#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103456.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103456_Fobs loop_ _publ_author_name 'Norberg, Stefan T.' _publ_section_title ; New phosphate langbeinites, K~2~MTi(PO~4~)~3~ (M = Er, Yb or Y), and an alternative description of the langbeinite framework ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 743 _journal_page_last 749 _journal_volume 58 _journal_year 2002 _space_group_IT_number 198 _symmetry_space_group_name_Hall 'P 2ac 2ab 3' _symmetry_space_group_name_H-M 'P 21 3' _[local]_cod_data_source_file os0095KErTPsup2.hkl _[local]_cod_data_source_block KErTP loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma 0 0 2 1266.57 1084.47 27.73 0 0 4 6792.41 7452.51 85.14 0 0 6 6139.99 6417.21 87.74 0 0 8 939.02 1003.53 26.23 0 0 10 1145.69 1083.05 32.67 0 0 12 3733.66 3445.13 60.31 0 0 14 4327.06 4012.42 72.03 0 1 2 899.49 901.41 24.05 0 1 3 56103.82 53103.90 1383.2 0 1 4 927.56 1178.85 20.44 0 1 5 12935.00 12662.54 122.24 0 1 6 12594.79 12574.59 125.30 0 1 7 4326.49 4442.17 57.43 0 1 8 4801.62 5067.57 64.22 0 1 9 10576.82 10573.60 130.26 0 1 10 820.65 854.27 27.26 0 1 11 90.44 94.81 33.48 0 1 12 4315.76 4136.73 60.22 0 1 13 559.26 551.53 30.68 0 1 14 84.37 108.99 36.54 0 2 1 24014.79 22907.46 934.62 0 2 2 1214.25 1354.82 24.51 0 2 3 10503.96 10262.99 100.52 0 2 4 1800.73 1951.44 134.29 0 2 5 7171.94 7291.75 82.86 0 2 6 13425.11 13623.26 484.16 0 2 7 116.12 93.48 21.86 0 2 8 366.98 377.88 19.17 0 2 9 553.70 552.18 23.75 0 2 10 1047.23 948.93 28.71 0 2 11 58.37 75.52 29.91 0 2 12 1865.16 1765.22 39.86 0 2 13 9338.81 9216.48 125.27 0 2 14 219.88 211.31 26.59 0 3 1 47413.90 46475.30 1830.1 0 3 2 1263.90 1102.04 23.79 0 3 3 1213.92 1127.27 22.38 0 3 4 20557.40 20522.23 616.11 0 3 5 7854.33 7772.56 434.35 0 3 6 1958.36 2005.55 28.83 0 3 7 23.24 9.21 26.88 0 3 8 7866.88 8061.29 98.99 0 3 9 5213.74 4998.77 70.30 0 3 10 7577.65 7435.03 101.49 0 3 11 1114.97 1131.14 31.64 0 3 12 709.68 687.90 30.61 0 3 13 534.01 517.08 30.22 0 4 1 292.75 214.77 16.61 0 4 2 636.21 425.82 68.65 0 4 3 808.82 853.26 72.30 0 4 4 6428.61 6449.12 78.83 0 4 5 744.31 755.87 20.04 0 4 6 2247.99 2232.95 32.01 0 4 7 18491.17 18683.83 179.88 0 4 8 200.11 167.29 24.61 0 4 9 658.29 626.50 25.24 0 4 10 1439.54 1511.92 33.14 0 4 11 4944.51 5152.68 67.00 0 4 12 4413.46 4620.95 61.66 0 4 13 40.50 96.00 35.07 0 5 1 3723.13 3833.64 49.90 0 5 2 29410.65 28409.72 1026.7 0 5 3 17888.27 18305.38 630.47 0 5 4 1113.66 1256.70 22.84 0 5 5 4368.54 4605.62 57.88 0 5 6 51.18 19.76 25.54 0 5 7 417.39 408.01 20.51 0 5 8 1831.76 1746.50 33.70 0 5 9 9966.74 10052.43 127.15 0 5 10 487.29 512.23 24.96 0 5 11 222.27 184.63 29.73 0 5 12 1359.63 1249.71 37.77 0 5 13 54.99 74.63 41.78 0 6 1 7633.62 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17686.46 17351.42 182.35 0 9 3 69.37 5.06 26.17 0 9 4 60.91 60.41 27.10 0 9 5 4982.92 5073.98 66.10 0 9 6 2180.22 2213.62 40.03 0 9 7 54.41 38.85 30.77 0 9 8 1029.39 1219.48 33.31 0 9 9 417.09 449.59 26.84 0 9 10 573.56 590.98 30.85 0 10 1 4223.41 4131.68 56.92 0 10 2 293.19 245.55 22.44 0 10 3 116.06 57.64 24.56 0 10 4 2875.90 3059.18 44.61 0 10 5 2370.20 2175.95 42.06 0 10 6 5457.38 5396.14 73.43 0 10 7 699.02 747.27 30.03 0 10 8 1344.36 1384.95 37.06 0 10 9 45.30 5.65 37.73 0 10 10 3496.12 3449.68 57.69 0 11 1 4681.48 4734.87 62.47 0 11 2 343.51 341.85 24.40 0 11 3 4606.74 4674.92 61.61 0 11 4 3032.01 3023.80 48.17 0 11 5 413.64 451.50 27.19 0 11 6 178.00 162.10 30.81 0 11 7 51.41 5.26 33.29 0 11 8 2127.23 2118.04 45.95 0 12 1 237.37 230.00 30.37 0 12 2 3306.57 3030.95 51.04 0 12 3 3789.32 3727.09 56.26 0 12 4 1755.28 1860.30 40.03 0 12 5 -42.02 2.20 40.96 0 12 6 1689.79 1564.72 40.86 0 12 7 2284.93 2020.98 46.76 0 13 1 -37.34 33.68 40.93 0 13 2 1994.92 1967.56 43.72 0 13 3 315.19 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6 9 662.98 623.16 33.67 -2 -6 -9 513.93 542.99 32.46 2 6 10 -8.99 17.35 51.16 -2 -6 -10 -47.82 10.63 45.80 2 6 11 2857.57 2894.78 63.26 -2 -6 -11 3003.16 3018.39 65.06 2 6 12 1482.46 1451.81 50.05 -2 -6 -12 1446.93 1551.21 51.49 2 7 3 383.72 252.24 24.12 -2 -7 -3 281.66 285.35 22.76 2 7 4 1591.24 1500.52 36.61 -2 -7 -4 1362.89 1346.78 35.10 2 7 5 7197.61 7917.17 120.40 -2 -7 -5 8223.13 8138.54 137.01 2 7 6 10284.06 10585.72 168.85 -2 -7 -6 9135.04 9538.64 151.07 2 7 7 3099.28 3125.86 57.51 -2 -7 -7 2719.17 2909.89 54.54 2 7 8 1225.73 1212.76 40.07 -2 -7 -8 1131.68 1110.95 40.07 2 7 9 3159.16 3321.11 62.81 -2 -7 -9 3344.26 3392.01 64.54 2 7 10 4741.18 4940.86 81.76 -2 -7 -10 4262.98 4475.11 77.22 2 7 11 1278.03 1295.14 48.06 -2 -7 -11 1554.38 1330.70 49.93 2 7 12 673.83 626.08 40.50 -2 -7 -12 698.79 756.19 41.92 2 8 3 2505.69 2255.26 46.79 -2 -8 -3 1990.27 2067.03 41.75 2 8 4 2895.65 2964.84 52.60 -2 -8 -4 2848.39 2921.52 52.52 2 8 5 114.96 95.12 25.22 -2 -8 -5 227.03 237.25 36.62 2 8 6 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52.71 39.97 -2 -10 -6 58.69 67.34 39.23 2 10 7 190.07 199.95 42.00 -2 -10 -7 288.84 284.45 32.87 2 10 8 1902.38 2028.02 54.07 -2 -10 -8 2121.39 2324.08 57.29 2 10 9 242.14 260.70 47.74 -2 -10 -9 127.30 215.30 56.14 2 11 3 2406.66 2225.17 54.13 -2 -11 -3 2040.27 2273.05 51.20 2 11 4 432.19 304.32 34.51 -2 -11 -4 203.03 302.67 44.05 2 11 5 1599.64 1662.02 49.13 -2 -11 -5 1756.13 1783.60 50.88 2 11 6 4705.11 4864.67 81.89 -2 -11 -6 5473.15 5409.05 93.42 2 11 7 713.32 658.63 40.51 -2 -11 -7 508.95 592.29 37.40 2 11 8 581.20 557.54 41.70 -2 -11 -8 477.59 470.96 38.00 2 12 3 2858.08 2871.53 61.99 -2 -12 -3 2883.20 2946.22 62.68 2 12 4 2711.87 2655.68 62.02 -2 -12 -4 2843.32 2828.00 63.58 2 12 5 628.77 582.43 39.68 -2 -12 -5 739.07 655.45 39.62 2 12 6 1999.76 2001.51 58.50 -2 -12 -6 1761.52 1669.50 54.79 2 12 7 923.52 962.36 46.15 -2 -12 -7 994.64 905.13 44.74 2 13 3 1458.57 1571.99 50.30 -2 -13 -3 1575.75 1521.21 50.88 2 13 4 1941.90 1982.53 57.79 -2 -13 -4 1968.79 2046.92 56.38 2 13 5 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4 9 6 807.35 888.06 37.20 -4 -9 -6 909.90 881.01 38.41 4 9 7 838.62 758.16 39.81 -4 -9 -7 666.28 613.70 36.12 4 9 8 532.40 414.10 37.15 -4 -9 -8 388.45 454.45 35.42 4 9 9 514.34 555.85 38.19 -4 -9 -9 599.82 573.30 39.24 4 9 10 1408.94 1408.42 50.19 -4 -9 -10 1643.60 1590.06 52.57 4 10 5 3501.14 3247.43 67.38 -4 -10 -5 2637.89 2939.30 58.40 4 10 6 2236.49 2358.62 55.51 -4 -10 -6 2271.66 2094.85 54.63 4 10 7 2102.61 2005.63 55.07 -4 -10 -7 1818.11 1882.97 52.63 4 10 8 941.26 1001.45 43.72 -4 -10 -8 848.74 869.93 43.24 4 10 9 1788.93 1781.46 54.14 -4 -10 -9 1711.10 1716.08 54.87 4 11 5 530.95 570.34 37.96 -4 -11 -5 487.79 485.34 36.40 4 11 6 1935.11 2088.20 56.94 -4 -11 -6 2005.67 2005.07 55.61 4 11 7 3659.52 3772.30 74.88 -4 -11 -7 3822.41 3956.64 76.97 4 11 8 1419.74 1333.73 51.87 -4 -11 -8 1333.21 1377.04 49.36 4 12 5 52.80 54.54 51.56 -4 -12 -5 -2.03 53.47 52.21 4 12 6 628.64 687.74 43.63 -4 -12 -6 659.74 677.19 42.63 5 5 5 19478.96 19880.13 424.81 -5 -5 -5 18023.81 18566.88 399.18 5 5 6 2969.64 3098.75 53.33 -5 -5 -6 3289.48 3306.30 57.31 5 5 7 3895.28 3747.57 68.94 -5 -5 -7 3476.69 3536.83 60.53 5 5 8 2015.41 1948.79 47.90 -5 -5 -8 2185.56 2188.21 48.96 5 5 9 1051.60 1042.72 40.52 -5 -5 -9 1192.65 1189.74 42.91 5 5 10 1323.83 1183.65 45.66 -5 -5 -10 1161.22 1226.67 43.45 5 5 11 2510.10 2653.89 59.93 -5 -5 -11 2296.68 2375.75 57.89 5 5 12 875.35 899.63 44.04 -5 -5 -12 817.43 762.28 44.07 5 6 6 1816.09 1982.59 43.63 -5 -6 -6 1922.63 1837.47 45.05 5 6 7 9705.60 10024.27 159.29 -5 -6 -7 10079.53 9881.96 163.99 5 6 8 3988.28 4064.62 68.43 -5 -6 -8 3409.15 3578.03 63.13 5 6 9 423.09 391.82 33.19 -5 -6 -9 534.25 497.31 33.72 5 6 10 2403.26 2448.82 58.58 -5 -6 -10 2312.00 2445.23 56.33 5 6 11 2752.79 2717.52 64.29 -5 -6 -11 2395.51 2690.14 60.81 5 7 6 2023.39 2095.76 46.93 -5 -7 -6 2187.97 2159.98 49.18 5 7 7 1070.78 1027.28 39.19 -5 -7 -7 1125.86 1083.29 39.66 5 7 8 1275.71 1214.21 41.88 -5 -7 -8 1384.15 1327.12 44.23 5 7 9 189.62 192.71 45.88 -5 -7 -9 226.02 185.63 31.62 5 7 10 1129.27 1108.89 43.84 -5 -7 -10 1157.47 1142.18 45.16 5 7 11 1942.53 1863.51 55.68 -5 -7 -11 1671.63 1634.65 53.28 5 8 6 5525.82 5517.76 94.05 -5 -8 -6 4697.44 5011.88 84.07 5 8 7 2587.31 2888.34 57.40 -5 -8 -7 3156.54 3186.22 63.56 5 8 8 1655.76 1630.62 49.09 -5 -8 -8 1595.98 1485.85 47.93 5 8 9 1415.28 1451.06 47.88 -5 -8 -9 1563.48 1434.92 49.66 5 8 10 2942.44 2797.65 67.41 -5 -8 -10 2985.99 2983.44 67.52 5 9 6 4414.53 4389.46 77.31 -5 -9 -6 4332.46 4255.88 76.88 5 9 7 106.01 96.61 40.91 -5 -9 -7 153.56 87.63 31.91 5 9 8 2344.14 2395.01 57.58 -5 -9 -8 2789.78 2635.08 62.76 5 9 9 134.61 181.06 48.91 -5 -9 -9 165.70 177.42 45.67 5 10 6 1093.94 1124.59 43.67 -5 -10 -6 1261.45 1212.24 45.01 5 10 7 2994.57 2913.61 66.82 -5 -10 -7 2968.90 3012.66 65.21 5 10 8 449.70 487.27 38.04 -5 -10 -8 418.81 380.32 38.03 5 11 6 2267.09 2331.46 58.52 -5 -11 -6 2420.25 2484.85 60.79 5 11 7 971.30 986.65 44.32 -5 -11 -7 1133.24 1106.22 47.36 6 6 6 4149.92 4535.14 127.61 -6 -6 -6 3927.94 3802.70 119.03 6 6 7 699.15 660.47 33.53 -6 -6 -7 790.21 785.92 36.39 6 6 8 1492.92 1492.28 44.14 -6 -6 -8 1756.26 1649.31 47.20 6 6 9 232.12 285.12 32.03 -6 -6 -9 248.69 210.12 32.61 6 6 10 222.13 174.15 32.68 -6 -6 -10 194.11 172.37 32.08 6 6 11 953.30 894.39 44.07 -6 -6 -11 867.76 817.34 43.29 6 7 7 2000.19 1933.26 49.15 -6 -7 -7 2061.13 1990.11 50.29 6 7 8 2855.62 2725.47 60.16 -6 -7 -8 2373.95 2434.90 56.74 6 7 9 8409.21 8472.00 142.69 -6 -7 -9 7863.05 7694.12 134.15 6 7 10 1097.95 1232.30 45.60 -6 -7 -10 1290.54 1365.93 47.74 6 8 7 17.94 15.57 52.48 -6 -8 -7 96.48 48.14 37.98 6 8 8 1298.51 1251.71 46.51 -6 -8 -8 1216.63 1241.74 45.01 6 8 9 623.08 581.39 39.63 -6 -8 -9 458.28 425.20 36.52 6 8 10 227.58 188.55 35.53 -6 -8 -10 133.63 170.94 54.66 6 9 7 3.13 12.95 45.85 -6 -9 -7 11.99 4.45 54.45 6 9 8 4961.08 4970.96 86.37 -6 -9 -8 5020.51 4950.74 87.76 6 9 9 188.67 145.47 44.36 -6 -9 -9 133.09 125.81 47.20 6 10 7 1054.04 1001.85 44.12 -6 -10 -7 1201.04 1229.12 47.39 6 10 8 172.67 97.83 35.33 -6 -10 -8 61.78 119.11 56.93 7 7 7 7263.11 7415.68 217.72 -7 -7 -7 8620.02 8154.17 253.58 7 7 8 118.44 133.79 50.34 -7 -7 -8 91.45 182.97 54.18 7 7 9 1591.84 1639.91 51.81 -7 -7 -9 1651.42 1614.72 53.00 7 7 10 903.43 855.24 44.39 -7 -7 -10 776.70 864.27 42.86 7 8 8 398.72 344.17 35.55 -7 -8 -8 360.92 342.64 35.46 7 8 9 362.97 264.47 35.66 -7 -8 -9 185.92 228.33 49.61 7 9 8 864.38 967.91 44.81 -7 -9 -8 951.26 964.65 45.70 8 8 8 3888.36 4032.04 133.40 -8 -8 -8 4939.05 4619.63 154.07