#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180894 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/34/2103441.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103441_Fobs loop_ _publ_author_name 'Zakaria, Choudhury M.' 'Ferguson, George' 'Lough, Alan J.' 'Glidewell, Christopher' _publ_section_title ; Ferrocene-1,1'-dicarboxylic acid as a building block in supramolecular chemistry: supramolecular structures in one, two and three dimensions ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 786 _journal_page_last 802 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 97.513 _cell_angle_beta 99.090 _cell_angle_gamma 91.108 _cell_length_a 9.7360 _cell_length_b 13.6610 _cell_length_c 22.8547 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.8380 _cod_data_source_file na0136VIIIsup9.hkl _cod_data_source_block VIII #BEGIN Tags that were not found in dictionaries: _shelx_title ' k0178 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 213.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 2907.33 3067.50 274.63 o 4 0 0 5184.46 5213.29 133.23 o 5 0 0 2118.52 2054.41 53.12 o 6 0 0 2189.41 2170.04 68.18 o 7 0 0 882.68 942.81 26.31 o 8 0 0 477.49 494.22 12.75 o 10 0 0 137.23 183.82 33.71 o 11 0 0 477.66 420.95 52.49 o -11 1 0 0.05 0.07 35.19 o -10 1 0 0.27 18.49 33.69 o -8 1 0 741.44 714.49 48.06 o -7 1 0 87.60 115.35 5.99 o -6 1 0 548.60 554.40 14.27 o -5 1 0 6642.69 6939.03 227.74 o -4 1 0 594.62 550.47 19.56 o -3 1 0 3416.29 3163.13 101.51 o -2 1 0 495.74 723.22 72.41 o 2 1 0 527.04 619.82 40.74 o 3 1 0 2794.66 2744.70 57.74 o 4 1 0 229.94 242.34 9.75 o 5 1 0 397.29 373.94 12.01 o 6 1 0 513.36 542.87 18.02 o 7 1 0 1076.42 1002.68 30.85 o 8 1 0 3200.04 3339.83 83.43 o 9 1 0 815.24 760.79 29.29 o 10 1 0 1921.92 1991.28 116.05 o 11 1 0 18.74 24.93 28.45 o -11 2 0 41.44 55.04 41.18 o -10 2 0 2.65 6.29 26.20 o -9 2 0 237.47 257.78 29.22 o -8 2 0 16.80 23.14 22.46 o -7 2 0 2457.08 2603.34 62.09 o -6 2 0 325.48 411.90 9.75 o -5 2 0 5637.73 5942.46 161.14 o -4 2 0 36.89 43.51 5.99 o -3 2 0 14479.37 14889.10 631.67 o -2 2 0 105.16 205.43 12.75 o -1 2 0 12973.34 15994.54 900.79 o 0 2 0 662.96 651.06 5.32 o 1 2 0 9207.48 11299.04 501.63 o 2 2 0 2702.40 3274.88 172.60 o 3 2 0 1357.34 1482.83 44.74 o 4 2 0 2446.98 2233.94 67.84 o 5 2 0 1707.02 1851.09 44.63 o 6 2 0 2959.18 3119.34 103.39 o 7 2 0 10.67 12.28 8.24 o 8 2 0 164.91 150.44 9.74 o 9 2 0 11.84 29.65 8.98 o 10 2 0 253.06 233.27 14.99 o 11 2 0 47.83 58.18 27.71 o -11 3 0 275.68 284.15 36.72 o -9 3 0 365.15 360.01 28.49 o -8 3 0 832.55 750.02 53.34 o -7 3 0 167.69 178.10 7.49 o -6 3 0 4694.62 5011.81 133.40 o -5 3 0 2306.61 2399.54 77.42 o -4 3 0 18007.01 18396.77 898.15 o -3 3 0 611.08 570.12 13.55 o -2 3 0 4079.22 3936.70 89.92 o -1 3 0 1938.84 1803.07 46.87 o 0 3 0 2469.23 2011.61 41.11 o 1 3 0 8862.39 7645.78 418.61 o 2 3 0 1.47 10.71 5.99 o 3 3 0 1566.23 1330.02 30.34 o 4 3 0 1450.67 1450.22 52.18 o 5 3 0 9334.27 9571.04 227.90 o 6 3 0 332.57 369.35 12.00 o 7 3 0 2020.08 2044.54 47.59 o 8 3 0 269.65 261.95 14.99 o 9 3 0 152.94 127.05 13.48 o 10 3 0 677.43 636.17 25.51 o 11 3 0 20.33 65.66 15.72 o -11 4 0 256.88 280.76 41.21 o -10 4 0 40.38 47.02 35.94 o -9 4 0 307.83 322.90 42.72 o -8 4 0 20.32 30.92 5.24 o -7 4 0 374.23 344.60 13.50 o -6 4 0 32.64 45.75 6.74 o -5 4 0 37.74 57.96 7.49 o -4 4 0 2845.49 3149.92 127.39 o -3 4 0 522.52 422.88 11.28 o -2 4 0 1797.34 1855.41 49.48 o -1 4 0 5986.91 4916.97 165.41 o 0 4 0 3491.13 3516.22 148.49 o 1 4 0 48.85 121.05 7.49 o 2 4 0 3767.61 3132.98 98.26 o 3 4 0 48.94 65.09 5.24 o 4 4 0 3768.63 3677.77 104.26 o 5 4 0 0.46 0.07 7.49 o 6 4 0 35.76 48.52 8.99 o 7 4 0 45.77 51.90 8.99 o 8 4 0 344.44 363.38 14.24 o 10 4 0 323.19 274.84 27.73 o -11 5 0 285.90 326.34 35.97 o -10 5 0 170.48 190.28 40.45 o -8 5 0 203.59 170.61 8.99 o -7 5 0 2284.98 2347.99 57.45 o -6 5 0 601.97 552.40 18.77 o -5 5 0 43.21 195.83 7.49 o -4 5 0 435.14 434.13 14.26 o -3 5 0 70.48 152.44 5.99 o -2 5 0 64.98 109.07 6.74 o -1 5 0 17871.76 17734.34 634.80 o 0 5 0 1181.60 856.71 34.80 o 1 5 0 25.97 82.75 8.99 o 2 5 0 2517.54 2134.51 54.18 o 3 5 0 58.00 110.78 11.98 o 4 5 0 345.57 391.99 18.01 o 5 5 0 1615.73 1734.68 55.87 o 6 5 0 311.14 277.27 14.25 o 7 5 0 524.03 499.12 24.01 o 8 5 0 233.37 221.51 13.49 o 9 5 0 5.76 1.12 20.96 o 10 5 0 150.12 105.99 20.22 o -10 6 0 158.92 129.74 28.47 o -9 6 0 3.00 4.49 7.49 o -8 6 0 38.66 45.90 8.99 o -7 6 0 469.85 474.99 18.00 o -6 6 0 326.20 315.82 12.75 o -5 6 0 2481.94 2462.66 62.92 o -4 6 0 2920.48 2910.00 87.51 o -3 6 0 14472.84 14370.32 304.50 o -2 6 0 223.96 236.51 11.25 o -1 6 0 176.73 289.45 10.50 o 0 6 0 1271.14 1381.87 49.13 o 1 6 0 4887.98 4205.03 128.62 o 2 6 0 4051.38 3830.37 127.63 o 3 6 0 4162.90 4508.34 109.74 o 4 6 0 1498.77 1468.57 30.95 o 5 6 0 0.24 4.72 10.48 o 6 6 0 836.62 858.97 24.80 o 7 6 0 781.05 736.91 28.54 o 8 6 0 316.24 320.59 35.23 o 9 6 0 709.81 666.73 30.77 o 10 6 0 421.96 401.16 23.24 o -10 7 0 55.15 66.35 24.71 o -9 7 0 723.40 718.55 39.03 o -8 7 0 26.35 35.04 10.48 o -7 7 0 476.26 561.61 32.25 o -6 7 0 1445.91 1477.34 46.71 o -5 7 0 228.69 263.68 14.99 o -4 7 0 246.80 300.46 14.99 o -3 7 0 3570.92 3643.60 106.16 o -2 7 0 88.94 131.69 9.74 o -1 7 0 46.80 178.99 11.98 o 0 7 0 867.50 912.28 24.09 o 1 7 0 264.50 332.45 15.75 o 2 7 0 9826.71 9563.15 263.48 o 3 7 0 416.86 600.55 35.27 o 4 7 0 4087.56 3853.45 100.07 o 5 7 0 475.09 520.35 25.51 o 6 7 0 723.95 808.25 50.31 o 7 7 0 15.81 25.16 10.48 o 8 7 0 143.63 148.09 20.97 o 9 7 0 248.76 275.30 18.73 o 10 7 0 144.50 148.83 20.97 o -10 8 0 2.83 15.27 14.97 o -9 8 0 20.56 27.93 11.98 o -8 8 0 9.36 23.88 15.72 o -7 8 0 24.38 82.21 12.73 o -6 8 0 167.05 157.63 11.99 o -5 8 0 1585.20 1678.29 47.50 o -4 8 0 415.65 477.20 14.25 o -3 8 0 183.49 493.93 19.48 o -2 8 0 2118.91 2041.46 42.41 o -1 8 0 125.58 289.58 18.73 o 0 8 0 157.47 248.94 13.49 o 1 8 0 0.40 82.88 12.73 o 2 8 0 7.30 173.85 14.97 o 3 8 0 70.47 91.00 13.48 o 4 8 0 483.07 516.18 25.51 o 5 8 0 149.54 146.09 15.73 o 6 8 0 50.66 161.83 20.97 o 7 8 0 145.04 103.23 19.48 o 8 8 0 286.24 265.90 49.46 o 9 8 0 98.93 56.69 16.48 o -9 9 0 418.37 447.72 19.49 o -8 9 0 997.63 1087.33 44.32 o -7 9 0 568.30 573.26 24.01 o -6 9 0 47.83 65.37 11.98 o -5 9 0 383.34 382.82 18.00 o -4 9 0 145.99 201.91 13.49 o -3 9 0 5.03 31.97 9.73 o -2 9 0 162.57 241.95 15.74 o -1 9 0 2129.32 1969.17 53.73 o 0 9 0 224.18 229.89 16.49 o 1 9 0 593.25 546.82 22.53 o 2 9 0 1667.31 1798.74 61.13 o 3 9 0 724.52 835.08 36.06 o 4 9 0 773.77 823.15 30.80 o 5 9 0 317.84 335.40 22.49 o 6 9 0 1121.22 1108.81 66.16 o 8 9 0 164.56 186.08 21.72 o 9 9 0 193.90 208.94 25.47 o -9 10 0 56.23 63.43 15.73 o -8 10 0 7.02 54.21 25.46 o -7 10 0 0.51 13.33 22.46 o -6 10 0 10.88 39.23 15.72 o -5 10 0 462.40 514.46 20.25 o -4 10 0 478.81 409.75 22.51 o -3 10 0 440.56 411.15 18.75 o -2 10 0 2209.07 2345.68 56.71 o -1 10 0 1275.25 1227.82 45.94 o 0 10 0 701.78 853.72 27.79 o 1 10 0 759.15 793.13 34.56 o 2 10 0 710.32 638.91 30.04 o 3 10 0 302.36 429.10 23.99 o 4 10 0 591.00 565.78 43.53 o 5 10 0 0.74 6.59 16.47 o 6 10 0 250.34 264.15 29.23 o 7 10 0 238.35 251.24 38.21 o 8 10 0 24.84 52.26 24.71 o -8 11 0 3.29 17.44 17.22 o -7 11 0 7.12 50.69 15.72 o -6 11 0 110.68 109.28 15.73 o -5 11 0 92.99 80.44 18.72 o -4 11 0 179.67 249.94 19.48 o -3 11 0 0.10 2.62 14.97 o -2 11 0 385.23 494.55 23.25 o -1 11 0 25.38 48.82 14.23 o 0 11 0 215.07 422.87 24.73 o 1 11 0 10.75 37.14 14.97 o 2 11 0 544.95 872.07 48.77 o 3 11 0 2169.74 2278.15 85.32 o 4 11 0 110.55 192.35 29.96 o 7 11 0 0.50 27.70 23.21 o 8 11 0 17.59 77.94 36.69 o -8 12 0 0.36 1.42 22.46 o -7 12 0 1086.62 1053.39 44.33 o -6 12 0 319.62 334.13 28.48 o -5 12 0 460.53 516.98 43.49 o -4 12 0 147.62 223.38 20.97 o -3 12 0 1013.07 1163.77 62.38 o -2 12 0 785.48 691.41 33.79 o -1 12 0 732.28 887.79 36.04 o 0 12 0 1.51 5.54 16.47 o 1 12 0 7.00 0.15 15.72 o 2 12 0 22.18 14.23 23.96 o 3 12 0 104.93 64.86 25.47 o 4 12 0 870.65 818.67 57.83 o 6 12 0 126.69 122.39 37.45 o 7 12 0 39.18 51.74 27.71 o -7 13 0 0.39 24.48 20.96 o -6 13 0 349.91 334.22 28.48 o -5 13 0 35.78 17.00 27.71 o -4 13 0 8.68 19.92 31.45 o -3 13 0 0.06 35.71 16.47 o -2 13 0 58.91 119.89 26.96 o -1 13 0 371.92 549.24 22.49 o 0 13 0 9.07 9.81 23.96 o 1 13 0 355.88 332.32 26.99 o 2 13 0 18.95 120.92 28.45 o 3 13 0 764.35 844.73 60.05 o 4 13 0 7.22 77.57 32.19 o 5 13 0 410.30 380.77 46.48 o 6 13 0 16.03 17.89 37.44 o -6 14 0 15.77 106.02 40.43 o -5 14 0 30.56 33.69 23.21 o -3 14 0 12.40 49.72 25.46 o -2 14 0 26.73 138.37 28.45 o 0 14 0 2.28 5.24 33.69 o 1 14 0 13.50 19.39 28.45 o 2 14 0 19.78 1.12 27.70 o 3 14 0 149.00 170.56 24.72 o 4 14 0 10.05 79.29 32.20 o 5 14 0 311.74 440.36 56.21 o -4 15 0 147.02 158.87 38.95 o -3 15 0 2.03 1.20 29.20 o -2 15 0 437.26 460.19 36.74 o 3 15 0 17.56 64.54 41.93 o -2 16 0 2.77 19.09 24.71 o -1 16 0 109.68 72.12 42.69 o 0 16 0 0.79 25.08 37.44 o 1 16 0 150.56 172.13 32.21 o -1 -16 1 52.85 55.19 44.93 o 2 -16 1 0.06 1.05 39.68 o -4 -15 1 171.85 196.11 32.21 o -3 -15 1 94.76 148.36 41.19 o -2 -15 1 224.85 234.96 32.97 o -1 -15 1 68.32 36.77 32.20 o 2 -15 1 65.88 168.19 32.20 o 3 -15 1 0.09 24.48 22.46 o 4 -15 1 26.07 79.52 35.19 o -5 -14 1 642.18 618.00 42.76 o -3 -14 1 409.14 417.89 42.73 o -2 -14 1 0.14 33.69 29.20 o 1 -14 1 367.95 436.97 26.99 o 3 -14 1 3.27 0.37 27.70 o 4 -14 1 760.06 798.89 69.05 o 5 -14 1 162.02 246.00 49.44 o 6 -14 1 516.85 461.25 30.00 o -6 -13 1 9.96 49.94 26.95 o -3 -13 1 89.20 206.41 34.45 o -2 -13 1 598.30 478.91 37.51 o -1 -13 1 352.87 448.07 40.48 o 0 -13 1 105.31 97.29 24.72 o 1 -13 1 845.06 994.86 44.31 o 2 -13 1 52.62 64.70 28.46 o 3 -13 1 281.77 300.08 31.48 o 4 -13 1 9.00 0.90 18.72 o 5 -13 1 96.28 119.90 35.95 o 6 -13 1 65.07 77.13 32.95 o 7 -13 1 65.56 146.47 20.97 o -7 -12 1 0.25 45.60 25.46 o -6 -12 1 47.82 170.06 37.44 o -4 -12 1 93.08 273.29 37.45 o -3 -12 1 6.39 43.13 15.72 o -2 -12 1 7.02 62.59 17.22 o -1 -12 1 11.97 11.76 23.21 o 0 -12 1 274.54 251.31 20.99 o 1 -12 1 2987.96 3108.53 84.07 o 2 -12 1 0.17 51.36 13.48 o 3 -12 1 526.12 631.43 31.51 o 4 -12 1 609.26 586.25 25.51 o 5 -12 1 63.13 91.44 19.47 o 6 -12 1 82.95 118.10 29.96 o 7 -12 1 463.63 533.71 33.74 o 8 -12 1 45.17 1.27 19.47 o -8 -11 1 180.75 170.12 28.47 o -7 -11 1 0.08 2.25 22.46 o -5 -11 1 69.27 46.58 27.71 o -4 -11 1 1530.49 1690.53 85.84 o -3 -11 1 54.43 194.85 23.96 o -2 -11 1 2510.18 3013.61 103.62 o -1 -11 1 4.82 23.51 15.72 o 0 -11 1 1071.78 1312.57 44.37 o 1 -11 1 92.30 218.41 20.97 o 2 -11 1 465.04 393.83 23.25 o 3 -11 1 72.99 105.82 11.98 o 4 -11 1 92.24 54.52 11.98 o 5 -11 1 38.74 37.59 15.72 o 6 -11 1 134.47 110.41 14.23 o 7 -11 1 174.31 154.70 23.97 o 8 -11 1 1.07 0.67 26.20 o -8 -10 1 3.00 5.84 20.96 o -5 -10 1 497.97 542.64 31.50 o -4 -10 1 225.87 271.43 21.73 o -3 -10 1 1157.26 1150.62 47.40 o -2 -10 1 365.07 346.09 21.00 o -1 -10 1 2.97 29.12 13.48 o 0 -10 1 87.76 194.22 20.22 o 1 -10 1 102.35 154.15 17.23 o 2 -10 1 23.48 177.16 17.97 o 3 -10 1 99.48 89.06 15.73 o 4 -10 1 33.44 61.55 13.48 o 5 -10 1 42.67 75.78 15.73 o 6 -10 1 671.94 631.59 31.52 o 7 -10 1 138.18 171.23 15.73 o 8 -10 1 1062.06 1002.08 52.59 o 9 -10 1 2.53 14.23 15.72 o -9 -9 1 99.86 88.67 24.71 o -8 -9 1 205.40 182.21 22.48 o -6 -9 1 8.29 71.13 16.47 o -5 -9 1 269.88 309.55 21.74 o -4 -9 1 106.64 139.62 16.48 o -3 -9 1 2429.73 2614.48 89.33 o -2 -9 1 1118.82 1251.39 43.66 o -1 -9 1 26.59 227.49 19.47 o 0 -9 1 352.09 334.37 13.50 o 1 -9 1 111.20 229.38 16.48 o 2 -9 1 621.11 664.63 26.28 o 3 -9 1 933.18 955.55 24.06 o 4 -9 1 3.24 18.19 11.98 o 5 -9 1 846.06 929.54 37.57 o 6 -9 1 1067.71 1036.65 53.38 o 7 -9 1 150.61 175.22 14.23 o 8 -9 1 370.08 357.43 25.49 o 9 -9 1 39.31 44.70 14.98 o -9 -8 1 50.37 32.50 20.22 o -8 -8 1 2357.69 2473.91 75.47 o -7 -8 1 3.03 38.11 20.96 o -6 -8 1 3738.74 3878.53 104.85 o -5 -8 1 143.89 141.97 15.73 o -4 -8 1 21.44 63.12 13.48 o -3 -8 1 2664.40 2658.29 84.97 o -2 -8 1 231.50 239.43 14.99 o -1 -8 1 1748.55 1743.86 44.61 o 0 -8 1 741.35 730.60 24.81 o 1 -8 1 5347.52 5063.23 111.04 o 2 -8 1 628.11 777.56 26.29 o 3 -8 1 5971.76 5889.00 138.08 o 4 -8 1 784.68 711.60 24.05 o 5 -8 1 1475.63 1534.96 45.21 o 6 -8 1 140.63 133.42 14.98 o 7 -8 1 1813.22 1785.17 54.27 o 8 -8 1 287.94 258.26 17.99 o 9 -8 1 9.56 18.04 12.73 o 10 -8 1 72.23 62.23 19.47 o -10 -7 1 12.00 0.07 14.97 o -9 -7 1 77.20 86.87 17.97 o -8 -7 1 74.31 22.09 23.96 o -7 -7 1 101.02 74.45 20.22 o -6 -7 1 194.20 171.07 16.48 o -5 -7 1 618.63 622.96 17.27 o -4 -7 1 203.68 543.14 29.23 o -3 -7 1 2023.49 1731.39 54.51 o -2 -7 1 747.07 841.85 32.34 o -1 -7 1 904.69 895.92 33.13 o 0 -7 1 567.86 649.79 23.30 o 1 -7 1 6006.11 5617.42 149.20 o 2 -7 1 381.52 408.77 17.26 o 3 -7 1 3733.92 3926.28 113.13 o 4 -7 1 711.66 788.43 20.29 o 5 -7 1 258.61 303.37 14.24 o 6 -7 1 53.04 97.80 9.74 o 7 -7 1 253.78 304.43 17.24 o 8 -7 1 296.08 310.37 14.24 o 9 -7 1 26.79 57.06 11.23 o 10 -7 1 772.10 757.49 25.52 o -10 -6 1 101.16 115.11 16.48 o -9 -6 1 817.29 813.01 59.31 o -8 -6 1 94.48 60.07 13.48 o -7 -6 1 19.67 50.99 11.98 o -6 -6 1 322.57 334.47 13.50 o -5 -6 1 377.54 507.74 25.50 o -4 -6 1 756.50 759.78 26.31 o -3 -6 1 4410.77 3870.73 121.46 o -2 -6 1 3206.77 3096.98 99.43 o -1 -6 1 695.63 652.20 27.84 o 0 -6 1 3578.91 3092.53 100.71 o 1 -6 1 900.79 746.91 20.35 o 2 -6 1 414.16 273.61 8.26 o 3 -6 1 1136.48 1382.30 30.16 o 4 -6 1 6599.09 6732.16 144.34 o 5 -6 1 243.13 301.57 10.49 o 6 -6 1 176.13 163.95 11.99 o 7 -6 1 96.08 168.07 11.98 o 8 -6 1 0.37 13.33 8.98 o 9 -6 1 10.64 18.34 8.98 o 10 -6 1 338.44 352.87 29.98 o -10 -5 1 181.87 194.78 19.48 o -9 -5 1 215.02 205.45 14.99 o -8 -5 1 722.91 721.92 30.78 o -7 -5 1 1020.12 993.02 36.84 o -6 -5 1 440.01 483.15 20.26 o -5 -5 1 6744.76 6872.91 167.36 o -4 -5 1 874.45 712.20 20.32 o -3 -5 1 6921.62 6499.48 200.58 o -2 -5 1 2905.15 2726.83 84.21 o -1 -5 1 8320.01 7943.79 261.11 o 0 -5 1 416.59 333.38 14.28 o 1 -5 1 1626.73 1677.03 50.11 o 2 -5 1 414.82 626.40 27.04 o 3 -5 1 1602.04 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