#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180894 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/34/2103457.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103457_Fobs loop_ _publ_author_name 'Norberg, Stefan T.' _publ_section_title ; New phosphate langbeinites, K~2~MTi(PO~4~)~3~ (M = Er, Yb or Y), and an alternative description of the langbeinite framework ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 743 _journal_page_last 749 _journal_volume 58 _journal_year 2002 _space_group_IT_number 198 _symmetry_space_group_name_Hall 'P 2ac 2ab 3' _symmetry_space_group_name_H-M 'P 21 3' _cod_data_source_file os0095KYbTPsup3.hkl _cod_data_source_block KYbTP loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma 0 0 2 1815.80 2040.02 81.12 0 0 4 7920.20 8230.35 110.31 0 0 6 9785.10 10247.64 128.70 0 0 8 1059.19 1087.64 59.91 0 0 10 722.63 733.18 64.88 0 0 12 4861.41 4608.50 109.04 0 0 14 4924.63 4754.38 125.40 0 1 2 38.69 262.24 88.79 0 1 3 72054.56 73895.65 2107.9 0 1 4 1110.34 1269.33 47.21 0 1 5 13913.26 13789.87 139.21 0 1 6 13518.95 13666.34 133.67 0 1 7 4757.73 4736.18 62.15 0 1 8 5139.52 5329.52 67.34 0 1 9 14242.77 14060.69 146.77 0 1 10 1556.27 1574.74 56.91 0 1 11 288.25 217.77 77.39 0 1 12 4098.72 4103.97 82.44 0 1 13 703.73 882.53 76.47 0 1 14 32.48 52.75 110.71 0 2 1 28714.38 29439.38 915.23 0 2 2 1264.36 1412.83 55.87 0 2 3 9537.89 9354.10 288.79 0 2 4 1996.62 2280.90 51.01 0 2 5 9643.72 9494.34 101.64 0 2 6 15145.03 14885.85 415.46 0 2 7 -88.66 3.49 68.96 0 2 8 355.10 408.65 54.61 0 2 9 280.86 403.07 65.97 0 2 10 1223.76 1140.98 55.69 0 2 11 30.29 136.46 86.32 0 2 12 2475.09 2551.40 73.94 0 2 13 10685.28 10564.91 125.58 0 2 14 193.24 266.47 85.66 0 3 1 51967.89 53793.21 901.95 0 3 2 522.76 629.67 54.46 0 3 3 993.17 971.43 46.52 0 3 4 26284.88 25458.75 943.17 0 3 5 7592.33 7499.83 80.12 0 3 6 1728.95 1797.53 47.82 0 3 7 65.07 26.76 50.83 0 3 8 9651.55 9970.90 99.30 0 3 9 5134.78 5217.34 74.56 0 3 10 9620.41 9427.94 102.19 0 3 11 1041.24 1031.90 60.82 0 3 12 709.77 740.63 70.97 0 3 13 492.94 637.41 86.05 0 4 1 715.07 716.21 45.96 0 4 2 733.07 658.83 45.06 0 4 3 329.05 432.41 47.18 0 4 4 7500.12 7038.76 277.79 0 4 5 1313.88 1249.09 44.49 0 4 6 3317.29 3363.87 55.64 0 4 7 21954.93 21811.32 525.75 0 4 8 421.90 354.03 46.37 0 4 9 279.37 398.08 67.22 0 4 10 1320.89 1336.62 58.04 0 4 11 6203.61 6428.22 93.42 0 4 12 5177.80 5094.77 93.28 0 4 13 285.46 390.42 100.13 0 5 1 3954.25 4109.67 56.96 0 5 2 30507.47 31333.56 895.42 0 5 3 21343.76 22972.96 617.93 0 5 4 626.71 587.80 41.05 0 5 5 5570.89 5440.50 203.80 0 5 6 24.30 23.26 73.27 0 5 7 183.64 220.90 69.10 0 5 8 1337.74 1302.62 54.14 0 5 9 13170.24 13071.63 342.37 0 5 10 491.77 610.51 76.94 0 5 11 127.86 240.42 89.77 0 5 12 1435.45 1438.38 72.29 0 5 13 84.79 139.68 107.22 0 6 1 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47.99 0 9 2 19860.92 20203.96 642.56 0 9 3 99.77 4.33 82.76 0 9 4 108.60 281.15 80.93 0 9 5 4527.68 4544.62 75.08 0 9 6 2738.21 2706.25 69.89 0 9 7 -37.45 57.17 91.80 0 9 8 1894.74 1815.44 69.43 0 9 9 322.70 353.11 72.96 0 9 10 670.80 817.75 76.66 0 10 1 4914.34 4858.27 74.53 0 10 2 125.44 232.94 77.36 0 10 3 -30.51 8.14 77.37 0 10 4 2988.58 3137.33 68.41 0 10 5 3062.79 2979.96 72.51 0 10 6 5876.71 5855.93 91.76 0 10 7 1555.38 1553.63 67.32 0 10 8 1802.83 1741.62 72.43 0 10 9 -165.15 7.99 107.52 0 10 10 3830.12 3632.73 92.44 0 11 1 5425.00 5569.19 86.85 0 11 2 54.87 131.79 85.85 0 11 3 6113.38 6538.77 91.00 0 11 4 3404.88 3334.84 76.50 0 11 5 492.60 492.33 75.76 0 11 6 129.49 264.13 91.95 0 11 7 21.13 11.67 93.22 0 11 8 2383.91 2225.68 80.15 0 12 1 292.32 239.87 78.93 0 12 2 3890.92 3850.74 83.42 0 12 3 3588.33 3766.84 82.38 0 12 4 1896.31 2012.21 71.28 0 12 5 38.27 11.10 99.83 0 12 6 2680.51 2582.70 82.10 0 12 7 2438.00 2249.99 81.80 0 13 1 -26.99 2.39 102.41 0 13 2 2805.91 2969.22 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