#------------------------------------------------------------------------------
#$Date: 2016-04-02 23:00:04 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180894 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/34/2103459.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103459_Fobs
loop_
_publ_author_name
'Norberg, Stefan T.'
_publ_section_title
;
 New phosphate langbeinites, K~2~<i>M</i>Ti(PO~4~)~3~ (<i>M</i> = Er,
 Yb or Y), and an alternative description of the langbeinite framework
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              743
_journal_page_last               749
_journal_volume                  58
_journal_year                    2002
_space_group_IT_number           198
_symmetry_space_group_name_Hall  'P 2ac 2ab 3'
_symmetry_space_group_name_H-M   'P 21 3'
_cod_data_source_file            os0095KCrTPsup5.hkl
_cod_data_source_block           KCrTP
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_calc
_refln_F_squared_sigma
0 0 2 52.31 40.48 4.53
0 0 4 574.49 320.57 8.11
0 0 6 4186.30 4149.52 38.49
0 0 8 246.68 268.37 6.43
0 0 10 350.50 315.62 8.42
0 0 12 387.25 403.26 10.17
0 0 14 2836.05 2875.69 38.79
0 1 2 526.10 506.21 7.10
0 1 3 25629.74 24716.57 814.70
0 1 4 2217.53 1738.85 20.57
0 1 5 915.17 915.83 10.99
0 1 6 9424.11 9328.52 61.51
0 1 7 982.53 1008.51 11.89
0 1 8 191.37 203.97 5.45
0 1 9 857.75 800.07 10.52
0 1 10 78.31 73.19 5.61
0 1 11 113.40 109.92 6.42
0 1 12 4953.77 4916.63 54.48
0 1 13 518.46 506.30 11.29
0 1 14 253.94 232.72 9.39
0 1 15 -6.17 2.11 14.52
0 2 1 3734.90 3700.53 25.31
0 2 2 44.43 60.17 3.84
0 2 3 2696.45 2922.09 22.39
0 2 4 2442.51 2584.81 22.21
0 2 5 797.29 836.63 9.90
0 2 6 2122.62 2026.07 23.44
0 2 7 41.25 32.65 4.00
0 2 8 4116.51 4258.58 39.51
0 2 9 487.04 497.73 7.86
0 2 10 13.18 4.76 9.05
0 2 11 304.90 317.31 8.03
0 2 12 1716.88 1732.11 21.36
0 2 13 3238.80 3270.17 39.54
0 2 14 228.45 228.20 9.56
0 2 15 801.08 822.21 15.38
0 3 1 26616.47 25350.79 1005.1
0 3 2 9062.40 9147.73 181.02
0 3 3 845.12 859.07 10.45
0 3 4 5987.81 5869.80 41.54
0 3 5 227.25 237.47 4.59
0 3 6 3990.36 3920.06 34.78
0 3 7 59.75 48.02 4.20
0 3 8 478.47 469.04 7.60
0 3 9 3637.14 3603.63 39.62
0 3 10 3212.92 3175.50 38.03
0 3 11 122.60 123.77 6.61
0 3 12 1837.30 1882.04 23.38
0 3 13 1901.70 1958.63 23.43
0 3 14 2106.09 2068.57 24.92
0 3 15 135.78 135.18 9.84
0 4 1 1838.30 1691.65 18.50
0 4 2 486.20 369.73 6.16
0 4 3 102.47 73.81 3.88
0 4 4 2819.93 2965.75 26.16
0 4 5 461.78 444.95 6.33
0 4 6 2234.07 2203.35 25.67
0 4 7 5591.60 5701.80 47.39
0 4 8 1486.45 1561.19 18.42
0 4 9 295.30 271.68 7.17
0 4 10 182.05 175.14 6.78
0 4 11 1036.44 1049.17 13.51
0 4 12 2660.45 2622.54 33.11
0 4 13 2.26 .03 11.97
0 4 14 1802.49 1791.97 22.30
0 4 15 1405.77 1488.34 20.39
0 5 1 128.57 143.40 3.89
0 5 2 7459.59 7285.40 49.79
0 5 3 4956.52 5166.75 38.20
0 5 4 1984.87 1933.24 22.72
0 5 5 2377.82 2433.37 26.17
0 5 6 2755.46 2846.64 30.19
0 5 7 1360.01 1401.50 16.40
0 5 8 55.22 51.81 4.80
0 5 9 5043.71 5179.18 50.33
0 5 10 199.94 186.55 7.18
0 5 11 114.30 124.23 6.76
0 5 12 127.72 122.95 7.81
0 5 13 29.39 20.89 8.87
0 5 14 755.12 753.62 14.86
0 5 15 12.08 1.59 36.02
0 6 1 8968.73 9092.29 59.45
0 6 2 3606.63 3644.89 31.96
0 6 3 10917.14 10768.66 70.95
0 6 4 1041.12 964.47 12.86
0 6 5 115.37 126.47 4.74
0 6 6 3124.63 3125.81 34.00
0 6 7 1075.45 1092.81 13.11
0 6 8 2282.88 2304.50 28.73
0 6 9 315.34 305.51 7.85
0 6 10 1079.75 1062.15 13.68
0 6 11 2582.80 2568.83 32.16
0 6 12 270.92 288.77 9.63
0 6 13 200.34 190.45 9.20
0 6 14 266.16 266.87 11.02
0 7 1 2350.14 2428.56 26.06
0 7 2 5173.97 5270.77 42.83
0 7 3 8462.40 8565.29 61.43
0 7 4 3060.71 3142.39 32.48
0 7 5 289.05 297.65 6.41
0 7 6 1145.47 1117.10 13.94
0 7 7 2201.03 2289.27 27.34
0 7 8 1.58 3.29 8.56
0 7 9 173.60 184.22 7.18
0 7 10 797.08 803.15 12.32
0 7 11 1134.20 1130.65 15.65
0 7 12 80.03 77.33 7.85
0 7 13 -2.93 20.66 13.09
0 7 14 487.96 501.75 13.29
0 8 1 404.71 404.35 6.78
0 8 2 6595.20 6848.99 52.99
0 8 3 22.29 17.66 6.34
0 8 4 18.02 13.61 7.32
0 8 5 3050.66 3144.38 35.51
0 8 6 1110.22 1084.51 13.86
0 8 7 228.40 236.77 7.21
0 8 8 352.96 335.92 8.34
0 8 9 723.17 706.67 11.68
0 8 10 752.66 781.72 12.88
0 8 11 1365.56 1394.17 17.63
0 8 12 249.77 245.14 9.89
0 8 13 12.00 4.58 12.66
0 9 1 1739.68 1753.96 21.33
0 9 2 4420.86 4323.88 43.35
0 9 3 237.10 251.47 6.34
0 9 4 260.57 248.12 7.02
0 9 5 2478.22 2495.61 30.58
0 9 6 2780.92 2753.49 33.50
0 9 7 372.88 353.77 8.73
0 9 8 291.99 302.60 8.41
0 9 9 42.25 43.08 8.38
0 9 10 645.46 648.29 12.23
0 9 11 443.81 424.48 11.56
0 9 12 399.64 406.27 12.01
0 10 1 234.62 225.09 6.99
0 10 2 14.73 4.80 7.08
0 10 3 8.72 4.42 8.94
0 10 4 1803.52 1867.11 22.35
0 10 5 251.71 226.20 7.63
0 10 6 1143.05 1123.48 14.10
0 10 7 90.02 82.97 6.57
0 10 8 855.45 824.30 13.34
0 10 9 77.12 77.71 7.67
0 10 10 1017.20 1025.16 15.77
0 10 11 273.77 270.81 10.71
0 10 12 574.98 574.01 13.93
0 11 1 2777.09 2782.82 33.72
0 11 2 319.49 316.73 8.14
0 11 3 1388.77 1340.46 17.41
0 11 4 34.28 41.94 9.06
0 11 5 605.40 611.45 10.78
0 11 6 36.40 65.61 10.50
0 11 7 82.87 81.80 7.44
0 11 8 17.14 27.90 12.79
0 11 9 80.65 62.40 7.75
0 11 10 10.89 2.00 12.87
0 11 11 794.87 778.00 15.73
0 12 1 273.52 289.23 8.31
0 12 2 984.92 975.89 13.44
0 12 3 2479.93 2475.65 30.90
0 12 4 266.84 261.90 8.92
0 12 5 6.01 .12 10.30
0 12 6 340.96 331.16 10.06
0 12 7 889.78 918.29 14.65
0 12 8 721.26 757.93 13.82
0 12 9 125.07 141.11 9.52
0 12 10 224.21 243.16 11.15
0 13 1 29.45 33.38 10.56
0 13 2 2752.58 2781.83 33.10
0 13 3 412.54 415.87 10.70
0 13 4 21.58 26.10 12.33
0 13 5 546.75 544.56 12.00
0 13 6 223.90 230.25 9.73
0 13 7 185.84 187.38 9.88
0 13 8 356.71 354.83 11.98
0 13 9 2403.78 2313.06 65.74
0 14 1 69.21 76.62 10.10
0 14 2 26.46 38.40 11.61
0 14 3 599.49 594.73 12.70
0 14 4 19.70 18.87 12.26
0 14 5 2607.23 2635.94 31.80
0 14 6 19.02 6.07 13.16
0 14 7 182.21 184.17 10.41
0 15 1 816.02 816.86 15.45
0 15 2 368.11 382.78 11.91
0 15 3 401.93 404.11 12.39
0 15 4 390.65 383.93 12.41
0 15 5 418.40 403.73 28.23
1 1 1 4413.67 4154.27 62.50
-1 -1 -1 4323.79 4170.81 61.40
1 1 2 2340.52 2282.80 24.63
-1 -1 -2 2662.56 2624.55 26.74
1 1 3 8751.88 8537.30 66.52
-1 -1 -3 8436.33 8366.16 64.52
1 1 4 272.01 234.09 6.03
-1 -1 -4 236.96 207.83 5.89
1 1 5 154.98 135.71 5.21
-1 -1 -5 206.62 185.27 5.60
1 1 6 8116.79 7865.32 71.14
-1 -1 -6 7861.32 7550.87 69.44
1 1 7 518.41 564.00 9.05
-1 -1 -7 549.25 578.03 9.21
1 1 8 1339.55 1373.78 21.13
-1 -1 -8 1497.84 1486.17 23.75
1 1 9 3903.35 3966.54 51.81
-1 -1 -9 3884.30 4010.80 51.91
1 1 10 1857.91 1837.41 29.88
-1 -1 -10 1812.26 1812.29 28.72
1 1 11 531.10 530.87 12.16
-1 -1 -11 569.20 583.24 12.57
1 1 12 2302.62 2310.21 36.90
-1 -1 -12 2342.51 2321.78 37.11
1 1 13 443.26 443.39 13.69
-1 -1 -13 425.31 425.89 13.56
1 1 14 982.52 1017.48 20.31
-1 -1 -14 916.73 933.50 19.52
1 1 15 791.81 800.31 19.58
-1 -1 -15 707.34 734.93 19.01
1 2 2 1766.89 1747.90 21.92
-1 -2 -2 1737.83 1712.99 21.75
1 2 3 15143.26 15871.06 778.87
-1 -2 -3 15638.15 15822.99 110.40
1 2 4 1329.36 1087.25 20.54
-1 -2 -4 1391.09 1170.94 21.26
1 2 5 267.15 258.66 6.14
-1 -2 -5 261.17 241.19 6.11
1 2 6 2006.44 1964.98 29.39
-1 -2 -6 2023.65 1968.79 29.42
1 2 7 3827.18 3704.05 45.49
-1 -2 -7 3450.33 3535.77 42.90
1 2 8 734.56 734.33 11.60
-1 -2 -8 761.42 760.78 12.52
1 2 9 291.81 282.67 8.59
-1 -2 -9 302.31 288.76 8.43
1 2 10 2529.76 2558.57 39.81
-1 -2 -10 2493.65 2483.46 39.29
1 2 11 1298.96 1303.29 20.59
-1 -2 -11 1436.18 1411.78 23.19
1 2 12 188.20 204.16 9.91
-1 -2 -12 175.43 172.64 10.01
1 2 13 1483.56 1467.15 24.13
-1 -2 -13 1483.18 1473.93 23.93
1 2 14 195.10 195.61 11.90
-1 -2 -14 203.40 181.44 11.35
1 2 15 187.99 229.73 13.77
-1 -2 -15 210.00 203.13 13.17
1 3 2 6919.16 7261.41 56.23
-1 -3 -2 6897.31 7122.79 56.10
1 3 3 2258.07 2088.93 27.41
-1 -3 -3 2038.58 1896.17 25.72
1 3 4 3873.06 3911.86 40.09
-1 -3 -4 3827.70 3804.32 39.74
1 3 5 2718.17 2797.01 33.70
-1 -3 -5 2809.49 2828.16 34.67
1 3 6 12525.52 12400.74 101.94
-1 -3 -6 12374.00 12400.30 100.85
1 3 7 11827.67 11836.33 100.99
-1 -3 -7 11830.52 12022.59 102.00
1 3 8 4380.98 4359.69 53.86
-1 -3 -8 4338.37 4371.86 53.87
1 3 9 458.46 464.87 10.59
-1 -3 -9 497.49 497.77 11.01
1 3 10 2046.06 2105.37 33.23
-1 -3 -10 1847.08 1909.73 29.96
1 3 11 162.66 160.50 9.06
-1 -3 -11 152.44 165.44 8.98
1 3 12 320.17 311.60 11.76
-1 -3 -12 334.34 314.27 12.25
1 3 13 90.07 94.77 9.93
-1 -3 -13 124.63 110.17 10.19
1 3 14 1.74 31.45 18.62
-1 -3 -14 46.65 34.93 9.52
1 3 15 407.35 390.26 15.55
-1 -3 -15 437.40 391.53 15.97
1 4 2 514.50 493.73 8.16
-1 -4 -2 737.09 669.71 11.96
1 4 3 5693.68 5726.91 52.03
-1 -4 -3 5503.13 5569.02 51.01
1 4 4 11287.27 11657.89 90.00
-1 -4 -4 11235.22 11573.46 89.82
1 4 5 1641.05 1626.92 24.54
-1 -4 -5 1470.66 1538.11 22.83
1 4 6 1268.87 1291.29 19.82
-1 -4 -6 1313.28 1285.74 19.97
1 4 7 2223.17 2174.52 34.10
-1 -4 -7 1838.59 1920.57 28.91
1 4 8 2349.22 2327.72 35.02
-1 -4 -8 2385.09 2420.03 35.40
1 4 9 3483.23 3538.75 50.68
-1 -4 -9 3544.30 3501.54 51.48
1 4 10 981.12 964.67 16.17
-1 -4 -10 946.24 965.73 15.70
1 4 11 2627.86 2606.44 41.93
-1 -4 -11 2673.78 2708.21 41.59
1 4 12 401.50 399.86 12.79
-1 -4 -12 418.95 406.81 13.03
1 4 13 418.18 432.84 13.99
-1 -4 -13 447.32 448.94 14.39
1 4 14 120.87 124.13 11.37
-1 -4 -14 125.43 132.74 11.47
1 4 15 515.81 500.32 17.47
-1 -4 -15 560.83 563.10 18.40
1 5 2 3321.98 3160.45 37.06
-1 -5 -2 3111.63 3023.14 35.57
1 5 3 225.99 193.15 5.92
-1 -5 -3 224.53 194.78 5.86
1 5 4 7343.74 7638.02 66.98
-1 -5 -4 7497.20 7754.45 68.02
1 5 5 581.52 623.92 9.72
-1 -5 -5 535.23 604.71 9.13
1 5 6 733.19 733.99 11.73
-1 -5 -6 676.61 717.35 10.82
1 5 7 1492.34 1438.52 23.70
-1 -5 -7 1468.43 1477.78 24.05
1 5 8 130.47 124.75 7.22
-1 -5 -8 140.57 125.68 7.06
1 5 9 1167.24 1195.00 19.24
-1 -5 -9 1347.57 1361.01 21.14
1 5 10 366.84 378.76 11.03
-1 -5 -10 326.22 346.12 10.63
1 5 11 827.53 805.82 15.78
-1 -5 -11 805.67 851.71 15.96
1 5 12 591.39 587.28 15.40
-1 -5 -12 637.24 615.77 15.83
1 5 13 698.32 658.58 16.90
-1 -5 -13 571.38 579.59 15.97
1 5 14 580.06 602.75 17.58
-1 -5 -14 624.31 618.45 18.03
1 6 2 5066.01 4993.20 51.40
-1 -6 -2 5144.26 5121.39 52.15
1 6 3 370.16 376.71 7.67
-1 -6 -3 350.04 376.65 7.64
1 6 4 1972.26 1943.30 30.14
-1 -6 -4 1902.69 2006.16 27.93
1 6 5 7401.77 7535.66 72.10
-1 -6 -5 7577.46 7742.92 73.74
1 6 6 444.50 424.53 9.34
-1 -6 -6 396.05 354.15 8.99
1 6 7 165.21 157.85 7.16
-1 -6 -7 174.29 157.32 7.44
1 6 8 4047.44 4155.93 55.81
-1 -6 -8 4164.63 4267.42 57.24
1 6 9 542.01 539.66 12.36
-1 -6 -9 591.70 586.21 12.68
1 6 10 498.22 484.50 12.75
-1 -6 -10 521.36 537.77 12.82
1 6 11 45.69 28.09 8.17
-1 -6 -11 -1.94 33.54 17.05
1 6 12 1259.05 1292.25 21.58
-1 -6 -12 1301.85 1315.25 22.03
1 6 13 212.97 207.09 12.49
-1 -6 -13 262.00 245.50 12.28
1 6 14 1545.93 1529.28 27.09
-1 -6 -14 1470.23 1504.90 26.33
1 7 2 485.01 494.00 8.84
-1 -7 -2 458.46 469.08 8.66
1 7 3 985.96 968.98 15.40
-1 -7 -3 842.70 864.53 13.63
1 7 4 25.97 20.21 7.71
-1 -7 -4 45.97 38.27 5.39
1 7 5 1062.95 1051.42 16.59
-1 -7 -5 1187.04 1187.72 18.86
1 7 6 1677.01 1680.27 26.41
-1 -7 -6 1668.74 1734.99 26.06
1 7 7 1486.84 1495.45 23.24
-1 -7 -7 1325.40 1409.30 20.96
1 7 8 2787.62 2815.31 43.03
-1 -7 -8 2849.22 2935.56 43.59
1 7 9 626.51 645.48 13.33
-1 -7 -9 605.33 634.69 13.43
1 7 10 896.42 863.66 16.53
-1 -7 -10 805.24 838.71 16.18
1 7 11 141.19 142.89 10.25
-1 -7 -11 130.75 135.10 10.49
1 7 12 464.75 459.57 14.65
-1 -7 -12 453.64 459.66 14.78
1 7 13 289.18 266.90 13.80
-1 -7 -13 228.82 219.29 13.12
1 7 14 184.07 190.09 12.97
-1 -7 -14 214.57 189.62 14.11
1 8 2 338.62 368.00 8.24
-1 -8 -2 324.90 355.24 8.30
1 8 3 2400.86 2299.94 36.79
-1 -8 -3 2258.09 2186.45 33.97
1 8 4 422.48 427.79 9.68
-1 -8 -4 459.11 449.18 9.95
1 8 5 3239.43 3263.75 47.64
-1 -8 -5 3052.72 3146.95 46.41
1 8 6 437.29 417.76 10.92
-1 -8 -6 432.90 428.65 10.73
1 8 7 431.10 456.37 11.04
-1 -8 -7 493.13 527.70 11.71
1 8 8 863.05 832.21 15.37
-1 -8 -8 901.42 899.20 15.78
1 8 9 2131.61 2145.96 34.17
-1 -8 -9 2116.22 2135.15 33.55
1 8 10 600.49 594.92 14.78
-1 -8 -10 618.97 594.52 15.31
1 8 11 93.44 91.62 9.91
-1 -8 -11 84.81 80.69 9.71
1 8 12 367.64 389.29 14.26
-1 -8 -12 426.56 435.40 14.48
1 8 13 779.55 793.01 20.03
-1 -8 -13 706.97 697.24 18.93
1 9 2 1538.34 1549.19 24.45
-1 -9 -2 1490.42 1510.74 24.06
1 9 3 259.39 256.27 8.67
-1 -9 -3 258.31 261.62 8.73
1 9 4 3997.31 4042.17 54.59
-1 -9 -4 3874.38 3965.76 54.23
1 9 5 1719.01 1647.10 26.90
-1 -9 -5 1438.66 1529.30 22.70
1 9 6 251.01 250.20 9.70
-1 -9 -6 216.96 209.44 9.18
1 9 7 747.81 756.83 14.58
-1 -9 -7 676.66 708.44 14.02
1 9 8 658.75 675.91 14.29
-1 -9 -8 670.86 668.41 14.39
1 9 9 1374.64 1364.79 21.68
-1 -9 -9 1312.51 1342.08 21.29
1 9 10 560.46 546.39 15.20
-1 -9 -10 586.39 561.00 15.63
1 9 11 370.62 364.27 13.42
-1 -9 -11 374.06 376.42 14.06
1 9 12 422.74 431.83 16.17
-1 -9 -12 395.96 414.50 15.98
1 10 2 853.74 857.64 14.41
-1 -10 -2 859.53 883.72 14.35
1 10 3 235.17 197.54 8.76
-1 -10 -3 203.50 195.83 8.96
1 10 4 2333.60 2337.84 37.12
-1 -10 -4 2199.82 2289.71 35.61
1 10 5 1451.42 1432.69 23.05
-1 -10 -5 1426.06 1425.22 22.23
1 10 6 491.28 506.46 12.54
-1 -10 -6 490.61 496.25 12.58
1 10 7 3679.49 3744.62 54.57
-1 -10 -7 3706.18 3753.26 55.06
1 10 8 807.17 771.60 16.75
-1 -10 -8 638.29 659.02 15.63
1 10 9 1075.84 1055.28 19.83
-1 -10 -9 937.12 969.18 18.78
1 10 10 655.17 641.02 16.72
-1 -10 -10 620.84 621.43 16.55
1 10 11 478.69 430.83 15.95
-1 -10 -11 454.98 432.10 16.29
1 10 12 28.14 41.67 11.54
-1 -10 -12 32.46 45.01 18.14
1 11 2 1379.34 1358.04 21.53
-1 -11 -2 1283.00 1290.19 19.98
1 11 3 354.08 349.09 10.93
-1 -11 -3 392.64 406.46 11.43
1 11 4 1505.70 1521.30 24.57
-1 -11 -4 1415.31 1432.22 21.98
1 11 5 1812.22 1826.35 29.90
-1 -11 -5 1810.10 1843.84 28.61
1 11 6 662.21 699.29 15.19
-1 -11 -6 675.30 681.85 15.62
1 11 7 655.92 657.67 15.87
-1 -11 -7 643.37 659.93 16.19
1 11 8 904.92 894.24 18.71
-1 -11 -8 1052.05 1041.51 19.92
1 11 9 76.56 58.83 10.05
-1 -11 -9 60.03 62.88 14.56
1 11 10 132.74 133.60 12.10
-1 -11 -10 119.74 101.26 11.30
1 11 11 713.35 674.43 19.27
-1 -11 -11 691.05 692.38 19.28
1 12 2 604.13 603.57 13.92
-1 -12 -2 645.22 655.89 14.40
1 12 3 852.70 827.01 17.13
-1 -12 -3 778.56 810.87 16.44
1 12 4 59.04 42.90 8.53
-1 -12 -4 -8.64 13.75 14.90
1 12 5 46.42 52.71 12.63
-1 -12 -5 54.09 63.36 9.03
1 12 6 136.18 147.47 10.76
-1 -12 -6 127.14 125.97 10.42
1 12 7 594.36 584.75 16.08
-1 -12 -7 642.04 633.73 16.74
1 12 8 1060.56 1049.93 21.08
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