#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180894 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/34/2103427.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103427_Fobs loop_ _publ_author_name 'Ross II, C. R.' 'Bauer, M. R.' 'Nielson, R. M.' 'Abrahams, S. C.' _publ_section_title ; Aminoguanidinium(1+) pentafluorozirconate: multiple redetermination and comparisons ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 841 _journal_page_last 848 _journal_volume 58 _journal_year 2002 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.6404 _cell_length_b 6.8981 _cell_length_c 15.9872 _exptl_crystal_F_000 504.00 _reflns_d_resolution_high 0.8204 _cod_data_source_file br01122sup3.hkl _cod_data_source_block 2 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x+1/2, -y, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' 'x-1/2, y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 18563.88 17203.10 34.08 o 4 0 0 706.45 761.04 15.23 o 6 0 0 4624.99 4721.97 137.15 o 8 0 0 2805.64 2944.78 98.30 o 2 1 0 4705.54 4626.87 49.51 o 4 1 0 18932.86 20014.60 243.01 o 6 1 0 3472.56 3548.23 80.39 o 8 1 0 7.35 7.03 0.93 o 0 2 0 73975.45 87515.11 130.05 o 2 2 0 2483.52 2409.82 49.20 o 4 2 0 133.59 137.72 8.75 o 6 2 0 2559.82 2523.66 141.90 o 2 3 0 5974.19 6045.17 176.76 o 4 3 0 15914.94 16665.59 887.86 o 6 3 0 3322.26 3356.32 176.80 o 0 4 0 41900.88 45877.09 110.87 o 2 4 0 5775.09 5740.92 97.75 o 4 4 0 119.13 116.85 13.10 o 6 4 0 2243.20 2205.62 138.21 o 2 5 0 1165.78 1176.15 58.62 o 4 5 0 4042.59 4000.71 358.68 o 6 5 0 1004.16 960.89 77.00 o 0 6 0 8241.21 8123.46 49.74 o 2 6 0 1347.64 1293.34 21.02 o 4 6 0 10.99 18.62 3.54 o 2 7 0 1424.41 1435.96 56.43 o 4 7 0 2912.03 2972.92 115.62 o 0 8 0 2377.68 2316.71 20.18 o 2 8 0 542.79 557.92 6.55 o 1 0 1 65.03 94.73 1.34 o 2 0 1 13366.58 12355.42 124.17 o 3 0 1 20.15 18.09 0.90 o 4 0 1 15872.28 15309.30 172.16 o 5 0 1 233.20 235.35 3.71 o 6 0 1 7499.20 7390.57 136.32 o 7 0 1 1058.52 996.60 13.86 o 8 0 1 0.21 1.18 1.48 o 0 1 1 22359.16 24889.02 981.66 o 1 1 1 2.45 11.72 2.07 o 2 1 1 4702.13 4771.94 43.54 o 3 1 1 1753.64 1769.05 23.20 o 4 1 1 87.96 92.37 1.12 o 5 1 1 442.30 427.18 7.82 o 6 1 1 4168.97 4132.67 55.04 o 7 1 1 80.92 83.02 2.01 o 8 1 1 2114.46 2080.97 20.60 o 1 2 1 82.48 96.59 5.70 o 2 2 1 1977.84 1943.58 52.95 o 3 2 1 1.77 5.18 1.13 o 4 2 1 4170.79 4150.57 138.01 o 5 2 1 156.05 154.35 7.41 o 6 2 1 3339.27 3378.40 116.78 o 7 2 1 717.10 705.09 24.15 o 0 3 1 23408.61 26302.98 348.94 o 1 3 1 32.98 34.68 1.01 o 2 3 1 5908.44 5940.03 93.43 o 3 3 1 1346.50 1315.13 42.39 o 4 3 1 4.04 9.65 2.17 o 5 3 1 403.93 394.28 16.97 o 6 3 1 3389.27 3496.74 109.97 o 7 3 1 79.93 79.14 2.39 o 1 4 1 127.60 128.71 1.96 o 2 4 1 4098.95 4130.57 85.18 o 3 4 1 43.68 48.03 2.00 o 4 4 1 6245.03 6160.20 269.78 o 5 4 1 95.36 92.02 2.97 o 6 4 1 3284.50 3292.35 125.67 o 7 4 1 463.51 450.81 12.42 o 0 5 1 3626.94 3685.73 64.84 o 1 5 1 8.15 14.64 4.08 o 2 5 1 797.23 793.99 16.95 o 3 5 1 310.04 315.14 7.84 o 4 5 1 15.47 14.60 2.99 o 5 5 1 129.04 122.29 3.66 o 6 5 1 1315.01 1288.21 41.57 o 1 6 1 32.69 33.98 1.89 o 2 6 1 1027.97 1022.02 10.46 o 3 6 1 19.19 21.82 1.43 o 4 6 1 1891.28 1853.15 73.25 o 5 6 1 33.59 36.30 1.13 o 0 7 1 3580.03 3488.32 97.61 o 1 7 1 16.69 21.02 2.63 o 2 7 1 1302.11 1273.49 24.61 o 3 7 1 157.99 158.15 4.34 o 4 7 1 1.10 12.64 4.37 o 1 8 1 18.20 22.98 1.68 o 2 8 1 424.32 441.02 10.09 o 0 0 2 23446.96 17547.97 456.25 o 1 0 2 1323.35 1369.26 17.62 o 2 0 2 6152.19 6109.54 31.98 o 3 0 2 17411.32 16929.90 308.14 o 4 0 2 6.24 10.62 1.13 o 5 0 2 1209.80 1276.59 27.85 o 6 0 2 3491.00 3509.06 75.84 o 7 0 2 407.84 424.50 8.59 o 8 0 2 2133.09 2133.79 44.81 o 1 1 2 8502.69 8812.91 91.25 o 2 1 2 1836.99 1723.36 14.70 o 3 1 2 2348.68 2490.02 30.21 o 4 1 2 3516.33 3458.45 51.05 o 5 1 2 90.85 103.04 6.29 o 6 1 2 2787.17 2737.82 41.94 o 7 1 2 1509.72 1574.12 20.19 o 0 2 2 1142.63 1089.50 8.18 o 1 2 2 337.71 344.19 4.90 o 2 2 2 107.54 96.73 2.87 o 3 2 2 7614.16 7753.04 162.86 o 4 2 2 39.08 43.08 1.94 o 5 2 2 361.90 372.34 9.79 o 6 2 2 1889.95 1879.85 54.51 o 7 2 2 193.52 189.08 6.05 o 1 3 2 6086.21 6233.25 58.83 o 2 3 2 2959.98 2829.67 93.57 o 3 3 2 1508.54 1482.81 42.04 o 4 3 2 4724.61 4511.94 127.09 o 5 3 2 92.13 95.62 4.10 o 6 3 2 2691.44 2764.47 108.45 o 7 3 2 1224.28 1243.11 34.66 o 0 4 2 7203.88 7397.63 190.44 o 1 4 2 452.36 454.24 10.85 o 2 4 2 2189.32 2185.49 44.01 o 3 4 2 4853.45 4789.98 183.31 o 4 4 2 1.18 11.99 4.04 o 5 4 2 653.07 641.43 29.15 o 6 4 2 1650.11 1654.64 48.37 o 7 4 2 173.44 165.46 6.35 o 1 5 2 1167.44 1146.53 10.10 o 2 5 2 416.51 414.69 10.30 o 3 5 2 286.90 271.20 6.11 o 4 5 2 1095.29 1037.14 22.22 o 5 5 2 48.49 53.34 1.48 o 6 5 2 830.33 799.12 26.61 o 0 6 2 1570.25 1594.41 15.57 o 1 6 2 111.29 106.25 3.35 o 2 6 2 494.71 502.15 14.78 o 3 6 2 1340.76 1311.06 38.70 o 4 6 2 0.16 12.57 5.97 o 5 6 2 247.67 250.90 5.15 o 1 7 2 854.19 827.87 9.24 o 2 7 2 740.92 743.81 17.80 o 3 7 2 156.24 154.79 4.28 o 4 7 2 1367.65 1346.16 37.57 o 0 8 2 670.88 698.60 7.85 o 1 8 2 39.72 40.09 1.77 o 2 8 2 251.22 255.57 3.77 o 1 0 3 12147.38 11068.48 228.84 o 2 0 3 2756.27 2714.85 18.47 o 3 0 3 5162.85 5447.71 71.15 o 4 0 3 8662.44 8840.30 123.36 o 5 0 3 755.66 793.16 12.52 o 6 0 3 1078.02 1130.04 16.79 o 7 0 3 2382.27 2416.17 48.44 o 0 1 3 18503.56 17615.32 415.26 o 1 1 3 3335.42 3248.69 22.26 o 2 1 3 186.58 167.94 4.09 o 3 1 3 9463.07 10046.79 91.44 o 4 1 3 9.80 10.76 1.09 o 5 1 3 1120.26 1161.63 19.80 o 6 1 3 808.90 819.11 12.08 o 7 1 3 539.51 541.94 9.19 o 1 2 3 1682.07 1591.68 29.98 o 2 2 3 47.86 51.46 5.54 o 3 2 3 1758.16 1832.83 41.85 o 4 2 3 2035.56 2135.57 66.27 o 5 2 3 483.08 477.41 10.72 o 6 2 3 210.51 222.63 3.46 o 7 2 3 1464.23 1483.31 34.98 o 0 3 3 14419.83 15204.21 163.97 o 1 3 3 1876.84 1822.19 18.24 o 2 3 3 1373.86 1372.99 33.36 o 3 3 3 7948.70 8271.41 221.09 o 4 3 3 15.87 14.79 1.72 o 5 3 3 1432.18 1433.16 62.24 o 6 3 3 851.12 844.77 20.75 o 7 3 3 482.53 480.87 19.46 o 1 4 3 3831.66 3934.60 57.68 o 2 4 3 1276.05 1342.41 28.43 o 3 4 3 1500.59 1514.24 62.01 o 4 4 3 3373.09 3421.95 82.36 o 5 4 3 365.09 357.29 16.48 o 6 4 3 567.79 587.76 19.33 o 7 4 3 1245.69 1198.64 38.87 o 0 5 3 1915.26 1970.48 45.58 o 1 5 3 360.37 348.09 7.02 o 2 5 3 128.53 144.25 2.20 o 3 5 3 2128.70 2105.73 44.01 o 4 5 3 2.11 4.09 1.82 o 5 5 3 462.80 437.96 14.63 o 6 5 3 357.58 342.43 10.14 o 1 6 3 1057.66 1045.00 9.67 o 2 6 3 387.35 411.41 13.70 o 3 6 3 370.74 377.76 5.78 o 4 6 3 1002.67 1017.42 33.50 o 5 6 3 156.18 153.54 6.01 o 0 7 3 2119.33 2087.64 16.70 o 1 7 3 262.87 261.59 4.08 o 2 7 3 552.88 562.14 7.74 o 3 7 3 1367.10 1403.96 32.23 o 4 7 3 0.67 2.30 0.84 o 1 8 3 457.46 466.96 9.41 o 2 8 3 213.46 215.62 2.96 o 0 0 4 3737.70 3664.81 70.96 o 1 0 4 111.41 126.84 2.67 o 2 0 4 6347.60 6092.15 74.65 o 3 0 4 17306.98 16491.51 331.95 o 4 0 4 50.76 58.59 2.28 o 5 0 4 2921.69 2934.98 40.07 o 6 0 4 654.52 633.62 13.01 o 7 0 4 876.88 873.56 19.99 o 1 1 4 3821.25 3556.81 50.78 o 2 1 4 1476.85 1507.78 15.87 o 3 1 4 1792.56 1747.92 19.85 o 4 1 4 882.61 875.57 15.43 o 5 1 4 7.12 84.33 24.76 o 6 1 4 674.08 653.13 13.50 o 7 1 4 2665.01 2580.83 35.23 o 0 2 4 75.32 85.72 1.78 o 1 2 4 69.44 78.24 2.18 o 2 2 4 682.81 664.75 28.83 o 3 2 4 5609.14 5653.81 147.32 o 4 2 4 122.37 119.19 3.42 o 5 2 4 765.04 781.78 25.19 o 6 2 4 277.73 288.49 7.35 o 7 2 4 404.08 387.82 7.93 o 1 3 4 5537.13 5440.39 39.03 o 2 3 4 1850.70 1888.72 34.81 o 3 3 4 1842.36 1786.76 47.32 o 4 3 4 1428.31 1446.53 64.29 o 5 3 4 32.46 32.01 1.68 o 6 3 4 759.72 744.75 20.38 o 7 3 4 2296.14 2249.61 62.95 o 0 4 4 1575.20 1581.60 13.88 o 1 4 4 247.28 249.34 3.75 o 2 4 4 1668.28 1631.77 50.79 o 3 4 4 5754.71 5600.96 224.82 o 4 4 4 9.68 12.80 1.48 o 5 4 4 1661.83 1631.97 55.63 o 6 4 4 349.51 353.38 10.02 o 1 5 4 884.80 884.47 8.33 o 2 5 4 283.72 300.86 4.57 o 3 5 4 415.88 413.80 13.20 o 4 5 4 254.37 258.56 12.60 o 5 5 4 27.14 26.12 2.00 o 6 5 4 203.58 200.64 9.59 o 0 6 4 316.85 324.28 6.60 o 1 6 4 91.58 89.97 1.95 o 2 6 4 356.96 355.78 13.73 o 3 6 4 1642.50 1632.88 47.37 o 4 6 4 6.51 8.06 1.39 o 5 6 4 666.92 673.30 18.88 o 1 7 4 1353.48 1372.47 22.19 o 2 7 4 401.77 403.15 10.68 o 3 7 4 393.35 394.26 11.32 o 4 7 4 455.16 456.68 17.75 o 0 8 4 180.62 181.58 3.88 o 1 8 4 54.28 57.46 1.12 o 1 0 5 13490.42 12262.96 147.97 o 2 0 5 2818.24 2807.99 11.57 o 3 0 5 3424.45 3435.59 41.17 o 4 0 5 1538.50 1611.70 26.39 o 5 0 5 373.26 381.55 6.30 o 6 0 5 516.41 521.07 7.92 o 7 0 5 4170.08 4153.08 59.31 o 0 1 5 303.44 273.91 3.57 o 1 1 5 426.10 394.09 5.10 o 2 1 5 3314.56 3562.22 28.81 o 3 1 5 10677.41 10765.64 93.60 o 4 1 5 273.80 289.17 5.35 o 5 1 5 1428.62 1444.61 22.98 o 6 1 5 15.30 14.92 1.27 o 7 1 5 489.30 493.23 8.41 o 1 2 5 1182.99 1097.71 12.73 o 2 2 5 419.24 395.76 4.86 o 3 2 5 671.12 668.62 11.11 o 4 2 5 187.22 193.09 4.90 o 5 2 5 209.59 206.15 5.43 o 6 2 5 121.26 123.07 4.65 o 7 2 5 2551.74 2530.95 81.04 o 0 3 5 803.36 753.22 29.74 o 1 3 5 807.28 783.38 9.07 o 2 3 5 2612.29 2692.70 76.98 o 3 3 5 9796.10 9916.72 388.76 o 4 3 5 174.48 174.23 8.59 o 5 3 5 2122.84 2141.15 67.27 o 6 3 5 30.83 36.75 4.79 o 7 3 5 508.60 502.97 17.61 o 1 4 5 4931.93 4989.23 25.42 o 2 4 5 625.09 608.33 16.76 o 3 4 5 1162.92 1124.83 28.10 o 4 4 5 570.65 551.04 21.81 o 5 4 5 252.87 265.72 11.00 o 6 4 5 216.58 214.38 4.49 o 0 5 5 8.05 19.17 1.99 o 1 5 5 155.74 162.54 2.37 o 2 5 5 331.76 331.10 10.55 o 3 5 5 2557.75 2492.05 79.05 o 4 5 5 40.93 46.95 1.53 o 5 5 5 670.22 663.64 14.46 o 6 5 5 4.45 7.09 1.20 o 1 6 5 1367.29 1381.79 10.41 o 2 6 5 84.23 86.98 2.77 o 3 6 5 292.58 298.04 5.29 o 4 6 5 127.38 127.76 5.54 o 5 6 5 132.81 135.87 5.77 o 0 7 5 195.76 190.49 6.70 o 1 7 5 248.38 243.18 3.98 o 2 7 5 266.04 269.30 7.59 o 3 7 5 2012.07 2025.37 49.34 o 1 8 5 641.48 649.58 9.68 o 0 0 6 11.21 13.08 2.15 o 1 0 6 9548.12 9047.41 133.65 o 2 0 6 904.79 941.99 14.42 o 3 0 6 16244.76 15448.29 403.99 o 4 0 6 61.35 100.09 18.35 o 5 0 6 6092.21 5836.08 102.42 o 6 0 6 15.27 16.24 1.66 o 7 0 6 888.66 895.24 28.16 o 1 1 6 3676.26 3650.53 78.87 o 2 1 6 896.08 922.89 8.10 o 3 1 6 1384.71 1414.36 10.33 o 4 1 6 292.53 292.14 5.78 o 5 1 6 2548.31 2508.81 27.07 o 6 1 6 103.06 104.98 1.51 o 7 1 6 3421.70 3471.55 51.30 o 0 2 6 755.49 740.68 8.88 o 1 2 6 3057.01 3009.14 40.86 o 2 2 6 61.58 66.79 5.23 o 3 2 6 4946.27 5100.38 84.48 o 4 2 6 79.24 100.06 8.42 o 5 2 6 1987.38 1987.22 47.68 o 6 2 6 0.27 3.25 1.55 o 7 2 6 344.87 328.95 11.83 o 1 3 6 6592.15 6590.99 79.67 o 2 3 6 650.47 638.89 17.06 o 3 3 6 1596.23 1590.72 43.17 o 4 3 6 267.73 278.46 12.67 o 5 3 6 1829.08 1842.68 49.60 o 6 3 6 32.34 34.62 1.47 o 7 3 6 2989.15 3043.18 82.33 o 0 4 6 4.09 13.01 5.49 o 1 4 6 2414.20 2326.12 37.95 o 2 4 6 161.72 154.94 4.82 o 3 4 6 6536.08 6668.07 161.48 o 4 4 6 19.79 21.31 1.88 o 5 4 6 2975.90 2931.48 58.36 o 6 4 6 6.53 16.59 5.13 o 1 5 6 1199.28 1202.88 11.86 o 2 5 6 74.25 71.14 2.03 o 3 5 6 280.41 290.48 9.91 o 4 5 6 13.26 16.89 1.38 o 5 5 6 772.29 735.11 29.05 o 6 5 6 38.77 38.96 1.05 o 0 6 6 24.33 20.54 2.63 o 1 6 6 634.00 618.59 8.88 o 2 6 6 10.50 12.86 1.38 o 3 6 6 2061.05 2097.19 49.32 o 4 6 6 10.58 14.38 1.05 o 5 6 6 1084.18 1066.68 37.05 o 1 7 6 1945.01 1940.99 33.02 o 2 7 6 54.58 60.51 2.83 o 3 7 6 345.97 346.41 12.84 o 0 8 6 2.98 6.11 1.43 o 1 0 7 32129.48 28987.17 687.49 o 2 0 7 380.31 418.37 14.49 o 3 0 7 4353.95 4340.15 99.79 o 4 0 7 195.65 203.04 7.95 o 5 0 7 146.05 143.62 3.00 o 6 0 7 434.42 446.23 8.50 o 7 0 7 4298.51 4275.26 76.53 o 0 1 7 6559.64 6669.62 93.15 o 1 1 7 447.94 618.55 68.82 o 2 1 7 13.19 20.29 1.38 o 3 1 7 10065.22 10311.48 113.99 o 4 1 7 311.12 301.39 4.23 o 5 1 7 5488.06 5457.09 80.39 o 6 1 7 113.60 109.88 1.59 o 7 1 7 599.46 605.28 12.39 o 1 2 7 7675.53 7732.76 170.96 o 2 2 7 103.65 119.04 2.40 o 3 2 7 1089.31 1116.21 25.11 o 4 2 7 317.89 329.14 20.13 o 5 2 7 63.36 59.25 1.92 o 6 2 7 436.76 445.26 11.66 o 7 2 7 2560.16 2539.38 63.66 o 0 3 7 3086.41 3038.82 91.29 o 1 3 7 936.75 939.21 13.51 o 2 3 7 5.90 17.40 6.00 o 3 3 7 9081.37 9262.09 188.69 o 4 3 7 173.86 169.15 5.37 o 5 3 7 5363.71 5541.22 273.04 o 6 3 7 78.82 88.41 6.51 o 1 4 7 9673.45 9650.17 147.74 o 2 4 7 34.38 42.59 3.27 o 3 4 7 1556.51 1522.83 38.57 o 4 4 7 157.06 162.20 4.95 o 5 4 7 119.88 121.56 6.98 o 6 4 7 215.14 208.95 6.56 o 0 5 7 1267.17 1182.44 13.85 o 1 5 7 193.51 195.24 3.43 o 2 5 7 32.56 34.55 1.73 o 3 5 7 2204.32 2164.57 55.58 o 4 5 7 74.89 73.32 3.66 o 5 5 7 1672.29 1641.25 63.89 o 1 6 7 2357.15 2364.42 41.92 o 2 6 7 0.79 2.75 3.16 o 3 6 7 422.24 436.43 5.83 o 4 6 7 112.61 117.55 3.32 o 0 7 7 278.74 281.27 5.78 o 1 7 7 260.75 262.08 4.31 o 2 7 7 10.98 17.92 2.64 o 3 7 7 1818.12 1828.65 54.66 o 0 0 8 9301.89 9263.01 157.74 o 1 0 8 3119.16 3183.29 14.28 o 2 0 8 111.66 90.76 2.17 o 3 0 8 10546.38 9818.77 212.37 o 4 0 8 390.29 386.17 5.87 o 5 0 8 8560.45 8152.83 168.93 o 6 0 8 1720.80 1727.60 13.43 o 7 0 8 788.58 799.19 29.72 o 1 1 8 10967.98 11196.35 169.98 o 2 1 8 934.83 950.08 10.82 o 3 1 8 1305.66 1327.54 18.92 o 4 1 8 2476.95 2498.16 34.35 o 5 1 8 422.63 428.46 5.67 o 6 1 8 945.74 958.64 14.21 o 7 1 8 2382.27 2407.52 29.74 o 0 2 8 6045.76 6363.79 28.72 o 1 2 8 705.08 704.93 7.10 o 2 2 8 64.88 56.57 2.98 o 3 2 8 2858.72 2903.99 44.58 o 4 2 8 308.96 300.34 8.31 o 5 2 8 3433.44 3461.89 93.06 o 6 2 8 1371.49 1391.68 23.97 o 7 2 8 310.39 307.82 9.03 o 1 3 8 10734.88 11163.21 87.52 o 2 3 8 782.20 793.50 22.12 o 3 3 8 1464.18 1466.27 35.71 o 4 3 8 1779.34 1804.69 35.36 o 5 3 8 373.03 372.52 12.94 o 6 3 8 710.00 719.19 19.83 o 0 4 8 3307.86 3383.72 48.86 o 1 4 8 978.32 952.07 8.97 o 2 4 8 167.94 158.78 4.20 o 3 4 8 4236.22 4203.32 75.57 o 4 4 8 133.67 131.00 6.10 o 5 4 8 3746.71 3746.96 111.55 o 6 4 8 847.74 837.69 17.83 o 1 5 8 1993.51 2012.17 17.24 o 2 5 8 407.30 390.55 7.46 o 3 5 8 284.75 279.51 4.14 o 4 5 8 807.48 802.19 29.23 o 5 5 8 159.48 157.97 5.51 o 0 6 8 1157.30 1121.61 30.29 o 1 6 8 254.80 267.65 4.57 o 2 6 8 126.53 128.55 1.98 o 3 6 8 1244.99 1239.03 19.76 o 4 6 8 47.39 49.59 2.26 o 1 7 8 1981.52 2000.20 49.89 o 2 7 8 229.43 221.97 6.74 o 3 7 8 335.21 330.62 4.31 o 1 0 9 9300.70 8929.98 192.78 o 2 0 9 2686.83 2583.21 18.28 o 3 0 9 788.89 743.14 16.93 o 4 0 9 5978.05 5681.25 128.39 o 5 0 9 2211.74 2092.37 50.35 o 6 0 9 2040.73 2003.73 36.46 o 7 0 9 1532.06 1526.84 30.81 o 0 1 9 14703.57 14699.68 114.10 o 1 1 9 2981.65 3022.76 34.26 o 2 1 9 1680.81 1705.87 16.28 o 3 1 9 1172.15 1233.37 20.78 o 4 1 9 0.36 3.44 1.41 o 5 1 9 3255.13 3253.15 61.99 o 6 1 9 1784.14 1806.06 26.71 o 7 1 9 133.26 146.15 5.65 o 1 2 9 1217.62 1264.74 35.17 o 2 2 9 1394.24 1354.23 32.18 o 3 2 9 29.62 34.12 1.90 o 4 2 9 3698.64 3715.57 68.05 o 5 2 9 1486.33 1459.55 33.72 o 6 2 9 1361.61 1362.79 29.65 o 0 3 9 9734.74 9800.88 231.84 o 1 3 9 2316.37 2378.85 63.64 o 2 3 9 1563.15 1579.75 49.42 o 3 3 9 1960.00 2032.70 55.20 o 4 3 9 0.02 6.12 1.90 o 5 3 9 3191.44 3249.27 102.93 o 6 3 9 1342.86 1362.81 57.12 o 1 4 9 3418.62 3454.34 41.44 o 2 4 9 1213.59 1191.73 10.39 o 3 4 9 293.04 302.55 6.42 o 4 4 9 2767.02 2832.59 81.73 o 5 4 9 937.43 926.71 35.89 o 6 4 9 1002.77 980.22 35.28 o 0 5 9 3140.83 3223.72 121.95 o 1 5 9 531.40 530.37 11.51 o 2 5 9 572.16 568.78 10.44 o 3 5 9 407.54 418.96 9.41 o 4 5 9 1.02 4.21 1.23 o 5 5 9 897.06 863.98 34.83 o 1 6 9 858.42 857.74 8.56 o 2 6 9 487.18 498.26 13.79 o 3 6 9 58.46 64.02 2.63 o 4 6 9 1116.10 1089.69 29.71 o 0 7 9 1456.34 1417.07 65.83 o 1 7 9 354.22 347.26 8.95 o 2 7 9 376.58 379.46 12.66 o 0 0 10 13277.97 12871.03 748.45 o 1 0 10 156.89 179.81 6.97 o 2 0 10 5919.56 5950.81 143.65 o 3 0 10 866.28 896.71 10.16 o 4 0 10 38.76 38.48 2.14 o 5 0 10 2646.13 2598.15 73.11 o 6 0 10 1933.97 1924.91 47.54 o 1 1 10 1513.89 1520.11 26.10 o 2 1 10 2379.42 2343.02 18.17 o 3 1 10 25.26 22.09 1.24 o 4 1 10 4349.39 4367.71 65.67 o 5 1 10 21.92 24.83 1.64 o 6 1 10 2640.06 2628.44 49.11 o 0 2 10 6031.87 6062.81 32.46 o 1 2 10 9.82 12.06 2.75 o 2 2 10 2632.18 2677.36 35.08 o 3 2 10 8.69 27.30 6.58 o 4 2 10 11.37 18.20 1.78 o 5 2 10 785.80 793.24 26.69 o 6 2 10 1359.66 1318.82 31.23 o 1 3 10 2254.06 2229.08 25.31 o 2 3 10 2132.44 2123.36 47.42 o 3 3 10 20.92 23.57 1.60 o 4 3 10 3832.00 3822.37 81.79 o 5 3 10 36.11 38.41 2.61 o 6 3 10 2138.15 2084.20 62.07 o 0 4 10 5439.42 5226.46 126.27 o 1 4 10 83.70 80.66 1.97 o 2 4 10 2332.77 2322.14 41.40 o 3 4 10 434.14 443.18 17.01 o 4 4 10 23.45 26.67 2.08 o 5 4 10 1159.25 1151.45 39.58 o 1 5 10 247.26 253.31 3.76 o 2 5 10 739.07 727.09 9.46 o 3 5 10 5.48 9.91 1.24 o 4 5 10 1559.56 1488.15 26.95 o 5 5 10 16.14 14.40 1.49 o 0 6 10 1842.84 1758.74 53.22 o 1 6 10 17.77 18.56 1.24 o 2 6 10 813.35 812.04 15.95 o 3 6 10 108.28 108.21 2.40 o 1 7 10 552.28 553.74 17.69 o 1 0 11 941.24 993.56 19.39 o 2 0 11 4667.92 4650.82 133.79 o 3 0 11 0.65 14.18 5.13 o 4 0 11 6735.05 6400.94 216.24 o 5 0 11 58.16 60.20 2.25 o 6 0 11 2231.18 2224.70 50.56 o 0 1 11 6804.59 7065.06 118.40 o 1 1 11 3.61 13.71 2.28 o 2 1 11 3386.42 3401.32 46.76 o 3 1 11 336.79 382.79 39.42 o 4 1 11 28.35 41.69 4.92 o 5 1 11 611.43 646.26 20.85 o 6 1 11 1284.80 1296.68 22.88 o 1 2 11 20.80 64.45 19.09 o 2 2 11 2103.15 2194.85 29.73 o 3 2 11 148.42 142.20 2.49 o 4 2 11 3424.85 3407.92 58.52 o 5 2 11 21.80 24.26 2.33 o 6 2 11 1262.81 1224.06 25.62 o 0 3 11 6506.88 6660.14 90.72 o 1 3 11 37.76 35.86 1.65 o 2 3 11 3337.32 3295.98 32.02 o 3 3 11 16.19 24.94 6.54 o 4 3 11 9.77 10.88 2.45 o 5 3 11 686.09 689.03 15.92 o 6 3 11 1123.44 1088.87 23.34 o 1 4 11 300.68 289.64 5.25 o 2 4 11 2249.05 2232.12 27.28 o 3 4 11 1.77 2.64 1.72 o 4 4 11 3357.85 3313.49 158.97 o 5 4 11 26.66 27.56 1.13 o 0 5 11 2078.36 2098.12 18.61 o 1 5 11 0.26 8.97 3.79 o 2 5 11 1137.45 1110.96 37.16 o 3 5 11 89.70 105.06 6.33 o 4 5 11 13.03 15.48 1.03 o 1 6 11 27.30 29.01 1.53 o 2 6 11 889.75 880.38 20.23 o 3 6 11 0.24 2.43 1.28 o 0 0 12 9643.39 9220.50 279.21 o 1 0 12 294.54 271.11 5.22 o 2 0 12 4814.35 4646.48 54.23 o 3 0 12 94.82 112.30 6.13 o 4 0 12 38.56 44.41 1.92 o 5 0 12 370.39 390.81 18.18 o 6 0 12 1085.11 1101.88 17.74 o 1 1 12 180.41 195.78 6.83 o 2 1 12 2386.98 2351.04 20.01 o 3 1 12 0.55 2.10 1.60 o 4 1 12 4251.25 4265.88 57.27 o 5 1 12 62.92 63.55 1.27 o 6 1 12 763.03 755.84 12.70 o 0 2 12 3285.27 3394.75 65.84 o 1 2 12 48.62 50.32 2.17 o 2 2 12 1735.90 1754.28 55.52 o 3 2 12 552.46 537.30 11.24 o 4 2 12 3.04 10.97 3.58 o 5 2 12 38.30 43.17 4.79 o 6 2 12 683.08 670.00 18.84 o 1 3 12 338.69 348.16 8.93 o 2 3 12 2461.18 2434.74 19.49 o 3 3 12 6.14 12.13 1.75 o 4 3 12 4106.21 4208.51 107.08 o 5 3 12 44.65 47.04 1.43 o 0 4 12 4517.55 4515.94 58.26 o 1 4 12 87.28 90.10 1.86 o 2 4 12 2220.26 2198.03 23.98 o 3 4 12 36.71 36.28 2.01 o 4 4 12 9.00 12.76 1.94 o 5 4 12 118.35 110.04 4.39 o 1 5 12 3.72 10.30 4.38 o 2 5 12 871.48 859.03 23.89 o 3 5 12 8.23 7.35 1.31 o 4 5 12 1571.20 1537.16 46.43 o 0 6 12 1642.16 1667.57 80.68 o 1 6 12 12.19 13.56 0.96 o 2 6 12 786.62 787.07 14.89 o 1 0 13 112.46 113.99 2.64 o 2 0 13 4329.24 4253.36 92.10 o 3 0 13 63.12 60.03 2.01 o 4 0 13 3660.16 3739.23 77.86 o 5 0 13 32.89 31.10 1.45 o 6 0 13 1834.84 1886.06 37.68 o 0 1 13 319.54 428.52 23.47 o 1 1 13 99.67 94.14 2.54 o 2 1 13 2462.26 2485.43 41.52 o 3 1 13 308.21 310.83 3.29 o 4 1 13 65.80 71.53 3.12 o 5 1 13 22.94 27.97 1.95 o 1 2 13 38.94 64.14 13.04 o 2 2 13 1741.70 1878.80 69.47 o 3 2 13 171.77 167.77 5.53 o 4 2 13 1429.29 1467.53 36.91 o 5 2 13 41.11 43.85 3.64 o 0 3 13 1120.52 1181.23 26.04 o 1 3 13 46.65 53.47 2.35 o 2 3 13 2536.10 2532.23 19.43 o 3 3 13 128.08 127.49 4.58 o 4 3 13 19.60 20.85 1.42 o 5 3 13 8.13 8.31 2.29 o 1 4 13 3.37 19.44 5.71 o 2 4 13 1918.87 1951.90 44.14 o 3 4 13 42.85 47.52 1.42 o 4 4 13 2015.55 1976.19 44.11 o 0 5 13 260.74 254.36 5.23 o 1 5 13 53.69 63.80 3.88 o 2 5 13 713.65 687.99 6.57 o 3 5 13 173.88 164.72 3.40 o 1 6 13 23.58 25.16 0.88 o 0 0 14 4540.48 4393.76 207.62 o 1 0 14 240.73 247.44 3.72 o 2 0 14 4977.20 4741.44 157.00 o 3 0 14 920.51 874.72 12.92 o 4 0 14 0.34 3.82 2.25 o 5 0 14 297.53 307.94 9.69 o 1 1 14 1672.25 1680.85 9.25 o 2 1 14 2808.61 2839.98 30.80 o 3 1 14 536.41 498.60 4.95 o 4 1 14 3179.42 3157.64 48.44 o 5 1 14 9.71 14.69 1.58 o 0 2 14 1016.05 1071.14 38.58 o 1 2 14 272.02 273.44 3.99 o 2 2 14 1900.72 1889.87 23.98 o 3 2 14 1112.77 1084.40 9.94 o 4 2 14 9.44 12.92 1.37 o 5 2 14 397.53 382.88 10.46 o 1 3 14 1084.99 1087.45 19.27 o 2 3 14 2610.70 2633.87 34.10 o 3 3 14 313.56 302.17 5.65 o 4 3 14 3102.38 3178.79 84.48 o 0 4 14 2186.91 2175.90 25.04 o 1 4 14 129.92 131.23 2.08 o 2 4 14 2217.65 2164.68 34.67 o 3 4 14 614.99 603.82 16.87 o 4 4 14 0.02 4.34 1.64 o 1 5 14 787.38 782.53 10.41 o 2 5 14 828.28 774.21 13.27 o 1 0 15 1601.90 1593.88 25.03 o 2 0 15 3594.99 3496.07 111.53 o 3 0 15 172.42 185.51 6.10 o 4 0 15 4723.06 4708.30 161.19 o 5 0 15 221.11 228.73 3.55 o 0 1 15 3683.26 3731.82 95.83 o 1 1 15 348.62 357.45 4.69 o 2 1 15 2611.43 2608.23 43.21 o 3 1 15 1330.32 1349.34 11.35 o 4 1 15 54.83 56.02 1.53 o 5 1 15 1517.94 1546.83 18.44 o 1 2 15 1441.14 1485.69 13.02 o 2 2 15 1534.16 1520.51 25.44 o 3 2 15 167.02 177.20 4.32 o 4 2 15 2118.98 2114.26 59.37 o 0 3 15 3843.05 3962.75 102.67 o 1 3 15 263.51 268.11 3.92 o 2 3 15 2454.15 2477.57 61.22 o 3 3 15 1019.25 1042.91 22.77 o 4 3 15 47.55 44.73 1.14 o 1 4 15 948.31 953.15 10.82 o 2 4 15 1625.96 1579.98 23.18 o 3 4 15 125.65 121.48 3.82 o 0 5 15 1027.11 995.48 9.64 o 1 5 15 155.32 146.54 3.92 o 0 0 16 438.27 471.54 42.46 o 1 0 16 705.13 687.12 9.45 o 2 0 16 1967.46 1928.29 54.57 o 3 0 16 2021.24 2025.85 30.32 o 4 0 16 0.00 5.12 1.49 o 1 1 16 2837.27 2812.09 25.45 o 2 1 16 1134.14 1120.32 21.99 o 3 1 16 249.26 251.48 3.83 o 4 1 16 534.04 552.81 15.88 o 0 2 16 22.02 36.67 2.25 o 1 2 16 530.22 515.78 6.90 o 2 2 16 579.28 576.56 13.03 o 3 2 16 1516.59 1522.79 26.06 o 4 2 16 7.44 6.43 0.91 o 1 3 16 2236.85 2258.51 38.67 o 2 3 16 1068.88 1079.41 13.27 o 3 3 16 224.50 230.32 5.15 o 0 4 16 239.83 242.65 5.17 o 1 4 16 368.07 366.16 4.67 o 2 4 16 826.59 792.83 6.14 o 1 0 17 6032.99 5960.88 49.70 o 2 0 17 294.76 298.02 10.45 o 3 0 17 572.75 560.59 8.62 o 0 1 17 2.89 5.15 1.35 o 1 1 17 1029.08 1038.52 8.42 o 2 1 17 64.53 62.09 1.87 o 3 1 17 2480.94 2506.32 8.52 o 1 2 17 4104.05 4184.39 58.05 o 2 2 17 21.81 19.73 1.54 o 3 2 17 353.96 342.77 6.46 o 0 3 17 86.02 96.86 8.75 o 1 3 17 775.32 751.26 13.84 o 2 3 17 145.54 133.23 3.48 o 0 0 18 64.45 62.19 2.29 o 1 0 18 897.45 907.54 8.68 o 2 0 18 30.92 34.43 2.29 o 3 0 18 2038.81 2085.76 31.04 o 1 1 18 3523.64 3588.26 31.06 o 2 1 18 14.50 23.70 2.10 o 0 2 18 61.74 69.86 6.93 o 1 2 18 592.33 604.48 5.95 o 2 2 18 233.01 241.16 5.22 o 1 3 18 3030.98 3014.45 11.24 o 1 0 19 3689.71 3667.25 36.66 o 0 1 19 475.63 487.96 11.51 o 1 1 19 159.65 158.52 1.74 o