#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103281.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103281_Fobs loop_ _publ_author_name 'Quesada, Antonio' 'Marchal, Antonio' 'Melguizo, Manuel' 'Nogueras, Manuel' 'S\'anchez, Adolfo' 'Low, John N.' 'Cannon, Debbie' 'Farrell, Dorcas M. M.' 'Glidewell, Christopher' _publ_section_title ; Amino-substituted O^6^-benzyl-5-nitrosopyrimidines: interplay of molecular, molecular-electronic and supramolecular structures ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 300 _journal_page_last 315 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.580 _cell_angle_gamma 90.000 _cell_length_a 11.6769 _cell_length_b 13.3621 _cell_length_c 21.4781 _exptl_crystal_F_000 1408.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file na01333sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 00SRC458 in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 300.75 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13014.78 11744.83 424.80 o 4 0 0 14455.48 13697.58 340.01 o 6 0 0 1919.85 2131.06 50.22 o 8 0 0 35.15 58.92 38.15 o 10 0 0 264.80 199.41 41.56 o 12 0 0 147.45 166.69 62.49 o 14 0 0 8.56 69.62 69.62 o 1 1 0 496.65 411.13 23.90 o 2 1 0 71.98 52.95 3.47 o 3 1 0 23.43 17.37 4.18 o 4 1 0 388.44 357.35 8.17 o 5 1 0 40.19 40.83 3.45 o 6 1 0 2826.31 2909.72 60.89 o 7 1 0 654.17 671.29 16.67 o 8 1 0 152.60 157.10 33.11 o 9 1 0 274.76 264.43 35.28 o 10 1 0 540.86 567.38 70.71 o 11 1 0 149.95 184.68 44.97 o 12 1 0 1.90 45.19 36.71 o 13 1 0 0.26 -33.85 56.60 o 14 1 0 97.62 27.97 61.75 o 0 2 0 33.99 40.29 6.91 o 1 2 0 7264.41 6579.46 94.28 o 2 2 0 75.45 67.04 3.54 o 3 2 0 420.39 370.00 7.11 o 4 2 0 0.91 2.64 2.88 o 5 2 0 244.91 258.70 26.34 o 6 2 0 1193.96 1241.81 24.50 o 7 2 0 0.27 -2.75 2.75 o 8 2 0 1.98 15.71 6.64 o 9 2 0 136.16 122.86 9.02 o 10 2 0 71.97 71.75 29.29 o 11 2 0 117.13 125.98 31.67 o 12 2 0 45.62 27.91 49.00 o 13 2 0 9.64 9.97 53.71 o 14 2 0 4.72 33.18 73.50 o 1 3 0 1810.57 1970.18 29.73 o 2 3 0 7296.98 6636.85 93.09 o 3 3 0 7362.11 7474.67 103.68 o 4 3 0 4195.70 3740.47 63.24 o 5 3 0 137.06 93.71 4.99 o 6 3 0 3154.29 3164.38 144.48 o 7 3 0 234.94 237.44 7.74 o 8 3 0 2286.12 2448.80 54.12 o 9 3 0 0.29 3.32 8.27 o 10 3 0 56.94 63.29 11.11 o 11 3 0 119.38 122.41 55.75 o 12 3 0 214.12 234.83 55.44 o 13 3 0 716.85 631.52 66.26 o 14 3 0 30.03 -64.97 81.91 o 0 4 0 450.39 468.44 13.53 o 1 4 0 374.82 335.58 8.92 o 2 4 0 33.47 26.50 4.23 o 3 4 0 264.62 230.63 7.14 o 4 4 0 0.70 -2.89 4.46 o 5 4 0 89.23 73.70 5.16 o 6 4 0 0.09 -4.40 4.56 o 7 4 0 140.57 147.80 9.69 o 8 4 0 547.72 472.06 32.15 o 9 4 0 3.28 2.46 5.05 o 10 4 0 1006.86 1065.26 37.95 o 11 4 0 0.02 -9.00 9.00 o 12 4 0 125.63 110.72 16.13 o 13 4 0 2.48 -47.45 66.83 o 1 5 0 385.91 354.19 11.09 o 2 5 0 0.54 3.39 5.37 o 3 5 0 18.90 22.35 5.33 o 4 5 0 641.82 629.35 15.19 o 5 5 0 28.43 25.26 6.91 o 6 5 0 268.65 288.72 9.77 o 7 5 0 1011.98 1152.98 29.03 o 8 5 0 198.98 196.78 9.92 o 9 5 0 294.01 276.33 22.75 o 10 5 0 16.71 23.19 7.42 o 11 5 0 37.60 55.12 15.19 o 12 5 0 20.09 -6.82 49.67 o 13 5 0 56.18 45.74 80.94 o 0 6 0 1181.95 1292.01 31.78 o 1 6 0 9637.57 10297.03 144.18 o 2 6 0 460.16 495.55 12.89 o 3 6 0 58.25 70.34 6.46 o 4 6 0 899.01 988.06 19.29 o 5 6 0 392.63 370.45 11.29 o 6 6 0 0.88 -1.91 5.84 o 7 6 0 369.63 380.79 12.73 o 8 6 0 482.42 472.91 14.44 o 9 6 0 2451.20 2675.01 64.19 o 10 6 0 5.16 4.48 9.50 o 11 6 0 187.96 192.65 16.67 o 12 6 0 86.79 70.51 27.44 o 13 6 0 5.32 -3.57 65.28 o 1 7 0 1901.36 1903.50 34.05 o 2 7 0 242.66 239.24 11.34 o 3 7 0 33.46 45.77 7.06 o 4 7 0 78.53 108.40 8.55 o 5 7 0 72.14 76.26 7.68 o 6 7 0 42.01 45.73 6.75 o 7 7 0 24.71 25.76 7.79 o 8 7 0 246.41 255.69 12.61 o 9 7 0 14.46 7.60 8.95 o 10 7 0 137.92 143.11 14.81 o 11 7 0 410.67 386.71 21.51 o 12 7 0 99.68 89.63 40.35 o 13 7 0 26.64 -4.69 25.66 o 0 8 0 5605.32 6597.68 158.68 o 1 8 0 305.88 303.51 13.38 o 2 8 0 73.48 85.10 10.97 o 3 8 0 296.42 324.51 14.21 o 4 8 0 190.69 178.97 10.76 o 5 8 0 300.14 263.49 13.62 o 6 8 0 2789.57 2861.94 59.32 o 7 8 0 353.05 350.25 14.05 o 8 8 0 1697.86 1731.63 46.45 o 9 8 0 841.55 946.81 25.99 o 10 8 0 1024.01 1086.40 33.81 o 11 8 0 426.57 492.84 26.50 o 12 8 0 15.82 -5.87 16.12 o 13 8 0 10.56 136.15 107.92 o 1 9 0 0.08 12.07 9.81 o 2 9 0 596.72 587.35 18.19 o 3 9 0 474.06 464.48 18.25 o 4 9 0 496.62 446.01 17.36 o 5 9 0 159.95 166.05 12.50 o 6 9 0 683.44 681.50 21.56 o 7 9 0 394.96 405.06 17.65 o 8 9 0 75.71 60.69 12.92 o 9 9 0 546.26 537.37 21.87 o 10 9 0 172.45 168.63 25.58 o 11 9 0 13.94 0.15 21.76 o 12 9 0 26.04 38.68 39.26 o 0 10 0 221.97 228.92 22.13 o 1 10 0 3.09 2.35 10.30 o 2 10 0 0.43 -10.47 12.44 o 3 10 0 5.28 -5.20 9.75 o 4 10 0 530.31 518.60 21.51 o 5 10 0 15.08 4.03 10.32 o 6 10 0 143.13 140.93 17.60 o 7 10 0 197.95 192.01 15.71 o 8 10 0 4.18 11.98 12.25 o 9 10 0 56.45 68.65 14.78 o 10 10 0 0.92 -21.82 21.82 o 11 10 0 167.42 246.26 36.41 o 12 10 0 0.98 -21.61 23.43 o 1 11 0 109.98 116.82 15.36 o 2 11 0 0.01 0.90 11.88 o 3 11 0 135.08 159.79 16.58 o 4 11 0 4.36 15.40 13.08 o 5 11 0 1203.94 1268.14 35.56 o 6 11 0 2690.43 2882.44 82.10 o 7 11 0 924.01 898.22 34.84 o 8 11 0 729.34 780.61 38.44 o 9 11 0 58.42 47.29 19.12 o 10 11 0 7.23 10.05 25.66 o 11 11 0 108.36 144.80 34.94 o 0 12 0 0.16 18.36 19.78 o 1 12 0 324.45 311.58 20.15 o 2 12 0 1.15 15.71 13.79 o 3 12 0 185.71 157.23 18.35 o 4 12 0 51.82 54.51 15.11 o 5 12 0 417.00 418.11 24.07 o 6 12 0 515.80 547.83 31.05 o 7 12 0 166.97 166.51 19.62 o 8 12 0 66.18 49.22 25.54 o 9 12 0 31.91 49.14 30.31 o 10 12 0 50.85 89.74 72.88 o 1 13 0 0.47 -3.98 17.20 o 2 13 0 86.55 86.45 20.03 o 3 13 0 130.33 134.18 21.82 o 4 13 0 171.95 166.08 24.16 o 5 13 0 478.46 504.27 28.63 o 6 13 0 63.99 64.89 18.69 o 7 13 0 28.52 37.09 23.38 o 8 13 0 11.08 16.44 29.49 o 9 13 0 20.11 -5.34 36.50 o 0 14 0 895.12 736.64 64.36 o 1 14 0 4.85 0.92 25.46 o 2 14 0 2.43 30.92 22.60 o 3 14 0 83.05 124.37 25.53 o 4 14 0 0.47 -23.48 23.48 o 5 14 0 29.57 30.49 21.75 o 6 14 0 49.36 115.41 33.51 o 7 14 0 2.70 5.80 35.44 o 8 14 0 21.32 65.42 32.87 o 1 15 0 28.45 20.96 33.95 o 2 15 0 12.35 25.12 28.29 o 3 15 0 30.77 78.38 44.02 o 4 15 0 0.08 9.78 41.54 o 5 15 0 40.17 21.35 38.65 o 6 15 0 57.41 56.49 32.41 o 7 15 0 43.80 57.37 78.31 o 1 16 0 7.62 -32.64 32.64 o 2 16 0 109.04 136.66 36.17 o 3 16 0 90.71 140.09 104.12 o 4 16 0 56.13 54.40 82.57 o 5 16 0 142.40 201.54 55.48 o 1 17 0 141.46 164.36 41.25 o -11 0 1 146.59 164.99 52.10 o -9 0 1 18.45 55.51 31.32 o -7 0 1 211.82 165.14 26.05 o -5 0 1 87.94 118.62 20.93 o -1 0 1 32.31 -1.86 1.86 o 1 0 1 7.11 74.20 11.79 o 3 0 1 348.01 401.95 11.06 o 5 0 1 107.52 139.45 7.08 o 7 0 1 92.78 68.43 10.68 o 9 0 1 4.36 55.36 43.26 o 11 0 1 68.82 3.41 48.53 o 13 0 1 17.06 38.30 66.06 o -14 1 1 129.73 116.32 56.01 o -13 1 1 4.35 -13.89 36.89 o -12 1 1 117.61 77.38 36.82 o -11 1 1 336.66 304.39 64.04 o -10 1 1 87.92 96.76 37.99 o -9 1 1 642.42 664.91 64.66 o -8 1 1 0.31 -24.50 24.50 o -7 1 1 1021.34 997.85 26.50 o -6 1 1 5536.61 5697.72 120.31 o -5 1 1 282.71 232.64 13.06 o -4 1 1 63.68 60.77 3.69 o -3 1 1 160.35 153.72 4.92 o -2 1 1 164.77 126.69 2.80 o -1 1 1 2894.34 2539.50 110.63 o 0 1 1 2897.28 1927.31 690.91 o 1 1 1 1496.86 1306.00 20.33 o 2 1 1 109.28 106.42 3.57 o 3 1 1 1366.38 1296.20 27.15 o 4 1 1 589.41 573.28 35.93 o 5 1 1 348.49 225.25 19.37 o 6 1 1 3658.56 3776.02 85.47 o 7 1 1 0.52 -4.99 5.68 o 8 1 1 389.28 403.50 10.86 o 9 1 1 903.05 874.98 30.99 o 10 1 1 61.21 31.01 41.25 o 11 1 1 270.79 304.72 50.55 o 12 1 1 0.46 68.55 36.79 o 13 1 1 59.66 155.61 107.15 o 14 1 1 48.52 -31.48 75.05 o -14 2 1 38.61 45.49 50.25 o -13 2 1 140.49 92.73 89.16 o -12 2 1 133.05 258.96 64.66 o -11 2 1 14.51 66.82 33.07 o -10 2 1 39.55 42.95 39.54 o -9 2 1 437.27 486.08 16.24 o -8 2 1 620.56 705.82 28.76 o -7 2 1 292.70 281.29 11.64 o -6 2 1 2667.47 2758.41 56.05 o -5 2 1 304.61 282.29 6.75 o -4 2 1 40.46 52.41 3.26 o -3 2 1 4076.39 3894.61 58.99 o -2 2 1 14.33 21.51 2.34 o -1 2 1 46.43 45.17 2.66 o 0 2 1 16.86 15.95 2.63 o 1 2 1 19656.81 17607.84 245.14 o 2 2 1 269.89 253.04 6.30 o 3 2 1 430.15 347.74 8.09 o 4 2 1 918.31 924.78 19.37 o 5 2 1 649.31 611.27 17.97 o 6 2 1 52.09 53.42 7.86 o 7 2 1 179.05 174.92 6.92 o 8 2 1 620.38 671.07 15.82 o 9 2 1 1149.89 1143.98 26.74 o 10 2 1 247.43 227.08 14.65 o 11 2 1 75.02 89.12 33.63 o 12 2 1 7.63 61.70 43.88 o 13 2 1 17.75 -10.73 70.48 o 14 2 1 58.12 -17.52 101.57 o -13 3 1 149.13 215.41 52.50 o -12 3 1 6.55 1.71 54.43 o -10 3 1 358.82 371.18 18.15 o -9 3 1 50.87 65.14 15.00 o -8 3 1 1.30 -0.13 5.10 o -7 3 1 457.54 498.41 12.16 o -6 3 1 247.10 215.42 8.15 o -5 3 1 50.91 52.39 4.72 o -4 3 1 505.97 500.36 10.37 o -3 3 1 1452.25 1435.86 21.98 o -2 3 1 17825.94 15697.59 413.25 o -1 3 1 3984.82 3722.85 54.75 o 0 3 1 32046.03 28515.20 935.56 o 1 3 1 685.86 613.30 10.96 o 2 3 1 775.08 734.27 12.52 o 3 3 1 1434.16 1317.60 21.82 o 4 3 1 497.81 512.74 10.04 o 5 3 1 48.54 36.43 4.01 o 6 3 1 345.16 380.88 10.06 o 7 3 1 20.28 10.11 6.03 o 8 3 1 155.06 142.97 7.12 o 9 3 1 181.59 179.25 9.86 o 10 3 1 91.69 90.79 12.09 o 11 3 1 126.91 130.90 12.72 o 12 3 1 123.02 106.13 41.53 o 13 3 1 37.12 -49.16 68.38 o -13 4 1 342.73 444.72 86.22 o -12 4 1 368.56 432.16 70.09 o -11 4 1 65.38 57.66 10.23 o -10 4 1 1554.12 1669.96 82.80 o -9 4 1 2.31 9.25 4.46 o -8 4 1 1127.06 1210.15 29.44 o -7 4 1 1141.51 1271.82 69.25 o -6 4 1 1795.14 2055.36 34.69 o -5 4 1 699.11 708.85 13.56 o -4 4 1 62.65 60.33 5.46 o -3 4 1 711.14 709.73 12.77 o -2 4 1 6820.22 6835.41 99.72 o -1 4 1 3495.10 3020.96 103.23 o 0 4 1 3990.70 3637.69 67.46 o 1 4 1 1999.08 1763.81 26.84 o 2 4 1 7.12 -0.45 3.85 o 3 4 1 128.11 136.01 6.36 o 4 4 1 2299.35 2425.99 53.73 o 5 4 1 47.44 61.81 5.76 o 6 4 1 1922.89 1970.58 49.93 o 7 4 1 0.01 6.24 6.12 o 8 4 1 124.61 155.93 9.99 o 9 4 1 542.99 553.64 16.24 o 10 4 1 359.91 381.45 14.25 o 11 4 1 189.34 174.91 13.60 o 12 4 1 73.68 72.50 19.45 o 13 4 1 186.73 182.82 80.79 o -13 5 1 135.71 147.93 75.67 o -12 5 1 9.75 33.80 17.83 o -11 5 1 16.28 43.83 27.61 o -10 5 1 482.81 492.93 16.16 o -9 5 1 0.01 1.53 5.63 o -8 5 1 2200.62 2371.35 58.93 o -7 5 1 419.43 384.78 11.39 o -6 5 1 346.56 396.65 19.76 o -5 5 1 167.14 202.95 8.96 o -4 5 1 787.90 741.08 14.99 o -3 5 1 359.54 369.77 18.22 o -2 5 1 752.72 758.36 20.98 o -1 5 1 0.20 0.18 4.61 o 0 5 1 1162.01 1121.71 19.55 o 1 5 1 54.01 49.75 5.19 o 2 5 1 350.08 355.71 10.31 o 3 5 1 136.81 136.09 6.51 o 4 5 1 0.18 -4.51 4.51 o 5 5 1 228.01 226.86 8.45 o 6 5 1 53.89 43.57 6.81 o 7 5 1 75.01 78.85 7.42 o 8 5 1 45.63 46.68 7.05 o 9 5 1 1.58 -0.54 10.14 o 10 5 1 387.87 408.63 15.48 o 11 5 1 98.85 87.26 16.70 o 12 5 1 81.18 91.35 16.50 o 13 5 1 94.91 124.98 70.40 o -13 6 1 54.32 -10.54 75.83 o -12 6 1 136.15 142.83 24.24 o -11 6 1 8.08 10.44 7.11 o -10 6 1 1.71 3.51 11.15 o -9 6 1 9.41 14.19 7.26 o -8 6 1 14.93 -1.60 6.78 o -7 6 1 14.83 23.68 7.69 o -6 6 1 571.79 630.22 17.11 o -5 6 1 1275.42 1398.30 32.98 o -4 6 1 445.99 432.09 12.36 o -3 6 1 1205.62 1205.00 23.01 o -2 6 1 59.02 56.44 6.69 o -1 6 1 618.67 614.11 13.37 o 0 6 1 75.52 80.67 7.59 o 1 6 1 2267.95 2438.91 36.98 o 2 6 1 4.29 3.99 5.63 o 3 6 1 272.30 263.50 10.16 o 4 6 1 127.96 116.09 7.91 o 5 6 1 351.35 361.96 11.02 o 6 6 1 4.34 3.46 6.60 o 7 6 1 162.28 162.11 9.21 o 8 6 1 1227.26 1340.46 33.64 o 9 6 1 218.98 208.44 11.21 o 10 6 1 3.43 4.18 12.16 o 11 6 1 100.25 88.12 9.00 o 12 6 1 0.58 12.58 90.25 o 13 6 1 0.58 91.64 75.83 o -13 7 1 13.68 -3.76 23.47 o -12 7 1 67.99 83.81 25.78 o -11 7 1 2.59 8.00 25.74 o -10 7 1 2140.19 2313.64 57.43 o -9 7 1 25.05 21.75 9.59 o -8 7 1 1122.05 1121.89 25.47 o -7 7 1 4.19 3.75 7.38 o -6 7 1 1232.13 1374.36 30.65 o -5 7 1 362.90 356.29 12.94 o -4 7 1 484.67 496.03 15.79 o -3 7 1 84.40 97.68 9.02 o -2 7 1 734.45 795.18 28.67 o -1 7 1 2693.02 3104.71 55.24 o 0 7 1 740.22 850.86 19.83 o 1 7 1 38.47 35.88 7.24 o 2 7 1 1895.01 2083.84 35.82 o 3 7 1 1768.73 2001.89 35.31 o 4 7 1 10.78 8.70 6.66 o 5 7 1 16.55 10.23 7.66 o 6 7 1 404.13 397.12 16.58 o 7 7 1 165.42 163.09 10.83 o 8 7 1 995.96 1072.69 25.55 o 9 7 1 137.21 139.60 11.58 o 10 7 1 18.94 15.38 8.88 o 11 7 1 24.00 30.67 14.18 o 12 7 1 1275.12 1198.17 64.59 o 13 7 1 4.00 37.37 29.91 o -13 8 1 9.41 12.41 109.63 o -12 8 1 100.38 141.37 54.12 o -11 8 1 57.68 59.05 21.23 o -10 8 1 119.99 145.11 11.86 o -9 8 1 61.87 67.23 11.35 o -8 8 1 473.59 505.77 17.57 o -7 8 1 1364.73 1506.10 34.32 o -6 8 1 57.15 48.58 8.96 o -5 8 1 28.04 28.68 8.70 o -4 8 1 35.84 28.45 8.31 o -3 8 1 296.33 295.11 13.89 o -2 8 1 174.44 151.11 10.75 o -1 8 1 916.83 1053.61 27.81 o 0 8 1 800.92 885.06 20.70 o 1 8 1 5.95 3.37 9.36 o 2 8 1 94.56 83.15 9.96 o 3 8 1 95.37 109.57 10.49 o 4 8 1 16.83 24.48 10.06 o 5 8 1 215.50 231.08 13.49 o 6 8 1 988.51 1062.94 29.64 o 7 8 1 407.95 416.18 16.38 o 8 8 1 587.69 559.66 19.46 o 9 8 1 129.28 146.66 14.41 o 10 8 1 185.33 238.98 22.20 o 11 8 1 205.16 236.25 22.23 o 12 8 1 5.04 -9.26 28.90 o 13 8 1 0.82 32.41 39.70 o -12 9 1 24.06 3.83 20.96 o -11 9 1 387.15 399.67 35.18 o -10 9 1 187.23 167.39 18.24 o -9 9 1 1.29 8.36 12.59 o -8 9 1 198.13 182.24 13.22 o -7 9 1 14.52 8.76 9.96 o -6 9 1 30.47 44.86 10.77 o -5 9 1 92.01 89.47 11.91 o -4 9 1 4.35 -1.25 7.87 o -3 9 1 207.18 219.66 13.90 o -2 9 1 3.59 10.59 9.57 o -1 9 1 100.71 122.61 11.65 o 0 9 1 1821.94 1840.84 36.60 o 1 9 1 52.35 58.61 10.86 o 2 9 1 1768.25 1907.86 44.64 o 3 9 1 545.45 584.86 18.27 o 4 9 1 157.16 139.12 11.60 o 5 9 1 1017.60 1099.26 40.67 o 6 9 1 205.99 208.42 13.58 o 7 9 1 388.65 381.70 18.19 o 8 9 1 328.85 334.36 17.42 o 9 9 1 60.16 54.82 11.97 o 10 9 1 41.89 50.27 19.13 o 11 9 1 0.06 -2.55 18.48 o 12 9 1 102.73 59.09 31.73 o -12 10 1 414.52 452.13 44.95 o -11 10 1 4.46 40.91 30.36 o -10 10 1 6.91 37.93 17.16 o -9 10 1 230.16 221.95 17.72 o -8 10 1 133.50 120.95 13.74 o -7 10 1 1628.48 1689.37 46.69 o -6 10 1 452.96 460.72 18.87 o -5 10 1 41.52 34.53 11.48 o -4 10 1 10.62 21.04 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