#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/35/2103566.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103566_Fobs
loop_
_publ_author_name
'In, Yasuko'
'Fujii, Mayumi'
'Sasada, Yasuhiro'
'Ishida, Toshimasa'
_publ_section_title
;
 Structural studies on C-amidated amino acids and peptides: structures
 of hydrochloride salts of C-amidated Ile, Val, Thr, Ser, Met, Trp, Gln
 and Arg, and comparison with their C-unamidated counterparts
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              72
_journal_page_last               81
_journal_volume                  57
_journal_year                    2001
_space_group_IT_number           4
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 96.489
_cell_angle_gamma                90.000
_cell_length_a                   7.5910
_cell_length_b                   5.0289
_cell_length_c                   11.7856
_exptl_crystal_F_000             196.00
_reflns_d_resolution_high        0.8345
_[local]_cod_data_source_file    oa0030metNH2sup5.hkl
_[local]_cod_data_source_block   metNH2
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' H-MET-NH2 C5H13N2OSCL Z=2 P21'
_shelx_refln_list_code           4
_shelx_F_calc_maximum            74.78
_shelx_F_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 447.26 502.03 2.32 o
2 0 0 5.48 -1.66 1.66 o
3 0 0 949.21 1209.99 4.59 o
4 0 0 674.77 776.84 7.34 o
5 0 0 41.47 51.26 2.90 o
6 0 0 373.78 461.79 5.03 o
7 0 0 44.76 50.13 6.15 o
8 0 0 11.57 12.11 0.82 o
9 0 0 0.88 -0.07 1.59 o
1 1 0 2545.21 2516.92 68.34 o
2 1 0 345.41 450.12 4.09 o
3 1 0 127.40 143.16 2.51 o
4 1 0 303.00 384.51 6.62 o
5 1 0 88.54 100.13 3.21 o
6 1 0 73.91 76.59 4.14 o
7 1 0 20.30 21.91 1.34 o
8 1 0 61.63 66.94 4.81 o
0 2 0 3409.04 2325.36 8.41 o
1 2 0 524.70 492.61 15.62 o
2 2 0 130.00 145.62 3.34 o
3 2 0 1509.88 1757.16 28.42 o
4 2 0 303.70 335.75 9.00 o
5 2 0 36.29 46.28 3.15 o
6 2 0 72.97 84.91 3.41 o
7 2 0 59.38 70.09 2.86 o
8 2 0 0.06 0.84 1.92 o
1 3 0 481.46 452.54 7.25 o
2 3 0 273.50 275.73 7.17 o
3 3 0 10.70 9.81 0.82 o
4 3 0 82.95 85.83 3.50 o
5 3 0 76.46 87.11 5.32 o
6 3 0 26.23 28.93 3.15 o
7 3 0 18.25 20.58 2.62 o
0 4 0 221.22 173.17 5.32 o
1 4 0 222.77 196.18 3.83 o
2 4 0 138.82 142.71 3.66 o
3 4 0 295.98 302.63 23.20 o
4 4 0 128.02 125.51 12.62 o
5 4 0 27.71 29.41 2.43 o
6 4 0 3.01 2.14 0.75 o
1 5 0 38.67 37.29 2.55 o
2 5 0 53.54 48.32 2.85 o
3 5 0 13.89 15.25 1.47 o
4 5 0 29.95 29.83 6.84 o
5 5 0 81.33 102.08 11.02 o
0 6 0 49.53 65.17 2.92 o
-9 0 1 30.87 31.20 2.60 o
-8 0 1 123.01 144.49 4.60 o
-7 0 1 69.48 83.07 4.59 o
-6 0 1 2.14 1.06 4.21 o
-5 0 1 282.94 354.23 5.79 o
-4 0 1 1364.04 1519.48 8.68 o
-3 0 1 0.18 11.06 1.03 o
-2 0 1 2018.58 2622.17 14.08 o
-1 0 1 33.65 28.95 1.45 o
0 0 1 147.23 111.32 1.05 o
1 0 1 219.40 265.81 2.27 o
2 0 1 496.43 666.00 4.41 o
3 0 1 233.72 249.03 3.91 o
4 0 1 197.71 240.75 4.76 o
5 0 1 27.53 28.77 2.45 o
6 0 1 25.47 34.17 2.85 o
7 0 1 401.38 442.56 6.93 o
8 0 1 63.47 69.23 3.70 o
-8 1 1 12.99 13.19 1.23 o
-7 1 1 71.64 81.50 4.55 o
-6 1 1 55.08 69.04 4.91 o
-5 1 1 162.07 183.46 5.09 o
-4 1 1 818.98 1017.97 7.75 o
-3 1 1 111.16 157.73 3.61 o
-2 1 1 90.66 111.24 3.05 o
-1 1 1 2356.52 2471.42 13.03 o
0 1 1 362.53 257.90 2.65 o
1 1 1 840.71 913.85 4.61 o
2 1 1 3854.25 4174.70 10.64 o
3 1 1 272.68 331.47 4.51 o
4 1 1 8.31 2.54 3.56 o
5 1 1 307.95 352.59 6.03 o
6 1 1 462.06 490.92 7.36 o
7 1 1 5.15 3.35 3.40 o
8 1 1 27.41 30.79 2.06 o
-8 2 1 91.24 104.67 3.80 o
-7 2 1 96.73 106.58 4.50 o
-6 2 1 21.04 26.06 2.34 o
-5 2 1 279.77 334.09 6.43 o
-4 2 1 179.16 212.36 5.13 o
-3 2 1 561.43 675.46 6.55 o
-2 2 1 259.15 309.97 4.49 o
-1 2 1 350.51 312.28 3.97 o
0 2 1 183.21 148.11 3.21 o
1 2 1 714.80 671.03 5.19 o
2 2 1 66.80 75.99 3.41 o
3 2 1 86.63 93.90 4.07 o
4 2 1 7.92 8.19 1.14 o
5 2 1 119.54 135.11 4.91 o
6 2 1 9.96 13.12 1.23 o
7 2 1 62.78 63.97 3.86 o
8 2 1 24.90 27.51 1.77 o
-7 3 1 48.57 41.62 3.61 o
-6 3 1 28.10 34.00 2.50 o
-5 3 1 52.18 64.91 4.77 o
-4 3 1 168.32 194.09 5.59 o
-3 3 1 70.54 85.22 4.44 o
-2 3 1 190.53 171.54 4.60 o
-1 3 1 468.48 400.40 5.57 o
0 3 1 11.11 10.70 1.07 o
1 3 1 283.05 261.37 4.93 o
2 3 1 346.00 311.05 5.36 o
3 3 1 79.66 84.24 4.27 o
4 3 1 22.76 24.23 2.02 o
5 3 1 291.41 286.06 5.98 o
6 3 1 151.23 137.80 4.55 o
7 3 1 15.56 13.90 1.37 o
-6 4 1 76.70 82.68 3.69 o
-5 4 1 76.89 74.80 4.22 o
-4 4 1 52.95 55.94 4.12 o
-3 4 1 204.10 186.49 5.57 o
-2 4 1 28.30 25.56 2.16 o
-1 4 1 67.63 52.57 4.55 o
0 4 1 266.72 233.02 5.73 o
1 4 1 118.76 114.91 4.91 o
2 4 1 0.99 2.21 2.43 o
3 4 1 16.38 17.91 1.65 o
4 4 1 10.40 8.71 1.00 o
5 4 1 101.41 76.27 3.82 o
6 4 1 22.25 15.38 1.30 o
-5 5 1 5.99 8.80 0.83 o
-4 5 1 12.48 13.60 1.30 o
-3 5 1 2.95 2.98 0.97 o
-2 5 1 120.51 105.18 4.32 o
-1 5 1 18.21 14.58 1.30 o
0 5 1 35.08 42.72 3.69 o
1 5 1 62.69 51.02 3.88 o
2 5 1 118.95 82.77 3.89 o
3 5 1 16.93 12.95 1.28 o
4 5 1 35.27 20.45 1.76 o
0 6 1 49.10 76.59 2.88 o
-9 0 2 22.82 18.64 1.56 o
-8 0 2 2.57 1.47 3.35 o
-7 0 2 116.69 133.94 5.08 o
-6 0 2 18.92 28.05 2.74 o
-5 0 2 2.66 -0.07 3.75 o
-4 0 2 30.03 37.26 2.36 o
-3 0 2 117.26 132.57 3.35 o
-2 0 2 890.47 984.03 5.18 o
-1 0 2 60.05 77.65 2.18 o
0 0 2 443.31 349.16 2.43 o
1 0 2 31.81 40.11 2.20 o
2 0 2 58.65 63.46 2.83 o
3 0 2 395.67 453.97 4.81 o
4 0 2 72.45 78.61 4.06 o
5 0 2 468.92 531.62 6.92 o
6 0 2 18.07 14.24 1.36 o
7 0 2 118.93 131.22 4.70 o
8 0 2 78.91 88.34 3.75 o
-8 1 2 98.49 100.91 4.23 o
-7 1 2 50.84 56.68 4.35 o
-6 1 2 180.57 207.93 5.97 o
-5 1 2 276.05 331.84 6.04 o
-4 1 2 22.75 28.92 2.43 o
-3 1 2 396.97 480.96 5.00 o
-2 1 2 3394.23 3506.05 9.71 o
-1 1 2 1356.30 1448.37 11.10 o
0 1 2 125.37 130.67 2.61 o
1 1 2 1989.51 2080.47 13.53 o
2 1 2 875.86 962.21 5.87 o
3 1 2 176.90 214.69 4.21 o
4 1 2 505.20 573.67 6.52 o
5 1 2 126.01 142.01 4.94 o
6 1 2 4.56 6.34 1.31 o
7 1 2 116.64 121.36 4.51 o
8 1 2 5.64 6.18 0.85 o
-8 2 2 13.49 15.40 1.50 o
-7 2 2 62.55 69.59 4.36 o
-6 2 2 16.28 26.45 2.30 o
-5 2 2 74.00 82.51 4.99 o
-4 2 2 80.54 95.17 4.50 o
-3 2 2 216.47 223.17 4.84 o
-2 2 2 75.58 109.33 3.70 o
-1 2 2 189.11 182.05 3.64 o
0 2 2 94.43 87.38 2.95 o
1 2 2 91.13 80.13 3.10 o
2 2 2 343.13 328.27 4.84 o
3 2 2 63.17 87.01 4.09 o
4 2 2 165.23 185.98 4.91 o
5 2 2 85.63 89.31 4.62 o
6 2 2 22.28 19.38 1.86 o
7 2 2 85.16 86.33 3.86 o
8 2 2 105.05 97.13 3.35 o
-7 3 2 53.80 57.30 3.70 o
-6 3 2 44.02 45.93 4.22 o
-5 3 2 165.68 172.24 5.62 o
-4 3 2 82.69 86.14 4.83 o
-3 3 2 232.50 250.09 5.50 o
-2 3 2 323.72 283.43 5.26 o
-1 3 2 308.83 295.81 5.21 o
0 3 2 1.20 4.65 1.04 o
1 3 2 652.86 591.74 6.51 o
2 3 2 205.31 192.93 4.75 o
3 3 2 168.33 150.07 5.00 o
4 3 2 116.06 98.04 4.71 o
5 3 2 41.19 30.82 2.47 o
6 3 2 15.07 19.25 1.63 o
7 3 2 46.97 44.17 2.89 o
-6 4 2 7.94 8.28 0.93 o
-5 4 2 14.19 14.94 1.49 o
-4 4 2 65.73 60.60 4.19 o
-3 4 2 24.07 22.95 2.08 o
-2 4 2 10.38 7.61 1.29 o
-1 4 2 29.54 28.98 2.71 o
0 4 2 82.48 87.82 4.75 o
1 4 2 36.07 36.85 2.74 o
2 4 2 88.87 71.80 4.53 o
3 4 2 69.27 45.69 4.03 o
4 4 2 91.74 61.33 3.74 o
5 4 2 16.13 12.41 1.12 o
6 4 2 35.92 27.69 2.68 o
-5 5 2 4.46 5.11 0.66 o
-4 5 2 89.58 67.15 3.61 o
-3 5 2 21.08 15.30 1.26 o
-2 5 2 90.04 71.79 4.14 o
-1 5 2 46.45 52.15 3.94 o
0 5 2 97.40 108.71 4.40 o
1 5 2 41.29 46.02 3.65 o
2 5 2 129.22 114.29 4.31 o
3 5 2 13.96 12.74 1.23 o
4 5 2 7.53 5.13 0.76 o
-9 0 3 12.24 11.84 1.11 o
-8 0 3 10.86 12.71 1.22 o
-7 0 3 41.47 50.80 4.14 o
-6 0 3 1043.95 1095.59 9.88 o
-5 0 3 17.45 18.06 1.68 o
-4 0 3 0.37 3.53 3.57 o
-3 0 3 917.43 1058.81 6.57 o
-2 0 3 133.66 159.66 3.30 o
-1 0 3 18.51 20.70 1.61 o
0 0 3 5591.88 4845.40 17.51 o
1 0 3 273.77 319.12 3.60 o
2 0 3 45.79 54.36 2.80 o
3 0 3 913.96 933.76 6.79 o
4 0 3 468.72 477.96 6.07 o
5 0 3 11.92 14.07 1.38 o
6 0 3 121.74 136.33 5.39 o
7 0 3 164.75 164.25 4.98 o
8 0 3 4.98 4.82 0.84 o
-8 1 3 16.06 14.85 1.41 o
-7 1 3 173.02 188.41 5.23 o
-6 1 3 247.93 280.77 6.33 o
-5 1 3 157.63 167.39 5.17 o
-4 1 3 574.39 648.15 6.67 o
-3 1 3 520.01 558.39 5.59 o
-2 1 3 42.90 48.66 2.89 o
-1 1 3 92.92 101.34 3.05 o
0 1 3 270.22 288.23 3.45 o
1 1 3 325.22 380.31 4.05 o
2 1 3 242.10 250.28 3.99 o
3 1 3 127.71 159.61 4.33 o
4 1 3 69.20 73.55 4.00 o
5 1 3 63.55 55.47 4.35 o
6 1 3 78.16 72.30 4.74 o
7 1 3 23.59 22.33 2.17 o
8 1 3 23.41 21.34 1.79 o
-8 2 3 23.55 21.63 1.51 o
-7 2 3 15.99 18.80 1.85 o
-6 2 3 239.32 260.05 6.34 o
-5 2 3 42.40 46.75 3.10 o
-4 2 3 54.73 61.38 4.38 o
-3 2 3 997.92 1021.51 7.94 o
-2 2 3 198.03 195.74 4.45 o
-1 2 3 80.25 75.05 3.47 o
0 2 3 1035.73 1027.65 6.53 o
1 2 3 153.47 140.75 3.79 o
2 2 3 129.97 130.93 4.18 o
3 2 3 722.69 672.82 7.02 o
4 2 3 287.98 291.90 5.73 o
5 2 3 37.62 30.53 2.77 o
6 2 3 73.06 63.76 3.92 o
7 2 3 65.05 60.32 3.57 o
8 2 3 15.13 15.89 1.48 o
-7 3 3 138.47 137.13 4.37 o
-6 3 3 50.29 49.21 4.24 o
-5 3 3 125.76 119.29 5.21 o
-4 3 3 84.05 80.97 4.87 o
-3 3 3 231.16 207.30 5.39 o
-2 3 3 192.79 160.46 4.67 o
-1 3 3 221.92 217.46 4.81 o
0 3 3 23.16 22.36 1.77 o
1 3 3 227.97 230.73 4.90 o
2 3 3 63.75 53.41 3.93 o
3 3 3 18.59 14.19 1.34 o
4 3 3 33.48 23.95 2.07 o
5 3 3 0.91 2.58 3.25 o
6 3 3 39.05 32.32 2.15 o
7 3 3 15.45 12.99 1.05 o
-6 4 3 25.47 23.76 2.01 o
-5 4 3 50.28 48.05 3.84 o
-4 4 3 56.91 44.67 3.98 o
-3 4 3 149.45 121.89 4.67 o
-2 4 3 94.29 82.32 4.94 o
-1 4 3 158.37 146.09 5.32 o
0 4 3 101.91 112.11 4.99 o
1 4 3 101.69 107.09 4.96 o
2 4 3 72.53 76.46 4.63 o
3 4 3 165.44 129.83 4.45 o
4 4 3 56.25 39.67 3.41 o
5 4 3 48.48 33.86 3.17 o
6 4 3 10.33 9.83 0.97 o
-4 5 3 3.56 2.38 2.89 o
-3 5 3 32.31 28.64 2.19 o
-2 5 3 187.03 189.70 4.82 o
-1 5 3 48.67 52.08 3.83 o
0 5 3 5.05 7.85 1.02 o
1 5 3 27.16 32.49 2.22 o
2 5 3 5.80 7.45 0.92 o
3 5 3 30.42 27.95 1.95 o
4 5 3 41.32 54.75 2.96 o
-8 0 4 249.62 263.35 5.16 o
-7 0 4 21.99 23.27 1.92 o
-6 0 4 0.10 3.36 1.32 o
-5 0 4 527.49 537.94 7.02 o
-4 0 4 807.73 821.64 7.27 o
-3 0 4 328.56 372.21 4.90 o
-2 0 4 2173.70 2259.15 8.67 o
-1 0 4 1157.51 1061.74 5.74 o
0 0 4 1253.71 1302.32 5.96 o
1 0 4 1333.38 1242.97 6.39 o
2 0 4 1230.24 1201.24 7.06 o
3 0 4 99.44 85.08 3.98 o
4 0 4 14.50 12.47 1.15 o
5 0 4 71.83 63.74 4.61 o
6 0 4 60.86 64.62 4.53 o
7 0 4 70.92 69.73 4.04 o
8 0 4 14.41 15.24 1.30 o
-8 1 4 23.10 25.81 2.12 o
-7 1 4 154.56 156.37 5.14 o
-6 1 4 335.85 330.36 6.80 o
-5 1 4 54.18 61.63 4.57 o
-4 1 4 815.17 840.30 7.65 o
-3 1 4 52.48 65.99 3.88 o
-2 1 4 575.67 587.73 5.31 o
-1 1 4 936.73 972.06 5.95 o
0 1 4 343.60 319.05 3.97 o
1 1 4 22.56 23.18 1.80 o
2 1 4 241.45 230.53 4.34 o
3 1 4 625.78 605.65 6.49 o
4 1 4 119.09 98.96 4.35 o
5 1 4 75.53 67.21 4.62 o
6 1 4 199.83 176.32 5.24 o
7 1 4 5.16 1.91 3.35 o
8 1 4 29.92 30.36 2.65 o
-8 2 4 89.12 96.39 3.76 o
-7 2 4 47.50 47.39 4.03 o
-6 2 4 42.38 42.78 2.88 o
-5 2 4 569.41 552.94 7.82 o
-4 2 4 279.24 267.92 5.78 o
-3 2 4 206.26 192.43 4.94 o
-2 2 4 164.34 155.29 4.46 o
-1 2 4 1106.00 970.49 7.28 o
0 2 4 95.89 120.85 3.85 o
1 2 4 15.20 13.19 1.19 o
2 2 4 378.17 324.60 5.24 o
3 2 4 199.82 169.76 4.69 o
4 2 4 60.69 52.41 4.33 o
5 2 4 51.50 50.06 4.43 o
6 2 4 19.56 19.01 1.71 o
7 2 4 12.08 7.79 0.91 o
-7 3 4 41.78 43.20 3.51 o
-6 3 4 40.81 36.01 2.57 o
-5 3 4 90.64 69.20 4.59 o
-4 3 4 302.99 244.54 6.20 o
-3 3 4 24.76 19.94 1.81 o
-2 3 4 60.55 45.45 4.18 o
-1 3 4 125.98 121.13 4.47 o
0 3 4 301.61 335.66 5.60 o
1 3 4 65.14 61.68 4.21 o
2 3 4 104.46 88.34 4.31 o
3 3 4 67.70 48.93 4.44 o
4 3 4 105.24 68.56 4.49 o
5 3 4 44.00 35.51 3.54 o
6 3 4 89.80 75.76 3.71 o
7 3 4 12.27 11.58 1.11 o
-6 4 4 106.05 96.29 3.74 o
-5 4 4 147.93 112.56 4.35 o
-4 4 4 58.20 44.45 3.93 o
-3 4 4 94.37 83.03 4.42 o
-2 4 4 11.01 15.01 1.50 o
-1 4 4 345.13 383.37 6.89 o
0 4 4 125.68 172.11 5.47 o
1 4 4 43.69 62.83 4.34 o
2 4 4 6.76 3.14 1.08 o
3 4 4 126.47 122.09 4.34 o
4 4 4 18.67 18.46 1.57 o
5 4 4 30.98 29.36 2.93 o
-4 5 4 42.28 50.87 3.18 o
-3 5 4 1.45 2.43 0.91 o
-2 5 4 22.49 23.96 2.19 o
-1 5 4 7.65 7.28 0.98 o
0 5 4 20.40 26.59 2.22 o
1 5 4 45.61 58.95 3.72 o
2 5 4 11.06 12.53 1.10 o
3 5 4 17.00 19.95 1.69 o
4 5 4 19.71 24.21 1.52 o
-8 0 5 0.33 0.08 3.02 o
-7 0 5 75.01 74.38 4.17 o
-6 0 5 174.67 156.48 5.60 o
-5 0 5 2.61 1.66 4.03 o
-4 0 5 513.29 491.77 6.34 o
-3 0 5 8.42 15.18 1.37 o
-2 0 5 1.12 -3.11 3.11 o
-1 0 5 172.20 186.18 3.61 o
0 0 5 1475.03 1566.82 7.32 o
1 0 5 6.08 3.48 0.89 o
2 0 5 382.71 359.54 5.14 o
3 0 5 0.12 -3.28 3.61 o
4 0 5 131.44 114.22 4.68 o
5 0 5 600.61 568.00 7.99 o
6 0 5 7.54 6.82 1.07 o
7 0 5 31.55 28.09 2.22 o
8 0 5 2.06 1.60 0.66 o
-8 1 5 52.45 50.15 3.49 o
-7 1 5 41.02 34.45 2.54 o
-6 1 5 61.58 63.07 5.16 o
-5 1 5 225.99 207.13 5.63 o
-4 1 5 28.68 31.66 2.59 o
-3 1 5 239.19 246.40 5.03 o
-2 1 5 572.07 491.15 5.65 o
-1 1 5 218.79 198.98 4.13 o
0 1 5 147.09 149.85 3.67 o
1 1 5 2688.51 2310.75 10.03 o
2 1 5 166.34 139.77 4.25 o
3 1 5 182.49 164.95 4.62 o
4 1 5 514.95 425.54 6.62 o
5 1 5 264.51 209.86 5.81 o
6 1 5 34.85 39.12 3.72 o
7 1 5 49.58 51.79 3.62 o
-8 2 5 7.65 8.56 0.82 o
-7 2 5 91.13 86.40 4.26 o
-6 2 5 51.24 49.69 4.26 o
-5 2 5 116.43 97.10 5.43 o
-4 2 5 63.21 58.88 4.80 o
-3 2 5 155.58 123.50 4.69 o
-2 2 5 128.76 105.37 4.21 o
-1 2 5 196.44 184.87 4.62 o
0 2 5 217.58 241.69 4.61 o
1 2 5 14.33 12.04 1.10 o
2 2 5 500.62 373.71 5.84 o
3 2 5 44.73 35.70 2.58 o
4 2 5 67.56 46.68 4.42 o
5 2 5 116.89 95.06 4.49 o
6 2 5 35.82 30.18 2.22 o
7 2 5 4.24 1.96 2.76 o
-7 3 5 31.30 30.10 1.99 o
-6 3 5 18.56 17.98 1.60 o
-5 3 5 58.07 44.78 2.77 o
-4 3 5 82.64 50.17 4.95 o
-3 3 5 153.17 107.73 5.05 o
-2 3 5 315.59 275.22 5.89 o
-1 3 5 42.21 52.05 4.26 o
0 3 5 114.76 125.88 4.63 o
1 3 5 381.75 435.19 6.50 o
2 3 5 132.07 126.14 4.80 o
3 3 5 152.00 133.38 5.13 o
4 3 5 216.72 173.83 5.00 o
5 3 5 98.56 92.00 4.15 o
6 3 5 21.70 22.16 1.89 o
-6 4 5 3.67 4.86 0.72 o
-5 4 5 19.12 15.61 1.44 o
-4 4 5 68.14 53.72 4.08 o
-3 4 5 59.31 54.65 4.14 o
-2 4 5 39.98 38.73 2.49 o
-1 4 5 97.96 99.46 4.85 o
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