o 12 2 0 270.44 324.18 15.62 o 14 2 0 585.54 561.49 30.71 o 16 2 0 142.15 205.31 42.80 o 18 2 0 36.05 28.31 28.31 o 1 3 0 515.51 5955.36 144.11 o 3 3 0 3836.33 1242.56 30.62 o 5 3 0 2143.84 2264.03 52.52 o 7 3 0 3732.62 3242.49 101.86 o 9 3 0 65.44 21.08 5.02 o 11 3 0 548.17 429.43 19.59 o 13 3 0 536.38 583.01 22.62 o 15 3 0 413.20 387.81 37.36 o 17 3 0 3.45 6.32 15.46 o 0 4 0 234.71 3654.20 112.45 o 2 4 0 1318.45 4056.34 95.18 o 4 4 0 24.61 -0.53 3.39 o 6 4 0 1756.71 2274.62 51.32 o 8 4 0 78.96 223.88 13.93 o 10 4 0 5.21 -0.46 4.09 o 12 4 0 31.99 15.74 5.60 o 14 4 0 207.69 178.94 16.42 o 16 4 0 0.06 -6.59 17.84 o 18 4 0 38.70 28.06 19.84 o 1 5 0 4563.19 8099.89 188.28 o 3 5 0 13.74 15.56 2.31 o 5 5 0 2890.94 2916.48 68.33 o 7 5 0 1775.45 2297.19 52.56 o 9 5 0 1141.78 1307.24 35.66 o 11 5 0 1709.21 1930.69 54.70 o 13 5 0 11.16 32.69 7.68 o 15 5 0 47.82 44.64 12.08 o 17 5 0 29.09 26.97 18.85 o 0 6 0 10792.27 7201.00 198.92 o 2 6 0 8163.97 6514.12 128.03 o 4 6 0 919.94 939.48 22.17 o 6 6 0 830.25 522.03 14.93 o 8 6 0 5330.54 5231.71 146.77 o 10 6 0 717.26 640.16 21.40 o 12 6 0 2808.68 3054.45 98.57 o 14 6 0 2.72 1.87 9.57 o 16 6 0 45.00 34.15 12.71 o 1 7 0 2417.66 2806.00 56.41 o 3 7 0 6696.31 7138.00 154.15 o 5 7 0 192.34 306.91 11.25 o 7 7 0 1144.67 1138.77 36.25 o 9 7 0 278.24 242.53 11.97 o 11 7 0 1742.55 1775.51 54.80 o 13 7 0 1846.89 2061.64 85.97 o 15 7 0 257.95 256.96 21.55 o 17 7 0 227.80 238.14 45.82 o 0 8 0 745.82 471.73 16.74 o 2 8 0 1084.11 958.32 22.43 o 4 8 0 2528.11 3003.47 71.91 o 6 8 0 424.92 396.93 13.28 o 8 8 0 0.41 6.70 4.37 o 10 8 0 3203.06 3517.07 110.69 o 12 8 0 262.62 305.16 16.49 o 14 8 0 998.77 995.03 60.91 o 16 8 0 21.65 -8.04 22.45 o 1 9 0 2215.01 1980.04 50.48 o 3 9 0 907.29 686.16 18.13 o 5 9 0 651.30 620.07 16.96 o 7 9 0 1215.12 1220.04 34.86 o 9 9 0 2197.72 2199.44 66.28 o 11 9 0 1220.86 1243.85 46.40 o 13 9 0 36.01 50.11 10.98 o 15 9 0 202.55 201.20 30.57 o 0 10 0 5497.21 6081.94 175.47 o 2 10 0 0.41 8.78 3.93 o 4 10 0 539.32 687.66 19.07 o 6 10 0 568.19 536.78 18.35 o 8 10 0 347.01 349.94 14.91 o 10 10 0 490.68 626.92 23.93 o 12 10 0 58.90 78.20 13.14 o 14 10 0 3.36 -3.38 13.95 o 16 10 0 18.15 3.60 37.69 o 1 11 0 93.52 40.28 6.14 o 3 11 0 1724.23 2151.99 46.37 o 5 11 0 10.63 13.68 4.49 o 7 11 0 266.79 301.47 14.33 o 9 11 0 924.21 1138.17 38.30 o 11 11 0 116.70 85.88 12.61 o 13 11 0 2.11 -7.19 11.06 o 15 11 0 6.33 -10.81 36.86 o 0 12 0 1.55 49.45 19.52 o 2 12 0 2339.22 1921.45 52.47 o 4 12 0 545.30 377.53 19.14 o 6 12 0 226.64 186.92 11.06 o 8 12 0 1232.61 1149.33 39.16 o 10 12 0 507.90 435.82 24.69 o 12 12 0 12.41 12.30 9.39 o 14 12 0 120.06 126.65 30.57 o 1 13 0 1273.52 1878.19 57.03 o 3 13 0 353.19 496.06 25.44 o 5 13 0 247.74 180.76 11.86 o 7 13 0 428.10 367.17 15.58 o 9 13 0 960.02 1034.59 42.85 o 11 13 0 537.05 718.61 37.32 o 13 13 0 512.41 622.53 69.27 o 0 14 0 2719.09 2050.04 107.41 o 2 14 0 1561.59 1130.84 43.12 o 4 14 0 511.83 558.15 26.60 o 6 14 0 221.84 208.53 14.75 o 8 14 0 17.13 6.54 7.99 o 10 14 0 1509.69 1492.26 67.77 o 12 14 0 563.74 710.57 71.12 o 1 15 0 2599.32 3463.58 120.19 o 3 15 0 422.90 696.56 33.42 o 5 15 0 4.68 15.29 7.44 o 7 15 0 489.36 504.91 27.45 o 9 15 0 1056.78 1377.91 71.16 o 11 15 0 558.71 621.69 63.91 o 0 16 0 952.84 660.27 39.57 o 2 16 0 464.44 243.55 15.43 o 4 16 0 608.76 428.04 24.81 o 6 16 0 135.41 105.15 13.71 o 8 16 0 1004.29 981.85 68.27 o 10 16 0 149.26 125.81 33.25 o 1 17 0 8.56 64.73 10.74 o 3 17 0 50.03 90.75 11.45 o 5 17 0 100.51 90.93 14.28 o 7 17 0 71.18 64.70 33.71 o 9 17 0 0.03 -8.13 28.81 o 0 18 0 17.65 93.35 19.76 o 2 18 0 40.80 86.25 13.46 o 4 18 0 22.81 18.40 13.13 o 6 18 0 10.93 -18.37 20.21 o 8 18 0 8.18 9.05 27.06 o 1 19 0 68.03 28.74 15.46 o 3 19 0 35.40 21.41 15.19 o 5 19 0 17.62 17.17 29.90 o 7 19 0 189.76 260.92 51.51 o 0 20 0 63.67 145.66 46.74 o 2 20 0 660.94 754.39 63.31 o 4 20 0 4.52 -36.35 36.35 o -17 1 1 0.68 -1.75 12.48 o -15 1 1 46.60 32.72 9.36 o -13 1 1 1795.99 1923.74 62.41 o -11 1 1 2391.01 2653.47 69.75 o -9 1 1 161.01 136.48 6.69 o -7 1 1 1538.06 1604.26 38.17 o -5 1 1 6057.45 6923.95 144.27 o -3 1 1 6356.06 6968.86 202.46 o -1 1 1 4720.97 4006.77 706.17 o 1 1 1 2607.28 2293.04 59.85 o 3 1 1 1180.22 1499.51 43.44 o 5 1 1 1900.05 2118.44 87.44 o 7 1 1 5979.00 6607.73 149.57 o 9 1 1 242.09 312.71 11.50 o 11 1 1 957.13 948.74 29.17 o 13 1 1 0.41 4.88 6.57 o 15 1 1 1284.21 1324.05 117.59 o 17 1 1 20.52 12.72 19.75 o -18 2 1 8.51 0.92 16.42 o -16 2 1 251.60 231.30 22.85 o -14 2 1 108.20 107.25 10.07 o -12 2 1 4506.63 4463.13 130.58 o -10 2 1 307.06 221.97 10.23 o -8 2 1 1371.57 1654.40 43.88 o -6 2 1 304.63 539.11 13.14 o -4 2 1 4221.28 3014.32 82.93 o -2 2 1 3218.02 2149.53 67.83 o 0 2 1 15402.27 15004.70 368.41 o 2 2 1 124.24 18.62 2.21 o 4 2 1 620.43 317.45 9.41 o 6 2 1 733.84 622.39 20.34 o 8 2 1 1425.81 1338.51 38.72 o 10 2 1 956.11 1087.68 41.78 o 12 2 1 2375.58 2513.97 109.75 o 14 2 1 765.92 706.45 36.46 o 16 2 1 41.62 39.39 17.56 o 18 2 1 236.84 220.72 40.29 o -17 3 1 158.66 107.30 24.38 o -15 3 1 1621.08 1647.96 76.45 o -13 3 1 368.98 435.69 20.25 o -11 3 1 2823.69 3273.52 110.85 o -9 3 1 663.63 601.55 15.06 o -7 3 1 44.66 90.50 4.56 o -5 3 1 602.60 853.21 20.89 o -3 3 1 2203.62 3187.45 85.50 o -1 3 1 4083.33 4499.00 104.99 o 1 3 1 7802.15 6615.62 146.77 o 3 3 1 503.47 964.52 28.68 o 5 3 1 520.74 319.31 9.18 o 7 3 1 3019.28 3100.21 83.33 o 9 3 1 1166.41 1093.70 32.52 o 11 3 1 3456.94 3434.95 124.01 o 13 3 1 180.31 145.82 13.52 o 15 3 1 5.98 15.50 11.00 o 17 3 1 510.56 536.33 133.69 o -18 4 1 27.75 18.09 20.77 o -16 4 1 572.60 674.19 45.39 o -14 4 1 2373.24 2180.27 88.19 o -12 4 1 809.96 672.34 24.06 o -10 4 1 1862.20 1564.25 43.78 o -8 4 1 150.00 157.76 8.44 o -6 4 1 29.30 7.90 2.56 o -4 4 1 23622.85 2194.66 8072.24 o -2 4 1 2170.22 1123.27 26.93 o 0 4 1 12899.19 12210.15 278.12 o 2 4 1 135.07 407.68 11.31 o 4 4 1 31.62 15.87 3.12 o 6 4 1 6613.12 6502.17 142.30 o 8 4 1 4736.92 5211.23 117.27 o 10 4 1 508.42 520.77 18.51 o 12 4 1 911.50 997.20 36.09 o 14 4 1 17.81 18.11 9.60 o 16 4 1 231.58 232.24 25.00 o -17 5 1 2.90 27.89 20.69 o -15 5 1 1289.06 1239.84 63.11 o -13 5 1 613.19 737.41 32.80 o -11 5 1 2487.21 3166.87 82.89 o -9 5 1 1354.98 1736.09 43.05 o -7 5 1 186.02 253.35 8.97 o -5 5 1 8484.39 10984.14 257.53 o -3 5 1 10074.18 12105.29 286.98 o -1 5 1 7528.87 8061.26 184.87 o 1 5 1 5123.51 4418.69 106.09 o 3 5 1 3947.37 5366.94 112.51 o 5 5 1 44.55 137.02 7.36 o 7 5 1 11129.79 12716.00 270.71 o 9 5 1 808.82 739.13 22.74 o 11 5 1 819.89 734.36 26.31 o 13 5 1 373.30 416.85 21.76 o 15 5 1 0.16 -4.74 11.79 o 17 5 1 445.39 428.70 62.15 o -16 6 1 130.26 89.01 20.77 o -14 6 1 447.46 416.25 28.75 o -12 6 1 136.00 184.07 11.44 o -10 6 1 3014.78 2475.74 67.89 o -8 6 1 692.83 819.27 25.40 o -6 6 1 2.29 15.39 2.69 o -4 6 1 2585.00 1826.43 40.40 o -2 6 1 587.55 1235.55 27.68 o 0 6 1 4389.81 4250.68 94.00 o 2 6 1 1247.47 856.06 21.20 o 4 6 1 2347.35 3317.18 77.41 o 6 6 1 274.26 183.89 8.85 o 8 6 1 912.16 960.06 24.52 o 10 6 1 2208.75 2679.73 77.54 o 12 6 1 437.14 362.77 17.95 o 14 6 1 119.66 97.63 14.41 o 16 6 1 3.08 -1.73 14.36 o -17 7 1 9.24 26.13 22.53 o -15 7 1 215.14 182.97 32.37 o -13 7 1 89.99 22.90 7.39 o -11 7 1 459.36 250.44 11.66 o -9 7 1 257.25 345.37 14.35 o -7 7 1 390.17 411.05 21.27 o -5 7 1 628.52 433.16 12.15 o -3 7 1 175.94 487.16 13.37 o -1 7 1 5701.68 5138.59 110.23 o 1 7 1 20.63 4.75 3.01 o 3 7 1 2692.16 2057.44 48.86 o 5 7 1 144.25 25.37 4.66 o 7 7 1 60.60 51.21 6.02 o 9 7 1 169.33 155.72 9.68 o 11 7 1 85.75 92.06 8.17 o 13 7 1 209.06 224.66 24.22 o 15 7 1 111.48 85.72 15.51 o 17 7 1 60.21 76.31 30.57 o -16 8 1 124.01 38.78 31.58 o -14 8 1 51.45 67.10 21.07 o -12 8 1 0.08 8.10 5.95 o -10 8 1 674.80 911.84 32.85 o -8 8 1 154.27 100.59 6.55 o -6 8 1 573.97 659.54 17.67 o -4 8 1 4.87 91.34 6.51 o -2 8 1 3.67 7.54 3.02 o 0 8 1 850.68 875.22 21.22 o 2 8 1 198.71 332.13 10.61 o 4 8 1 445.75 313.29 11.38 o 6 8 1 20.10 4.73 4.41 o 8 8 1 380.11 347.23 13.88 o 10 8 1 1751.40 1737.92 55.06 o 12 8 1 384.99 414.59 21.35 o 14 8 1 144.77 120.76 23.66 o 16 8 1 8.22 -10.72 19.68 o -15 9 1 607.21 529.45 76.14 o -13 9 1 415.26 403.99 29.16 o -11 9 1 417.01 623.91 23.70 o -9 9 1 3062.87 2526.12 76.36 o -7 9 1 923.98 909.97 26.09 o -5 9 1 674.21 514.08 18.56 o -3 9 1 2274.09 1877.04 42.49 o -1 9 1 593.73 917.74 24.16 o 1 9 1 109.71 129.74 7.42 o 3 9 1 3851.40 4769.22 104.48 o 5 9 1 194.52 100.31 7.35 o 7 9 1 446.27 447.95 17.46 o 9 9 1 3924.46 4148.49 120.06 o 11 9 1 190.02 139.94 12.65 o 13 9 1 592.84 632.33 39.58 o 15 9 1 20.71 -6.28 21.44 o -16 10 1 542.70 513.05 57.71 o -14 10 1 1164.53 1212.71 97.38 o -12 10 1 565.24 743.52 55.84 o -10 10 1 417.94 571.85 24.53 o -8 10 1 1782.01 1802.62 51.70 o -6 10 1 1434.07 1697.89 45.58 o -4 10 1 5098.66 5860.82 136.16 o -2 10 1 4843.06 5329.60 113.30 o 0 10 1 348.33 306.15 16.70 o 2 10 1 1115.13 990.22 25.29 o 4 10 1 89.64 143.03 8.85 o 6 10 1 3652.11 3917.59 103.34 o 8 10 1 3096.97 3222.29 112.72 o 10 10 1 235.57 200.07 14.51 o 12 10 1 69.26 42.21 10.62 o 14 10 1 47.50 44.41 15.73 o 16 10 1 129.88 126.23 34.93 o -15 11 1 745.51 995.53 111.99 o -13 11 1 1137.68 1018.44 93.77 o -11 11 1 2460.31 2379.32 109.44 o -9 11 1 22.10 6.26 4.73 o -7 11 1 1.30 3.69 4.52 o -5 11 1 1372.36 1112.29 31.07 o -3 11 1 3729.40 3265.52 84.98 o -1 11 1 7685.52 7426.07 160.69 o 1 11 1 755.09 927.25 26.87 o 3 11 1 230.31 161.61 14.76 o 5 11 1 1928.68 1692.93 49.65 o 7 11 1 1951.93 1997.22 56.13 o 9 11 1 959.98 1038.78 49.99 o 11 11 1 1134.29 1311.01 63.24 o 13 11 1 13.11 33.54 16.19 o 15 11 1 49.50 32.17 25.88 o -14 12 1 871.10 1085.74 97.75 o -12 12 1 1244.92 1263.36 89.46 o -10 12 1 205.59 288.15 17.62 o -8 12 1 522.04 553.48 25.21 o -6 12 1 35.81 55.44 6.78 o -4 12 1 0.65 5.69 4.98 o -2 12 1 3925.75 4136.43 110.75 o 0 12 1 503.76 539.94 18.39 o 2 12 1 974.22 766.77 23.43 o 4 12 1 1238.43 1466.52 46.30 o 6 12 1 5.92 9.49 6.17 o 8 12 1 421.87 344.93 17.05 o 10 12 1 1266.42 1260.44 45.10 o 12 12 1 997.25 984.09 68.36 o 14 12 1 60.58 59.81 30.41 o -13 13 1 318.16 385.90 46.15 o -11 13 1 403.42 385.76 22.31 o -9 13 1 39.46 51.57 7.99 o -7 13 1 60.93 70.33 8.36 o -5 13 1 0.86 7.13 5.51 o -3 13 1 459.50 389.29 18.55 o -1 13 1 56.16 45.47 7.76 o 1 13 1 674.67 820.92 27.43 o 3 13 1 1.54 20.78 6.53 o 5 13 1 21.45 9.09 8.73 o 7 13 1 148.78 144.14 10.19 o 9 13 1 91.25 110.42 12.41 o 11 13 1 862.33 1031.74 67.05 o 13 13 1 34.60 30.32 25.88 o -12 14 1 53.96 60.56 27.14 o -10 14 1 528.58 503.03 40.42 o -8 14 1 26.47 23.07 9.23 o -6 14 1 161.91 106.26 9.51 o -4 14 1 1887.43 2158.16 70.64 o -2 14 1 680.61 638.21 23.80 o 0 14 1 2420.05 2263.17 74.98 o 2 14 1 1130.79 1286.20 47.16 o 4 14 1 428.89 333.78 16.98 o 6 14 1 804.30 857.93 31.83 o 8 14 1 13.12 10.67 9.05 o 10 14 1 20.79 19.97 15.96 o 12 14 1 27.66 35.68 28.56 o -11 15 1 1.44 12.65 24.46 o -9 15 1 17.25 30.36 12.13 o -7 15 1 137.18 161.04 13.16 o -5 15 1 67.02 56.66 11.50 o -3 15 1 119.97 114.82 11.68 o -1 15 1 46.61 28.52 9.35 o 1 15 1 36.57 58.07 8.71 o 3 15 1 521.56 424.72 21.26 o 5 15 1 507.94 549.97 24.44 o 7 15 1 186.74 212.02 18.29 o 9 15 1 168.93 161.35 23.49 o 11 15 1 115.20 105.29 31.24 o -10 16 1 331.16 362.11 57.04 o -8 16 1 0.03 20.44 10.08 o -6 16 1 259.10 272.47 30.11 o -4 16 1 420.55 365.08 18.90 o -2 16 1 1312.54 1468.75 55.23 o 0 16 1 486.93 528.92 24.82 o 2 16 1 16.58 50.36 11.22 o 4 16 1 93.84 79.73 11.21 o 6 16 1 890.09 956.30 43.80 o 8 16 1 140.90 185.11 26.95 o 10 16 1 555.59 550.16 57.21 o -9 17 1 337.58 275.58 52.60 o -7 17 1 182.73 190.81 41.80 o -5 17 1 301.57 351.70 31.52 o -3 17 1 1216.74 1305.69 63.35 o -1 17 1 1260.99 1234.38 58.44 o 1 17 1 299.15 255.15 18.01 o 3 17 1 0.01 3.85 9.23 o 5 17 1 709.88 741.03 42.58 o 7 17 1 390.04 343.84 38.88 o 9 17 1 728.97 714.42 83.26 o -8 18 1 0.07 16.33 27.22 o -6 18 1 128.41 111.07 36.44 o -4 18 1 254.14 289.00 40.25 o -2 18 1 763.00 923.32 95.94 o 0 18 1 515.50 575.17 37.26 o 2 18 1 156.90 149.25 16.96 o 4 18 1 72.00 72.01 16.44 o 6 18 1 165.47 153.96 28.86 o 8 18 1 299.00 345.78 59.14 o -7 19 1 6.67 60.98 49.17 o -5 19 1 295.04 292.17 46.57 o -3 19 1 211.36 192.26 25.13 o -1 19 1 755.37 739.80 106.89 o 1 19 1 201.58 187.36 26.18 o 3 19 1 12.07 -20.48 20.48 o 5 19 1 19.72 24.02 19.10 o 7 19 1 211.49 123.05 38.62 o -4 20 1 360.23 439.34 59.56 o -2 20 1 303.92 304.98 57.88 o 0 20 1 179.84 213.99 46.28 o 2 20 1 9.75 -18.64 18.64 o 4 20 1 12.20 25.08 21.94 o -18 0 2 26.31 29.57 16.67 o -16 0 2 1264.74 1317.67 221.18 o -14 0 2 2682.09 3265.88 252.67 o -12 0 2 3365.57 3618.05 136.07 o -10 0 2 0.63 2.60 5.07 o -8 0 2 13400.56 15761.62 724.93 o -6 0 2 33.53 6.04 2.88 o -4 0 2 22020.98 22503.10 1132.90 o -2 0 2 3693.82 2639.71 85.24 o 4 0 2 3611.55 2602.07 84.77 o 6 0 2 486.59 324.56 23.20 o 8 0 2 539.92 521.41 22.59 o 10 0 2 1332.50 2071.27 89.68 o 12 0 2 19.02 4.83 10.02 o 14 0 2 2188.68 2303.84 168.28 o 16 0 2 352.36 169.62 36.19 o 18 0 2 311.01 189.89 37.27 o -17 1 2 245.52 239.92 21.71 o -15 1 2 1585.88 1390.53 63.19 o -13 1 2 980.22 824.37 49.33 o -11 1 2 416.83 438.51 17.06 o -9 1 2 752.66 653.77 16.72 o -7 1 2 3087.65 2195.72 51.27 o -5 1 2 1176.94 580.55 13.92 o -3 1 2 8644.41 7811.77 172.66 o -1 1 2 1355.18 1702.51 40.19 o 1 1 2 6336.11 6429.31 174.14 o 3 1 2 27506.87 31359.21 957.01 o 5 1 2 2.61 44.27 4.34 o 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