#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/36/2103618.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103618_Fobs loop_ _publ_author_name 'Arakcheeva, Alla' 'Chapuis, Gervais' 'Grinevitch, Vladimir' 'Shamray, Vladimir' _publ_section_title ; A novel perovskite-like Ta-bronze KTa~1+z~O~3~: preparation, stoichiometry, conductivity and crystal structure studies ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 157 _journal_page_last 162 _journal_volume 57 _journal_year 2001 _space_group_IT_number 221 _symmetry_space_group_name_Hall '-P 4 2 3' _symmetry_space_group_name_H-M 'P m -3 m' _[local]_cod_data_source_file os0066sup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma 0 0 1 671.1 673.5 0.5 0 1 1 818.1 817.1 0.4 1 1 1 393.9 403.6 0.7 0 0 2 963.4 960.2 0.6 0 1 2 606.1 605.1 0.4 1 1 2 736.5 736.5 0.4 0 2 2 840.9 839.5 0.5 1 2 2 530.0 531.9 0.5 2 2 2 735.3 739.4 0.8 0 0 3 529.7 530.1 0.8 0 1 3 652.3 653.9 0.5 1 1 3 368.5 367.2 0.6 0 2 3 470.9 470.3 0.5 1 2 3 586.0 588.6 0.4 2 2 3 420.7 421.5 0.6 0 3 3 536.4 533.6 1.0 1 3 3 312.0 307.8 0.7 2 3 3 488.7 488.4 0.6 3 3 3 263.6 258.4 1.4 0 0 4 661.9 663.6 1.2 0 1 4 426.9 425.5 0.7 1 1 4 536.6 538.1 0.7 0 2 4 599.4 601.2 0.6 1 2 4 385.7 384.7 0.5 2 2 4 549.9 549.3 0.6 0 3 4 350.9 349.5 0.8 1 3 4 450.8 451.5 0.5 2 3 4 326.5 320.4 0.6 3 3 4 386.2 384.4 1.1 0 4 4 464.8 467.1 1.4 1 4 4 302.7 297.6 1.1 2 4 4 435.8 432.7 1.0 3 4 4 254.9 255.2 1.5 4 4 4 350.9 349.8 2.8 0 0 5 349.0 350.0 1.4 0 1 5 446.6 451.0 0.7 1 1 5 262.7 262.5 0.8 0 2 5 324.3 320.7 1.0 1 2 5 413.6 416.0 0.6 2 2 5 297.6 295.3 1.1 0 3 5 383.7 383.8 1.1 1 3 5 221.8 222.4 1.0 2 3 5 357.8 355.8 0.8 3 3 5 192.4 191.1 1.7 0 4 5 256.0 254.8 1.4 1 4 5 331.4 332.2 0.9 2 4 5 239.5 237.6 1.0 3 4 5 289.7 287.8 1.2 4 4 5 192.8 197.1 2.8 0 5 5 275.7 286.9 2.4 1 5 5 162.7 167.9 2.0 2 5 5 263.9 268.2 1.7 3 5 5 144.9 148.3 1.5 4 5 5 220.5 222.3 1.4 5 5 5 115.7 120.7 4.9 0 0 6 438.1 437.4 2.5 0 1 6 283.8 281.5 1.3 1 1 6 366.6 363.6 1.2 0 2 6 406.3 406.0 1.2 1 2 6 258.6 261.1 1.0 2 2 6 381.5 377.8 1.4 0 3 6 246.1 242.4 1.6 1 3 6 312.8 313.4 1.0 2 3 6 226.8 226.5 1.2 3 3 6 268.8 272.5 1.6 0 4 6 329.9 329.8 1.6 1 4 6 208.4 213.6 1.2 2 4 6 306.8 308.9 1.2 3 4 6 186.8 188.9 0.9 4 4 6 254.1 257.1 1.2 0 5 6 189.2 187.8 1.2 1 5 6 242.7 239.6 0.8 2 5 6 173.5 177.7 1.0 3 5 6 209.2 211.8 0.9 4 5 6 151.6 153.1 1.1 5 5 6 171.3 170.4 1.2 0 6 6 243.9 243.7 1.5 1 6 6 164.3 162.6 1.5 2 6 6 232.8 230.5 1.3 3 6 6 145.9 147.5 1.6 4 6 6 196.6 197.2 1.1 5 6 6 126.3 124.4 1.5 0 0 7 213.0 227.5 3.1 0 1 7 296.7 292.2 1.8 1 1 7 174.5 174.0 2.3 0 2 7 211.5 212.7 1.9 1 2 7 270.6 272.8 1.3 2 2 7 193.8 199.6 2.8 0 3 7 253.6 254.5 2.4 1 3 7 152.0 152.3 1.1 2 3 7 238.0 238.7 0.9 3 3 7 132.3 135.3 1.6 0 4 7 173.2 177.5 1.3 1 4 7 221.5 225.2 0.8 2 4 7 167.0 168.1 1.0 3 4 7 198.1 199.7 1.0 4 4 7 150.8 145.2 1.5 0 5 7 200.7 198.7 1.3 1 5 7 122.7 121.8 1.2 2 5 7 188.8 188.0 1.0 3 5 7 113.4 111.1 1.2 4 5 7 164.4 161.6 0.9 5 5 7 98.3 95.3 1.6 0 6 7 138.4 138.3 1.3 1 6 7 175.0 171.4 0.8 2 6 7 133.7 132.6 1.0 3 6 7 159.1 155.5 0.9 4 6 7 113.8 118.2 1.0 0 7 7 147.5 146.8 1.8 1 7 7 95.4 93.9 1.3 2 7 7 132.0 140.8 1.2 0 0 8 277.3 280.4 2.6 0 1 8 183.7 186.8 1.7 1 1 8 231.3 234.2 1.6 0 2 8 261.4 263.6 1.3 1 2 8 174.4 176.2 1.1 2 2 8 248.0 248.3 1.2 0 3 8 167.8 166.0 1.5 1 3 8 207.3 207.1 1.0 2 3 8 157.4 157.5 1.1 3 3 8 186.6 184.8 1.3 0 4 8 222.1 221.8 1.1 1 4 8 153.1 150.2 1.0 2 4 8 211.5 210.3 0.8 3 4 8 140.2 136.4 1.1 4 4 8 180.8 181.3 1.2 0 5 8 133.9 134.9 1.3 1 5 8 168.1 166.5 0.9 2 5 8 133.1 129.3 1.1 3 5 8 148.6 151.4 0.9 0 6 8 171.1 173.1 1.0 1 6 8 115.7 119.7 1.0 0 0 9 157.9 148.7 3.0 0 1 9 188.5 185.4 1.4 1 1 9 118.5 116.2 2.0 0 2 9 146.0 141.0 1.6 1 2 9 178.7 175.7 1.0 2 2 9 137.9 134.1 1.6 0 3 9 174.4 166.3 1.5 1 3 9 110.5 104.9 1.4 2 3 9 160.7 158.3 1.1 3 3 9 89.6 95.9 1.9 0 4 9 121.6 121.7 1.5 1 4 9 150.9 151.4 1.1 2 4 9 109.3 116.7 1.2 0 0 10 182.2 181.1 2.5 0 1 10 116.8 122.9 1.7 1 1 10 148.0 154.0 1.5