#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103294.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103294_Fobs loop_ _publ_author_name 'Johansson, Maria H.' 'Otto, Stefanus' 'Oskarsson, \%Ake' _publ_section_title ; Structures of trans-[PtCl~2~(PBz~3~)~2~], trans-[PtI~2~(PBz~3~)~2~], trans-[Pt(NCS)~2~(PBz~3~)~2~]·0.5C~6~H~6~ and trans-[PdI~2~(PBz~3~)~2~] ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 244 _journal_page_last 250 _journal_volume 58 _journal_year 2002 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yac' _symmetry_space_group_name_H-M 'P 1 n 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.883 _cell_angle_gamma 90.000 _cell_length_a 11.2742 _cell_length_b 9.9942 _cell_length_c 18.0731 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.7300 _[local]_cod_data_source_file ns00074sup5.hkl _[local]_cod_data_source_block 4 #BEGIN Tags that were not found in dictionaries: _shelx_title ' sadny in Pn' _shelx_refln_list_code 4 _shelx_F_calc_maximum 262.69 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 -24 1173.31 1094.22 320.84 o 4 0 -24 39.15 253.27 319.00 o 6 0 -24 54.09 -229.60 347.50 o 1 1 -24 195.81 128.41 222.79 o 2 1 -24 651.98 250.27 238.06 o 3 1 -24 205.37 222.86 248.85 o 4 1 -24 27.44 100.92 226.07 o 5 1 -24 48.89 77.38 217.11 o 6 1 -24 12.49 -210.13 241.21 o 7 1 -24 43.51 69.18 311.42 o 1 2 -24 218.05 359.84 260.00 o 2 2 -24 93.62 162.87 240.84 o 3 2 -24 329.92 457.36 234.99 o 4 2 -24 195.27 405.28 216.03 o 5 2 -24 44.90 -0.24 232.36 o 6 2 -24 3.10 63.61 233.99 o 3 3 -24 171.74 356.31 229.96 o 4 3 -24 296.54 360.49 233.29 o 5 3 -24 95.14 -23.62 221.29 o -1 0 -23 79.03 222.94 347.04 o 1 0 -23 1132.23 941.84 282.46 o 3 0 -23 187.14 90.55 290.74 o 5 0 -23 205.62 309.12 324.98 o 7 0 -23 273.89 361.06 326.59 o -1 1 -23 54.85 425.87 233.31 o 0 1 -23 142.35 194.93 230.26 o 1 1 -23 662.48 903.78 225.03 o 2 1 -23 437.80 621.93 229.32 o 3 1 -23 165.79 10.94 205.42 o 4 1 -23 34.04 26.01 197.94 o 5 1 -23 81.47 61.41 201.39 o 6 1 -23 4.72 -76.13 202.52 o 7 1 -23 242.12 -142.83 225.03 o 8 1 -23 228.07 378.53 335.55 o -1 2 -23 94.85 -2.76 238.54 o 0 2 -23 167.70 189.35 236.81 o 1 2 -23 82.66 -90.22 226.91 o 2 2 -23 603.37 619.11 217.80 o 3 2 -23 243.94 569.25 201.01 o 4 2 -23 0.23 -139.59 200.88 o 5 2 -23 6.43 21.75 200.65 o 6 2 -23 34.20 91.59 253.50 o 7 2 -23 220.52 198.80 193.60 o 8 2 -23 375.61 500.45 197.34 o 0 3 -23 2.98 -102.07 239.77 o 1 3 -23 28.45 151.45 225.41 o 2 3 -23 399.40 304.42 213.13 o 3 3 -23 239.54 141.57 208.18 o 4 3 -23 168.97 61.59 160.68 o 5 3 -23 9.09 -12.29 171.23 o 6 3 -23 43.67 55.08 174.64 o 7 3 -23 171.80 303.52 194.88 o 8 3 -23 148.57 310.32 210.15 o 1 4 -23 10.09 14.14 237.79 o 2 4 -23 124.50 124.43 222.26 o 3 4 -23 170.25 139.64 169.42 o 4 4 -23 214.50 239.08 226.53 o 5 4 -23 164.67 109.51 178.66 o 6 4 -23 86.16 221.55 220.56 o 7 4 -23 75.89 -72.65 217.40 o 3 5 -23 203.85 137.22 183.66 o 4 5 -23 30.25 108.33 181.14 o -2 0 -22 398.82 363.59 298.32 o 0 0 -22 871.88 954.26 291.65 o 2 0 -22 267.84 485.63 269.59 o 4 0 -22 282.33 243.16 299.24 o 6 0 -22 501.43 578.71 281.54 o 10 0 -22 57.48 384.28 240.86 o -3 1 -22 82.43 220.05 268.21 o -2 1 -22 255.44 287.24 238.41 o -1 1 -22 144.26 237.25 219.00 o 0 1 -22 521.29 619.70 223.97 o 1 1 -22 246.60 23.68 207.68 o 2 1 -22 316.68 414.43 194.55 o 3 1 -22 51.13 142.87 182.62 o 4 1 -22 165.84 -4.93 185.40 o 5 1 -22 134.03 282.21 287.75 o 6 1 -22 168.18 62.29 191.73 o 7 1 -22 376.72 293.39 152.94 o 8 1 -22 857.34 814.08 182.09 o 9 1 -22 183.57 88.71 244.08 o 10 1 -22 51.42 -196.28 256.26 o -2 2 -22 408.06 198.95 239.17 o -1 2 -22 179.22 191.51 231.27 o 0 2 -22 163.87 206.79 224.20 o 1 2 -22 505.46 614.33 202.01 o 2 2 -22 447.54 519.48 192.33 o 3 2 -22 153.12 57.11 185.54 o 4 2 -22 151.01 24.07 182.45 o 5 2 -22 37.29 -128.12 147.50 o 6 2 -22 171.11 233.38 164.17 o 7 2 -22 440.04 449.51 166.74 o 8 2 -22 67.76 79.49 333.02 o 9 2 -22 235.27 362.90 257.18 o 10 2 -22 163.12 -6.89 279.24 o -2 3 -22 595.95 932.55 264.58 o -1 3 -22 49.37 -99.21 234.59 o 0 3 -22 80.72 -229.70 229.70 o 1 3 -22 285.83 320.62 205.14 o 2 3 -22 495.24 510.64 152.77 o 3 3 -22 436.18 328.27 147.25 o 4 3 -22 128.81 32.68 145.65 o 5 3 -22 69.50 -31.47 160.10 o 6 3 -22 264.92 434.77 162.21 o 7 3 -22 133.93 243.11 191.49 o 8 3 -22 28.69 273.95 201.93 o 9 3 -22 104.39 92.62 216.08 o -1 4 -22 91.10 258.91 317.05 o 0 4 -22 4.64 -228.73 228.73 o 1 4 -22 252.67 132.55 210.49 o 2 4 -22 412.04 134.41 154.89 o 3 4 -22 254.10 225.24 154.60 o 4 4 -22 248.89 205.06 209.93 o 5 4 -22 131.47 140.74 164.23 o 6 4 -22 69.12 78.49 188.19 o 7 4 -22 63.97 -164.38 193.66 o 8 4 -22 15.72 255.62 201.93 o 0 5 -22 10.52 244.80 242.60 o 1 5 -22 114.01 386.90 228.03 o 2 5 -22 314.79 402.12 233.09 o 3 5 -22 12.74 34.85 164.39 o 4 5 -22 626.30 642.01 177.45 o 5 5 -22 2.44 -12.96 205.47 o 6 5 -22 34.08 -67.55 232.36 o 7 5 -22 23.83 -64.47 203.57 o 2 6 -22 85.15 60.57 245.28 o 3 6 -22 121.10 5.08 170.52 o 4 6 -22 440.51 560.95 181.86 o 5 6 -22 84.09 -11.16 277.86 o -3 0 -21 932.88 663.75 355.32 o -1 0 -21 949.47 1085.26 286.60 o 1 0 -21 30.36 -39.53 234.20 o 3 0 -21 16.13 -226.15 245.00 o 5 0 -21 36.67 164.56 245.69 o 7 0 -21 2203.56 2126.85 282.46 o 9 0 -21 173.86 171.91 197.65 o 11 0 -21 251.58 540.79 255.80 o -4 1 -21 46.84 57.20 270.75 o -3 1 -21 427.65 238.94 251.67 o -2 1 -21 443.74 249.30 212.64 o -1 1 -21 467.84 518.45 207.30 o 0 1 -21 260.15 225.87 191.69 o 1 1 -21 173.54 74.96 185.67 o 2 1 -21 79.19 184.99 164.06 o 3 1 -21 12.92 171.75 179.15 o 4 1 -21 279.35 270.85 168.37 o 5 1 -21 126.30 79.08 119.75 o 6 1 -21 466.76 454.24 127.56 o 7 1 -21 1142.32 1234.30 145.32 o 8 1 -21 315.51 295.80 159.07 o 9 1 -21 134.32 449.55 218.80 o 10 1 -21 42.30 22.75 233.28 o 11 1 -21 55.44 2.12 243.62 o -4 2 -21 52.87 163.09 268.31 o -3 2 -21 269.28 284.89 234.60 o -2 2 -21 501.62 611.10 219.38 o -1 2 -21 105.77 93.45 277.98 o 0 2 -21 356.43 378.72 198.66 o 1 2 -21 445.46 437.37 183.92 o 2 2 -21 157.69 -9.55 164.59 o 3 2 -21 65.57 -14.52 132.13 o 4 2 -21 120.57 160.17 152.12 o 5 2 -21 473.20 539.70 197.49 o 6 2 -21 317.29 438.15 136.24 o 7 2 -21 108.90 60.79 160.20 o 8 2 -21 835.70 698.87 170.27 o 9 2 -21 221.70 99.29 234.43 o 10 2 -21 13.15 52.63 239.71 o -3 3 -21 192.84 138.53 245.67 o -2 3 -21 167.86 106.31 244.39 o -1 3 -21 29.30 219.35 205.75 o 0 3 -21 234.58 220.37 208.67 o 1 3 -21 662.87 528.57 189.33 o 2 3 -21 487.91 581.55 133.72 o 3 3 -21 24.98 72.63 138.42 o 4 3 -21 85.36 -8.34 147.89 o 5 3 -21 501.40 438.92 144.46 o 6 3 -21 91.79 117.19 136.76 o 7 3 -21 55.65 101.61 162.05 o 8 3 -21 360.22 160.76 175.78 o 9 3 -21 173.41 232.95 184.32 o 10 3 -21 40.64 -15.63 265.45 o -3 4 -21 61.11 79.64 262.79 o -2 4 -21 120.63 -8.50 227.09 o -1 4 -21 10.27 60.85 215.01 o 0 4 -21 214.50 305.49 199.61 o 1 4 -21 609.65 386.49 198.32 o 2 4 -21 582.70 499.92 148.87 o 3 4 -21 319.88 281.93 148.22 o 4 4 -21 277.77 230.88 146.25 o 5 4 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1051.43 1045.64 186.11 o 5 2 -20 249.69 247.51 124.49 o 6 2 -20 411.36 186.81 119.57 o 7 2 -20 946.32 777.68 134.49 o 8 2 -20 459.16 321.24 157.08 o 9 2 -20 29.46 213.88 162.87 o 10 2 -20 7.25 -38.38 228.45 o 11 2 -20 25.25 -29.65 241.78 o -4 3 -20 101.48 276.43 237.17 o -3 3 -20 181.21 395.40 231.05 o -2 3 -20 61.79 176.70 207.48 o -1 3 -20 350.84 339.71 213.97 o 0 3 -20 702.98 461.32 183.18 o 1 3 -20 261.83 313.62 169.00 o 2 3 -20 55.53 103.88 123.64 o 3 3 -20 273.32 277.69 131.76 o 4 3 -20 1075.49 1225.06 145.78 o 5 3 -20 56.48 109.36 146.38 o 6 3 -20 195.41 172.82 130.27 o 7 3 -20 411.93 467.64 162.00 o 8 3 -20 460.02 439.99 160.07 o 9 3 -20 292.51 210.80 171.47 o 10 3 -20 12.29 169.61 233.51 o 11 3 -20 50.97 142.49 242.70 o -4 4 -20 13.87 192.54 260.64 o -3 4 -20 37.13 -39.01 230.85 o -2 4 -20 19.64 176.29 218.04 o -1 4 -20 99.17 128.17 198.05 o 0 4 -20 409.40 378.28 207.08 o 1 4 -20 694.08 618.48 190.74 o 2 4 -20 597.22 494.79 135.40 o 3 4 -20 335.12 530.16 137.64 o 4 4 -20 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o 6 1 -19 321.22 318.79 84.00 o 7 1 -19 374.27 386.78 87.49 o 8 1 -19 26.60 -98.91 98.91 o 9 1 -19 18.55 60.15 122.37 o 10 1 -19 114.93 148.35 139.92 o 11 1 -19 90.18 88.50 184.34 o 12 1 -19 145.20 81.38 188.46 o -6 2 -19 43.83 110.56 263.46 o -5 2 -19 160.39 4.30 246.38 o -4 2 -19 604.53 538.30 209.61 o -3 2 -19 357.18 364.35 203.13 o -2 2 -19 805.39 1205.58 201.26 o -1 2 -19 425.83 506.97 176.50 o 0 2 -19 24.81 -4.65 168.65 o 1 2 -19 176.37 247.94 110.93 o 2 2 -19 216.98 401.19 112.68 o 3 2 -19 705.23 594.96 117.27 o 4 2 -19 1515.00 1391.47 133.57 o 5 2 -19 53.65 -98.70 105.96 o 6 2 -19 540.00 307.61 111.17 o 7 2 -19 987.18 987.10 120.35 o 8 2 -19 190.39 165.11 140.71 o 9 2 -19 53.87 -110.75 110.75 o 10 2 -19 58.05 -12.64 150.84 o 11 2 -19 283.80 329.84 167.39 o 12 2 -19 312.58 99.07 194.10 o -5 3 -19 219.37 109.91 233.42 o -4 3 -19 92.40 206.30 215.98 o -3 3 -19 247.52 259.07 212.23 o -2 3 -19 615.37 679.50 184.72 o -1 3 -19 355.34 253.25 173.47 o 0 3 -19 300.98 314.89 157.09 o 1 3 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