#------------------------------------------------------------------------------
#$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $
#$Revision: 691 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103567.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103567_Fobs
loop_
_publ_author_name
'In, Yasuko'
'Fujii, Mayumi'
'Sasada, Yasuhiro'
'Ishida, Toshimasa'
_publ_section_title
;
 Structural studies on C-amidated amino acids and peptides: structures
 of hydrochloride salts of C-amidated Ile, Val, Thr, Ser, Met, Trp, Gln
 and Arg, and comparison with their C-unamidated counterparts
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              72
_journal_page_last               81
_journal_volume                  57
_journal_year                    2001
_space_group_IT_number           4
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 100.047
_cell_angle_gamma                90.000
_cell_length_a                   7.6394
_cell_length_b                   5.2786
_cell_length_c                   14.5967
_exptl_crystal_F_000             252.00
_reflns_d_resolution_high        0.8504
_[local]_cod_data_source_file    oa0030trpNH2sup6.hkl
_[local]_cod_data_source_block   trpNH2
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' H-TRP-NH2 C11H14N3OCL Z=2 P21'
_shelx_refln_list_code           4
_shelx_F_calc_maximum            95.99
_shelx_F_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 -6 0 120.36 118.95 1.84 o
1 -6 0 52.21 49.73 1.17 o
2 -6 0 3.14 2.94 0.26 o
1 -5 0 76.00 76.02 1.65 o
2 -5 0 224.53 207.39 2.65 o
3 -5 0 12.90 13.00 0.93 o
4 -5 0 16.59 16.87 1.02 o
5 -5 0 14.61 17.43 0.96 o
0 -4 0 299.10 301.61 2.97 o
1 -4 0 289.84 288.98 2.83 o
2 -4 0 23.56 25.01 1.05 o
3 -4 0 81.07 71.14 1.73 o
4 -4 0 60.33 61.79 1.76 o
5 -4 0 46.16 46.42 1.52 o
6 -4 0 8.78 8.63 0.61 o
1 -3 0 292.27 283.31 2.32 o
2 -3 0 627.16 648.50 3.88 o
3 -3 0 430.24 435.01 3.67 o
4 -3 0 21.62 28.11 1.23 o
5 -3 0 192.06 205.26 3.03 o
6 -3 0 30.91 30.66 1.29 o
7 -3 0 13.50 14.14 0.94 o
0 -2 0 617.11 650.22 2.71 o
1 -2 0 477.02 477.86 2.40 o
2 -2 0 235.08 265.18 2.11 o
3 -2 0 204.42 194.46 2.21 o
4 -2 0 366.94 377.86 3.42 o
5 -2 0 67.27 71.03 1.68 o
6 -2 0 13.31 10.74 0.71 o
7 -2 0 12.44 9.98 0.72 o
8 -2 0 6.73 7.92 0.74 o
1 -1 0 474.03 506.24 3.89 o
2 -1 0 2331.12 2457.86 12.28 o
3 -1 0 261.93 257.13 2.21 o
4 -1 0 145.90 181.77 2.13 o
5 -1 0 6.28 8.08 0.63 o
6 -1 0 186.60 180.05 2.61 o
7 -1 0 27.82 27.18 1.27 o
8 -1 0 13.03 14.03 0.92 o
1 0 0 808.12 771.16 4.58 o
2 0 0 492.41 469.81 2.39 o
3 0 0 54.96 60.49 1.12 o
4 0 0 820.44 802.89 4.31 o
5 0 0 3.61 3.42 0.32 o
6 0 0 17.80 14.20 1.13 o
7 0 0 252.75 231.56 2.99 o
8 0 0 17.57 16.12 0.99 o
-2 -6 1 7.86 7.51 0.64 o
-1 -6 1 5.85 5.64 0.45 o
0 -6 1 4.66 5.20 0.35 o
1 -6 1 18.15 19.07 0.83 o
2 -6 1 20.44 17.81 0.79 o
-5 -5 1 6.86 6.50 0.59 o
-4 -5 1 131.09 134.16 2.28 o
-3 -5 1 52.38 50.27 1.44 o
-2 -5 1 149.39 132.39 2.19 o
-1 -5 1 1.02 0.54 0.69 o
0 -5 1 7.36 7.34 0.44 o
1 -5 1 3.74 3.63 0.33 o
2 -5 1 160.54 155.85 2.30 o
3 -5 1 7.36 6.91 0.57 o
4 -5 1 28.57 24.75 1.10 o
5 -5 1 45.68 51.12 1.33 o
-6 -4 1 33.49 38.27 1.30 o
-5 -4 1 26.50 28.74 1.24 o
-4 -4 1 67.07 73.09 1.90 o
-3 -4 1 28.56 25.17 1.25 o
-2 -4 1 23.05 21.29 0.99 o
-1 -4 1 138.26 137.20 2.01 o
0 -4 1 89.04 90.10 1.22 o
1 -4 1 63.58 58.29 1.38 o
2 -4 1 4.56 5.18 0.41 o
3 -4 1 256.76 235.40 2.91 o
4 -4 1 253.87 251.00 3.26 o
5 -4 1 72.83 73.82 1.89 o
6 -4 1 12.17 11.96 0.93 o
-7 -3 1 57.46 59.48 1.59 o
-6 -3 1 41.82 41.53 1.50 o
-5 -3 1 124.94 129.46 2.42 o
-4 -3 1 3.99 3.56 0.35 o
-3 -3 1 41.87 40.92 1.31 o
-2 -3 1 267.36 267.77 2.58 o
-1 -3 1 159.59 173.43 1.82 o
0 -3 1 47.70 46.81 1.37 o
1 -3 1 123.59 101.41 1.44 o
2 -3 1 49.19 46.28 1.10 o
3 -3 1 60.15 57.24 1.42 o
4 -3 1 9.80 9.59 0.69 o
5 -3 1 227.76 240.49 3.21 o
6 -3 1 92.39 95.09 2.05 o
7 -3 1 20.46 17.82 0.97 o
-8 -2 1 14.89 15.10 0.86 o
-7 -2 1 35.31 36.28 1.37 o
-6 -2 1 50.19 52.49 1.59 o
-5 -2 1 33.90 30.63 1.28 o
-4 -2 1 43.20 45.11 1.32 o
-3 -2 1 290.87 353.37 2.99 o
-2 -2 1 48.14 65.46 1.20 o
-1 -2 1 1384.76 1417.56 4.49 o
0 -2 1 1130.58 1172.94 31.69 o
1 -2 1 19.87 16.81 0.57 o
2 -2 1 67.59 89.77 1.23 o
3 -2 1 791.17 779.04 4.29 o
4 -2 1 420.20 420.58 3.62 o
5 -2 1 68.74 68.87 1.73 o
6 -2 1 20.03 19.55 1.21 o
7 -2 1 173.34 160.60 2.47 o
8 -2 1 14.94 16.06 0.87 o
-8 -1 1 39.02 37.07 1.25 o
-7 -1 1 21.56 17.79 1.14 o
-6 -1 1 83.65 88.98 1.91 o
-5 -1 1 75.37 80.82 1.71 o
-4 -1 1 432.78 480.95 3.43 o
-3 -1 1 780.82 819.54 4.04 o
-2 -1 1 411.72 429.39 2.56 o
-1 -1 1 419.55 409.46 2.18 o
0 -1 1 1707.01 1782.74 54.57 o
1 -1 1 1785.98 1796.02 13.79 o
2 -1 1 1747.16 1650.75 4.79 o
3 -1 1 48.59 54.03 1.09 o
4 -1 1 17.08 18.74 0.89 o
5 -1 1 279.96 288.06 3.07 o
6 -1 1 481.02 468.07 4.17 o
7 -1 1 16.56 14.32 1.07 o
8 -1 1 3.43 3.19 0.29 o
-8 0 1 0.55 0.69 0.73 o
-7 0 1 0.08 -0.94 0.94 o
-6 0 1 261.40 241.48 2.97 o
-5 0 1 260.15 254.41 2.70 o
-4 0 1 235.10 239.82 2.33 o
-3 0 1 132.60 163.58 1.72 o
-2 0 1 845.38 898.36 6.49 o
-1 0 1 1430.77 1345.73 10.38 o
0 0 1 75.01 67.29 5.24 o
1 0 1 13.27 17.39 0.43 o
2 0 1 22.31 18.36 0.68 o
3 0 1 679.47 704.85 3.53 o
4 0 1 991.36 993.43 4.91 o
5 0 1 2.65 2.71 0.30 o
6 0 1 171.92 169.37 2.56 o
7 0 1 20.37 21.28 1.19 o
8 0 1 52.33 46.65 1.35 o
-2 -6 2 30.27 28.46 0.93 o
-1 -6 2 25.77 22.76 0.88 o
0 -6 2 2.14 2.08 0.17 o
1 -6 2 37.75 35.40 1.02 o
-5 -5 2 11.20 13.47 0.98 o
-4 -5 2 0.55 -0.15 0.74 o
-3 -5 2 6.66 6.33 0.57 o
-2 -5 2 15.22 15.80 0.92 o
-1 -5 2 39.34 40.40 1.29 o
0 -5 2 158.32 169.07 3.32 o
1 -5 2 26.39 25.86 1.09 o
2 -5 2 48.68 47.19 1.42 o
3 -5 2 36.26 32.63 1.17 o
4 -5 2 1.18 0.38 0.64 o
-6 -4 2 37.31 41.24 1.32 o
-5 -4 2 28.72 29.09 1.34 o
-4 -4 2 3.08 2.20 0.35 o
-3 -4 2 38.69 36.86 1.41 o
-2 -4 2 34.04 32.00 1.18 o
-1 -4 2 173.00 166.43 2.21 o
0 -4 2 3.91 4.95 1.42 o
1 -4 2 85.48 80.02 1.63 o
2 -4 2 17.92 19.68 1.00 o
3 -4 2 131.79 124.59 2.18 o
4 -4 2 46.60 43.34 1.52 o
5 -4 2 53.08 53.24 1.58 o
6 -4 2 22.83 22.53 1.09 o
-7 -3 2 26.92 28.49 1.15 o
-6 -3 2 25.25 22.80 1.29 o
-5 -3 2 164.88 175.86 2.78 o
-4 -3 2 77.48 85.65 1.99 o
-3 -3 2 92.27 98.52 1.97 o
-2 -3 2 65.91 65.51 1.51 o
-1 -3 2 237.77 226.37 2.13 o
0 -3 2 215.57 235.53 18.97 o
1 -3 2 611.72 599.51 3.49 o
2 -3 2 23.26 26.07 0.90 o
3 -3 2 49.31 55.97 1.40 o
4 -3 2 17.02 17.27 1.08 o
5 -3 2 55.28 49.80 1.69 o
6 -3 2 7.75 7.74 0.69 o
7 -3 2 3.99 3.63 0.33 o
-8 -2 2 21.50 18.43 0.99 o
-7 -2 2 39.02 36.54 1.41 o
-6 -2 2 10.74 10.22 0.70 o
-5 -2 2 119.67 118.57 2.10 o
-4 -2 2 17.57 20.98 1.09 o
-3 -2 2 399.18 468.72 3.56 o
-2 -2 2 98.08 122.64 1.75 o
-1 -2 2 364.80 390.94 2.81 o
0 -2 2 8.67 14.89 1.53 o
1 -2 2 528.03 537.91 2.64 o
2 -2 2 220.07 191.53 1.79 o
3 -2 2 400.95 391.15 3.02 o
4 -2 2 4.61 5.56 0.47 o
5 -2 2 28.85 34.00 1.37 o
6 -2 2 44.39 40.85 1.47 o
7 -2 2 59.91 64.43 1.61 o
8 -2 2 31.31 31.15 1.05 o
-8 -1 2 18.73 16.20 1.00 o
-7 -1 2 30.01 25.12 1.22 o
-6 -1 2 69.76 68.07 1.79 o
-5 -1 2 121.92 119.05 1.99 o
-4 -1 2 126.25 135.04 1.87 o
-3 -1 2 33.29 37.31 1.01 o
-2 -1 2 135.56 144.67 1.49 o
-1 -1 2 2127.49 2345.68 17.16 o
0 -1 2 832.51 968.85 33.47 o
1 -1 2 916.02 967.52 5.67 o
2 -1 2 548.78 521.34 2.56 o
3 -1 2 103.15 115.53 1.53 o
4 -1 2 108.51 99.58 1.71 o
5 -1 2 96.41 98.49 1.91 o
6 -1 2 32.39 28.81 1.40 o
7 -1 2 5.07 5.60 0.50 o
8 -1 2 16.71 17.03 0.93 o
-8 0 2 27.24 25.33 1.16 o
-7 0 2 241.00 222.23 2.95 o
-6 0 2 1.19 0.57 0.32 o
-5 0 2 15.84 18.17 0.99 o
-4 0 2 191.55 229.43 2.34 o
-3 0 2 25.49 34.36 0.90 o
-2 0 2 2135.74 2142.48 18.35 o
-1 0 2 357.07 353.49 2.72 o
0 0 2 11.96 14.59 0.23 o
1 0 2 33.25 30.85 0.53 o
2 0 2 568.57 578.51 5.16 o
3 0 2 56.10 56.72 1.11 o
4 0 2 91.42 82.61 1.58 o
5 0 2 6.49 5.94 0.48 o
6 0 2 12.62 12.89 0.99 o
7 0 2 131.62 134.76 2.34 o
8 0 2 3.10 3.15 0.30 o
-1 -6 3 3.16 3.18 0.29 o
0 -6 3 5.31 5.85 0.35 o
1 -6 3 15.39 15.17 0.75 o
-5 -5 3 34.28 42.86 1.28 o
-4 -5 3 27.88 32.78 1.34 o
-3 -5 3 8.98 8.49 0.66 o
-2 -5 3 12.07 9.13 0.89 o
-1 -5 3 3.23 3.30 0.33 o
0 -5 3 183.97 200.51 6.17 o
1 -5 3 3.27 4.01 0.36 o
2 -5 3 110.07 103.46 1.93 o
3 -5 3 50.29 47.60 1.36 o
4 -5 3 36.51 33.97 1.20 o
-6 -4 3 1.88 1.80 0.28 o
-5 -4 3 41.39 40.95 1.52 o
-4 -4 3 83.90 100.10 2.33 o
-3 -4 3 244.64 270.05 3.62 o
-2 -4 3 103.46 102.17 2.18 o
-1 -4 3 35.99 35.42 1.17 o
0 -4 3 43.15 44.25 5.96 o
1 -4 3 178.54 167.53 2.25 o
2 -4 3 13.47 14.52 0.92 o
3 -4 3 19.51 18.73 1.07 o
4 -4 3 65.48 61.51 1.71 o
5 -4 3 9.86 10.21 0.95 o
6 -4 3 36.37 42.74 1.28 o
-7 -3 3 50.36 54.33 1.49 o
-6 -3 3 30.51 29.05 1.35 o
-5 -3 3 59.85 66.30 1.87 o
-4 -3 3 64.33 73.35 1.90 o
-3 -3 3 16.42 21.45 1.17 o
-2 -3 3 36.38 42.58 1.46 o
-1 -3 3 117.06 115.51 1.61 o
0 -3 3 114.08 121.72 6.95 o
1 -3 3 143.69 148.11 1.79 o
2 -3 3 67.86 66.30 1.38 o
3 -3 3 22.09 19.75 1.01 o
4 -3 3 88.74 85.81 1.90 o
5 -3 3 87.76 81.67 2.02 o
6 -3 3 30.33 26.71 1.22 o
7 -3 3 15.49 14.42 0.91 o
-8 -2 3 46.68 47.11 1.30 o
-7 -2 3 74.73 72.39 1.75 o
-6 -2 3 19.42 18.30 1.08 o
-5 -2 3 78.45 78.25 1.84 o
-4 -2 3 254.51 285.74 3.09 o
-3 -2 3 772.58 836.49 4.86 o
-2 -2 3 50.03 55.83 1.17 o
-1 -2 3 179.67 202.62 1.66 o
0 -2 3 95.40 93.10 4.36 o
1 -2 3 161.66 164.64 1.52 o
2 -2 3 33.16 28.50 0.82 o
3 -2 3 96.56 86.02 1.52 o
4 -2 3 154.53 151.92 2.24 o
5 -2 3 172.59 176.48 2.68 o
6 -2 3 78.10 77.30 1.94 o
7 -2 3 16.81 15.43 1.09 o
-8 -1 3 24.19 22.26 1.06 o
-7 -1 3 17.08 18.08 1.06 o
-6 -1 3 284.33 280.37 3.23 o
-5 -1 3 97.08 102.08 1.87 o
-4 -1 3 6.53 8.50 0.78 o
-3 -1 3 230.44 257.45 2.26 o
-2 -1 3 424.66 407.69 2.34 o
-1 -1 3 2807.51 3134.88 20.35 o
0 -1 3 2454.58 2741.67 93.85 o
1 -1 3 972.98 980.62 6.15 o
2 -1 3 359.81 343.09 2.15 o
3 -1 3 634.03 605.24 3.51 o
4 -1 3 167.65 164.18 2.18 o
5 -1 3 89.78 86.51 1.90 o
6 -1 3 46.65 44.13 1.55 o
7 -1 3 7.20 7.30 0.64 o
8 -1 3 24.86 24.51 0.96 o
-8 0 3 16.77 20.15 1.07 o
-7 0 3 0.77 0.62 0.63 o
-6 0 3 96.82 100.91 1.99 o
-5 0 3 60.08 73.05 1.63 o
-4 0 3 925.36 924.85 4.75 o
-3 0 3 12.65 11.38 0.66 o
-2 0 3 18.79 28.46 0.68 o
-1 0 3 1867.58 1875.01 13.42 o
0 0 3 49.28 44.01 2.82 o
1 0 3 9.29 7.56 0.42 o
2 0 3 72.59 76.32 1.04 o
3 0 3 75.01 81.30 1.32 o
4 0 3 4.84 5.33 0.46 o
5 0 3 67.57 58.11 1.55 o
6 0 3 61.58 51.99 1.62 o
7 0 3 14.45 12.84 1.09 o
8 0 3 6.92 6.93 0.54 o
-1 -6 4 49.41 50.24 1.24 o
0 -6 4 46.92 45.44 3.05 o
-5 -5 4 36.61 42.54 1.31 o
-4 -5 4 8.20 9.89 0.73 o
-3 -5 4 53.05 67.82 1.88 o
-2 -5 4 156.49 148.84 2.53 o
-1 -5 4 18.32 20.64 1.19 o
0 -5 4 2.28 2.59 0.23 o
1 -5 4 8.51 8.07 0.57 o
2 -5 4 44.85 42.53 1.30 o
3 -5 4 11.56 12.07 0.83 o
4 -5 4 14.37 13.80 0.85 o
-6 -4 4 5.37 6.27 0.50 o
-5 -4 4 57.07 56.15 1.70 o
-4 -4 4 273.41 318.16 4.02 o
-3 -4 4 14.98 16.49 1.34 o
-2 -4 4 156.28 176.12 3.04 o
-1 -4 4 284.65 283.20 3.06 o
0 -4 4 51.74 57.37 3.31 o
1 -4 4 76.51 68.19 1.53 o
2 -4 4 55.56 49.75 1.40 o
3 -4 4 79.40 81.51 1.82 o
4 -4 4 11.79 10.24 0.70 o
5 -4 4 26.88 24.76 1.21 o
6 -4 4 15.85 18.22 0.90 o
-7 -3 4 58.53 56.18 1.49 o
-6 -3 4 108.89 105.32 2.14 o
-5 -3 4 161.38 164.24 2.69 o
-4 -3 4 24.65 28.28 1.37 o
-3 -3 4 35.42 37.52 1.44 o
-2 -3 4 293.39 307.35 3.05 o
-1 -3 4 257.58 253.07 2.36 o
0 -3 4 38.89 45.85 3.21 o
1 -3 4 91.61 86.29 1.47 o
2 -3 4 522.35 518.31 3.70 o
3 -3 4 340.56 328.55 3.25 o
4 -3 4 4.40 4.48 0.44 o
5 -3 4 3.40 3.12 0.35 o
6 -3 4 12.26 12.49 0.99 o
7 -3 4 31.53 33.62 1.08 o
-8 -2 4 32.89 32.88 1.16 o
-7 -2 4 41.58 36.68 1.41 o
-6 -2 4 95.02 96.42 2.04 o
-5 -2 4 229.70 244.93 3.09 o
-4 -2 4 426.11 457.54 3.94 o
-3 -2 4 106.90 103.83 1.75 o
-2 -2 4 106.74 126.88 1.58 o
-1 -2 4 86.98 80.79 1.12 o
0 -2 4 807.81 820.07 30.87 o
1 -2 4 192.30 188.91 1.72 o
2 -2 4 100.71 98.72 1.41 o
3 -2 4 2.19 2.84 0.25 o
4 -2 4 72.98 70.57 1.64 o
5 -2 4 69.97 64.90 1.74 o
6 -2 4 5.73 6.44 0.62 o
7 -2 4 5.15 5.46 0.54 o
-8 -1 4 17.49 17.46 1.06 o
-7 -1 4 91.63 92.08 1.97 o
-6 -1 4 480.06 459.84 4.15 o
-5 -1 4 75.43 82.21 1.77 o
-4 -1 4 267.87 298.12 2.82 o
-3 -1 4 711.85 701.14 3.71 o
-2 -1 4 1012.67 966.41 3.66 o
-1 -1 4 1679.94 1652.89 4.30 o
0 -1 4 489.06 465.89 20.57 o
1 -1 4 387.91 376.99 2.05 o
2 -1 4 482.71 444.63 2.60 o
3 -1 4 61.54 64.90 1.27 o
4 -1 4 57.97 53.79 1.42 o
5 -1 4 24.42 23.12 1.26 o
6 -1 4 162.30 161.40 2.64 o
7 -1 4 1.99 2.11 0.29 o
8 -1 4 22.16 21.20 0.94 o
-8 0 4 38.12 32.30 1.24 o
-7 0 4 269.94 256.44 3.11 o
-6 0 4 19.90 22.31 1.20 o
-5 0 4 70.16 58.46 1.52 o
-4 0 4 1028.03 956.97 4.87 o
-3 0 4 17.16 19.91 0.76 o
-2 0 4 3.67 3.44 0.33 o
-1 0 4 1419.77 1363.55 12.29 o
0 0 4 9213.63 9855.10 498.69 o
1 0 4 76.80 86.39 0.96 o
2 0 4 765.03 720.23 3.22 o
3 0 4 7.84 10.83 0.74 o
4 0 4 325.38 307.60 2.98 o
5 0 4 57.94 57.14 1.61 o
6 0 4 17.40 15.85 1.12 o
7 0 4 33.70 32.94 1.28 o
8 0 4 7.19 8.79 0.76 o
-5 -5 5 1.88 2.85 0.28 o
-4 -5 5 13.37 16.02 1.14 o
-3 -5 5 32.30 43.45 1.70 o
-2 -5 5 301.74 301.49 3.61 o
-1 -5 5 19.02 18.22 1.14 o
0 -5 5 14.34 15.81 0.89 o
1 -5 5 23.31 22.87 1.04 o
2 -5 5 140.90 140.51 2.13 o
3 -5 5 4.12 4.19 0.36 o
4 -5 5 8.84 8.84 0.77 o
-6 -4 5 16.00 19.68 1.01 o
-5 -4 5 54.33 59.21 1.72 o
-4 -4 5 43.80 56.67 1.90 o
-3 -4 5 26.80 28.61 1.42 o
-2 -4 5 4.80 5.12 0.48 o
-1 -4 5 235.60 229.73 2.71 o
0 -4 5 81.37 84.27 1.28 o
1 -4 5 71.25 68.32 1.58 o
2 -4 5 104.38 109.08 1.97 o
3 -4 5 142.42 131.88 2.24 o
4 -4 5 156.04 156.04 2.50 o
5 -4 5 5.15 4.78 0.47 o
-7 -3 5 35.75 39.58 1.28 o
-6 -3 5 20.04 20.41 1.20 o
-5 -3 5 19.24 20.82 1.33 o
-4 -3 5 67.56 73.60 1.95 o
-3 -3 5 377.43 382.78 3.72 o
-2 -3 5 382.38 381.30 3.24 o
-1 -3 5 80.38 84.33 1.46 o
0 -3 5 59.52 53.43 0.88 o
1 -3 5 301.52 287.44 2.67 o
2 -3 5 79.42 79.83 1.56 o
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