#------------------------------------------------------------------------------
#$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $
#$Revision: 691 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103563.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103563_Fobs
loop_
_publ_author_name
'In, Yasuko'
'Fujii, Mayumi'
'Sasada, Yasuhiro'
'Ishida, Toshimasa'
_publ_section_title
;
 Structural studies on C-amidated amino acids and peptides: structures
 of hydrochloride salts of C-amidated Ile, Val, Thr, Ser, Met, Trp, Gln
 and Arg, and comparison with their C-unamidated counterparts
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              72
_journal_page_last               81
_journal_volume                  57
_journal_year                    2001
_space_group_IT_number           4
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 91.730
_cell_angle_gamma                90.000
_cell_length_a                   5.3377
_cell_length_b                   7.4572
_cell_length_c                   9.8990
_exptl_crystal_F_000             164.00
_reflns_d_resolution_high        0.8505
_[local]_cod_data_source_file    oa0030valNH2sup3.hkl
_[local]_cod_data_source_block   valNH2
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' H-VAL-NH2 C5H13N2OCL P21 Z=2'
_shelx_refln_list_code           4
_shelx_F_calc_maximum            57.81
_shelx_F_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 -8 0 74.38 73.06 1.01 o
1 -8 0 12.10 10.62 0.71 o
2 -8 0 35.54 36.22 5.00 o
1 -7 0 2.29 2.33 0.21 o
2 -7 0 142.13 133.89 25.21 o
3 -7 0 20.63 21.63 3.34 o
0 -6 0 46.45 45.22 0.83 o
1 -6 0 35.04 28.51 4.02 o
2 -6 0 2.26 2.09 0.32 o
3 -6 0 74.75 71.44 11.84 o
4 -6 0 9.15 7.31 1.30 o
1 -5 0 96.61 91.04 20.53 o
2 -5 0 77.42 71.21 11.78 o
3 -5 0 26.39 25.70 3.25 o
4 -5 0 9.60 8.27 1.42 o
5 -5 0 0.46 0.47 0.11 o
0 -4 0 1318.92 1167.04 4.48 o
1 -4 0 58.46 64.34 15.58 o
2 -4 0 106.58 116.71 18.33 o
3 -4 0 28.64 28.13 3.99 o
4 -4 0 5.95 6.46 1.05 o
5 -4 0 27.93 29.81 5.69 o
1 -3 0 70.30 59.11 13.04 o
2 -3 0 574.93 693.40 122.81 o
3 -3 0 27.56 29.99 4.56 o
4 -3 0 46.19 47.95 9.15 o
5 -3 0 51.84 52.69 8.15 o
0 -2 0 752.44 610.47 4.17 o
1 -2 0 445.83 400.80 121.58 o
2 -2 0 65.19 78.66 10.13 o
3 -2 0 366.00 456.17 72.29 o
4 -2 0 47.79 53.52 8.53 o
5 -2 0 168.91 172.58 28.38 o
6 -2 0 20.43 19.63 3.08 o
1 -1 0 2255.49 2303.83 510.51 o
2 -1 0 1043.72 1239.66 192.33 o
3 -1 0 52.04 59.25 8.52 o
4 -1 0 225.29 247.83 36.19 o
5 -1 0 14.92 14.83 2.22 o
6 -1 0 24.15 23.47 3.57 o
1 0 0 14.98 17.64 1.35 o
2 0 0 463.85 521.35 97.14 o
3 0 0 131.47 132.18 20.96 o
4 0 0 83.51 96.13 14.15 o
5 0 0 257.12 267.28 47.89 o
6 0 0 9.32 8.03 0.95 o
-2 -8 1 25.87 26.63 3.72 o
-1 -8 1 23.55 23.98 1.47 o
0 -8 1 13.25 12.78 0.76 o
1 -8 1 21.91 20.54 1.90 o
2 -8 1 32.21 30.00 3.99 o
-3 -7 1 29.13 33.15 4.70 o
-2 -7 1 9.45 9.89 1.13 o
-1 -7 1 3.05 2.97 0.79 o
0 -7 1 133.48 129.53 6.34 o
1 -7 1 4.07 3.16 0.43 o
2 -7 1 86.51 86.15 15.76 o
3 -7 1 34.36 32.46 5.87 o
-4 -6 1 25.00 27.27 4.29 o
-3 -6 1 26.07 26.58 3.64 o
-2 -6 1 20.44 23.67 3.05 o
-1 -6 1 215.99 191.90 28.57 o
0 -6 1 0.69 0.52 0.07 o
1 -6 1 336.45 317.25 78.04 o
2 -6 1 1.02 1.07 0.21 o
3 -6 1 41.09 41.75 8.78 o
4 -6 1 64.45 69.92 13.12 o
-5 -5 1 14.96 15.85 2.17 o
-4 -5 1 62.65 55.76 8.18 o
-3 -5 1 419.88 481.86 63.98 o
-2 -5 1 32.52 27.64 2.67 o
-1 -5 1 148.72 142.51 26.31 o
0 -5 1 146.44 132.82 11.24 o
1 -5 1 65.19 60.50 13.97 o
2 -5 1 244.51 241.24 67.31 o
3 -5 1 42.38 45.20 8.79 o
4 -5 1 46.26 46.27 7.95 o
5 -5 1 49.34 52.06 9.31 o
-5 -4 1 81.33 79.44 11.59 o
-4 -4 1 160.09 178.11 25.66 o
-3 -4 1 47.67 45.66 6.04 o
-2 -4 1 524.75 587.78 58.43 o
-1 -4 1 205.71 186.03 38.51 o
0 -4 1 319.75 312.64 45.32 o
1 -4 1 95.85 74.61 22.76 o
2 -4 1 0.67 0.62 0.06 o
3 -4 1 36.12 39.65 8.71 o
4 -4 1 204.89 223.35 45.89 o
5 -4 1 1.37 1.48 0.10 o
-5 -3 1 3.80 5.40 0.57 o
-4 -3 1 62.89 66.16 9.29 o
-3 -3 1 344.92 411.27 46.23 o
-2 -3 1 75.30 92.97 7.69 o
-1 -3 1 340.70 310.08 42.56 o
0 -3 1 182.12 174.19 37.64 o
1 -3 1 22.52 26.91 8.41 o
2 -3 1 587.19 652.32 199.39 o
3 -3 1 95.65 104.67 20.76 o
4 -3 1 89.72 100.75 19.08 o
5 -3 1 49.56 51.64 8.50 o
-6 -2 1 3.26 3.02 0.38 o
-5 -2 1 225.37 245.65 35.06 o
-4 -2 1 0.76 0.82 0.14 o
-3 -2 1 56.68 69.55 10.03 o
-2 -2 1 19.16 30.51 2.22 o
-1 -2 1 2268.92 2400.29 14.15 o
0 -2 1 164.94 149.06 45.23 o
1 -2 1 572.86 537.84 237.86 o
2 -2 1 86.56 108.70 20.54 o
3 -2 1 118.73 141.85 24.71 o
4 -2 1 244.65 259.37 48.15 o
5 -2 1 22.52 22.87 3.08 o
6 -2 1 16.76 16.54 2.39 o
-6 -1 1 37.03 36.27 4.51 o
-5 -1 1 9.30 8.97 1.57 o
-4 -1 1 16.88 17.81 2.67 o
-3 -1 1 545.52 632.44 66.73 o
-2 -1 1 117.06 137.10 10.56 o
-1 -1 1 438.48 548.14 7.00 o
0 -1 1 378.32 271.36 177.82 o
1 -1 1 101.85 110.70 32.26 o
2 -1 1 415.47 440.14 100.54 o
3 -1 1 235.96 261.06 47.24 o
4 -1 1 153.03 164.39 26.28 o
5 -1 1 16.43 15.67 2.58 o
6 -1 1 21.76 19.95 2.81 o
-6 0 1 0.13 0.01 0.14 o
-5 0 1 93.17 96.48 12.90 o
-4 0 1 53.15 56.09 8.43 o
-3 0 1 1.03 1.15 0.07 o
-2 0 1 1173.80 1390.31 240.79 o
-1 0 1 37.78 14.38 13.28 o
0 0 1 623.28 422.45 27.97 o
1 0 1 738.79 778.30 146.87 o
2 0 1 114.94 124.94 19.71 o
3 0 1 32.38 23.04 3.72 o
4 0 1 67.59 68.05 10.71 o
5 0 1 3.56 4.23 0.27 o
6 0 1 7.32 7.29 0.65 o
-2 -8 2 20.78 18.36 1.89 o
-1 -8 2 53.26 50.19 2.21 o
0 -8 2 9.28 8.60 0.38 o
1 -8 2 28.79 27.44 2.10 o
2 -8 2 52.57 52.79 5.60 o
-3 -7 2 26.04 25.88 3.70 o
-2 -7 2 130.55 127.42 11.67 o
-1 -7 2 24.97 25.99 0.79 o
0 -7 2 151.29 148.65 10.58 o
1 -7 2 30.99 31.57 4.24 o
2 -7 2 18.05 18.97 2.76 o
3 -7 2 68.81 72.56 12.53 o
-4 -6 2 32.30 34.97 5.05 o
-3 -6 2 28.14 26.23 2.52 o
-2 -6 2 3.70 3.25 0.46 o
-1 -6 2 385.11 332.08 30.24 o
0 -6 2 5.88 5.68 1.19 o
1 -6 2 248.17 244.21 55.77 o
2 -6 2 28.06 28.14 5.41 o
3 -6 2 23.33 22.56 4.51 o
4 -6 2 51.06 50.97 10.34 o
-5 -5 2 47.93 51.98 8.24 o
-4 -5 2 30.86 33.33 4.46 o
-3 -5 2 63.30 65.61 5.16 o
-2 -5 2 39.64 38.90 2.28 o
-1 -5 2 42.84 39.91 2.70 o
0 -5 2 93.09 75.52 12.04 o
1 -5 2 136.26 129.02 37.06 o
2 -5 2 78.41 71.77 20.66 o
3 -5 2 130.81 135.23 34.87 o
4 -5 2 57.00 55.27 10.88 o
5 -5 2 10.17 10.75 1.79 o
-5 -4 2 0.63 0.84 0.22 o
-4 -4 2 116.53 124.81 15.85 o
-3 -4 2 19.92 19.51 1.54 o
-2 -4 2 6.78 9.17 0.72 o
-1 -4 2 39.46 29.41 3.10 o
0 -4 2 58.84 62.48 12.19 o
1 -4 2 112.86 101.13 34.49 o
2 -4 2 96.64 106.74 32.02 o
3 -4 2 43.27 44.62 10.00 o
4 -4 2 48.43 51.61 10.87 o
5 -4 2 18.72 16.35 3.29 o
-5 -3 2 5.61 6.35 1.00 o
-4 -3 2 126.06 133.26 14.52 o
-3 -3 2 41.83 46.53 4.79 o
-2 -3 2 223.20 256.62 6.03 o
-1 -3 2 394.62 457.17 37.73 o
0 -3 2 22.88 22.96 4.73 o
1 -3 2 637.98 612.03 308.93 o
2 -3 2 58.01 58.65 15.01 o
3 -3 2 140.61 157.07 38.00 o
4 -3 2 7.27 7.30 1.88 o
5 -3 2 3.26 2.70 0.33 o
-6 -2 2 15.26 15.62 2.40 o
-5 -2 2 14.58 14.63 1.98 o
-4 -2 2 18.51 21.22 3.69 o
-3 -2 2 201.42 227.88 21.61 o
-2 -2 2 33.56 37.46 2.05 o
-1 -2 2 1272.94 1415.03 170.79 o
0 -2 2 141.72 127.62 46.68 o
1 -2 2 1068.75 1016.66 541.30 o
2 -2 2 222.26 219.85 68.13 o
3 -2 2 130.07 144.33 32.92 o
4 -2 2 22.97 22.22 4.52 o
5 -2 2 89.97 91.06 16.61 o
-6 -1 2 18.93 18.84 2.22 o
-5 -1 2 28.16 29.09 3.98 o
-4 -1 2 181.64 204.81 19.14 o
-3 -1 2 191.68 224.22 18.39 o
-2 -1 2 295.94 352.33 12.31 o
-1 -1 2 173.64 199.69 5.94 o
0 -1 2 453.83 270.96 83.94 o
1 -1 2 2332.90 1905.30 906.08 o
2 -1 2 389.13 411.52 124.15 o
3 -1 2 452.49 469.25 123.81 o
4 -1 2 156.87 158.77 30.95 o
5 -1 2 15.20 15.07 2.19 o
6 -1 2 76.05 70.90 11.33 o
-6 0 2 102.83 99.44 13.65 o
-5 0 2 0.90 0.91 0.08 o
-4 0 2 315.38 353.16 51.23 o
-3 0 2 4.03 5.57 0.42 o
-2 0 2 8.64 8.53 0.51 o
-1 0 2 188.57 229.17 15.93 o
0 0 2 726.19 577.24 35.66 o
1 0 2 201.07 214.37 23.91 o
2 0 2 745.94 816.17 135.37 o
3 0 2 333.13 342.21 67.09 o
4 0 2 70.98 70.86 11.89 o
5 0 2 135.39 136.49 22.84 o
6 0 2 0.04 0.10 0.10 o
-2 -8 3 26.00 26.95 2.25 o
-1 -8 3 2.74 2.99 0.16 o
0 -8 3 18.58 19.60 1.17 o
1 -8 3 3.63 3.18 0.34 o
-3 -7 3 5.31 6.07 0.35 o
-2 -7 3 62.08 63.62 2.74 o
-1 -7 3 5.62 6.82 0.32 o
0 -7 3 8.63 8.28 0.41 o
1 -7 3 4.68 5.19 0.31 o
2 -7 3 32.62 31.01 4.22 o
3 -7 3 27.70 27.33 4.25 o
-4 -6 3 4.20 4.39 0.73 o
-3 -6 3 104.38 104.28 7.16 o
-2 -6 3 12.78 16.65 0.54 o
-1 -6 3 46.41 39.95 0.58 o
0 -6 3 20.72 20.34 1.96 o
1 -6 3 96.97 93.54 17.41 o
2 -6 3 24.23 24.04 3.98 o
3 -6 3 52.69 53.10 10.86 o
4 -6 3 1.90 2.16 0.65 o
-4 -5 3 32.27 31.59 3.30 o
-3 -5 3 14.56 16.45 2.06 o
-2 -5 3 144.73 145.83 1.76 o
-1 -5 3 55.49 55.12 0.61 o
0 -5 3 42.95 42.48 6.78 o
1 -5 3 118.20 122.73 31.31 o
2 -5 3 214.03 205.95 61.60 o
3 -5 3 42.29 39.63 10.35 o
4 -5 3 36.20 34.97 8.26 o
-5 -4 3 8.85 8.37 1.47 o
-4 -4 3 44.66 44.12 4.72 o
-3 -4 3 43.96 46.54 4.20 o
-2 -4 3 241.38 257.49 7.66 o
-1 -4 3 125.20 128.02 1.54 o
0 -4 3 781.30 840.84 310.53 o
1 -4 3 29.74 27.81 6.77 o
2 -4 3 72.33 73.69 22.23 o
3 -4 3 111.13 100.75 27.04 o
4 -4 3 3.04 3.27 0.74 o
5 -4 3 78.70 76.95 15.78 o
-5 -3 3 26.18 26.12 4.25 o
-4 -3 3 203.07 221.01 21.89 o
-3 -3 3 13.39 15.71 1.91 o
-2 -3 3 570.32 674.10 20.53 o
-1 -3 3 420.44 415.16 46.86 o
0 -3 3 287.39 298.33 100.87 o
1 -3 3 213.95 184.71 67.95 o
2 -3 3 209.20 198.74 74.71 o
3 -3 3 57.35 63.16 13.56 o
4 -3 3 85.07 83.11 19.78 o
5 -3 3 9.48 9.05 2.21 o
-5 -2 3 205.31 212.18 23.20 o
-4 -2 3 122.44 128.01 13.76 o
-3 -2 3 319.80 362.71 23.77 o
-2 -2 3 190.13 202.83 0.98 o
-1 -2 3 322.54 309.36 11.87 o
0 -2 3 924.90 836.87 235.62 o
1 -2 3 76.27 70.09 21.80 o
2 -2 3 38.33 40.89 10.63 o
3 -2 3 140.67 138.38 38.50 o
4 -2 3 8.57 10.25 1.36 o
5 -2 3 122.71 120.91 25.83 o
-6 -1 3 5.37 5.82 0.78 o
-5 -1 3 9.11 10.47 0.61 o
-4 -1 3 194.18 207.39 20.35 o
-3 -1 3 7.50 7.28 0.74 o
-2 -1 3 566.30 650.08 18.09 o
-1 -1 3 684.11 659.91 7.05 o
0 -1 3 611.54 490.32 45.94 o
1 -1 3 501.85 481.41 149.12 o
2 -1 3 156.90 152.36 37.24 o
3 -1 3 152.46 144.49 36.89 o
4 -1 3 61.08 65.09 11.72 o
5 -1 3 10.96 8.97 1.52 o
-6 0 3 23.69 20.49 2.25 o
-5 0 3 39.98 42.21 5.02 o
-4 0 3 85.55 95.08 10.91 o
-3 0 3 21.44 20.07 2.57 o
-2 0 3 433.99 480.64 43.12 o
-1 0 3 182.30 165.68 8.70 o
0 0 3 3341.89 3067.24 312.54 o
1 0 3 1.37 1.67 0.10 o
2 0 3 149.27 160.52 22.23 o
3 0 3 31.91 25.21 3.39 o
4 0 3 3.32 3.31 0.21 o
5 0 3 223.15 217.25 37.21 o
6 0 3 0.24 0.24 0.22 o
-1 -8 4 24.63 26.18 0.53 o
0 -8 4 29.71 29.02 0.63 o
1 -8 4 76.56 72.81 4.47 o
-3 -7 4 63.11 68.89 5.96 o
-2 -7 4 1.26 1.66 0.18 o
-1 -7 4 6.25 7.06 0.43 o
0 -7 4 114.43 111.88 4.29 o
1 -7 4 11.84 11.54 0.32 o
2 -7 4 130.66 131.35 15.12 o
3 -7 4 25.37 22.68 2.62 o
-4 -6 4 20.98 24.33 2.27 o
-3 -6 4 6.32 6.35 0.69 o
-2 -6 4 17.66 22.70 0.53 o
-1 -6 4 79.42 77.71 3.12 o
0 -6 4 34.62 34.64 2.27 o
1 -6 4 129.42 132.84 20.84 o
2 -6 4 5.02 5.22 0.26 o
3 -6 4 35.86 37.19 6.34 o
-4 -5 4 4.14 3.45 0.40 o
-3 -5 4 165.36 183.12 7.26 o
-2 -5 4 3.87 3.43 0.24 o
-1 -5 4 68.92 70.71 6.39 o
0 -5 4 94.07 89.79 12.71 o
1 -5 4 21.82 20.85 2.43 o
2 -5 4 179.34 176.61 46.88 o
3 -5 4 44.39 41.48 7.42 o
4 -5 4 27.80 28.99 4.56 o
-5 -4 4 23.16 25.25 2.69 o
-4 -4 4 62.13 60.60 4.71 o
-3 -4 4 92.95 92.51 5.14 o
-2 -4 4 127.78 128.55 2.00 o
-1 -4 4 89.48 87.29 1.91 o
0 -4 4 294.78 301.24 72.82 o
1 -4 4 43.45 38.24 9.64 o
2 -4 4 7.05 7.40 1.92 o
3 -4 4 58.66 56.88 14.26 o
4 -4 4 54.63 56.86 13.52 o
5 -4 4 15.39 14.49 2.72 o
-5 -3 4 13.53 12.02 1.51 o
-4 -3 4 46.50 45.49 4.66 o
-3 -3 4 133.13 137.36 7.05 o
-2 -3 4 127.76 131.54 2.79 o
-1 -3 4 24.43 21.46 0.32 o
0 -3 4 43.60 36.08 4.71 o
1 -3 4 24.25 23.97 5.15 o
2 -3 4 309.52 290.52 105.46 o
3 -3 4 16.13 17.56 3.70 o
4 -3 4 14.63 16.81 3.96 o
5 -3 4 31.27 30.79 6.41 o
-5 -2 4 201.70 213.18 19.33 o
-4 -2 4 0.21 0.14 0.19 o
-3 -2 4 37.38 42.68 2.95 o
-2 -2 4 13.41 13.76 0.46 o
-1 -2 4 89.28 81.92 0.57 o
0 -2 4 162.68 138.78 16.86 o
1 -2 4 187.17 178.43 42.26 o
2 -2 4 1.45 2.05 0.50 o
3 -2 4 30.06 32.38 7.48 o
4 -2 4 135.43 128.10 35.12 o
5 -2 4 4.80 4.78 0.95 o
-5 -1 4 1.26 1.30 0.10 o
-4 -1 4 32.42 33.47 3.10 o
-3 -1 4 303.16 325.29 17.65 o
-2 -1 4 53.69 53.64 1.93 o
-1 -1 4 463.91 422.12 6.24 o
0 -1 4 231.11 212.28 13.44 o
1 -1 4 101.56 104.51 17.01 o
2 -1 4 564.33 586.39 142.79 o
3 -1 4 64.16 67.68 14.10 o
4 -1 4 25.94 26.77 5.19 o
5 -1 4 9.46 8.53 1.21 o
-5 0 4 147.23 153.23 16.85 o
-4 0 4 22.64 20.98 1.76 o
-3 0 4 24.29 28.62 2.89 o
-2 0 4 570.24 618.28 50.01 o
-1 0 4 85.10 77.45 2.93 o
0 0 4 2275.71 2280.46 234.73 o
1 0 4 1.59 1.46 0.19 o
2 0 4 100.08 98.53 10.91 o
3 0 4 197.51 183.00 27.04 o
4 0 4 126.83 119.95 19.22 o
5 0 4 13.20 10.91 1.46 o
-2 -7 5 32.52 30.63 2.04 o
-1 -7 5 17.43 18.52 0.37 o
0 -7 5 57.14 54.92 1.20 o
1 -7 5 10.04 9.44 0.44 o
2 -7 5 1.28 1.39 0.09 o
-3 -6 5 10.24 9.75 0.82 o
-2 -6 5 2.85 2.91 0.39 o
-1 -6 5 177.97 171.17 7.45 o
0 -6 5 1.21 1.22 0.10 o
1 -6 5 57.74 60.47 5.06 o
2 -6 5 16.07 15.00 1.00 o
3 -6 5 20.67 19.74 1.33 o
-4 -5 5 1.38 1.42 0.16 o
-3 -5 5 174.80 173.55 8.75 o
-2 -5 5 71.70 67.72 1.04 o
-1 -5 5 4.16 4.55 0.25 o
0 -5 5 140.26 133.57 15.34 o
1 -5 5 110.11 113.37 16.21 o
2 -5 5 64.59 59.12 9.79 o
3 -5 5 29.79 29.51 3.97 o
4 -5 5 59.03 51.84 6.65 o
-4 -4 5 155.28 164.37 10.99 o
-3 -4 5 8.97 9.70 0.54 o
-2 -4 5 106.08 101.15 3.61 o
-1 -4 5 302.09 282.34 15.99 o
0 -4 5 18.48 20.34 1.95 o
1 -4 5 93.03 85.69 13.59 o
2 -4 5 92.50 92.48 19.49 o
3 -4 5 24.58 23.28 3.86 o
4 -4 5 33.78 33.06 6.05 o
-5 -3 5 15.18 15.02 2.39 o
-4 -3 5 30.07 31.52 2.44 o
-3 -3 5 220.10 220.20 4.32 o
-2 -3 5 251.60 247.56 6.32 o
-1 -3 5 185.80 179.25 9.55 o
0 -3 5 96.78 99.12 8.09 o
1 -3 5 377.67 389.34 90.24 o
2 -3 5 34.18 32.39 6.48 o
3 -3 5 142.04 136.65 36.32 o
4 -3 5 6.42 4.23 1.19 o
5 -3 5 3.14 3.27 0.57 o
-5 -2 5 9.90 9.21 1.23 o
-4 -2 5 4.38 4.11 0.57 o
-3 -2 5 69.85 73.62 3.42 o
-2 -2 5 33.57 35.65 0.60 o
-1 -2 5 866.12 862.39 64.73 o
0 -2 5 83.97 79.86 4.70 o
1 -2 5 37.75 35.97 4.24 o
2 -2 5 193.20 182.67 39.86 o
3 -2 5 56.69 49.31 11.17 o
4 -2 5 95.13 80.98 19.54 o
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