#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103484.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103484_Fobs loop_ _publ_author_name 'Vithana, Champika' 'Uekusa, Hidehiro' 'Sekine, Akiko' 'Ohashi, Yuji' _publ_section_title ; Modified photoreactivity due to mixed crystal~formation. II. Enhanced reactivity upon conformational mimicry and cavity enlargement ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 986 _journal_page_last 997 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.992 _cell_angle_gamma 90.000 _cell_length_a 11.5432 _cell_length_b 9.3978 _cell_length_c 19.5033 _exptl_crystal_F_000 888.00 _reflns_d_resolution_high 0.7689 _[local]_cod_data_source_file de0020mix-Iprimesup4.hkl _[local]_cod_data_source_block mix-Iprime #BEGIN Tags that were not found in dictionaries: _shelx_title ' mix6 after irradiation.' _shelx_refln_list_code 4 _shelx_F_calc_maximum 289.21 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 27609.22 21372.60 309.47 o 4 0 0 18355.28 17010.48 370.31 o 6 0 0 4707.80 6071.38 145.31 o 8 0 0 62.56 288.44 54.76 o 10 0 0 0.75 -10.30 49.34 o 12 0 0 12.75 53.13 59.10 o 14 0 0 0.02 -22.77 71.03 o 1 1 0 1181.71 1666.34 29.33 o 2 1 0 689.60 550.05 17.59 o 3 1 0 3393.26 6539.50 105.24 o 4 1 0 286.48 414.58 22.62 o 5 1 0 3132.45 5304.59 71.50 o 6 1 0 2397.42 3461.74 51.96 o 7 1 0 2.48 82.05 21.20 o 8 1 0 1454.58 2006.80 50.99 o 9 1 0 13.59 113.50 32.96 o 10 1 0 298.96 432.10 39.18 o 11 1 0 8.43 3.31 36.36 o 12 1 0 211.80 346.93 89.46 o 13 1 0 8.16 41.81 42.92 o 14 1 0 86.46 160.03 46.86 o 0 2 0 18055.16 14556.20 181.55 o 1 2 0 387.91 195.25 15.71 o 2 2 0 5987.49 6920.03 110.22 o 3 2 0 1713.79 2678.45 127.96 o 4 2 0 5094.23 5997.28 149.10 o 5 2 0 928.68 1094.92 42.56 o 6 2 0 3453.63 4433.93 81.84 o 7 2 0 392.01 876.42 39.17 o 8 2 0 553.47 679.85 27.56 o 9 2 0 429.95 630.66 36.57 o 10 2 0 107.69 131.22 32.81 o 11 2 0 6.61 404.91 41.65 o 12 2 0 20.95 50.06 61.81 o 13 2 0 7.93 178.56 46.14 o 14 2 0 0.67 -4.26 45.28 o 1 3 0 45.63 224.95 20.37 o 2 3 0 305.16 487.35 23.36 o 3 3 0 4432.13 4943.68 83.76 o 4 3 0 854.19 1063.50 32.70 o 5 3 0 700.85 1750.80 131.75 o 6 3 0 2068.18 1740.61 43.28 o 7 3 0 946.73 2093.25 53.64 o 8 3 0 153.03 431.20 32.03 o 9 3 0 87.06 155.68 27.04 o 10 3 0 126.35 209.88 29.11 o 11 3 0 76.75 192.05 32.36 o 12 3 0 247.24 364.46 83.50 o 13 3 0 13.10 88.22 49.24 o 14 3 0 10.54 44.66 55.34 o 0 4 0 183.75 492.98 66.55 o 1 4 0 4002.17 4733.32 44.76 o 2 4 0 11044.35 17136.38 165.13 o 3 4 0 905.10 859.60 18.74 o 4 4 0 1575.96 1815.34 41.20 o 5 4 0 12.27 22.69 23.30 o 6 4 0 3739.33 4991.96 91.39 o 7 4 0 154.98 424.50 35.05 o 8 4 0 1168.25 2530.41 61.71 o 9 4 0 123.75 83.36 34.50 o 10 4 0 28.16 90.57 31.00 o 11 4 0 7.00 96.83 30.75 o 12 4 0 8.42 82.64 35.38 o 13 4 0 4.90 166.05 49.17 o 14 4 0 0.12 53.97 49.73 o 1 5 0 20.92 8.32 11.20 o 2 5 0 167.01 241.11 12.78 o 3 5 0 126.25 89.85 14.02 o 4 5 0 0.65 6.02 15.35 o 5 5 0 572.21 1124.77 26.51 o 6 5 0 291.09 671.33 42.66 o 7 5 0 1564.75 3476.22 106.54 o 8 5 0 25.53 2.96 30.44 o 9 5 0 136.97 267.12 74.82 o 10 5 0 25.41 38.02 39.44 o 11 5 0 150.52 349.82 46.16 o 12 5 0 74.47 92.17 43.04 o 13 5 0 39.33 66.85 36.90 o 0 6 0 919.46 1621.07 42.52 o 1 6 0 2653.59 3104.69 71.77 o 2 6 0 716.74 862.34 33.43 o 3 6 0 1182.68 1460.05 34.43 o 4 6 0 325.40 641.87 22.43 o 5 6 0 615.21 1315.64 50.95 o 6 6 0 65.96 158.64 31.30 o 7 6 0 251.58 319.22 24.15 o 8 6 0 20.00 125.37 28.21 o 9 6 0 9.64 36.46 32.69 o 10 6 0 28.81 199.93 37.35 o 11 6 0 25.74 54.10 46.42 o 12 6 0 18.44 186.55 38.54 o 13 6 0 1.12 -51.16 51.16 o 1 7 0 262.19 223.93 38.43 o 2 7 0 81.97 144.71 20.17 o 3 7 0 21.66 83.17 22.73 o 4 7 0 113.77 210.44 27.49 o 5 7 0 131.29 201.60 28.44 o 6 7 0 0.70 18.27 25.98 o 7 7 0 95.08 294.63 29.93 o 8 7 0 8.82 -31.94 32.14 o 9 7 0 109.26 388.84 52.32 o 10 7 0 12.16 44.19 43.32 o 11 7 0 42.61 213.91 49.06 o 12 7 0 7.65 70.71 48.70 o 0 8 0 108.76 233.97 33.60 o 1 8 0 228.32 346.67 23.45 o 2 8 0 2.06 30.88 20.78 o 3 8 0 1.77 2.74 24.64 o 4 8 0 2.54 12.50 26.82 o 5 8 0 364.33 448.15 30.56 o 6 8 0 87.31 271.62 32.31 o 7 8 0 42.33 48.12 32.96 o 8 8 0 50.22 142.22 37.90 o 9 8 0 22.94 128.39 48.30 o 10 8 0 34.25 194.48 46.98 o 11 8 0 8.25 5.84 48.49 o 1 9 0 31.12 6.32 22.11 o 2 9 0 46.18 1.29 24.89 o 3 9 0 5.01 -7.01 26.21 o 4 9 0 5.31 6.06 27.77 o 5 9 0 48.55 104.64 36.04 o 6 9 0 11.42 58.05 37.04 o 7 9 0 54.22 133.91 44.27 o 8 9 0 2.18 68.03 40.38 o 9 9 0 21.12 135.11 50.93 o 10 9 0 0.09 41.61 51.10 o 0 10 0 0.25 28.50 36.52 o 1 10 0 207.65 528.11 30.27 o 2 10 0 1.27 40.51 29.58 o 3 10 0 86.69 295.83 41.23 o 4 10 0 0.05 32.78 34.58 o 5 10 0 102.85 209.92 40.14 o 6 10 0 11.90 48.97 42.98 o 7 10 0 24.54 119.12 49.73 o 8 10 0 2.95 46.74 49.62 o 1 11 0 0.82 -9.52 29.68 o 2 11 0 2.77 -24.05 51.03 o 3 11 0 4.68 17.57 35.05 o 4 11 0 0.29 30.45 45.77 o 5 11 0 6.67 68.75 44.65 o 6 11 0 0.48 9.53 45.61 o 0 12 0 0.34 24.80 47.45 o 1 12 0 9.76 36.46 38.51 o 2 12 0 0.04 2.31 39.75 o -13 0 1 59.63 31.45 57.47 o -11 0 1 27.56 -10.84 43.37 o -9 0 1 219.48 508.57 52.05 o -7 0 1 12.16 25.48 37.95 o -5 0 1 156.78 151.27 28.74 o -3 0 1 10.52 25.48 22.77 o -1 0 1 13175.76 7053.81 151.81 o 1 0 1 25978.12 24465.95 284.87 o 3 0 1 16.20 123.33 38.50 o 5 0 1 22886.86 32996.23 707.55 o 7 0 1 1135.10 1329.98 54.22 o 9 0 1 697.23 1833.12 78.07 o 11 0 1 27.18 -17.35 49.34 o 13 0 1 84.18 110.06 68.86 o -14 1 1 0.41 33.21 79.97 o -13 1 1 97.24 152.58 45.99 o -12 1 1 0.36 87.07 37.95 o -11 1 1 84.05 176.11 42.02 o -10 1 1 3.92 51.27 36.51 o -9 1 1 942.73 1341.43 45.42 o -8 1 1 119.62 204.31 54.76 o -7 1 1 1226.47 1081.70 28.35 o -6 1 1 141.02 235.75 18.35 o -5 1 1 12300.93 19360.88 236.74 o -4 1 1 16.73 28.17 17.19 o -3 1 1 12294.20 13595.82 209.13 o -2 1 1 293.37 561.35 30.36 o -1 1 1 70843.88 52849.23 628.07 o 0 1 1 1182.43 1111.30 48.07 o 1 1 1 27964.56 24333.05 254.51 o 2 1 1 2948.71 1499.33 97.33 o 3 1 1 8391.50 8716.41 137.41 o 4 1 1 622.21 1136.65 29.13 o 5 1 1 2645.87 3462.14 51.19 o 6 1 1 91.29 983.61 66.15 o 7 1 1 47.01 93.93 18.19 o 8 1 1 21.24 641.78 36.05 o 9 1 1 0.71 10.83 34.50 o 10 1 1 15.47 159.43 36.07 o 11 1 1 0.20 -34.77 39.28 o 12 1 1 12.72 115.88 38.02 o 13 1 1 25.38 19.37 43.90 o 14 1 1 0.73 131.12 49.59 o -14 2 1 4.50 33.47 48.06 o -13 2 1 82.51 201.85 72.65 o -12 2 1 36.32 112.12 45.81 o -11 2 1 189.77 301.40 33.22 o -10 2 1 2.73 253.84 36.42 o -9 2 1 355.78 458.13 33.36 o -8 2 1 0.04 529.53 26.35 o -7 2 1 304.90 457.03 32.34 o -6 2 1 0.03 773.15 48.25 o -5 2 1 110.54 153.85 24.94 o -4 2 1 363.55 867.91 88.92 o -3 2 1 818.19 1791.52 211.72 o -2 2 1 1340.70 3949.79 83.32 o -1 2 1 97.45 153.09 17.98 o 0 2 1 54.96 52.58 11.33 o 1 2 1 695.17 456.31 31.05 o 2 2 1 7966.57 13016.98 140.27 o 3 2 1 591.49 485.82 21.60 o 4 2 1 1.82 29.47 31.99 o 5 2 1 2298.88 2660.20 55.19 o 6 2 1 618.97 868.38 40.66 o 7 2 1 1640.45 2135.45 40.92 o 8 2 1 49.18 177.65 37.27 o 9 2 1 1013.27 959.12 46.01 o 10 2 1 75.34 65.12 26.25 o 11 2 1 659.90 895.56 48.14 o 12 2 1 22.08 82.75 42.68 o 13 2 1 153.77 350.17 51.60 o 14 2 1 7.94 22.40 48.50 o -14 3 1 8.04 66.15 64.52 o -13 3 1 26.34 154.10 42.96 o -12 3 1 19.51 138.71 64.52 o -11 3 1 267.60 393.33 33.85 o -10 3 1 16.00 61.85 27.62 o -9 3 1 112.89 199.86 25.76 o -8 3 1 4.70 49.36 28.26 o -7 3 1 3618.59 5429.53 110.61 o -6 3 1 694.00 685.26 42.29 o -5 3 1 3675.46 5397.96 123.08 o -4 3 1 189.02 230.31 27.11 o -3 3 1 4266.02 6343.71 219.72 o -2 3 1 1048.11 912.51 44.22 o -1 3 1 7816.90 10402.08 171.08 o 0 3 1 364.27 630.64 12.61 o 1 3 1 4178.35 4181.25 122.89 o 2 3 1 617.83 1130.67 38.64 o 3 3 1 2656.77 4970.13 83.05 o 4 3 1 1172.11 1889.55 40.94 o 5 3 1 1344.12 2476.10 52.52 o 6 3 1 1598.08 2138.21 50.61 o 7 3 1 353.76 771.50 35.81 o 8 3 1 80.30 356.76 46.36 o 9 3 1 47.79 16.96 26.39 o 10 3 1 0.73 171.80 42.67 o 11 3 1 19.67 71.75 30.22 o 12 3 1 1.17 240.44 44.04 o 13 3 1 14.88 31.81 40.98 o 14 3 1 11.39 54.42 49.59 o -14 4 1 0.60 4.70 43.85 o -13 4 1 36.48 88.14 58.35 o -12 4 1 55.25 153.62 37.40 o -11 4 1 22.61 132.29 32.98 o -10 4 1 13.39 219.93 30.10 o -9 4 1 76.88 98.75 32.58 o -8 4 1 1316.40 2389.53 60.56 o -7 4 1 2.31 139.89 29.71 o -6 4 1 757.45 1865.06 57.47 o -5 4 1 0.00 5.98 26.33 o -4 4 1 1583.25 1975.63 48.07 o -3 4 1 538.63 894.34 21.68 o -2 4 1 139.75 262.89 17.69 o -1 4 1 1824.34 2998.84 46.68 o 0 4 1 94.19 71.48 10.11 o 1 4 1 3157.35 4441.91 74.95 o 2 4 1 7319.24 9351.30 84.29 o 3 4 1 906.30 1048.95 24.96 o 4 4 1 1373.38 1610.90 38.71 o 5 4 1 61.35 6.23 24.23 o 6 4 1 1428.14 3070.72 136.09 o 7 4 1 1980.65 2367.19 55.97 o 8 4 1 727.04 1395.11 47.73 o 9 4 1 14.89 25.75 32.04 o 10 4 1 6.25 27.67 28.03 o 11 4 1 81.67 165.11 31.85 o 12 4 1 83.19 138.49 33.94 o 13 4 1 77.46 259.76 38.73 o 14 4 1 0.97 -55.40 55.40 o -13 5 1 34.65 70.71 36.00 o -12 5 1 18.40 69.11 35.06 o -11 5 1 140.44 315.93 35.17 o -10 5 1 15.96 82.21 63.31 o -9 5 1 72.81 147.66 33.01 o -8 5 1 6.73 37.28 28.87 o -7 5 1 2283.34 3633.37 66.14 o -6 5 1 807.32 1046.37 42.44 o -5 5 1 1141.54 2272.48 68.45 o -4 5 1 592.34 370.87 17.72 o -3 5 1 390.01 386.27 25.90 o -2 5 1 2232.28 2544.71 31.80 o -1 5 1 1759.02 2909.42 34.85 o 0 5 1 1866.84 2833.32 89.55 o 1 5 1 1932.99 1911.03 36.67 o 2 5 1 1296.14 1208.51 22.51 o 3 5 1 390.25 319.17 15.60 o 4 5 1 23.31 24.73 16.26 o 5 5 1 670.52 1090.68 67.78 o 6 5 1 131.78 317.16 26.00 o 7 5 1 376.24 1342.12 47.32 o 8 5 1 1.16 32.16 31.41 o 9 5 1 33.90 57.66 37.16 o 10 5 1 8.25 -4.34 38.34 o 11 5 1 1.12 121.82 36.02 o 12 5 1 22.44 119.29 40.24 o 13 5 1 0.11 7.63 38.19 o -13 6 1 2.84 -38.41 52.71 o -12 6 1 47.12 192.59 36.54 o -11 6 1 31.10 71.45 36.10 o -10 6 1 37.74 234.73 38.71 o -9 6 1 9.99 36.17 27.97 o -8 6 1 16.63 108.48 28.59 o -7 6 1 76.11 122.28 25.72 o -6 6 1 2.02 174.45 24.02 o -5 6 1 46.27 220.50 23.40 o -4 6 1 148.62 197.81 18.77 o -3 6 1 18.52 66.03 15.02 o -2 6 1 853.04 982.30 30.65 o -1 6 1 2.11 23.21 12.80 o 0 6 1 401.81 558.55 16.94 o 1 6 1 734.35 1159.14 23.00 o 2 6 1 136.39 92.94 13.07 o 3 6 1 493.72 540.38 31.27 o 4 6 1 580.76 975.24 25.29 o 5 6 1 527.37 908.87 24.95 o 6 6 1 392.50 948.52 30.14 o 7 6 1 242.55 272.45 43.90 o 8 6 1 267.17 372.69 28.14 o 9 6 1 8.59 7.17 32.27 o 10 6 1 97.53 338.20 54.54 o 11 6 1 6.60 -37.66 39.03 o 12 6 1 59.07 76.57 45.00 o 13 6 1 5.68 -55.23 55.23 o -12 7 1 19.73 43.55 46.54 o -11 7 1 21.45 109.66 48.53 o -10 7 1 36.70 117.67 45.89 o -9 7 1 59.72 211.44 41.32 o -8 7 1 50.27 50.36 29.58 o -7 7 1 53.58 172.66 29.36 o -6 7 1 138.53 354.44 30.51 o -5 7 1 179.21 244.51 25.77 o -4 7 1 576.22 858.92 30.42 o -3 7 1 191.55 328.61 24.35 o -2 7 1 490.01 1023.30 28.15 o -1 7 1 83.99 428.23 22.93 o 0 7 1 1218.44 1672.44 35.37 o 1 7 1 858.36 1290.27 52.51 o 2 7 1 362.45 573.33 28.80 o 3 7 1 24.49 57.58 20.96 o 4 7 1 409.97 471.83 29.17 o 5 7 1 9.10 38.51 24.13 o 6 7 1 21.33 150.99 27.57 o 7 7 1 42.77 151.74 35.07 o 8 7 1 1.33 38.02 38.51 o 9 7 1 13.14 137.71 39.49 o 10 7 1 0.14 22.17 67.50 o 11 7 1 0.22 46.13 53.68 o 12 7 1 0.02 10.78 47.42 o -11 8 1 12.79 30.94 54.08 o -10 8 1 28.62 187.09 128.77 o -9 8 1 2.32 9.76 60.72 o -8 8 1 8.62 144.37 38.84 o -7 8 1 39.40 136.41 35.04 o -6 8 1 24.69 106.69 62.26 o -5 8 1 33.19 253.70 29.09 o -4 8 1 23.46 7.07 25.51 o -3 8 1 68.50 144.63 24.47 o -2 8 1 44.89 47.64 24.60 o -1 8 1 572.11 713.52 37.25 o 0 8 1 292.80 313.54 24.90 o 1 8 1 132.98 121.61 38.97 o 2 8 1 17.66 53.83 21.94 o 3 8 1 8.46 20.59 23.04 o 4 8 1 81.49 219.02 26.96 o 5 8 1 24.84 58.46 30.07 o 6 8 1 376.89 659.40 74.82 o 7 8 1 7.00 16.92 34.06 o 8 8 1 87.16 324.32 44.04 o 9 8 1 10.30 44.41 60.72 o 10 8 1 69.24 323.86 106.81 o 11 8 1 4.28 -22.23 52.07 o -10 9 1 9.57 14.06 52.89 o -9 9 1 9.33 50.31 45.55 o -8 9 1 114.54 288.76 45.46 o -7 9 1 13.65 76.55 41.47 o -6 9 1 252.26 433.66 41.21 o -5 9 1 15.23 33.40 29.87 o -4 9 1 56.83 185.13 39.67 o -3 9 1 10.22 42.55 27.10 o -2 9 1 11.11 42.18 27.11 o -1 9 1 1.45 32.86 24.13 o 0 9 1 291.17 348.85 26.19 o 1 9 1 57.70 155.27 24.39 o 2 9 1 2.89 63.48 24.49 o 3 9 1 0.06 -24.67 26.79 o 4 9 1 35.43 44.81 28.73 o 5 9 1 1.82 27.19 35.56 o 6 9 1 18.03 27.97 39.05 o 7 9 1 15.28 102.21 41.32 o 8 9 1 1.25 -3.06 44.33 o 9 9 1 0.75 76.33 47.42 o 10 9 1 0.46 23.63 51.30 o -8 10 1 1.56 48.07 50.59 o -7 10 1 7.55 63.59 45.06 o -6 10 1 1.53 4.48 39.67 o -5 10 1 1.26 135.33 42.46 o -4 10 1 0.97 25.90 34.18 o -3 10 1 3.13 27.99 31.29 o -2 10 1 17.72 78.34 43.13 o -1 10 1 31.50 63.88 30.75 o 0 10 1 154.05 316.07 28.83 o 1 10 1 0.18 2.21 25.75 o 2 10 1 130.23 341.69 28.87 o 3 10 1 6.28 63.06 35.95 o 4 10 1 86.68 299.59 48.80 o 5 10 1 0.24 48.87 39.85 o 6 10 1 86.72 296.65 45.06 o 7 10 1 0.62 14.68 44.85 o 8 10 1 14.62 40.80 51.78 o -6 11 1 47.69 127.08 43.69 o -5 11 1 0.46 31.13 44.28 o -4 11 1 60.58 150.46 41.15 o -3 11 1 0.02 -13.99 42.56 o -2 11 1 60.39 174.32 34.88 o -1 11 1 0.14 9.34 32.71 o 0 11 1 40.28 52.08 30.66 o 1 11 1 0.12 29.74 29.00 o 2 11 1 17.84 49.81 36.42 o 3 11 1 9.60 36.10 37.93 o 4 11 1 8.58 22.57 43.10 o 5 11 1 0.15 -26.88 45.00 o 6 11 1 1.76 17.06 48.48 o -2 12 1 6.92 -1.49 39.60 o -1 12 1 0.08 -34.72 34.72 o 0 12 1 3.76 50.52 37.22 o 1 12 1 0.03 18.67 39.51 o 2 12 1 6.70 55.65 41.20 o -14 0 2 98.27 260.79 72.11 o -12 0 2 84.27 144.76 60.18 o -10 0 2 39.70 146.93 39.58 o -8 0 2 326.69 943.40 48.80 o -6 0 2 6804.02 6797.36 159.94 o -4 0 2 6867.19 4655.73 108.44 o -2 0 2 7255.68 3385.94 76.99 o 0 0 2 26324.56 19387.29 280.36 o 2 0 2 651.20 579.65 45.48 o 4 0 2 0.14 -12.47 24.94 o 6 0 2 327.70 407.72 31.45 o 8 0 2 0.75 -36.87 36.87 o 10 0 2 0.83 -1.08 51.51 o 12 0 2 1.82 -7.05 54.22 o 14 0 2 42.48 92.71 77.53 o -14 1 2 9.96 -28.18 50.60 o -13 1 2 0.89 180.23 43.92 o -12 1 2 4.47 -22.32 40.41 o -11 1 2 2.19 225.47 58.28 o -10 1 2 1.35 -20.58 36.11 o -9 1 2 88.55 593.76 37.90 o -8 1 2 82.08 189.99 29.30 o -7 1 2 108.34 239.24 28.25 o -6 1 2 1061.26 1143.81 25.80 o -5 1 2 1808.50 3411.32 53.65 o -4 1 2 2045.34 2202.27 43.50 o -3 1 2 611.32 660.99 24.13 o -2 1 2 51.36 4.63 10.68 o -1 1 2 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