#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180894 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/34/2103428.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103428_Fobs loop_ _publ_author_name 'Ross II, C. R.' 'Bauer, M. R.' 'Nielson, R. M.' 'Abrahams, S. C.' _publ_section_title ; Aminoguanidinium(1+) pentafluorozirconate: multiple redetermination and comparisons ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 841 _journal_page_last 848 _journal_volume 58 _journal_year 2002 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.6485 _cell_length_b 6.9340 _cell_length_c 16.0344 _exptl_crystal_F_000 504.00 _reflns_d_resolution_high 0.7118 _cod_data_source_file br01123sup4.hkl _cod_data_source_block 3 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 16595.00 16987.97 510.60 o 4 0 0 783.14 854.35 28.98 o 6 0 0 3006.95 3021.31 97.06 o 8 0 0 1590.92 1590.71 56.23 o 2 1 0 3542.29 3426.47 73.55 o 4 1 0 15072.00 16075.94 343.75 o 6 1 0 2764.06 2866.36 65.15 o 8 1 0 15.98 20.67 4.49 o 0 2 0 65224.45 61590.59 1849.24 o 2 2 0 1878.24 1746.03 54.46 o 4 2 0 159.15 162.61 7.02 o 6 2 0 1569.40 1628.72 54.25 o 8 2 0 846.87 873.51 35.14 o 2 3 0 4494.56 4472.13 136.42 o 4 3 0 11773.41 11888.90 362.71 o 6 3 0 2437.76 2493.71 81.49 o 8 3 0 18.96 17.65 1.85 o 0 4 0 33786.48 33137.99 997.49 o 2 4 0 4632.41 4544.48 140.33 o 4 4 0 129.89 122.98 5.37 o 6 4 0 1297.85 1196.61 43.43 o 8 4 0 824.46 817.73 34.63 o 2 5 0 740.00 765.50 27.42 o 4 5 0 2552.28 2504.89 80.58 o 6 5 0 665.49 643.60 26.81 o 8 5 0 1.84 7.86 1.91 o 0 6 0 5187.48 5091.69 157.88 o 2 6 0 831.14 826.95 30.40 o 4 6 0 11.46 13.02 1.59 o 6 6 0 449.48 426.60 17.73 o 2 7 0 847.98 848.48 32.71 o 4 7 0 1604.53 1548.94 54.62 o 6 7 0 449.21 499.94 21.65 o 0 8 0 1283.23 1246.43 45.10 o 2 8 0 306.64 298.77 12.55 o 4 8 0 2.40 6.74 1.89 o 2 9 0 98.96 99.55 4.18 o 1 0 1 25.60 38.71 0.82 o 2 0 1 11199.61 11482.34 244.30 o 3 0 1 28.71 23.82 1.02 o 4 0 1 12491.67 12628.86 270.74 o 5 0 1 145.93 146.95 4.43 o 6 0 1 5855.83 5838.48 127.97 o 7 0 1 689.56 633.95 18.29 o 8 0 1 3.98 4.66 3.19 o 9 0 1 366.49 381.46 11.23 o 0 1 1 19345.25 18870.09 283.24 o 1 1 1 0.16 0.86 0.46 o 2 1 1 3820.50 3755.03 57.20 o 3 1 1 1434.13 1454.50 23.03 o 4 1 1 30.27 35.38 0.73 o 5 1 1 309.99 294.79 6.05 o 6 1 1 2709.41 2714.81 43.68 o 7 1 1 78.88 77.89 1.80 o 8 1 1 1134.71 1149.49 21.45 o 9 1 1 16.13 13.38 0.90 o 1 2 1 122.67 133.37 2.72 o 2 2 1 1314.23 1203.83 27.06 o 3 2 1 0.05 1.14 1.11 o 4 2 1 2881.12 2805.08 62.04 o 5 2 1 93.54 95.96 2.88 o 6 2 1 2507.73 2509.53 57.81 o 7 2 1 444.43 429.41 12.57 o 8 2 1 1.60 4.80 1.02 o 9 2 1 262.56 266.86 7.75 o 0 3 1 19180.84 19117.21 406.53 o 1 3 1 16.10 19.39 0.44 o 2 3 1 4575.68 4498.77 97.28 o 3 3 1 1012.84 1009.58 23.80 o 4 3 1 0.98 6.52 0.76 o 5 3 1 266.23 251.63 13.65 o 6 3 1 2072.66 2042.91 48.25 o 7 3 1 70.08 67.61 2.03 o 8 3 1 1042.10 1028.09 28.46 o 1 4 1 83.02 79.30 1.69 o 2 4 1 3018.87 2939.94 65.23 o 3 4 1 44.29 58.65 5.15 o 4 4 1 4387.41 4317.93 94.51 o 5 4 1 53.18 50.19 1.54 o 6 4 1 2268.40 2294.58 54.13 o 7 4 1 257.16 248.32 9.36 o 8 4 1 2.60 8.06 1.32 o 0 5 1 2460.03 2466.53 55.03 o 1 5 1 2.94 4.42 0.76 o 2 5 1 502.53 528.45 14.31 o 3 5 1 188.31 187.73 5.53 o 4 5 1 1.76 4.86 2.56 o 5 5 1 73.76 71.95 2.11 o 6 5 1 700.40 726.05 20.76 o 7 5 1 28.32 25.94 1.34 o 8 5 1 428.18 431.60 12.44 o 1 6 1 14.41 15.06 0.55 o 2 6 1 588.67 577.59 16.09 o 3 6 1 14.76 16.84 0.89 o 4 6 1 1073.61 1098.54 27.87 o 5 6 1 15.48 15.53 1.68 o 6 6 1 636.76 625.02 18.28 o 7 6 1 79.26 78.42 2.34 o 0 7 1 2188.35 2180.91 50.96 o 1 7 1 8.50 11.17 0.62 o 2 7 1 793.79 788.92 21.42 o 3 7 1 81.68 81.48 2.25 o 4 7 1 4.46 14.36 1.38 o 5 7 1 51.95 54.57 1.84 o 6 7 1 339.27 345.59 10.27 o 1 8 1 9.14 10.58 2.07 o 2 8 1 221.72 228.85 7.06 o 3 8 1 7.15 8.15 2.92 o 4 8 1 393.80 385.72 16.67 o 5 8 1 3.44 2.84 1.21 o 0 9 1 180.87 183.74 5.37 o 1 9 1 0.72 1.51 0.81 o 2 9 1 68.03 73.05 2.26 o 3 9 1 7.57 4.99 4.68 o 0 0 2 20402.21 21128.04 448.96 o 1 0 2 1115.71 1162.34 18.00 o 2 0 2 5124.06 5287.94 113.59 o 3 0 2 15061.01 15855.53 337.51 o 4 0 2 20.22 19.26 0.68 o 5 0 2 863.21 935.11 22.86 o 6 0 2 2228.96 2236.86 51.62 o 7 0 2 335.45 344.86 10.39 o 8 0 2 1147.41 1090.63 35.63 o 9 0 2 56.87 59.48 2.04 o 1 1 2 7582.39 7808.61 83.25 o 2 1 2 1264.49 1164.04 18.35 o 3 1 2 2218.89 2304.90 35.79 o 4 1 2 2516.41 2469.65 38.68 o 5 1 2 41.14 42.50 1.22 o 6 1 2 2152.43 2122.54 34.91 o 7 1 2 949.58 970.45 17.83 o 8 1 2 0.18 6.24 2.03 o 9 1 2 345.85 339.80 7.08 o 0 2 2 600.66 543.71 12.71 o 1 2 2 247.62 243.71 4.55 o 2 2 2 18.37 12.91 0.59 o 3 2 2 6162.99 6253.39 134.23 o 4 2 2 18.31 19.10 1.25 o 5 2 2 225.38 252.79 12.61 o 6 2 2 1134.56 1120.09 27.62 o 7 2 2 159.75 158.97 4.90 o 8 2 2 612.25 621.39 17.46 o 9 2 2 47.57 50.32 2.89 o 1 3 2 5005.44 5048.27 76.93 o 2 3 2 2117.24 2033.36 45.05 o 3 3 2 1280.30 1275.36 29.50 o 4 3 2 3342.32 3272.48 71.93 o 5 3 2 44.24 47.76 1.45 o 6 3 2 1922.63 1925.26 45.82 o 7 3 2 723.27 734.98 20.67 o 8 3 2 3.27 6.84 1.16 o 0 4 2 5679.05 5735.41 123.62 o 1 4 2 336.40 334.63 6.64 o 2 4 2 1671.36 1638.79 37.24 o 3 4 2 3593.77 3474.77 76.46 o 4 4 2 7.60 12.52 0.97 o 5 4 2 433.16 426.05 12.04 o 6 4 2 934.60 916.60 33.00 o 7 4 2 126.74 128.81 3.75 o 8 4 2 647.80 613.43 18.12 o 1 5 2 807.92 807.86 14.16 o 2 5 2 231.60 228.07 6.81 o 3 5 2 206.12 193.10 6.72 o 4 5 2 672.48 634.63 17.45 o 5 5 2 21.56 26.76 1.08 o 6 5 2 534.56 531.30 15.43 o 7 5 2 282.41 282.69 8.24 o 0 6 2 936.84 953.35 24.04 o 1 6 2 62.60 58.10 1.21 o 2 6 2 280.93 273.13 8.23 o 3 6 2 803.89 797.44 21.10 o 4 6 2 0.34 3.58 0.97 o 5 6 2 136.49 138.59 4.21 o 6 6 2 308.34 305.42 8.83 o 7 6 2 35.27 38.03 1.67 o 1 7 2 516.61 507.49 10.38 o 2 7 2 426.50 440.67 12.90 o 3 7 2 92.97 92.78 2.62 o 4 7 2 770.72 752.69 21.35 o 5 7 2 15.81 19.14 1.25 o 6 7 2 371.20 393.34 16.17 o 0 8 2 376.70 391.85 11.70 o 1 8 2 19.78 19.37 0.82 o 2 8 2 142.90 144.47 4.20 o 3 8 2 213.36 204.27 6.00 o 4 8 2 1.10 6.80 1.68 o 5 8 2 56.61 57.04 2.08 o 1 9 2 59.29 60.16 1.37 o 2 9 2 36.82 40.88 1.64 o 3 9 2 7.99 10.01 1.28 o 1 0 3 10533.96 10768.55 162.04 o 2 0 3 2073.51 2090.19 45.39 o 3 0 3 4859.67 5062.00 108.89 o 4 0 3 6780.67 7070.19 151.92 o 5 0 3 488.69 510.47 13.89 o 6 0 3 796.60 809.89 20.82 o 7 0 3 1527.05 1520.93 37.36 o 8 0 3 18.04 17.28 1.10 o 9 0 3 916.61 922.25 47.83 o 0 1 3 16480.35 15041.55 226.35 o 1 1 3 2893.97 2819.96 30.43 o 2 1 3 92.06 76.84 4.93 o 3 1 3 7823.24 8045.47 121.81 o 4 1 3 14.99 17.12 0.45 o 5 1 3 678.40 713.37 12.78 o 6 1 3 469.11 475.26 10.94 o 7 1 3 433.96 419.76 8.79 o 8 1 3 523.89 518.62 10.77 o 9 1 3 92.09 98.34 2.01 o 1 2 3 1172.82 1092.16 17.50 o 2 2 3 2.82 0.58 0.77 o 3 2 3 1584.80 1599.17 36.18 o 4 2 3 1390.45 1457.71 33.62 o 5 2 3 293.03 308.99 9.02 o 6 2 3 143.26 151.24 4.60 o 7 2 3 898.64 892.08 23.71 o 8 2 3 1.26 -1.31 1.79 o 9 2 3 609.19 602.31 18.33 o 0 3 3 11832.42 11464.65 244.42 o 1 3 3 1451.93 1423.81 22.58 o 2 3 3 1043.77 1026.79 23.71 o 3 3 3 6170.50 6211.50 134.19 o 4 3 3 18.21 17.98 0.79 o 5 3 3 889.06 877.93 22.37 o 6 3 3 489.78 495.79 14.20 o 7 3 3 356.97 360.43 10.62 o 8 3 3 497.18 508.93 19.13 o 1 4 3 2975.98 2946.43 45.88 o 2 4 3 937.85 965.11 23.23 o 3 4 3 1228.32 1222.04 29.13 o 4 4 3 2362.82 2402.31 54.28 o 5 4 3 203.78 196.48 5.89 o 6 4 3 398.81 390.90 11.68 o 7 4 3 710.90 682.45 20.33 o 8 4 3 5.93 2.50 3.12 o 0 5 3 1306.38 1318.07 30.82 o 1 5 3 225.87 228.47 4.78 o 2 5 3 81.18 87.95 2.63 o 3 5 3 1423.35 1406.45 33.30 o 4 5 3 0.59 0.21 1.82 o 5 5 3 260.24 259.48 7.77 o 6 5 3 187.87 188.83 5.77 o 7 5 3 113.67 109.80 3.26 o 1 6 3 650.74 633.47 12.19 o 2 6 3 229.62 228.08 6.93 o 3 6 3 241.83 251.02 7.64 o 4 6 3 569.21 561.20 16.96 o 5 6 3 74.51 74.23 2.84 o 6 6 3 114.94 127.61 4.22 o 7 6 3 260.03 278.41 8.43 o 0 7 3 1310.39 1266.74 31.60 o 1 7 3 149.73 148.52 3.07 o 2 7 3 353.05 361.95 10.66 o 3 7 3 784.87 756.41 21.41 o 4 7 3 1.10 4.90 1.12 o 5 7 3 275.14 278.99 8.44 o 6 7 3 136.57 141.37 4.34 o 1 8 3 257.39 253.91 5.30 o 2 8 3 119.43 127.38 3.77 o 3 8 3 67.12 73.35 2.27 o 4 8 3 217.78 217.80 6.31 o 5 8 3 24.12 24.46 1.53 o 0 9 3 111.61 107.20 4.33 o 1 9 3 19.38 20.09 0.92 o 2 9 3 26.13 29.95 1.53 o 3 9 3 105.50 104.33 3.18 o 0 0 4 3074.47 3372.16 72.61 o 1 0 4 45.96 66.93 1.90 o 2 0 4 5626.40 5689.12 121.84 o 3 0 4 14156.76 14630.79 312.36 o 4 0 4 24.60 30.72 0.94 o 5 0 4 1903.74 1958.72 44.50 o 6 0 4 418.07 404.01 11.57 o 7 0 4 678.05 674.97 18.80 o 8 0 4 565.75 559.35 16.19 o 9 0 4 36.47 35.37 1.66 o 1 1 4 2835.65 2672.25 28.87 o 2 1 4 1197.65 1216.78 19.24 o 3 1 4 1595.48 1576.21 25.07 o 4 1 4 597.00 594.98 10.67 o 5 1 4 2.56 16.39 6.62 o 6 1 4 462.07 463.96 9.59 o 7 1 4 1632.18 1607.92 27.93 o 8 1 4 0.27 -1.55 3.38 o 9 1 4 963.95 961.13 19.54 o 0 2 4 128.49 149.31 4.18 o 1 2 4 104.01 126.17 2.69 o 2 2 4 499.66 454.65 11.45 o 3 2 4 4132.64 4154.11 89.82 o 4 2 4 80.50 78.73 2.34 o 5 2 4 404.29 421.26 12.29 o 6 2 4 167.92 177.08 5.48 o 7 2 4 317.26 317.14 9.43 o 8 2 4 285.51 286.97 8.30 o 1 3 4 4141.53 3905.41 60.07 o 2 3 4 1432.88 1409.74 32.20 o 3 3 4 1528.27 1517.20 34.61 o 4 3 4 983.60 980.32 23.89 o 5 3 4 6.90 7.50 0.99 o 6 3 4 500.59 503.06 13.96 o 7 3 4 1327.19 1254.07 32.53 o 8 3 4 1.51 -0.34 1.64 o 0 4 4 1252.43 1249.48 28.64 o 1 4 4 171.23 162.24 3.46 o 2 4 4 1315.50 1296.48 30.30 o 3 4 4 4098.42 4018.63 88.69 o 4 4 4 1.67 1.83 2.44 o 5 4 4 1051.53 1043.45 26.40 o 6 4 4 202.78 196.52 5.78 o 7 4 4 336.45 331.39 9.91 o 8 4 4 272.82 272.60 8.09 o 1 5 4 546.54 536.58 10.13 o 2 5 4 185.36 187.52 5.64 o 3 5 4 313.02 312.90 9.36 o 4 5 4 152.05 154.69 4.73 o 5 5 4 8.35 9.35 2.83 o 6 5 4 122.45 126.71 3.77 o 7 5 4 519.14 493.29 14.69 o 0 6 4 185.51 181.66 5.55 o 1 6 4 48.67 49.42 1.02 o 2 6 4 219.33 220.14 6.46 o 3 6 4 939.21 884.84 23.38 o 4 6 4 2.00 1.68 3.73 o 5 6 4 361.35 369.76 10.92 o 6 6 4 68.53 68.03 2.11 o 7 6 4 117.94 125.83 3.75 o 1 7 4 812.74 811.50 15.68 o 2 7 4 239.00 241.37 7.24 o 3 7 4 248.75 246.15 7.33 o 4 7 4 258.13 259.54 7.76 o 5 7 4 16.25 17.20 1.36 o 6 7 4 114.61 120.05 3.49 o 0 8 4 106.93 108.12 4.57 o 1 8 4 27.86 32.28 1.00 o 2 8 4 87.54 90.57 2.74 o 3 8 4 300.86 313.29 9.07 o 4 8 4 0.07 2.13 6.84 o 5 8 4 165.31 160.48 4.93 o 1 9 4 81.15 89.16 1.95 o 2 9 4 20.65 22.32 1.39 o 3 9 4 28.94 29.79 1.66 o 1 0 5 10920.90 11076.13 166.90 o 2 0 5 2376.05 2439.97 53.29 o 3 0 5 2993.35 3091.84 67.81 o 4 0 5 1203.42 1242.17 28.83 o 5 0 5 178.13 178.52 5.59 o 6 0 5 380.48 373.23 10.82 o 7 0 5 2486.20 2504.55 58.49 o 8 0 5 33.84 38.79 2.05 o 9 0 5 1139.74 1122.38 31.29 o 0 1 5 211.89 188.01 3.77 o 1 1 5 247.27 231.55 3.31 o 2 1 5 2984.30 3250.48 49.84 o 3 1 5 8188.62 8241.33 124.96 o 4 1 5 244.26 246.33 5.13 o 5 1 5 835.53 878.93 15.41 o 6 1 5 3.67 9.14 2.68 o 7 1 5 385.38 394.01 8.24 o 8 1 5 254.62 246.23 5.09 o 9 1 5 93.23 91.88 1.97 o 1 2 5 628.38 556.70 9.48 o 2 2 5 299.78 272.38 7.70 o 3 2 5 533.68 525.84 13.57 o 4 2 5 124.25 131.67 3.84 o 5 2 5 89.37 95.12 2.80 o 6 2 5 82.76 86.23 2.97 o 7 2 5 1452.26 1485.19 44.57 o 8 2 5 13.72 16.73 1.18 o 0 3 5 589.65 557.50 13.78 o 1 3 5 538.80 522.50 9.31 o 2 3 5 2159.14 2169.39 48.34 o 3 3 5 7121.43 7040.10 152.19 o 4 3 5 144.13 142.90 4.26 o 5 3 5 1313.53 1350.42 32.34 o 6 3 5 10.91 12.08 1.63 o 7 3 5 369.09 371.85 11.40 o 8 3 5 217.50 213.46 6.37 o 1 4 5 3666.83 3621.87 56.05 o 2 4 5 441.75 412.71 11.54 o 3 4 5 907.44 902.09 22.45 o 4 4 5 406.08 387.72 24.32 o 5 4 5 120.86 123.93 3.55 o 6 4 5 143.66 143.54 4.19 o 7 4 5 1218.75 1210.78 32.23 o 8 4 5 15.29 19.63 1.41 o 0 5 5 1.44 2.58 0.57 o 1 5 5 82.44 90.26 1.93 o 2 5 5 227.01 227.07 6.68 o 3 5 5 1598.88 1547.43 36.78 o 4 5 5 29.16 34.25 1.18 o 5 5 5 382.00 389.14 11.81 o 6 5 5 0.73 1.91 1.17 o 7 5 5 116.59 117.42 3.54 o 1 6 5 800.56 810.52 14.88 o 2 6 5 40.59 38.36 1.25 o 3 6 5 180.59 188.57 5.90 o 4 6 5 70.74 71.91 2.23 o 5 6 5 59.12 65.65 2.01 o 6 6 5 32.34 28.94 1.65 o 7 6 5 460.31 457.29 13.47 o 0 7 5 117.49 122.35 3.62 o 1 7 5 138.75 152.50 3.19 o 2 7 5 156.14 151.60 4.39 o 3 7 5 1116.74 1110.48 29.06 o 4 7 5 15.92 16.58 1.17 o 5 7 5 457.04 477.11 14.28 o 6 7 5 5.23 6.51 1.23 o 1 8 5 354.14 358.04 7.49 o 2 8 5 10.44 11.64 1.10 o 3 8 5 66.40 69.99 2.21 o 4 8 5 27.21 31.39 2.89 o 0 9 5 1.33 3.15 2.34 o 1 9 5 16.12 19.15 1.01 o 2 9 5 6.02 8.15 1.19 o 0 0 6 7.88 6.77 0.42 o 1 0 6 8142.61 8364.12 126.50 o 2 0 6 893.59 941.73 21.75 o 3 0 6 12770.35 12989.42 277.54 o 4 0 6 38.30 37.74 1.10 o 5 0 6 4209.60 4276.67 94.55 o 6 0 6 6.52 6.40 0.82 o 7 0 6 685.67 687.40 19.58 o 8 0 6 294.83 289.24 8.99 o 9 0 6 193.34 205.17 8.51 o 1 1 6 2558.33 2433.29 26.57 o 2 1 6 794.29 852.16 14.06 o 3 1 6 1206.93 1214.03 19.87 o 4 1 6 254.57 239.76 5.06 o 5 1 6 1654.31 1646.05 27.04 o 6 1 6 77.07 78.11 1.65 o 7 1 6 2018.92 2028.15 34.36 o 8 1 6 1.31 2.67 2.10 o 0 2 6 673.25 677.43 16.01 o 1 2 6 2351.87 2318.83 36.04 o 2 2 6 62.21 63.10 1.92 o 3 2 6 3503.77 3560.77 77.89 o 4 2 6 58.04 53.51 1.65 o 5 2 6 1224.61 1233.33 29.81 o 6 2 6 0.00 0.05 1.81 o 7 2 6 272.71 269.40 8.04 o 8 2 6 162.64 168.43 5.15 o 1 3 6 4820.34 4638.13 71.32 o 2 3 6 521.11 538.28 13.90 o 3 3 6 1268.37 1232.25 28.99 o 4 3 6 203.09 206.01 6.03 o 5 3 6 1102.67 1095.14 27.31 o 6 3 6 22.32 23.89 1.72 o 7 3 6 1676.16 1670.14 42.02 o 8 3 6 1.24 -0.24 3.12 o 0 4 6 2.09 1.80 2.36 o 1 4 6 1730.55 1688.08 27.40 o 2 4 6 140.59 141.54 4.16 o 3 4 6 4614.34 4638.59 101.71 o 4 4 6 11.38 12.23 0.76 o 5 4 6 1892.72 1872.95 44.17 o 6 4 6 2.61 2.27 0.86 o 7 4 6 302.64 303.27 8.80 o 8 4 6 91.33 95.27 2.80 o 1 5 6 751.85 742.75 13.57 o 2 5 6 49.06 52.69 4.61 o 3 5 6 197.07 195.62 5.86 o 4 5 6 7.65 9.05 0.80 o 5 5 6 400.52 397.94 11.64 o 6 5 6 22.54 24.88 1.24 o 7 5 6 659.10 693.05 19.67 o 0 6 6 18.89 19.27 0.89 o 1 6 6 361.74 372.24 7.85 o 2 6 6 6.55 8.91 4.61 o 3 6 6 1188.32 1188.81 30.07 o 4 6 6 6.70 8.43 0.93 o 5 6 6 579.96 584.91 16.93 o 6 6 6 0.21 0.40 0.80 o 1 7 6 1164.74 1170.49 21.27 o 2 7 6 29.76 30.93 3.30 o 3 7 6 209.49 210.15 14.20 o 4 7 6 14.06 15.61 1.98 o 5 7 6 154.33 159.20 8.74 o 0 8 6 1.30 -1.03 3.35 o 1 8 6 111.53 115.36 2.48 o 2 8 6 1.49 -0.08 2.46 o 3 8 6 420.21 429.38 13.03 o 4 8 6 1.56 -0.23 1.61 o 1 9 6 126.07 129.12 2.78 o 2 9 6 0.54 -1.45 5.15 o 1 0 7 27221.34 28146.15 424.22 o 2 0 7 427.13 457.98 11.66 o 3 0 7 3803.44 3897.37 84.97 o 4 0 7 107.93 113.88 3.49 o 5 0 7 40.29 41.98 1.31 o 6 0 7 323.57 338.23 13.77 o 7 0 7 2561.60 2509.03 58.57 o 8 0 7 1.60 5.29 1.38 o 0 1 7 5634.67 5722.48 87.08 o 1 1 7 287.38 297.60 4.06 o 2 1 7 0.57 1.61 1.75 o 3 1 7 7616.58 7802.33 118.35 o 4 1 7 255.46 250.88 5.31 o 5 1 7 3948.76 3999.50 62.52 o 6 1 7 61.39 60.27 1.36 o 7 1 7 459.24 456.63 9.64 o 8 1 7 25.07 26.75 0.93 o 1 2 7 5796.70 5777.45 88.01 o 2 2 7 131.48 143.29 4.28 o 3 2 7 905.86 926.04 22.27 o 4 2 7 194.70 198.74 7.76 o 5 2 7 11.38 15.38 0.85 o 6 2 7 316.16 309.98 9.17 o 7 2 7 1460.50 1449.72 36.76 o 8 2 7 2.88 4.43 1.02 o 0 3 7 2440.65 2406.30 53.61 o 1 3 7 669.55 655.19 11.55 o 2 3 7 0.09 3.06 2.41 o 3 3 7 6406.74 6478.94 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614.26 601.07 15.65 o 4 0 9 4299.90 4396.11 96.37 o 5 0 9 1442.18 1424.04 34.10 o 6 0 9 1494.03 1502.95 36.24 o 7 0 9 857.20 855.52 23.44 o 8 0 9 0.48 2.01 3.22 o 0 1 9 11977.41 11816.03 178.78 o 1 1 9 2423.23 2493.96 27.63 o 2 1 9 1238.29 1237.58 20.35 o 3 1 9 777.47 841.36 14.69 o 4 1 9 0.74 2.35 0.91 o 5 1 9 2385.44 2417.68 39.02 o 6 1 9 1051.03 1043.88 18.94 o 7 1 9 106.47 110.86 3.21 o 8 1 9 525.01 521.73 10.85 o 1 2 9 840.85 842.98 14.39 o 2 2 9 893.02 880.71 21.49 o 3 2 9 13.49 14.15 0.76 o 4 2 9 2526.04 2540.59 57.40 o 5 2 9 937.59 934.96 24.04 o 6 2 9 973.69 940.81 24.83 o 7 2 9 422.42 424.34 12.50 o 8 2 9 0.02 1.10 0.98 o 0 3 9 7259.99 6981.63 150.91 o 1 3 9 1728.97 1709.75 27.81 o 2 3 9 1091.18 1112.46 26.75 o 3 3 9 1305.09 1323.99 31.74 o 4 3 9 0.71 1.90 0.98 o 5 3 9 2164.04 2197.12 51.15 o 6 3 9 746.09 748.61 21.38 o 7 3 9 116.71 122.41 4.99 o 8 3 9 422.55 431.36 12.93 o 1 4 9 2507.38 2438.23 39.08 o 2 4 9 765.09 759.45 19.73 o 3 4 9 209.81 212.52 6.35 o 4 4 9 1752.44 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14 454.38 455.02 9.55 o 2 5 14 444.58 432.97 13.26 o 3 5 14 98.53 93.84 2.78 o 4 5 14 535.04 536.88 16.59 o 5 5 14 4.32 5.23 1.75 o 0 6 14 347.83 398.32 18.67 o 1 6 14 37.96 36.47 1.08 o 2 6 14 377.30 382.81 11.72 o 3 6 14 195.01 192.48 5.60 o 4 6 14 0.02 0.73 4.26 o 1 7 14 131.10 133.81 2.92 o 2 7 14 292.13 290.24 11.64 o 1 0 15 934.22 975.55 17.54 o 2 0 15 2449.45 2391.75 55.28 o 3 0 15 105.57 116.12 3.51 o 4 0 15 2988.00 2942.80 67.69 o 5 0 15 104.74 103.48 2.92 o 6 0 15 298.14 284.19 9.10 o 0 1 15 2515.87 2593.37 41.83 o 1 1 15 205.61 210.16 3.14 o 2 1 15 1935.09 1926.14 31.92 o 3 1 15 755.48 758.44 14.55 o 4 1 15 55.04 52.41 1.21 o 5 1 15 857.10 894.39 17.36 o 6 1 15 163.36 164.66 3.49 o 1 2 15 829.09 852.80 15.83 o 2 2 15 1012.17 1017.10 26.32 o 3 2 15 106.84 114.33 3.50 o 4 2 15 1299.59 1287.44 32.69 o 5 2 15 85.32 81.06 4.07 o 6 2 15 89.89 87.33 2.62 o 0 3 15 2436.07 2399.77 55.75 o 1 3 15 149.54 146.16 3.09 o 2 3 15 1654.46 1634.28 39.68 o 3 3 15 554.86 549.53 15.68 o 4 3 15 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22.00 o 4 2 16 1.12 -0.17 3.36 o 5 2 16 1402.15 1387.89 35.97 o 6 2 16 119.39 115.47 3.50 o 1 3 16 1240.87 1267.99 22.64 o 2 3 16 635.68 637.73 17.69 o 3 3 16 126.50 131.70 4.02 o 4 3 16 406.74 408.59 12.42 o 5 3 16 143.86 143.86 4.38 o 0 4 16 139.39 128.73 3.79 o 1 4 16 198.71 198.08 4.10 o 2 4 16 500.99 481.50 14.69 o 3 4 16 561.85 567.56 16.87 o 4 4 16 1.16 1.55 2.06 o 5 4 16 877.95 889.18 26.46 o 1 5 16 546.29 560.09 11.71 o 2 5 16 133.11 132.49 3.92 o 3 5 16 66.97 67.89 2.18 o 4 5 16 90.00 83.98 2.93 o 0 6 16 23.46 23.38 1.42 o 1 6 16 76.18 80.28 1.77 o 2 6 16 110.40 120.89 3.58 o 3 6 16 239.76 246.67 7.32 o 1 0 17 3882.10 3910.65 62.30 o 2 0 17 184.25 182.39 5.46 o 3 0 17 354.49 348.20 10.31 o 4 0 17 199.74 194.77 5.86 o 5 0 17 299.54 292.81 8.50 o 6 0 17 29.73 29.35 1.60 o 0 1 17 0.18 0.92 0.66 o 1 1 17 630.75 641.91 9.24 o 2 1 17 48.17 46.65 1.12 o 3 1 17 1377.92 1365.46 24.42 o 4 1 17 8.53 8.08 0.86 o 5 1 17 1838.67 1816.87 31.92 o 6 1 17 5.81 2.88 2.72 o 1 2 17 2558.06 2549.39 42.02 o 2 2 17 13.77 11.14 1.12 o 3 2 17 216.86 213.73 6.35 o 4 2 17 14.03 16.46 1.64 o 5 2 17 226.54 227.20 6.80 o 0 3 17 39.70 43.35 1.54 o 1 3 17 442.51 443.87 9.32 o 2 3 17 91.18 89.15 2.72 o 3 3 17 1128.67 1108.43 29.80 o 4 3 17 8.66 8.90 1.19 o 5 3 17 1347.75 1341.68 35.93 o 1 4 17 1744.91 1706.03 30.14 o 2 4 17 65.90 60.15 1.93 o 3 4 17 158.79 144.38 5.56 o 4 4 17 84.04 85.02 3.24 o 0 5 17 2.45 10.41 5.62 o 1 5 17 175.49 179.00 4.14 o 2 5 17 3.63 -1.17 4.27 o 3 5 17 520.53 504.15 15.20 o 1 6 17 639.24 647.15 13.85 o 2 6 17 8.82 9.00 1.39 o 0 0 18 42.76 39.71 1.51 o 1 0 18 531.66 534.97 11.07 o 2 0 18 16.41 20.24 1.64 o 3 0 18 1098.15 1079.06 28.64 o 4 0 18 1.15 -4.57 4.57 o 5 0 18 2096.77 2075.04 51.10 o 1 1 18 2133.15 2132.60 25.32 o 2 1 18 4.83 5.03 2.96 o 3 1 18 163.16 164.46 3.48 o 4 1 18 2.21 2.21 2.30 o 5 1 18 253.03 265.95 5.54 o 0 2 18 31.86 36.44 2.78 o 1 2 18 339.22 337.10 7.00 o 2 2 18 127.59 133.17 3.95 o 3 2 18 649.69 648.05 18.22 o 4 2 18 0.59 -0.20 1.01 o 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1.30 o 1 0 20 184.02 185.62 3.89 o 2 0 20 111.49 107.05 3.06 o 3 0 20 500.15 508.49 15.23 o 4 0 20 58.80 63.52 2.23 o 1 1 20 665.53 652.57 9.40 o 2 1 20 296.87 308.76 6.69 o 3 1 20 30.56 27.69 1.11 o 4 1 20 241.43 236.81 4.98 o 0 2 20 102.81 94.50 3.53 o 1 2 20 91.75 95.24 2.01 o 2 2 20 188.99 179.55 5.31 o 3 2 20 233.54 229.81 9.52 o 1 3 20 645.54 640.62 13.37 o 2 3 20 183.08 182.84 5.67 o 3 3 20 39.77 37.34 1.81 o 0 4 20 33.82 28.70 2.65 o 1 4 20 89.43 94.92 2.19 o 1 0 21 573.71 567.47 12.06 o 2 0 21 257.89 256.75 9.17 o 3 0 21 29.16 28.40 1.65 o 0 1 21 162.76 169.76 3.61 o 1 1 21 99.06 103.04 1.53 o 2 1 21 592.58 584.85 12.43 o 3 1 21 260.39 260.74 5.31 o 1 2 21 218.16 222.53 4.70 o 2 2 21 264.24 258.19 8.14 o 0 3 21 120.90 122.97 3.53 o 1 3 21 90.89 92.36 2.03 o 0 0 22 343.77 349.42 10.91 o 1 0 22 3.24 -2.97 2.97 o 1 1 22 435.91 441.11 6.53 o 0 2 22 344.04 355.44 10.85 o