#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103291.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103291_Fobs loop_ _publ_author_name 'Johansson, Maria H.' 'Otto, Stefanus' 'Oskarsson, \%Ake' _publ_section_title ; Structures of trans-[PtCl~2~(PBz~3~)~2~], trans-[PtI~2~(PBz~3~)~2~], trans-[Pt(NCS)~2~(PBz~3~)~2~]·0.5C~6~H~6~ and trans-[PdI~2~(PBz~3~)~2~] ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 244 _journal_page_last 250 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.498 _cell_angle_beta 82.755 _cell_angle_gamma 88.594 _cell_length_a 9.4657 _cell_length_b 10.6085 _cell_length_c 19.0178 _exptl_crystal_F_000 872.00 _reflns_d_resolution_high 0.6722 _[local]_cod_data_source_file ns00071sup2.hkl _[local]_cod_data_source_block 1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 266.43 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 35450.13 28565.50 698.44 o 2 0 0 32997.11 30133.45 220.51 o 3 0 0 14352.81 13386.82 91.26 o 4 0 0 7158.61 6739.14 47.14 o 5 0 0 4522.02 4170.97 42.03 o 6 0 0 5157.73 5146.53 91.90 o 7 0 0 4754.13 4757.23 39.07 o 8 0 0 3459.52 3350.11 55.14 o 9 0 0 1967.68 1920.36 30.74 o 10 0 0 871.08 923.96 40.84 o 11 0 0 712.61 688.35 38.18 o 12 0 0 482.67 503.16 36.05 o 13 0 0 115.51 155.39 33.66 o -13 1 0 0.21 41.38 31.66 o -12 1 0 28.54 19.42 27.94 o -11 1 0 18.60 -11.44 23.02 o -10 1 0 0.22 10.40 11.49 o -9 1 0 320.59 294.86 13.50 o -8 1 0 66.33 55.95 13.28 o -7 1 0 0.06 -4.09 13.77 o -6 1 0 117.26 115.90 13.77 o -5 1 0 1.21 7.95 8.86 o -4 1 0 1754.67 1841.65 44.70 o -3 1 0 100.90 106.63 9.31 o -2 1 0 3373.75 3278.26 98.18 o -1 1 0 379.21 409.78 8.93 o 0 1 0 1329.20 1320.47 362.48 o 1 1 0 97.55 106.85 3.81 o 2 1 0 18313.16 18189.49 260.23 o 3 1 0 1359.10 1347.44 13.82 o 4 1 0 107.86 106.09 6.90 o 5 1 0 0.46 0.96 8.85 o 6 1 0 234.57 223.10 9.71 o 7 1 0 509.53 495.08 13.43 o 8 1 0 0.27 -4.41 12.08 o 9 1 0 186.56 173.46 30.20 o 10 1 0 8.35 -15.03 21.02 o 11 1 0 35.42 44.70 24.08 o 12 1 0 0.30 -21.29 26.61 o 13 1 0 0.62 -29.53 31.13 o -12 2 0 689.56 655.49 40.84 o -11 2 0 1705.85 1793.77 57.21 o -10 2 0 1486.67 1469.90 47.90 o -9 2 0 1387.25 1409.51 83.23 o -8 2 0 3869.03 4054.61 137.96 o -7 2 0 4249.80 4282.54 47.50 o -6 2 0 6675.53 6539.76 176.34 o -5 2 0 3911.16 3809.39 44.37 o -4 2 0 8368.49 8506.84 94.52 o -3 2 0 9693.38 9258.61 79.42 o -2 2 0 20663.07 20744.03 329.95 o -1 2 0 70986.55 64188.48 248.56 o 0 2 0 5178.39 5761.87 77.23 o 1 2 0 25030.10 24869.59 247.57 o 2 2 0 14916.64 15241.15 109.75 o 3 2 0 8464.96 8224.49 42.49 o 4 2 0 8776.42 8351.25 49.39 o 5 2 0 5797.78 5520.79 70.13 o 6 2 0 4115.31 4123.47 103.59 o 7 2 0 3727.22 3693.10 101.14 o 8 2 0 2683.27 2658.64 87.61 o 9 2 0 1582.97 1538.07 49.76 o 10 2 0 1983.71 1942.64 60.27 o 11 2 0 845.07 1035.05 47.63 o 12 2 0 402.62 389.14 36.98 o 13 2 0 189.96 196.23 32.59 o -12 3 0 3.67 -28.27 28.27 o -11 3 0 11.29 9.95 14.95 o -10 3 0 68.86 59.38 12.84 o -9 3 0 209.60 215.26 24.88 o -8 3 0 232.01 212.86 22.48 o -7 3 0 73.90 41.51 19.69 o -6 3 0 3.99 14.17 14.38 o -5 3 0 23.24 20.18 7.83 o -4 3 0 4393.28 4662.44 75.27 o -3 3 0 4062.48 4276.00 68.51 o -2 3 0 5974.86 6079.50 54.95 o -1 3 0 1294.31 1359.69 86.41 o 0 3 0 117.18 136.55 10.26 o 1 3 0 11353.38 11378.87 101.47 o 2 3 0 2634.03 2581.97 63.86 o 3 3 0 44.56 63.09 11.80 o 4 3 0 13.88 12.49 6.76 o 5 3 0 535.01 558.78 20.07 o 6 3 0 29.23 50.02 10.94 o 7 3 0 36.90 48.33 9.98 o 8 3 0 7.95 -11.28 11.28 o 9 3 0 153.40 147.94 23.28 o 10 3 0 40.52 90.87 22.62 o 11 3 0 20.39 -12.77 23.95 o 12 3 0 10.58 5.06 27.94 o 13 3 0 26.29 -14.77 31.00 o -11 4 0 465.04 451.97 19.82 o -10 4 0 459.64 507.82 19.33 o -9 4 0 1687.81 1780.19 58.73 o -8 4 0 2435.78 2569.57 38.02 o -7 4 0 5979.21 6355.14 65.38 o -6 4 0 1102.87 1224.89 19.93 o -5 4 0 4384.59 4661.03 78.74 o -4 4 0 7274.42 7736.02 238.21 o -3 4 0 11475.10 11862.78 75.78 o -2 4 0 7672.55 7696.25 578.99 o -1 4 0 20532.41 21428.91 165.03 o 0 4 0 10403.76 10603.00 234.55 o 1 4 0 27896.81 27694.73 395.75 o 2 4 0 11079.96 11159.63 101.94 o 3 4 0 15716.12 15546.67 348.90 o 4 4 0 11119.14 10882.53 107.69 o 5 4 0 8387.47 8262.91 245.70 o 6 4 0 3954.84 3922.72 111.52 o 7 4 0 3058.70 2842.22 100.43 o 8 4 0 2663.36 2677.86 50.62 o 9 4 0 1976.87 1791.77 57.34 o 10 4 0 996.42 1122.05 46.96 o 11 4 0 370.74 402.84 33.53 o 12 4 0 184.83 156.32 30.87 o -12 5 0 9.28 53.48 47.63 o -11 5 0 8.23 30.47 38.45 o -10 5 0 1.37 9.98 33.66 o -9 5 0 93.78 142.61 14.01 o -8 5 0 45.77 70.87 11.82 o -7 5 0 3.14 16.73 10.17 o -6 5 0 180.40 219.86 16.01 o -5 5 0 910.13 948.69 22.84 o -4 5 0 1.50 0.09 25.54 o -3 5 0 187.90 206.71 13.59 o -2 5 0 8.18 17.44 10.09 o -1 5 0 405.45 504.76 20.29 o 0 5 0 1697.46 1774.97 33.39 o 1 5 0 1387.87 1351.02 18.97 o 2 5 0 0.94 -8.86 8.86 o 3 5 0 2409.70 2425.33 95.13 o 4 5 0 85.21 81.92 9.55 o 5 5 0 15.91 32.10 23.32 o 6 5 0 19.17 36.42 17.90 o 7 5 0 16.18 1.66 11.85 o 8 5 0 41.84 16.23 20.09 o 9 5 0 150.43 131.04 22.35 o 10 5 0 27.34 8.91 19.42 o 11 5 0 58.25 60.40 25.94 o 12 5 0 12.72 -15.43 30.20 o -12 6 0 325.59 394.73 52.68 o -11 6 0 386.83 388.48 47.89 o -10 6 0 1031.78 940.72 55.88 o -9 6 0 1836.64 1730.84 70.64 o -8 6 0 2873.26 3017.95 176.68 o -7 6 0 2144.62 2311.51 41.25 o -6 6 0 5476.02 5608.72 84.35 o -5 6 0 6297.32 6544.29 88.14 o -4 6 0 6789.03 6906.92 64.28 o -3 6 0 12006.56 12478.31 249.85 o -2 6 0 7980.19 8813.25 100.78 o -1 6 0 3019.95 2733.50 36.47 o 0 6 0 6154.98 6131.98 55.84 o 1 6 0 3991.47 3629.20 64.32 o 2 6 0 9907.22 9534.66 114.86 o 3 6 0 8058.62 8022.10 169.72 o 4 6 0 8527.88 7873.79 215.09 o 5 6 0 3479.00 3492.53 36.40 o 6 6 0 1699.62 1722.35 112.42 o 7 6 0 1182.41 1193.61 27.94 o 8 6 0 996.40 1018.95 43.64 o 9 6 0 1097.13 1087.73 46.56 o 10 6 0 340.57 356.01 32.99 o 11 6 0 211.42 211.13 28.34 o 12 6 0 171.61 167.50 33.13 o -12 7 0 9.64 -44.70 56.01 o -11 7 0 0.08 -47.23 47.23 o -10 7 0 4.45 -2.53 36.72 o -9 7 0 1.93 -33.13 33.13 o -8 7 0 31.55 -30.20 30.20 o -7 7 0 137.28 112.41 18.70 o -6 7 0 328.65 373.43 20.09 o -5 7 0 2.26 -15.06 42.04 o -4 7 0 261.38 318.96 34.86 o -3 7 0 670.64 725.32 35.46 o -2 7 0 563.15 557.16 20.14 o -1 7 0 12.09 -3.22 11.49 o 0 7 0 175.14 178.99 16.10 o 1 7 0 2.21 -12.22 12.22 o 2 7 0 180.05 202.24 14.82 o 3 7 0 124.00 118.27 18.66 o 4 7 0 207.78 227.99 13.00 o 5 7 0 53.48 58.34 14.85 o 6 7 0 9.90 4.03 13.50 o 7 7 0 25.62 67.32 20.49 o 8 7 0 1.30 10.78 19.42 o 9 7 0 63.29 81.55 24.21 o 10 7 0 175.01 135.17 25.94 o 11 7 0 22.15 38.58 25.54 o -11 8 0 378.38 388.34 53.61 o -10 8 0 618.79 624.62 54.68 o -9 8 0 683.00 630.74 51.09 o -8 8 0 880.70 874.73 55.08 o -7 8 0 1664.67 1594.34 68.78 o -6 8 0 2619.59 2757.37 84.61 o -5 8 0 1700.68 1782.47 45.10 o -4 8 0 5151.38 5688.52 253.97 o -3 8 0 2884.94 3013.43 47.10 o -2 8 0 2947.61 3002.10 77.10 o -1 8 0 779.51 863.29 50.02 o 0 8 0 1120.39 1163.29 63.99 o 1 8 0 4851.35 4596.39 54.47 o 2 8 0 6019.35 5926.80 62.79 o 3 8 0 4975.69 4998.60 114.28 o 4 8 0 4557.72 4649.95 87.88 o 5 8 0 5097.34 5217.15 74.44 o 6 8 0 2174.10 2035.97 121.73 o 7 8 0 1213.03 1143.61 47.36 o 8 8 0 1062.77 963.34 45.37 o 9 8 0 498.38 453.93 33.79 o 10 8 0 224.23 204.08 30.33 o 11 8 0 210.61 225.24 32.59 o -10 9 0 31.56 94.46 45.77 o -9 9 0 0.12 -16.36 39.11 o -8 9 0 0.15 -33.26 33.26 o -7 9 0 0.70 12.11 29.93 o -6 9 0 3.39 -27.94 27.94 o -5 9 0 67.09 43.90 31.26 o -4 9 0 316.27 339.90 22.66 o -3 9 0 32.45 36.37 16.16 o -2 9 0 251.81 232.79 18.25 o -1 9 0 492.17 456.06 21.49 o 0 9 0 1.64 24.57 18.83 o 1 9 0 304.66 334.78 20.57 o 2 9 0 2.47 -3.56 14.30 o 3 9 0 137.41 107.43 17.43 o 4 9 0 290.45 243.60 19.11 o 5 9 0 80.58 82.23 19.49 o 6 9 0 18.50 42.38 17.56 o 7 9 0 17.24 -5.59 21.15 o 8 9 0 13.57 -4.12 23.15 o 9 9 0 0.57 30.73 24.08 o 10 9 0 18.18 38.45 27.81 o -9 10 0 476.50 407.37 50.82 o -8 10 0 681.70 669.45 52.68 o -7 10 0 1359.16 1233.01 66.25 o -6 10 0 1828.44 1763.04 75.30 o -5 10 0 3583.07 3289.13 97.65 o -4 10 0 2576.72 2299.99 79.03 o -3 10 0 2589.26 2650.36 93.33 o -2 10 0 1411.18 1520.75 95.52 o -1 10 0 1505.33 1567.60 76.36 o 0 10 0 3052.81 2963.07 69.65 o 1 10 0 3867.49 3812.13 165.70 o 2 10 0 1899.42 1866.49 39.55 o 3 10 0 1988.40 1965.23 40.07 o 4 10 0 1469.32 1307.51 49.49 o 5 10 0 624.47 723.87 40.04 o 6 10 0 593.62 624.75 38.98 o 7 10 0 426.86 488.12 34.86 o 8 10 0 279.10 268.07 31.13 o 9 10 0 116.02 50.29 27.94 o -8 11 0 27.53 41.64 43.64 o -7 11 0 13.77 -17.43 40.58 o -6 11 0 20.77 -7.05 35.26 o -5 11 0 75.69 70.64 32.99 o -4 11 0 111.89 119.47 36.98 o -3 11 0 265.53 232.95 37.25 o -2 11 0 105.40 71.84 30.47 o -1 11 0 0.66 -10.14 18.20 o 0 11 0 190.43 209.10 19.46 o 1 11 0 252.05 261.57 34.46 o 2 11 0 5.79 7.15 18.34 o 3 11 0 20.46 48.69 24.35 o 4 11 0 1.83 -22.22 22.22 o 5 11 0 11.34 0.40 24.35 o 6 11 0 7.28 34.32 25.68 o 7 11 0 0.86 -23.15 26.47 o 8 11 0 0.58 -28.47 28.47 o 9 11 0 13.23 14.10 32.06 o -7 12 0 430.65 445.95 52.42 o -6 12 0 669.53 660.54 59.20 o -5 12 0 706.66 677.17 54.81 o -4 12 0 698.80 706.04 54.81 o -3 12 0 948.17 923.16 56.94 o -2 12 0 913.04 836.68 52.02 o -1 12 0 801.18 709.63 48.56 o 0 12 0 927.40 984.09 95.46 o 1 12 0 754.13 774.62 42.57 o 2 12 0 688.26 672.39 30.40 o 3 12 0 429.26 400.85 34.06 o 4 12 0 759.72 779.74 44.44 o 5 12 0 841.25 907.06 47.76 o 6 12 0 677.64 723.60 42.04 o 7 12 0 395.75 463.91 37.78 o 8 12 0 175.70 198.63 34.32 o -6 13 0 13.30 32.46 46.96 o -5 13 0 1.73 -7.05 41.91 o -4 13 0 30.35 13.57 39.78 o -3 13 0 53.71 -5.45 36.59 o -2 13 0 36.96 18.76 34.86 o -1 13 0 3.06 -25.14 33.79 o 0 13 0 0.98 3.46 31.40 o 1 13 0 41.90 1.60 34.46 o 2 13 0 34.96 88.47 30.60 o 3 13 0 74.35 73.30 31.80 o 4 13 0 164.43 257.30 36.32 o 5 13 0 77.90 -14.77 30.73 o 6 13 0 34.32 -33.93 33.93 o 7 13 0 39.20 65.46 34.32 o -4 14 0 560.10 622.36 52.95 o -3 14 0 570.09 672.12 54.68 o -2 14 0 701.57 699.79 53.22 o -1 14 0 812.89 772.96 57.61 o 0 14 0 630.49 602.27 50.29 o 4 14 0 295.61 346.97 39.25 o 5 14 0 312.69 383.69 43.10 o 6 14 0 205.49 214.06 41.24 o -2 15 0 39.67 77.56 48.29 o -1 15 0 32.20 -22.22 43.77 o 1 -15 1 480.19 433.97 50.82 o -6 -14 1 15.98 31.40 36.98 o -5 -14 1 12.32 8.78 38.32 o 0 -14 1 15.22 18.09 39.91 o 1 -14 1 2.17 0.13 36.32 o 2 -14 1 6.87 -5.06 40.84 o 3 -14 1 55.74 89.14 40.71 o 4 -14 1 88.35 88.47 44.57 o -7 -13 1 151.80 252.11 36.32 o -6 -13 1 225.62 255.70 34.59 o -5 -13 1 661.09 693.53 42.97 o -4 -13 1 723.21 738.63 44.57 o -3 -13 1 753.17 780.68 44.57 o -1 -13 1 654.38 701.65 48.96 o 0 -13 1 623.34 557.83 44.44 o 1 -13 1 719.54 692.87 49.89 o 2 -13 1 520.78 497.43 43.50 o 3 -13 1 483.61 511.00 45.63 o 4 -13 1 528.80 507.41 52.15 o 5 -13 1 450.35 414.02 51.75 o 6 -13 1 381.22 489.59 54.28 o -8 -12 1 29.87 18.49 33.93 o -7 -12 1 38.00 52.95 30.47 o -6 -12 1 72.19 108.16 29.80 o -5 -12 1 101.29 103.64 29.14 o -4 -12 1 26.51 -27.27 27.27 o -3 -12 1 47.07 63.86 25.54 o -2 -12 1 1.02 -8.44 36.52 o -1 -12 1 4.63 -14.24 24.75 o 0 -12 1 96.63 73.84 28.87 o 1 -12 1 24.43 21.15 29.93 o 2 -12 1 1.78 2.26 30.07 o 3 -12 1 26.88 7.85 33.26 o 4 -12 1 4.40 15.96 36.05 o 5 -12 1 1.43 -5.06 37.52 o 6 -12 1 2.18 -39.78 39.78 o 7 -12 1 2.22 -9.71 44.44 o -9 -11 1 128.90 153.79 34.99 o -8 -11 1 148.29 116.28 30.20 o -7 -11 1 319.35 355.35 31.40 o -6 -11 1 615.17 592.82 39.51 o -5 -11 1 743.41 711.49 40.71 o -4 -11 1 1002.26 1043.30 46.03 o -3 -11 1 1267.63 1259.61 122.40 o -2 -11 1 1186.01 1104.05 96.85 o -1 -11 1 1500.74 1519.11 103.37 o 0 -11 1 810.11 885.46 117.07 o 1 -11 1 990.44 832.69 48.96 o 2 -11 1 1019.00 925.82 51.22 o 3 -11 1 1079.45 1039.84 54.95 o 4 -11 1 1005.93 1066.98 61.73 o 5 -11 1 1586.88 1466.76 71.71 o 6 -11 1 1268.78 1332.92 69.98 o 7 -11 1 1009.35 994.60 63.86 o 8 -11 1 532.52 465.64 54.01 o -9 -10 1 4.00 -13.17 29.40 o -8 -10 1 4.02 -25.01 25.01 o -7 -10 1 9.39 -19.69 23.81 o -6 -10 1 12.64 22.75 22.48 o -5 -10 1 2.78 6.12 21.02 o -4 -10 1 77.18 56.01 24.08 o -3 -10 1 214.10 191.72 19.25 o -2 -10 1 203.91 167.91 30.33 o -1 -10 1 140.47 111.31 16.97 o 0 -10 1 225.01 186.68 27.14 o 1 -10 1 14.80 19.03 15.28 o 2 -10 1 78.90 79.95 20.95 o 3 -10 1 20.14 22.62 28.34 o 4 -10 1 208.35 197.30 35.52 o 5 -10 1 8.75 -32.20 32.20 o 6 -10 1 8.74 4.79 31.53 o 7 -10 1 59.25 84.35 34.99 o 8 -10 1 38.05 41.11 37.38 o 9 -10 1 23.51 6.65 41.77 o -10 -9 1 121.82 104.84 29.40 o -9 -9 1 225.52 251.18 31.26 o -8 -9 1 414.43 413.35 34.99 o -7 -9 1 646.61 675.31 37.52 o -6 -9 1 1482.37 1535.67 54.95 o -5 -9 1 1814.86 1787.52 55.48 o -4 -9 1 4113.56 4155.04 175.68 o -3 -9 1 4085.13 4020.13 55.46 o -2 -9 1 5912.53 5623.80 65.83 o -1 -9 1 4002.39 3977.60 153.53 o 0 -9 1 5861.14 5856.47 66.38 o 1 -9 1 2782.05 2947.00 45.98 o 2 -9 1 1642.39 1790.43 36.82 o 3 -9 1 2891.71 2962.18 71.24 o 4 -9 1 3570.80 3344.48 90.60 o 5 -9 1 3696.59 3610.16 98.18 o 6 -9 1 2080.54 2041.22 76.36 o 7 -9 1 885.07 861.70 55.74 o 8 -9 1 750.58 825.91 56.54 o 9 -9 1 307.01 288.70 43.64 o 10 -9 1 423.56 502.76 53.61 o -11 -8 1 16.87 52.68 29.14 o -10 -8 1 59.94 26.34 24.48 o -9 -8 1 24.05 38.32 23.41 o -8 -8 1 9.62 38.32 24.08 o -7 -8 1 0.35 -3.06 18.76 o -6 -8 1 12.95 21.28 13.64 o -5 -8 1 5.63 6.90 11.33 o -4 -8 1 992.41 954.72 34.86 o -3 -8 1 30.74 30.16 13.35 o -2 -8 1 486.27 514.51 32.73 o -1 -8 1 79.77 91.08 32.46 o 0 -8 1 5.23 12.28 17.16 o 1 -8 1 250.06 246.49 15.24 o 2 -8 1 191.88 208.06 60.80 o 3 -8 1 0.07 -9.84 14.35 o 4 -8 1 526.75 619.59 79.42 o 5 -8 1 432.09 498.82 23.70 o 6 -8 1 10.96 18.89 27.54 o 7 -8 1 1.95 -17.16 28.20 o 8 -8 1 0.52 -31.53 31.53 o 9 -8 1 5.35 -34.86 34.86 o 10 -8 1 2.30 -40.84 40.84 o 11 -8 1 7.26 -12.37 46.70 o -11 -7 1 251.65 268.34 30.87 o -10 -7 1 573.85 562.62 39.38 o -9 -7 1 595.21 565.68 36.72 o -8 -7 1 1511.57 1374.03 50.55 o -7 -7 1 1863.79 1711.42 55.48 o -6 -7 1 2719.14 2757.14 167.16 o -5 -7 1 2766.64 2815.57 80.07 o -4 -7 1 1100.51 1165.64 26.86 o -3 -7 1 4220.78 4280.24 50.23 o -2 -7 1 7942.98 8207.40 204.75 o -1 -7 1 6028.89 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