#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180894 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/34/2103495.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103495_Fobs loop_ _publ_author_name 'Langkilde, Annette' 'Oddershede, Jette' 'Larsen, Sine' _publ_section_title ; Diastereomeric salts of lactic acid and 1-phenylethylamine, their structures and relative stabilities ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 1044 _journal_page_last 1050 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.8465 _cell_length_b 6.9702 _cell_length_c 24.2478 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.7983 _cod_data_source_file os0096Rsup2.hkl _cod_data_source_block R #BEGIN Tags that were not found in dictionaries: _shelx_refln_list_code 4 _shelx_f_calc_maximum 107.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 339.38 299.27 6.15 o 4 0 0 400.58 382.53 7.82 o 6 0 0 2.41 2.16 0.45 o 8 0 0 36.57 32.90 0.99 o 1 1 0 253.23 224.09 4.58 o 2 1 0 392.03 448.86 8.99 o 3 1 0 655.21 627.56 12.67 o 4 1 0 423.71 440.20 8.93 o 5 1 0 395.99 408.74 8.34 o 6 1 0 153.73 152.51 3.42 o 7 1 0 0.01 0.24 0.36 o 8 1 0 38.23 38.11 1.08 o 0 2 0 360.58 334.47 6.79 o 1 2 0 1105.81 1180.24 23.05 o 2 2 0 101.85 124.08 2.50 o 3 2 0 9.70 7.49 0.40 o 4 2 0 56.81 61.60 1.52 o 5 2 0 247.86 247.01 5.02 o 6 2 0 161.32 166.05 3.68 o 7 2 0 101.54 105.42 2.47 o 8 2 0 28.83 29.15 0.86 o 1 3 0 2.00 1.91 0.26 o 2 3 0 0.21 0.30 0.24 o 3 3 0 24.49 29.59 0.89 o 4 3 0 136.84 136.03 2.94 o 5 3 0 6.92 7.01 0.56 o 6 3 0 21.90 21.44 0.94 o 7 3 0 10.66 12.21 0.62 o 8 3 0 81.09 83.33 1.79 o 0 4 0 649.02 732.36 14.10 o 1 4 0 1031.76 1099.95 21.81 o 2 4 0 713.68 753.12 14.53 o 3 4 0 552.47 640.47 13.19 o 4 4 0 22.84 29.35 1.04 o 5 4 0 110.03 122.12 2.88 o 6 4 0 32.47 32.91 1.13 o 7 4 0 107.39 101.58 2.25 o 1 5 0 91.55 91.26 2.14 o 2 5 0 21.81 18.25 0.79 o 3 5 0 1601.31 1764.75 35.24 o 4 5 0 90.57 93.55 2.35 o 5 5 0 50.86 52.94 1.54 o 6 5 0 31.08 28.42 0.97 o 7 5 0 3.38 3.25 0.29 o 0 6 0 1350.08 1277.56 26.52 o 1 6 0 25.04 25.02 1.02 o 2 6 0 58.01 71.19 1.94 o 3 6 0 272.42 289.76 5.92 o 4 6 0 48.00 62.42 1.71 o 5 6 0 9.63 12.96 0.64 o 6 6 0 4.60 4.14 0.34 o 1 7 0 6.49 7.23 0.59 o 2 7 0 25.96 26.67 1.01 o 3 7 0 5.28 6.21 0.51 o 4 7 0 2.59 2.05 0.36 o 5 7 0 3.13 3.07 0.30 o 0 8 0 144.15 144.64 3.11 o 1 8 0 33.02 33.72 1.02 o 2 8 0 14.85 13.88 0.60 o 3 8 0 0.13 0.15 0.25 o 1 0 1 228.61 191.42 3.83 o 2 0 1 399.59 371.32 7.46 o 3 0 1 585.13 511.12 10.44 o 4 0 1 102.19 99.43 2.14 o 5 0 1 969.64 913.90 18.82 o 6 0 1 169.67 167.57 3.69 o 7 0 1 2.29 2.00 0.41 o 8 0 1 37.93 34.16 1.02 o -8 1 1 101.00 96.08 2.14 o -7 1 1 13.09 13.92 0.73 o -6 1 1 105.42 104.97 2.55 o -5 1 1 48.90 44.66 1.28 o -4 1 1 306.68 300.66 6.13 o -3 1 1 213.27 232.96 4.74 o -2 1 1 3338.32 3550.71 65.78 o -1 1 1 3696.79 3918.09 71.86 o 0 1 1 59.25 55.78 1.11 o 1 1 1 3703.26 3903.10 71.61 o 2 1 1 3338.35 3566.11 65.77 o 3 1 1 216.84 237.38 4.82 o 4 1 1 306.07 297.40 6.03 o 5 1 1 48.61 45.12 1.29 o 6 1 1 105.22 105.75 2.57 o 7 1 1 13.24 14.58 0.75 o 8 1 1 102.24 96.44 2.15 o -8 2 1 1.37 2.10 0.30 o -7 2 1 6.72 8.02 0.57 o -6 2 1 149.91 151.72 3.42 o -5 2 1 40.19 46.04 1.34 o -4 2 1 110.87 121.52 2.61 o -3 2 1 1588.69 1798.47 35.72 o -2 2 1 159.59 189.93 3.86 o -1 2 1 286.48 296.62 6.12 o 0 2 1 1628.02 1547.41 29.50 o 1 2 1 290.07 296.18 6.11 o 2 2 1 160.34 191.29 3.92 o 3 2 1 1593.26 1789.01 35.63 o 4 2 1 108.27 121.15 2.60 o 5 2 1 40.69 46.46 1.35 o 6 2 1 148.94 148.12 3.35 o 7 2 1 6.47 8.34 0.57 o 8 2 1 1.51 2.32 0.31 o -8 3 1 6.62 6.03 0.35 o -7 3 1 16.37 16.97 0.72 o -6 3 1 110.27 106.36 2.57 o -5 3 1 57.17 57.05 1.59 o -4 3 1 0.80 2.20 0.37 o -3 3 1 43.22 38.88 1.07 o -2 3 1 267.83 295.06 5.96 o -1 3 1 416.03 456.52 9.55 o 0 3 1 86.12 80.16 1.68 o 1 3 1 420.52 464.57 9.68 o 2 3 1 271.96 298.25 6.12 o 3 3 1 42.53 37.22 1.04 o 4 3 1 0.78 1.85 0.37 o 5 3 1 56.66 57.30 1.60 o 6 3 1 111.32 108.00 2.60 o 7 3 1 16.08 16.87 0.72 o 8 3 1 6.53 6.21 0.36 o -7 4 1 39.05 40.33 1.12 o -6 4 1 169.05 170.39 3.67 o -5 4 1 175.33 174.28 3.83 o -4 4 1 9.71 11.84 0.67 o -3 4 1 192.25 202.72 4.14 o -2 4 1 47.14 48.52 1.28 o -1 4 1 182.39 220.05 4.47 o 0 4 1 1127.76 1245.00 24.35 o 1 4 1 184.44 221.20 4.50 o 2 4 1 46.83 48.90 1.28 o 3 4 1 193.22 204.53 4.18 o 4 4 1 9.45 10.82 0.65 o 5 4 1 175.49 173.45 3.82 o 6 4 1 169.67 170.05 3.66 o 7 4 1 39.03 38.54 1.09 o -7 5 1 21.97 21.29 0.64 o -6 5 1 39.54 40.68 1.20 o -5 5 1 35.22 40.25 1.29 o -4 5 1 124.42 123.46 2.90 o -3 5 1 49.21 50.17 1.47 o -2 5 1 155.83 161.69 3.47 o -1 5 1 102.40 106.94 2.43 o 0 5 1 318.00 301.57 6.16 o 1 5 1 104.11 105.94 2.41 o 2 5 1 156.86 165.04 3.53 o 3 5 1 49.66 51.92 1.50 o 4 5 1 125.26 124.75 2.93 o 5 5 1 35.35 40.55 1.30 o 6 5 1 39.01 39.97 1.19 o 7 5 1 21.97 21.58 0.64 o -6 6 1 24.09 23.87 0.74 o -5 6 1 34.62 35.96 1.12 o -4 6 1 24.44 23.33 0.94 o -3 6 1 120.90 141.48 3.24 o -2 6 1 133.99 139.36 3.21 o -1 6 1 215.67 211.59 4.51 o 0 6 1 92.43 93.50 2.35 o 1 6 1 211.21 208.32 4.45 o 2 6 1 132.67 140.48 3.22 o 3 6 1 120.61 141.55 3.24 o 4 6 1 24.66 22.98 0.93 o 5 6 1 34.10 35.83 1.11 o 6 6 1 23.95 23.62 0.73 o -5 7 1 59.38 61.03 1.40 o -4 7 1 39.89 40.72 1.16 o -3 7 1 56.26 59.51 1.58 o -2 7 1 62.48 63.50 1.73 o -1 7 1 112.48 105.60 2.55 o 0 7 1 30.23 29.18 1.09 o 1 7 1 110.96 105.01 2.53 o 2 7 1 63.07 62.68 1.71 o 3 7 1 55.73 58.47 1.56 o 4 7 1 40.16 42.44 1.19 o 5 7 1 59.98 62.04 1.41 o -3 8 1 6.32 5.75 0.38 o -2 8 1 1.45 0.82 0.32 o -1 8 1 1.03 1.14 0.34 o 0 8 1 17.61 16.52 0.70 o 1 8 1 1.10 1.02 0.34 o 2 8 1 1.46 1.09 0.32 o 3 8 1 6.40 5.90 0.38 o 0 0 2 3380.82 2930.91 53.40 o 1 0 2 3369.84 3513.62 63.91 o 2 0 2 927.32 840.34 16.76 o 3 0 2 673.20 645.43 12.88 o 4 0 2 64.23 75.36 1.71 o 5 0 2 105.30 113.01 2.53 o 6 0 2 2.59 2.93 0.47 o 7 0 2 91.55 88.47 2.20 o 8 0 2 98.25 94.26 2.13 o -8 1 2 55.03 50.82 1.31 o -7 1 2 28.11 28.56 1.05 o -6 1 2 171.22 170.13 3.74 o -5 1 2 229.62 221.97 4.51 o -4 1 2 245.88 254.75 5.17 o -3 1 2 888.68 864.42 16.96 o -2 1 2 1908.14 1963.98 37.29 o -1 1 2 8471.25 9531.49 173.25 o 0 1 2 1837.95 1683.06 31.25 o 1 1 2 8454.25 9529.46 173.23 o 2 1 2 1918.15 1977.19 37.55 o 3 1 2 885.38 844.51 16.59 o 4 1 2 246.78 255.54 5.18 o 5 1 2 233.42 223.97 4.58 o 6 1 2 171.97 169.16 3.73 o 7 1 2 28.03 28.32 1.04 o 8 1 2 55.24 51.01 1.31 o -8 2 2 48.73 48.28 1.21 o -7 2 2 4.96 5.59 0.50 o -6 2 2 14.66 13.91 0.77 o -5 2 2 69.06 72.40 1.84 o -4 2 2 5.24 4.44 0.39 o -3 2 2 87.33 87.35 1.88 o -2 2 2 486.32 509.24 10.36 o -1 2 2 4119.23 4553.54 83.96 o 0 2 2 11.61 9.05 0.33 o 1 2 2 4119.93 4551.83 83.93 o 2 2 2 486.26 506.22 10.30 o 3 2 2 88.31 89.18 1.91 o 4 2 2 4.83 3.81 0.38 o 5 2 2 69.36 71.25 1.82 o 6 2 2 14.82 13.61 0.76 o 7 2 2 4.85 5.37 0.50 o 8 2 2 48.47 48.16 1.21 o -8 3 2 25.34 24.52 0.70 o -7 3 2 119.78 116.27 2.60 o -6 3 2 18.14 18.21 0.86 o -5 3 2 307.66 311.73 6.33 o -4 3 2 103.26 98.60 2.27 o -3 3 2 268.61 287.51 5.85 o -2 3 2 532.81 598.52 12.42 o -1 3 2 287.98 309.62 6.36 o 0 3 2 303.36 293.92 6.03 o 1 3 2 287.75 315.32 6.43 o 2 3 2 531.38 601.37 12.47 o 3 3 2 269.25 286.90 5.84 o 4 3 2 101.81 95.86 2.22 o 5 3 2 309.07 314.57 6.41 o 6 3 2 18.22 18.48 0.87 o 7 3 2 121.13 118.37 2.63 o 8 3 2 24.91 23.25 0.68 o -7 4 2 7.42 6.09 0.44 o -6 4 2 121.78 119.80 2.75 o -5 4 2 60.99 66.88 1.85 o -4 4 2 101.86 115.69 2.67 o -3 4 2 74.04 77.67 1.89 o -2 4 2 16.61 16.70 0.67 o -1 4 2 615.38 685.05 14.12 o 0 4 2 573.47 614.65 12.50 o 1 4 2 615.76 685.09 14.34 o 2 4 2 16.48 15.96 0.65 o 3 4 2 75.24 80.01 1.93 o 4 4 2 101.75 114.19 2.64 o 5 4 2 60.56 65.67 1.83 o 6 4 2 123.46 122.78 2.80 o 7 4 2 7.65 7.21 0.45 o -7 5 2 17.76 18.02 0.57 o -6 5 2 14.78 12.94 0.64 o -5 5 2 56.25 58.92 1.65 o -4 5 2 57.98 66.41 1.85 o -3 5 2 96.05 94.43 2.30 o -2 5 2 1318.34 1464.71 29.49 o -1 5 2 133.76 123.21 2.73 o 0 5 2 823.82 849.33 17.33 o 1 5 2 133.16 122.85 2.72 o 2 5 2 1318.25 1452.19 29.23 o 3 5 2 96.91 96.66 2.34 o 4 5 2 59.08 68.57 1.88 o 5 5 2 55.65 57.18 1.62 o 6 5 2 14.62 11.85 0.62 o 7 5 2 17.47 18.16 0.57 o -6 6 2 12.20 11.75 0.49 o -5 6 2 35.90 36.34 1.12 o -4 6 2 132.05 143.31 3.19 o -3 6 2 72.82 84.66 2.18 o -2 6 2 77.02 85.09 2.20 o -1 6 2 114.00 113.77 2.73 o 0 6 2 299.35 274.95 5.68 o 1 6 2 113.21 112.81 2.70 o 2 6 2 77.33 83.03 2.16 o 3 6 2 73.38 85.99 2.21 o 4 6 2 131.64 144.02 3.21 o 5 6 2 36.24 35.81 1.11 o 6 6 2 11.89 11.74 0.49 o -5 7 2 10.62 7.96 0.40 o -4 7 2 40.03 44.53 1.22 o -3 7 2 53.30 50.07 1.40 o -2 7 2 156.91 153.57 3.39 o -1 7 2 117.71 102.62 2.49 o 0 7 2 18.51 22.34 0.94 o 1 7 2 118.72 110.19 2.63 o 2 7 2 157.04 159.16 3.49 o 3 7 2 52.27 51.15 1.42 o 4 7 2 40.44 44.61 1.23 o 5 7 2 10.09 7.61 0.39 o -3 8 2 10.13 9.98 0.46 o -2 8 2 3.36 2.61 0.36 o -1 8 2 108.15 103.64 2.33 o 0 8 2 19.20 19.36 0.75 o 1 8 2 108.66 97.88 2.23 o 2 8 2 3.65 3.39 0.37 o 3 8 2 10.07 10.60 0.48 o 1 0 3 1719.47 1633.42 30.36 o 2 0 3 547.80 525.32 10.31 o 3 0 3 7.44 8.29 0.38 o 4 0 3 0.27 0.96 0.27 o 5 0 3 399.93 380.99 7.77 o 6 0 3 472.45 461.80 9.34 o 7 0 3 55.72 51.40 1.50 o 8 0 3 56.01 52.56 1.35 o -8 1 3 173.88 167.47 3.43 o -7 1 3 158.92 156.24 3.43 o -6 1 3 7.18 7.11 0.60 o -5 1 3 96.78 93.04 2.19 o -4 1 3 590.06 611.55 12.40 o -3 1 3 51.07 44.42 1.06 o -2 1 3 400.31 388.05 7.94 o -1 1 3 1014.45 960.66 18.59 o 0 1 3 440.10 424.72 8.64 o 1 1 3 1019.44 979.62 18.94 o 2 1 3 399.54 385.82 7.90 o 3 1 3 49.72 43.00 1.04 o 4 1 3 594.69 611.58 12.42 o 5 1 3 96.66 93.12 2.19 o 6 1 3 7.04 7.49 0.60 o 7 1 3 159.65 157.25 3.45 o 8 1 3 173.60 166.65 3.41 o -8 2 3 38.41 37.68 1.01 o -7 2 3 38.22 41.77 1.27 o -6 2 3 53.20 52.61 1.58 o -5 2 3 146.44 160.91 3.46 o -4 2 3 178.61 190.91 3.87 o -3 2 3 302.16 340.16 6.99 o -2 2 3 218.82 224.75 4.54 o -1 2 3 916.26 940.26 18.90 o 0 2 3 13.24 17.70 0.48 o 1 2 3 919.63 944.83 18.95 o 2 2 3 219.02 226.40 4.56 o 3 2 3 300.29 330.99 6.80 o 4 2 3 178.40 188.92 3.85 o 5 2 3 146.31 159.27 3.44 o 6 2 3 52.70 53.51 1.59 o 7 2 3 38.11 40.10 1.25 o 8 2 3 38.97 39.05 1.03 o -8 3 3 6.43 5.43 0.33 o -7 3 3 17.73 16.04 0.69 o -6 3 3 25.08 24.06 0.98 o -5 3 3 168.54 160.28 3.50 o -4 3 3 191.05 192.73 3.98 o -3 3 3 353.39 367.26 7.48 o -2 3 3 696.97 787.25 15.87 o -1 3 3 491.37 551.21 11.33 o 0 3 3 603.16 672.78 13.46 o 1 3 3 493.67 551.11 11.31 o 2 3 3 703.59 795.42 16.00 o 3 3 3 351.23 366.31 7.46 o 4 3 3 190.78 190.95 3.95 o 5 3 3 167.36 158.78 3.47 o 6 3 3 25.31 24.31 0.99 o 7 3 3 17.89 14.76 0.67 o 8 3 3 6.44 5.82 0.34 o -7 4 3 26.03 26.28 0.85 o -6 4 3 7.26 5.78 0.52 o -5 4 3 26.20 22.23 0.96 o -4 4 3 62.03 66.61 1.77 o -3 4 3 129.13 129.64 2.84 o -2 4 3 67.29 69.38 1.67 o -1 4 3 321.74 335.40 6.87 o 0 4 3 79.59 81.22 1.82 o 1 4 3 319.53 327.97 6.72 o 2 4 3 68.07 69.01 1.66 o 3 4 3 129.06 129.40 2.83 o 4 4 3 61.70 65.85 1.75 o 5 4 3 26.74 23.07 0.98 o 6 4 3 6.81 5.13 0.51 o 7 4 3 26.01 26.12 0.84 o -6 5 3 26.50 25.22 0.89 o -5 5 3 58.09 55.76 1.58 o -4 5 3 177.71 180.62 3.94 o -3 5 3 301.23 306.60 6.26 o -2 5 3 77.45 77.33 1.94 o -1 5 3 36.84 42.64 1.25 o 0 5 3 129.67 144.31 3.10 o 1 5 3 36.25 42.05 1.24 o 2 5 3 77.05 77.34 1.94 o 3 5 3 299.85 305.55 6.23 o 4 5 3 178.47 186.17 4.05 o 5 5 3 58.27 55.54 1.58 o 6 5 3 26.67 25.49 0.90 o -6 6 3 55.29 61.00 1.41 o -5 6 3 83.58 91.58 2.15 o -4 6 3 44.93 49.42 1.45 o -3 6 3 97.55 101.58 2.50 o -2 6 3 301.73 302.41 6.19 o -1 6 3 355.84 357.15 7.32 o 0 6 3 189.17 198.30 4.27 o 1 6 3 357.70 359.58 7.35 o 2 6 3 302.17 302.96 6.19 o 3 6 3 98.84 102.37 2.51 o 4 6 3 45.01 49.78 1.46 o 5 6 3 83.50 91.19 2.14 o 6 6 3 55.46 61.46 1.42 o -5 7 3 11.05 10.38 0.44 o -4 7 3 39.94 36.85 1.07 o -3 7 3 33.73 34.60 1.09 o -2 7 3 2.70 1.80 0.45 o -1 7 3 98.38 93.06 2.32 o 0 7 3 349.62 347.61 7.17 o 1 7 3 97.47 97.49 2.39 o 2 7 3 2.49 2.34 0.45 o 3 7 3 32.87 34.15 1.09 o 4 7 3 39.65 37.03 1.07 o 5 7 3 11.47 10.60 0.44 o -3 8 3 9.00 7.62 0.41 o -2 8 3 19.13 18.03 0.67 o -1 8 3 19.70 15.63 0.66 o 0 8 3 1.14 1.53 0.34 o 1 8 3 19.72 16.90 0.69 o 2 8 3 18.98 18.01 0.67 o 3 8 3 9.16 8.99 0.44 o 0 0 4 190.31 154.35 3.13 o 1 0 4 199.77 162.35 3.29 o 2 0 4 2695.41 2760.09 51.50 o 3 0 4 487.68 479.97 9.94 o 4 0 4 81.94 85.93 1.92 o 5 0 4 1.69 0.73 0.34 o 6 0 4 98.51 103.66 2.54 o 7 0 4 4.60 5.43 0.52 o 8 0 4 55.19 51.45 1.32 o -8 1 4 18.20 18.93 0.69 o -7 1 4 179.97 177.33 3.81 o -6 1 4 99.85 99.06 2.45 o -5 1 4 137.42 136.69 2.99 o -4 1 4 67.05 69.12 1.63 o -3 1 4 891.34 897.98 17.66 o -2 1 4 1671.98 1669.04 32.18 o -1 1 4 2046.83 1845.41 34.70 o 0 1 4 1123.97 1065.62 20.43 o 1 1 4 2040.50 1837.48 34.67 o 2 1 4 1665.76 1621.35 31.37 o 3 1 4 893.19 884.62 17.41 o 4 1 4 68.45 70.57 1.66 o 5 1 4 138.08 136.83 2.99 o 6 1 4 99.70 98.33 2.43 o 7 1 4 179.13 176.82 3.79 o 8 1 4 18.39 18.55 0.68 o -8 2 4 5.63 5.15 0.38 o -7 2 4 33.76 31.72 1.07 o -6 2 4 44.51 42.30 1.37 o -5 2 4 46.13 47.94 1.39 o -4 2 4 194.73 193.83 3.95 o -3 2 4 784.17 850.99 17.12 o -2 2 4 1931.02 2107.03 40.56 o -1 2 4 1046.66 1056.56 21.14 o 0 2 4 1521.76 1432.70 27.71 o 1 2 4 1050.02 1056.61 21.10 o 2 2 4 1922.83 2099.02 40.38 o 3 2 4 787.61 849.95 17.07 o 4 2 4 195.56 193.20 3.94 o 5 2 4 45.10 47.45 1.38 o 6 2 4 45.29 42.05 1.37 o 7 2 4 32.64 32.86 1.09 o 8 2 4 5.87 5.75 0.39 o -7 3 4 10.70 12.03 0.60 o -6 3 4 18.32 16.83 0.82 o -5 3 4 93.98 93.26 2.33 o -4 3 4 181.70 190.93 3.95 o -3 3 4 195.06 196.05 3.99 o -2 3 4 79.95 82.25 1.80 o -1 3 4 1443.53 1531.61 30.58 o 0 3 4 1550.35 1630.88 32.25 o 1 3 4 1442.75 1560.34 31.02 o 2 3 4 79.68 81.25 1.79 o 3 3 4 197.43 199.32 4.05 o 4 3 4 180.34 187.80 3.90 o 5 3 4 93.83 92.60 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