#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:20 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180896 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/36/2103603.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103603_Fobs loop_ _publ_author_name 'Hardie, Michaele J.' 'Martin, Anthony' 'Pinkerton, A. Alan' 'Zhurova, Elizabeth A.' _publ_section_title ; Anisotropic thermal expansion of potassium dinitramide: a variable-temperature crystallographic study ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 113 _journal_page_last 118 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _exptl_crystal_F_000 288.00 _cod_data_source_file br0101kdn200sup5.hkl _cod_data_source_block kdn200 #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 392.90 423.83 15.77 o 4 0 0 11.22 21.84 2.53 o 6 0 0 102.76 125.42 6.78 o 8 0 0 159.66 172.87 14.53 o 1 1 0 225.28 231.39 6.65 o 2 1 0 1656.61 1686.87 40.99 o 3 1 0 3.10 3.80 1.21 o 4 1 0 296.20 285.27 8.31 o 5 1 0 74.58 77.60 3.81 o 6 1 0 185.91 191.29 6.43 o 7 1 0 72.46 81.87 3.87 o 8 1 0 61.33 66.13 5.87 o 0 2 0 1.97 1.28 1.07 o 1 2 0 3472.95 3490.94 63.20 o 2 2 0 880.27 936.96 21.08 o 3 2 0 75.18 63.78 4.33 o 4 2 0 244.20 231.93 8.44 o 5 2 0 799.69 781.18 24.03 o 6 2 0 0.68 -0.05 1.76 o 7 2 0 38.61 36.80 3.22 o 8 2 0 0.06 0.50 2.38 o 1 3 0 13322.06 12591.10 283.13 o 2 3 0 340.47 368.49 7.98 o 3 3 0 222.38 207.24 5.03 o 4 3 0 79.76 80.65 2.68 o 5 3 0 27.43 27.87 1.69 o 6 3 0 131.07 76.86 16.60 o 7 3 0 257.16 273.80 10.43 o 8 3 0 0.01 -1.57 3.06 o 0 4 0 1119.00 1066.12 32.45 o 1 4 0 938.88 946.31 22.52 o 2 4 0 11.46 15.49 1.58 o 3 4 0 7.72 8.69 1.28 o 4 4 0 66.89 65.44 2.43 o 5 4 0 19.97 18.58 1.52 o 6 4 0 35.20 19.87 9.09 o 7 4 0 0.08 1.41 2.18 o 8 4 0 89.51 81.46 6.42 o 1 5 0 258.08 263.54 8.81 o 2 5 0 1730.07 1724.37 39.16 o 3 5 0 19.02 19.95 1.64 o 4 5 0 110.37 115.44 4.57 o 5 5 0 60.00 57.82 2.80 o 6 5 0 478.53 469.26 15.89 o 7 5 0 0.54 0.55 2.26 o 0 6 0 3212.21 3425.87 124.04 o 1 6 0 837.14 830.08 20.27 o 2 6 0 109.80 118.53 4.55 o 3 6 0 0.20 -0.29 1.19 o 4 6 0 160.87 173.24 5.45 o 5 6 0 317.34 215.55 53.98 o 6 6 0 121.27 86.98 36.49 o 7 6 0 0.10 2.84 2.84 o 1 7 0 417.59 435.85 11.60 o 2 7 0 174.67 179.54 5.53 o 3 7 0 164.13 172.41 6.12 o 4 7 0 6.21 5.76 1.56 o 5 7 0 1.90 1.10 1.79 o 6 7 0 0.51 -0.14 2.52 o 7 7 0 151.03 158.29 9.05 o 0 8 0 54.88 58.58 4.79 o 1 8 0 329.96 341.98 10.66 o 2 8 0 72.34 60.86 10.42 o 3 8 0 435.91 449.33 13.20 o 4 8 0 25.23 22.98 2.32 o 5 8 0 361.60 258.33 127.24 o 6 8 0 0.93 -0.05 2.60 o 1 9 0 123.09 119.49 6.25 o 2 9 0 133.94 142.47 5.64 o 3 9 0 36.27 41.56 2.93 o 4 9 0 8.53 4.39 1.91 o 5 9 0 17.34 12.37 6.94 o 0 10 0 742.63 817.01 33.06 o 1 10 0 11.82 12.40 2.49 o 2 10 0 0.85 1.13 1.90 o 3 10 0 61.57 66.98 3.82 o 4 10 0 49.79 47.21 3.89 o 5 10 0 0.11 -0.76 3.09 o 1 11 0 12.03 13.53 3.01 o 2 11 0 314.04 338.84 15.98 o 3 11 0 1.81 0.28 2.04 o 0 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3594.20 3628.08 61.86 o 2 2 1 242.27 231.94 7.49 o 3 2 1 42.06 43.98 2.72 o 4 2 1 2010.83 2147.30 55.65 o 5 2 1 532.13 541.40 17.48 o 6 2 1 30.23 31.96 3.64 o 7 2 1 157.81 157.39 7.09 o 8 2 1 92.14 93.05 5.38 o -8 3 1 400.19 391.01 18.33 o -7 3 1 32.27 32.98 3.22 o -6 3 1 7.67 6.33 2.04 o -5 3 1 84.42 88.57 3.04 o -4 3 1 585.49 589.75 12.97 o -3 3 1 85.35 103.14 7.88 o -2 3 1 635.57 689.32 16.28 o -1 3 1 1379.94 1387.48 34.94 o 0 3 1 200.35 227.90 6.03 o 1 3 1 21.36 29.48 1.34 o 2 3 1 670.32 651.23 12.69 o 3 3 1 1.40 0.99 0.95 o 4 3 1 414.56 432.33 12.65 o 5 3 1 244.73 239.40 7.93 o 6 3 1 863.35 861.42 26.82 o 7 3 1 80.49 84.17 4.99 o 8 3 1 11.04 10.09 2.97 o -8 4 1 3.56 2.24 2.42 o -7 4 1 21.69 15.73 4.80 o -6 4 1 249.76 249.23 8.50 o -5 4 1 692.96 705.65 17.15 o -4 4 1 1277.97 1254.15 30.84 o -3 4 1 15.82 17.36 1.53 o -2 4 1 407.62 399.20 10.04 o -1 4 1 1309.61 1288.71 32.70 o 0 4 1 623.29 579.25 14.24 o 1 4 1 193.35 177.36 4.33 o 2 4 1 250.09 270.50 6.26 o 3 4 1 210.41 196.22 5.84 o 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-6 7 1 18.74 11.29 5.12 o -5 7 1 4.85 3.43 1.85 o -4 7 1 249.03 187.38 46.45 o -3 7 1 342.13 342.62 9.25 o -2 7 1 456.33 444.69 12.78 o -1 7 1 59.84 72.41 4.03 o 0 7 1 154.08 157.90 5.97 o 1 7 1 352.42 350.03 9.69 o 2 7 1 104.11 103.47 3.50 o 3 7 1 104.55 107.98 4.53 o 4 7 1 13.19 14.22 1.99 o 5 7 1 78.71 76.60 6.31 o 6 7 1 185.11 196.16 11.51 o -6 8 1 86.09 59.04 22.86 o -5 8 1 12.50 12.14 2.47 o -4 8 1 6.26 3.78 1.82 o -3 8 1 4.53 3.65 1.51 o -2 8 1 729.35 759.20 20.71 o -1 8 1 7.82 8.96 1.74 o 0 8 1 10.03 10.12 1.98 o 1 8 1 14.01 16.18 2.47 o 2 8 1 208.81 217.93 6.88 o 3 8 1 3.35 2.26 1.65 o 4 8 1 764.67 641.88 84.51 o 5 8 1 3.59 3.23 2.18 o 6 8 1 76.62 75.30 7.24 o -5 9 1 50.81 48.03 3.88 o -4 9 1 188.75 208.01 8.97 o -3 9 1 123.36 129.40 5.30 o -2 9 1 78.84 83.58 4.65 o -1 9 1 114.93 118.12 4.91 o 0 9 1 153.00 158.57 7.06 o 1 9 1 7.69 7.38 1.90 o 2 9 1 395.08 416.26 12.57 o 3 9 1 63.71 71.56 3.85 o 4 9 1 63.86 54.42 13.10 o 5 9 1 127.50 129.21 7.86 o -5 10 1 83.63 73.36 9.90 o -4 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103.07 o 1 1 2 6.41 5.03 1.18 o 2 1 2 2336.08 2471.47 55.25 o 3 1 2 233.02 223.04 7.99 o 4 1 2 504.06 489.83 13.37 o 5 1 2 230.86 235.93 7.53 o 6 1 2 18.94 19.00 2.13 o 7 1 2 33.19 36.66 2.85 o 8 1 2 4.72 5.16 2.72 o -8 2 2 0.35 2.58 2.96 o -7 2 2 83.85 91.78 23.07 o -6 2 2 206.13 193.55 9.21 o -5 2 2 1045.63 1011.51 21.29 o -4 2 2 72.90 82.40 4.14 o -3 2 2 81.93 79.06 3.88 o -2 2 2 828.09 808.54 23.65 o -1 2 2 1960.78 1815.41 49.81 o 0 2 2 1692.17 1744.87 41.58 o 1 2 2 83.20 78.68 3.21 o 2 2 2 37.18 32.45 2.08 o 3 2 2 1950.51 1959.98 56.50 o 4 2 2 9.07 8.59 1.87 o 5 2 2 86.46 80.49 4.41 o 6 2 2 30.06 32.22 3.07 o 7 2 2 103.56 107.74 5.70 o 8 2 2 120.99 120.51 6.27 o -8 3 2 11.64 12.84 3.48 o -7 3 2 368.49 387.49 13.60 o -6 3 2 2.95 4.07 2.07 o -5 3 2 101.63 107.36 5.87 o -4 3 2 26.59 32.68 2.69 o -3 3 2 533.88 495.41 15.65 o -2 3 2 515.85 553.21 13.87 o -1 3 2 360.36 384.70 10.66 o 0 3 2 1547.20 1691.90 35.44 o 1 3 2 9077.04 9024.26 170.56 o 2 3 2 67.33 64.59 2.52 o 3 3 2 2.13 1.23 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2.55 2.20 o -6 6 2 287.44 293.24 9.80 o -5 6 2 8.40 6.55 1.80 o -4 6 2 20.12 17.77 2.94 o -3 6 2 197.08 202.40 6.02 o -2 6 2 535.84 569.72 15.70 o -1 6 2 107.62 112.58 4.77 o 0 6 2 647.72 633.63 17.10 o 1 6 2 292.95 302.43 9.32 o 2 6 2 938.16 927.79 24.67 o 3 6 2 34.05 32.38 1.96 o 4 6 2 24.54 21.67 4.89 o 5 6 2 8.74 6.88 1.76 o 6 6 2 3.73 -0.10 1.94 o 7 6 2 1.31 -0.70 2.88 o -7 7 2 21.20 24.96 3.89 o -6 7 2 48.85 40.24 7.98 o -5 7 2 26.33 22.94 2.43 o -4 7 2 14.58 18.04 2.12 o -3 7 2 78.60 78.45 3.28 o -2 7 2 44.66 45.51 2.74 o -1 7 2 0.42 0.01 1.37 o 0 7 2 538.10 538.52 17.37 o 1 7 2 1608.14 1593.53 40.90 o 2 7 2 62.42 61.22 3.92 o 3 7 2 21.80 23.97 2.10 o 4 7 2 169.06 165.89 6.97 o 5 7 2 26.19 25.37 2.85 o 6 7 2 0.06 0.35 2.79 o -6 8 2 0.03 1.74 2.52 o -5 8 2 772.49 485.47 223.21 o -4 8 2 1.61 2.10 1.82 o -3 8 2 104.94 89.16 11.51 o -2 8 2 42.57 48.01 2.91 o -1 8 2 447.08 474.02 15.62 o 0 8 2 15.06 16.54 2.33 o 1 8 2 12.46 11.76 2.23 o 2 8 2 7.40 6.46 1.80 o 3 8 2 140.98 149.12 6.70 o 4 8 2 9.93 11.56 2.41 o 5 8 2 91.90 98.30 6.16 o 6 8 2 0.24 0.20 3.04 o -5 9 2 95.81 93.24 6.84 o -4 9 2 10.64 12.80 3.63 o -3 9 2 240.93 185.88 52.16 o -2 9 2 50.92 45.57 3.49 o -1 9 2 0.95 1.12 2.29 o 0 9 2 368.50 357.82 12.73 o 1 9 2 192.62 186.87 7.92 o 2 9 2 30.43 29.89 2.67 o 3 9 2 132.60 128.90 5.99 o 4 9 2 0.62 1.57 2.25 o 5 9 2 113.01 79.71 35.68 o -4 10 2 5.88 5.18 3.43 o -3 10 2 20.56 23.06 3.80 o -2 10 2 107.11 105.50 5.60 o -1 10 2 97.21 95.85 5.24 o 0 10 2 469.01 510.98 17.53 o 1 10 2 19.28 16.60 2.66 o 2 10 2 268.64 281.04 15.15 o 3 10 2 9.77 13.91 2.75 o 4 10 2 18.69 22.95 3.47 o -3 11 2 0.88 4.14 3.37 o -2 11 2 96.02 74.68 28.83 o -1 11 2 19.94 23.28 3.10 o 0 11 2 96.91 92.68 5.34 o 1 11 2 6.27 7.46 2.84 o 2 11 2 4.33 -0.18 2.36 o 3 11 2 1.49 0.07 2.79 o -7 0 3 845.48 913.83 52.90 o -5 0 3 395.57 314.35 16.27 o -3 0 3 243.92 218.80 9.17 o 1 0 3 1643.13 1675.43 77.53 o 3 0 3 328.73 296.94 12.36 o 5 0 3 973.72 929.47 34.24 o 7 0 3 335.95 366.87 16.04 o -8 1 3 82.38 82.72 8.20 o -7 1 3 2.80 2.93 2.81 o -6 1 3 0.46 1.71 1.76 o -5 1 3 1065.65 1039.62 31.18 o -4 1 3 251.07 263.07 11.01 o -3 1 3 144.61 123.65 10.19 o -2 1 3 61.34 66.77 2.36 o -1 1 3 231.28 260.20 6.88 o 0 1 3 1209.99 1219.50 56.93 o 1 1 3 170.56 149.16 7.12 o 2 1 3 811.34 772.97 17.05 o 3 1 3 47.84 50.49 2.70 o 4 1 3 0.92 0.28 1.59 o 5 1 3 1124.86 1112.76 28.59 o 6 1 3 61.47 59.41 3.89 o 7 1 3 50.70 50.35 3.96 o -8 2 3 45.86 39.52 4.67 o -7 2 3 1.94 1.60 2.68 o -6 2 3 172.52 176.89 7.21 o -5 2 3 98.39 106.91 7.63 o -4 2 3 912.21 873.58 26.46 o -3 2 3 80.82 81.40 4.00 o -2 2 3 2679.63 2920.05 99.61 o -1 2 3 597.96 626.47 18.70 o 0 2 3 20.01 20.81 1.69 o 1 2 3 108.52 129.61 6.74 o 2 2 3 39.72 28.10 1.83 o 3 2 3 250.10 242.35 7.79 o 4 2 3 586.50 554.74 17.81 o 5 2 3 40.88 43.23 4.56 o 6 2 3 904.77 889.60 27.93 o 7 2 3 2.70 1.93 2.63 o -8 3 3 177.36 181.89 10.70 o -7 3 3 26.82 25.46 4.15 o -6 3 3 942.34 918.92 28.31 o -5 3 3 9.59 7.85 1.94 o -4 3 3 244.18 234.63 8.70 o -3 3 3 453.87 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