#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103639.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103639_Fobs loop_ _publ_author_name 'Greenberg, Mark' 'Shteiman, Vitaly' 'Kaftory, Menahem' _publ_section_title ; Topochemically controlled solid-state methyl rearrangement in thiocyanurates ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 428 _journal_page_last 434 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.991 _cell_angle_gamma 90.000 _cell_length_a 7.6570 _cell_length_b 14.3610 _cell_length_c 8.4330 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.8407 _[local]_cod_data_source_file av00379bsup3.hkl _[local]_cod_data_source_block 9b #BEGIN Tags that were not found in dictionaries: _shelx_title ' plates P21/c (N14 cba-trans)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 115.57 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 365.19 367.59 15.16 o 2 0 0 12274.26 12884.96 516.30 o 3 0 0 1521.90 1459.81 59.96 o 4 0 0 0.06 0.00 7.67 o 5 0 0 60.48 44.46 7.15 o 6 0 0 50.81 35.09 8.52 o 7 0 0 21.35 8.52 10.56 o 8 0 0 2.39 0.00 13.46 o 1 1 0 66.32 72.91 3.92 o 2 1 0 10793.59 10667.82 427.72 o 3 1 0 139.53 114.13 7.32 o 4 1 0 224.45 185.33 10.56 o 5 1 0 330.66 336.25 17.20 o 6 1 0 0.61 0.00 7.49 o 7 1 0 1.32 0.00 8.35 o 8 1 0 12.98 7.95 5.29 o 0 2 0 10226.96 9475.11 379.35 o 1 2 0 563.49 552.75 23.17 o 2 2 0 13356.03 13745.51 550.71 o 3 2 0 101.69 86.02 6.47 o 4 2 0 939.48 894.96 38.16 o 5 2 0 8.29 0.00 6.81 o 6 2 0 1.97 0.00 7.67 o 7 2 0 68.96 56.21 9.37 o 8 2 0 0.68 0.00 11.16 o 1 3 0 113.52 101.69 7.84 o 2 3 0 6498.52 6696.71 268.97 o 3 3 0 157.49 131.67 8.01 o 4 3 0 2883.47 3030.67 123.33 o 5 3 0 2.31 0.00 6.64 o 6 3 0 27.72 0.00 8.52 o 7 3 0 0.01 0.00 8.35 o 8 3 0 4.36 0.00 11.75 o 0 4 0 819.74 811.84 35.09 o 1 4 0 658.09 636.05 26.74 o 2 4 0 727.18 746.60 31.34 o 3 4 0 331.07 300.14 14.31 o 4 4 0 2657.22 2757.45 112.59 o 5 4 0 30.19 12.78 7.15 o 6 4 0 547.03 550.02 26.57 o 7 4 0 74.40 74.10 10.90 o 8 4 0 0.38 0.00 5.03 o 1 5 0 874.88 882.36 36.62 o 2 5 0 61.36 38.67 4.77 o 3 5 0 52.06 28.11 5.62 o 4 5 0 745.84 733.48 32.19 o 5 5 0 380.28 424.48 20.95 o 6 5 0 511.40 505.23 25.21 o 7 5 0 0.58 0.00 8.86 o 8 5 0 101.96 94.82 15.84 o 0 6 0 204.95 186.69 9.54 o 1 6 0 1.60 0.00 3.41 o 2 6 0 145.86 155.18 8.69 o 3 6 0 393.66 399.62 18.57 o 4 6 0 160.95 129.29 9.54 o 5 6 0 14.69 11.07 7.15 o 6 6 0 311.62 327.22 18.40 o 7 6 0 32.93 25.41 7.92 o 1 7 0 125.29 85.51 6.30 o 2 7 0 0.07 0.00 4.09 o 3 7 0 343.49 358.22 17.20 o 4 7 0 58.92 70.52 7.84 o 5 7 0 0.09 0.00 7.15 o 6 7 0 416.44 452.76 23.51 o 7 7 0 1.76 0.00 19.25 o 0 8 0 2.13 0.00 3.75 o 1 8 0 1372.46 1434.08 59.79 o 2 8 0 113.72 89.60 7.15 o 3 8 0 434.15 416.14 19.93 o 4 8 0 151.52 155.35 10.90 o 5 8 0 11.23 0.00 7.32 o 6 8 0 41.86 37.99 9.20 o 7 8 0 25.83 19.71 9.03 o 1 9 0 1241.84 1280.10 53.83 o 2 9 0 12.94 0.00 5.11 o 3 9 0 243.09 244.78 13.63 o 4 9 0 177.30 158.59 11.41 o 5 9 0 85.49 72.39 9.54 o 6 9 0 0.13 0.00 8.35 o 7 9 0 6.14 0.00 5.69 o 0 10 0 9.60 6.13 4.09 o 1 10 0 219.77 194.19 11.24 o 2 10 0 43.71 30.83 6.13 o 3 10 0 41.52 25.55 6.64 o 4 10 0 25.13 8.52 7.32 o 5 10 0 2.16 0.00 7.67 o 6 10 0 3.70 0.00 8.86 o 1 11 0 91.88 79.21 7.67 o 2 11 0 141.40 153.31 10.39 o 3 11 0 1.42 0.00 5.96 o 4 11 0 29.73 18.06 7.49 o 5 11 0 48.27 50.42 9.03 o 6 11 0 0.75 0.00 8.01 o 0 12 0 233.25 234.22 13.29 o 1 12 0 204.36 221.27 13.29 o 2 12 0 77.56 60.98 8.01 o 3 12 0 354.15 355.33 19.08 o 4 12 0 9.98 0.00 7.67 o 5 12 0 1.54 0.00 8.01 o 6 12 0 22.55 21.63 9.37 o 1 13 0 310.78 310.87 17.20 o 2 13 0 14.76 3.75 6.47 o 3 13 0 32.50 22.14 7.49 o 4 13 0 33.10 9.71 8.52 o 5 13 0 82.10 71.88 11.07 o 0 14 0 35.11 37.64 7.49 o 1 14 0 37.43 15.67 7.32 o 2 14 0 0.73 0.00 6.81 o 3 14 0 3.63 0.00 7.15 o 4 14 0 2.15 0.00 7.67 o 1 15 0 92.93 103.23 10.05 o 2 15 0 75.20 78.36 9.88 o 3 15 0 7.45 0.00 7.84 o 4 15 0 15.38 0.00 9.03 o 0 16 0 131.09 163.87 12.43 o 1 16 0 32.92 29.98 8.01 o 2 16 0 8.52 0.00 8.52 o -8 1 1 28.02 19.98 5.69 o -7 1 1 18.29 1.87 8.35 o -6 1 1 4.74 0.00 6.98 o -5 1 1 177.20 175.11 11.07 o -4 1 1 328.88 336.93 16.01 o -3 1 1 910.16 996.48 41.39 o -2 1 1 903.53 880.82 36.62 o -1 1 1 92.32 86.70 4.60 o 0 1 1 6997.98 7155.94 491.43 o 1 1 1 37.04 9.71 3.58 o 2 1 1 781.49 808.94 33.73 o 3 1 1 525.77 527.20 23.17 o 4 1 1 19.63 0.00 6.13 o 5 1 1 314.35 298.60 16.18 o 6 1 1 263.96 280.55 16.52 o 7 1 1 105.15 84.15 11.07 o 8 1 1 65.75 66.09 11.75 o -8 2 1 1.24 0.00 22.83 o -7 2 1 59.36 41.56 11.41 o -6 2 1 234.56 213.78 13.80 o -5 2 1 1.12 0.00 5.96 o -4 2 1 50.56 26.91 5.79 o -3 2 1 10.96 0.17 4.43 o -2 2 1 9084.73 9144.65 366.74 o -1 2 1 484.33 500.97 20.95 o 0 2 1 5.66 0.00 2.56 o 1 2 1 2291.86 2331.94 94.37 o 2 2 1 862.12 973.66 40.37 o 3 2 1 828.56 809.11 34.24 o 4 2 1 895.52 893.60 38.33 o 5 2 1 11.73 0.00 7.15 o 6 2 1 155.15 141.72 11.92 o 7 2 1 4.97 0.00 8.69 o 8 2 1 11.20 0.00 9.88 o -8 3 1 11.12 0.55 7.15 o -7 3 1 39.49 18.40 8.69 o -6 3 1 4.62 0.00 7.49 o -5 3 1 38.79 10.39 6.81 o -4 3 1 2541.92 2716.74 110.89 o -3 3 1 10.64 0.00 4.43 o -2 3 1 186.77 183.63 10.39 o -1 3 1 2863.73 2845.00 114.64 o 0 3 1 460.61 518.21 19.25 o 1 3 1 2396.90 2437.04 98.46 o 2 3 1 73.76 50.76 5.11 o 3 3 1 13.75 0.00 5.11 o 4 3 1 204.57 170.85 10.90 o 5 3 1 9.11 0.00 7.15 o 6 3 1 0.11 0.00 7.84 o 7 3 1 7.92 0.00 13.12 o 8 3 1 1.68 0.00 9.20 o -8 4 1 0.09 0.00 11.41 o -7 4 1 40.83 32.36 9.37 o -6 4 1 127.42 119.58 10.90 o -5 4 1 157.42 137.63 10.39 o -4 4 1 366.81 447.14 20.61 o -3 4 1 0.01 0.00 4.43 o -2 4 1 72.79 72.22 6.98 o -1 4 1 1219.38 1173.13 48.04 o 0 4 1 1762.71 1783.27 64.90 o 1 4 1 108.67 121.79 8.01 o 2 4 1 1265.03 1292.02 53.49 o 3 4 1 164.04 170.17 9.88 o 4 4 1 869.95 947.09 40.71 o 5 4 1 143.35 138.49 10.90 o 6 4 1 10.81 0.00 7.84 o 7 4 1 0.31 0.00 8.86 o -8 5 1 1.73 0.00 9.71 o -7 5 1 69.17 32.36 10.39 o -6 5 1 276.94 269.48 16.69 o -5 5 1 184.43 179.20 11.92 o -4 5 1 428.41 378.49 18.06 o -3 5 1 266.58 273.22 13.46 o -2 5 1 1329.73 1262.55 51.95 o -1 5 1 841.50 836.71 34.75 o 0 5 1 545.21 535.24 16.69 o 1 5 1 639.50 712.53 29.98 o 2 5 1 2987.46 3298.79 134.74 o 3 5 1 443.66 455.32 20.95 o 4 5 1 3.42 0.00 6.30 o 5 5 1 73.52 53.49 8.69 o 6 5 1 91.31 72.73 10.56 o 7 5 1 4.74 0.00 8.69 o -8 6 1 107.89 112.89 17.80 o -7 6 1 151.11 165.93 9.02 o -6 6 1 395.75 423.12 22.48 o -5 6 1 91.98 78.19 8.86 o -4 6 1 164.68 151.60 10.39 o -3 6 1 1535.70 1563.71 64.56 o -2 6 1 450.55 451.57 20.10 o -1 6 1 101.10 96.24 5.96 o 0 6 1 3456.90 3765.79 132.18 o 1 6 1 30.10 23.85 4.43 o 2 6 1 67.30 95.90 6.98 o 3 6 1 144.91 125.03 8.69 o 4 6 1 37.86 0.00 14.65 o 5 6 1 1.39 0.00 7.32 o 6 6 1 0.31 0.00 8.01 o 7 6 1 51.54 40.54 10.22 o -8 7 1 86.95 94.96 8.20 o -7 7 1 285.51 334.82 13.59 o -6 7 1 46.41 28.45 8.52 o -5 7 1 631.63 679.14 31.68 o -4 7 1 12.85 0.00 6.47 o -3 7 1 0.10 0.00 5.11 o -2 7 1 435.16 460.09 20.61 o -1 7 1 16.32 6.81 3.58 o 0 7 1 81.80 104.67 5.37 o 1 7 1 64.74 56.55 5.45 o 2 7 1 4.26 0.00 8.52 o 3 7 1 72.57 78.19 7.67 o 4 7 1 1.75 0.00 6.47 o 5 7 1 60.76 43.95 8.69 o 6 7 1 20.59 1.53 8.18 o 7 7 1 1.37 0.00 9.20 o -7 8 1 30.07 23.27 14.14 o -6 8 1 41.82 22.31 8.86 o -5 8 1 210.67 193.16 13.12 o -4 8 1 11.82 0.00 15.50 o -3 8 1 6.52 0.00 5.45 o -2 8 1 137.98 128.78 8.35 o -1 8 1 289.15 292.13 14.14 o 0 8 1 704.58 812.31 24.59 o 1 8 1 29.87 32.19 4.94 o 2 8 1 26.53 15.16 5.45 o 3 8 1 4.09 0.00 5.79 o 4 8 1 99.65 89.60 9.37 o 5 8 1 11.42 0.00 7.15 o 6 8 1 3.07 0.00 8.18 o 7 8 1 4.81 0.00 9.20 o -7 9 1 65.21 67.00 6.87 o -6 9 1 1.59 0.00 7.84 o -5 9 1 861.89 1004.49 44.46 o -4 9 1 124.55 121.96 10.22 o -3 9 1 532.91 521.58 28.96 o -2 9 1 629.17 680.50 30.15 o -1 9 1 35.62 11.24 4.77 o 0 9 1 74.05 86.50 4.52 o 1 9 1 41.97 37.47 5.45 o 2 9 1 469.90 513.57 23.68 o 3 9 1 6.89 0.00 6.13 o 4 9 1 4.36 0.00 6.98 o 5 9 1 79.52 83.47 9.37 o 6 9 1 41.73 36.96 9.71 o -7 10 1 28.39 33.96 6.20 o -6 10 1 56.80 76.65 9.88 o -5 10 1 137.71 136.61 11.75 o -4 10 1 133.70 130.99 10.56 o -3 10 1 1284.15 1339.72 56.89 o -2 10 1 67.42 56.89 6.98 o -1 10 1 21.34 5.11 4.77 o 0 10 1 456.00 465.12 15.27 o 1 10 1 156.09 136.95 9.03 o 2 10 1 5.05 0.00 5.79 o 3 10 1 123.73 133.21 10.39 o 4 10 1 150.93 169.15 12.43 o 5 10 1 0.04 0.00 7.32 o 6 10 1 8.54 0.00 8.52 o -6 11 1 0.71 0.00 7.84 o -5 11 1 0.01 0.00 7.32 o -4 11 1 28.49 19.93 7.49 o -3 11 1 920.00 975.02 42.76 o -2 11 1 22.51 24.02 6.64 o -1 11 1 1048.06 1085.91 46.67 o 0 11 1 3.16 0.00 3.37 o 1 11 1 12.13 0.00 14.65 o 2 11 1 181.54 185.50 11.92 o 3 11 1 0.93 0.00 5.79 o 4 11 1 10.50 0.00 7.15 o 5 11 1 30.00 30.83 8.52 o 6 11 1 0.10 0.00 33.90 o -6 12 1 28.60 0.00 9.54 o -5 12 1 9.87 0.00 8.01 o -4 12 1 70.40 75.29 9.20 o -3 12 1 61.24 38.67 8.18 o -2 12 1 14.51 2.73 5.79 o -1 12 1 928.15 945.55 41.56 o 0 12 1 3.04 0.24 3.59 o 1 12 1 23.57 21.29 5.96 o 2 12 1 1.00 0.00 5.96 o 3 12 1 5.69 0.00 6.47 o 4 12 1 5.40 10.73 9.03 o 5 12 1 2.64 0.00 8.18 o -5 13 1 1.58 0.00 7.49 o -4 13 1 35.59 37.47 8.86 o -3 13 1 8.46 0.00 6.47 o -2 13 1 58.07 39.01 7.67 o -1 13 1 914.72 948.62 41.90 o 0 13 1 5.09 0.00 4.10 o 1 13 1 726.12 765.84 34.75 o 2 13 1 138.96 146.83 11.41 o 3 13 1 10.51 0.00 7.32 o 4 13 1 42.24 35.09 8.86 o 5 13 1 39.39 21.63 9.71 o -5 14 1 25.85 20.61 9.20 o -4 14 1 23.60 16.69 8.35 o -3 14 1 81.08 81.42 9.20 o -2 14 1 48.13 36.45 8.35 o -1 14 1 13.29 10.05 6.81 o 0 14 1 159.99 180.81 12.35 o 1 14 1 844.17 947.09 42.58 o 2 14 1 34.99 33.73 8.52 o 3 14 1 276.29 314.28 18.40 o 4 14 1 110.61 103.23 11.24 o -4 15 1 20.26 1.53 9.20 o -3 15 1 0.29 0.00 7.49 o -2 15 1 18.74 1.70 7.84 o -1 15 1 6.72 0.00 7.15 o 0 15 1 7.80 0.00 4.64 o 1 15 1 103.73 93.18 9.88 o 2 15 1 41.42 27.42 8.01 o 3 15 1 167.76 184.14 14.14 o -3 16 1 6.59 0.00 8.01 o -2 16 1 4.62 0.00 7.32 o -1 16 1 1.04 0.51 6.47 o 0 16 1 12.76 3.51 8.18 o 1 16 1 84.59 93.18 10.56 o 2 16 1 6.07 0.00 7.49 o -8 0 2 6.00 0.00 10.14 o -7 0 2 233.55 262.32 16.18 o -6 0 2 16.52 5.28 7.49 o -5 0 2 58.57 23.00 8.18 o -4 0 2 63.01 60.47 6.64 o -3 0 2 1499.67 1318.25 54.17 o -2 0 2 267.38 214.80 13.46 o -1 0 2 809.67 813.37 33.56 o 0 0 2 2618.69 2898.79 334.55 o 1 0 2 3913.00 4471.57 180.05 o 2 0 2 29.28 33.22 4.94 o 3 0 2 1251.49 1315.36 54.85 o 4 0 2 326.11 335.06 16.86 o 5 0 2 0.34 0.00 7.32 o 6 0 2 0.96 0.00 7.67 o 7 0 2 115.85 124.52 12.95 o -8 1 2 19.04 23.59 5.83 o -7 1 2 0.05 0.00 8.86 o -6 1 2 42.63 40.20 8.52 o -5 1 2 629.58 673.35 29.81 o -4 1 2 10.83 0.00 8.52 o -3 1 2 51.23 20.44 13.46 o -2 1 2 635.12 530.44 22.66 o -1 1 2 1219.45 1248.59 50.76 o 0 1 2 167.78 152.04 9.79 o 1 1 2 384.00 386.33 17.20 o 2 1 2 614.84 605.39 25.89 o 3 1 2 124.95 80.06 7.15 o 4 1 2 1.21 0.00 6.13 o 5 1 2 152.42 147.00 12.26 o 6 1 2 77.71 98.46 10.22 o 7 1 2 2.00 0.00 8.52 o -8 2 2 24.71 15.96 6.39 o -7 2 2 2.74 0.00 8.01 o -6 2 2 6.64 0.00 7.67 o -5 2 2 24.35 1.70 6.81 o -4 2 2 0.81 0.00 4.77 o -3 2 2 618.54 656.83 27.94 o -2 2 2 484.53 415.63 18.23 o -1 2 2 282.00 255.17 12.09 o 0 2 2 215.78 198.82 19.08 o 1 2 2 1228.23 1382.81 56.55 o 2 2 2 11.67 0.00 4.26 o 3 2 2 185.36 165.23 9.88 o 4 2 2 64.73 45.14 7.67 o 5 2 2 2.17 0.00 9.03 o 6 2 2 17.21 10.56 8.69 o 7 2 2 3.48 0.00 8.69 o -8 3 2 17.07 13.02 5.92 o -7 3 2 13.68 0.00 8.52 o -6 3 2 15.34 0.00 7.84 o -5 3 2 110.84 118.04 9.20 o -4 3 2 162.01 142.91 9.03 o -3 3 2 7.54 0.34 4.43 o -2 3 2 26.89 14.48 3.92 o -1 3 2 2290.99 2224.80 89.94 o 0 3 2 9.60 0.00 3.58 o 1 3 2 453.83 475.93 20.61 o 2 3 2 21.48 2.21 4.43 o 3 3 2 350.53 327.22 16.01 o 4 3 2 27.91 0.00 7.32 o 5 3 2 261.75 232.68 14.82 o 6 3 2 58.49 51.27 9.71 o 7 3 2 7.94 0.00 8.86 o -8 4 2 26.90 11.11 19.42 o -7 4 2 79.50 81.93 10.22 o -6 4 2 212.53 226.72 14.65 o -5 4 2 75.33 82.61 8.52 o -4 4 2 120.91 97.43 7.84 o -3 4 2 2324.94 2345.57 95.73 o -2 4 2 0.61 0.00 3.75 o -1 4 2 1287.25 1470.20 59.96 o 0 4 2 90.45 85.25 3.73 o 1 4 2 747.12 789.35 33.22 o 2 4 2 85.67 73.93 6.47 o 3 4 2 204.49 186.52 10.73 o 4 4 2 625.25 672.33 30.49 o 5 4 2 23.52 3.58 7.84 o 6 4 2 23.06 0.00 9.88 o 7 4 2 52.09 57.23 10.56 o -8 5 2 0.31 0.00 12.01 o -7 5 2 97.43 98.80 10.73 o -6 5 2 45.56 29.47 9.71 o -5 5 2 344.58 366.40 18.40 o -4 5 2 123.28 103.91 8.01 o -3 5 2 15.55 1.53 6.30 o -2 5 2 133.75 108.51 7.15 o -1 5 2 1010.93 1014.88 42.24 o 0 5 2 0.03 0.00 2.16 o 1 5 2 316.34 309.00 14.48 o 2 5 2 1374.47 1411.09 58.60 o 3 5 2 5.64 0.00 5.45 o 4 5 2 113.22 107.48 9.54 o 5 5 2 7.56 0.00 7.84 o 6 5 2 66.68 51.95 10.22 o 7 5 2 8.43 0.00 9.71 o -8 6 2 2.95 0.00 7.32 o -7 6 2 104.67 99.29 8.26 o -6 6 2 40.92 16.35 8.01 o -5 6 2 0.27 0.00 6.81 o -4 6 2 255.15 272.71 14.31 o -3 6 2 0.03 0.00 4.43 o -2 6 2 22.00 10.05 4.09 o -1 6 2 180.11 183.46 9.37 o 0 6 2 1277.23 1370.84 68.90 o 1 6 2 18.81 8.52 4.26 o 2 6 2 674.43 767.04 33.05 o 3 6 2 17.25 7.49 5.96 o 4 6 2 16.68 0.00 6.81 o 5 6 2 3.34 0.00 7.67 o 6 6 2 18.10 0.00 8.69 o 7 6 2 0.99 0.00 9.20 o -8 7 2 2.99 0.00 5.42 o -7 7 2 416.89 549.45 19.63 o -6 7 2 0.01 0.00 7.15 o -5 7 2 387.72 393.48 19.93 o -4 7 2 447.13 461.28 21.80 o -3 7 2 27.74 33.39 5.62 o -2 7 2 84.10 64.56 5.96 o -1 7 2 594.62 560.07 24.36 o 0 7 2 845.48 908.21 32.96 o 1 7 2 929.63 981.66 41.56 o 2 7 2 46.14 32.71 5.96 o 3 7 2 20.42 16.18 6.47 o 4 7 2 19.24 0.00 6.98 o 5 7 2 17.50 16.69 7.84 o 6 7 2 34.01 9.37 9.20 o -7 8 2 37.50 24.87 7.58 o -6 8 2 13.54 0.00 8.35 o -5 8 2 513.70 531.80 25.55 o -4 8 2 16.40 5.62 6.30 o -3 8 2 564.31 543.55 24.70 o -2 8 2 2479.80 2579.27 106.12 o -1 8 2 211.73 222.63 11.58 o 0 8 2 1437.59 1581.39 55.19 o 1 8 2 717.81 785.60 33.90 o 2 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