#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:20 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180896 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/36/2103641.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103641_Fobs loop_ _publ_author_name 'Greenberg, Mark' 'Shteiman, Vitaly' 'Kaftory, Menahem' _publ_section_title ; Topochemically controlled solid-state methyl rearrangement in thiocyanurates ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 428 _journal_page_last 434 _journal_volume 57 _journal_year 2001 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.7120 _cell_length_b 6.7300 _cell_length_c 8.7310 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file av003712sup5.hkl _cod_data_source_block 12 #BEGIN Tags that were not found in dictionaries: _shelx_title ' exp121 Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 269.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6057.04 7199.89 288.42 o 4 0 0 6462.08 7377.17 295.98 o 6 0 0 65.91 72.73 5.49 o 8 0 0 10570.18 12546.11 506.21 o 10 0 0 19.12 32.96 5.49 o 12 0 0 636.25 634.87 28.86 o 14 0 0 143.89 153.04 10.99 o 16 0 0 128.09 157.96 12.63 o 18 0 0 1.23 4.92 8.79 o 2 1 0 2289.99 2212.96 89.21 o 4 1 0 439.75 406.64 17.46 o 6 1 0 2858.75 3061.48 124.17 o 8 1 0 72.78 70.08 6.02 o 10 1 0 281.54 275.96 15.21 o 12 1 0 224.61 219.33 12.96 o 14 1 0 113.18 118.94 10.11 o 16 1 0 285.46 291.87 17.44 o 18 1 0 115.12 116.48 12.78 o 0 2 0 72730.87 67730.56 2725.56 o 2 2 0 3698.46 3618.70 145.88 o 4 2 0 3964.36 3608.28 145.95 o 6 2 0 3.91 2.65 3.79 o 8 2 0 6063.73 6189.25 250.44 o 10 2 0 26.02 14.96 5.57 o 12 2 0 480.54 467.44 22.69 o 14 2 0 87.92 74.43 8.79 o 16 2 0 87.05 105.12 10.95 o 18 2 0 1.22 4.74 9.19 o 2 3 0 706.88 715.42 17.57 o 4 3 0 130.29 113.26 8.07 o 6 3 0 887.84 780.33 33.58 o 8 3 0 52.83 63.64 6.53 o 10 3 0 88.94 85.80 7.86 o 12 3 0 93.72 104.36 9.38 o 14 3 0 55.82 60.80 9.39 o 16 3 0 128.80 133.72 12.54 o 0 4 0 12219.39 12574.52 506.74 o 2 4 0 971.44 925.22 39.47 o 4 4 0 1113.11 986.78 42.18 o 6 4 0 9.93 12.31 5.17 o 8 4 0 1792.01 1622.60 68.32 o 10 4 0 21.92 21.21 6.69 o 12 4 0 182.12 176.90 12.42 o 14 4 0 20.91 25.95 8.09 o 16 4 0 28.81 21.02 9.36 o 2 5 0 163.84 155.69 10.30 o 4 5 0 30.38 31.82 6.21 o 6 5 0 131.15 131.25 9.96 o 8 5 0 30.66 30.30 7.20 o 10 5 0 9.15 22.54 6.88 o 12 5 0 14.90 19.89 7.82 o 14 5 0 14.12 18.94 9.05 o 0 6 0 1967.11 2099.32 88.62 o 2 6 0 199.54 194.14 12.92 o 4 6 0 173.67 179.93 12.61 o 6 6 0 14.35 8.52 6.88 o 8 6 0 369.51 380.70 20.95 o 10 6 0 8.27 0.00 8.88 o 12 6 0 31.44 43.37 9.81 o 2 7 0 37.88 30.87 8.30 o 4 7 0 5.87 0.00 8.79 o 6 7 0 11.35 0.00 8.45 o 8 7 0 9.82 13.45 8.49 o 0 8 0 266.57 285.43 18.90 o 1 0 1 1362.58 1592.86 64.17 o 2 0 1 314.56 373.31 15.66 o 3 0 1 116.58 115.53 6.06 o 4 0 1 4.78 8.33 3.26 o 5 0 1 1286.40 1458.96 59.60 o 6 0 1 718.90 831.09 34.81 o 7 0 1 284.18 364.41 16.61 o 8 0 1 529.82 638.66 27.73 o 9 0 1 611.23 568.96 25.27 o 10 0 1 146.48 160.23 9.94 o 11 0 1 3.79 7.01 5.47 o 12 0 1 196.53 218.38 12.63 o 13 0 1 676.71 725.41 33.01 o 14 0 1 107.62 103.79 9.81 o 15 0 1 1.30 7.58 7.35 o 16 0 1 16.98 19.70 10.38 o 17 0 1 310.84 338.27 19.87 o 18 0 1 4.47 24.24 9.60 o 0 1 1 2748.54 2690.82 108.28 o 1 1 1 4173.00 4310.01 173.09 o 2 1 1 2062.71 2011.06 81.27 o 3 1 1 4795.43 5009.09 201.30 o 4 1 1 42.38 52.84 4.32 o 5 1 1 408.77 379.75 16.72 o 6 1 1 965.06 981.29 40.87 o 7 1 1 1672.02 1755.18 72.48 o 8 1 1 1230.28 1271.07 53.07 o 9 1 1 564.34 547.18 24.45 o 10 1 1 139.68 139.02 9.11 o 11 1 1 881.69 871.43 38.07 o 12 1 1 21.55 8.71 6.34 o 13 1 1 95.36 102.66 9.19 o 14 1 1 22.25 35.42 7.80 o 15 1 1 59.65 57.20 8.98 o 16 1 1 126.94 123.68 12.01 o 17 1 1 52.39 58.90 10.85 o 18 1 1 5.23 6.82 8.86 o 1 2 1 751.97 747.76 31.23 o 2 2 1 258.22 254.37 11.67 o 3 2 1 109.20 88.64 5.74 o 4 2 1 6.27 0.00 4.22 o 5 2 1 795.32 759.50 32.14 o 6 2 1 281.78 278.23 13.43 o 7 2 1 171.95 202.09 10.63 o 8 2 1 308.94 330.32 15.81 o 9 2 1 380.02 350.77 17.01 o 10 2 1 101.67 96.22 8.33 o 11 2 1 3.60 7.39 5.78 o 12 2 1 136.65 142.62 10.28 o 13 2 1 450.65 451.53 22.43 o 14 2 1 85.04 81.06 9.15 o 15 2 1 0.67 0.00 7.92 o 16 2 1 12.27 11.36 8.67 o 17 2 1 221.10 242.24 16.63 o 18 2 1 3.30 0.00 9.55 o 0 3 1 1031.65 938.86 22.76 o 1 3 1 1436.20 1352.97 25.00 o 2 3 1 458.16 418.36 8.37 o 3 3 1 969.81 896.39 16.94 o 4 3 1 23.77 15.91 4.34 o 5 3 1 75.09 54.93 5.34 o 6 3 1 311.14 286.94 14.22 o 7 3 1 689.49 637.33 28.32 o 8 3 1 488.81 448.69 21.08 o 9 3 1 294.18 277.47 14.64 o 10 3 1 44.23 41.48 6.65 o 11 3 1 388.58 364.98 18.85 o 12 3 1 8.35 6.06 6.63 o 13 3 1 35.11 39.77 7.52 o 14 3 1 8.18 15.15 7.24 o 15 3 1 26.25 19.89 8.31 o 16 3 1 60.69 79.55 10.17 o 17 3 1 23.02 48.11 9.17 o 1 4 1 138.28 129.17 8.39 o 2 4 1 72.08 69.89 6.31 o 3 4 1 53.90 47.16 5.80 o 4 4 1 2.34 5.11 4.47 o 5 4 1 227.66 224.06 12.31 o 6 4 1 38.81 40.72 6.63 o 7 4 1 48.01 41.10 6.33 o 8 4 1 81.35 70.08 7.99 o 9 4 1 105.63 94.70 9.00 o 10 4 1 31.33 31.25 7.06 o 11 4 1 1.77 4.17 6.69 o 12 4 1 54.47 48.68 8.47 o 13 4 1 135.80 133.91 11.93 o 14 4 1 40.61 30.11 9.26 o 15 4 1 0.02 0.00 8.85 o 16 4 1 5.36 10.99 8.88 o 0 5 1 300.67 279.56 14.83 o 1 5 1 261.64 322.74 16.44 o 2 5 1 117.55 121.97 8.88 o 3 5 1 125.17 118.38 9.20 o 4 5 1 15.81 20.08 5.83 o 5 5 1 12.09 12.50 5.66 o 6 5 1 72.88 89.59 8.09 o 7 5 1 122.38 116.86 10.04 o 8 5 1 108.82 96.22 9.74 o 9 5 1 76.01 67.62 9.22 o 10 5 1 5.59 4.92 7.48 o 11 5 1 92.46 94.32 10.32 o 12 5 1 0.09 0.00 7.86 o 13 5 1 5.30 13.26 7.90 o 14 5 1 1.07 0.00 9.22 o 1 6 1 25.39 18.37 7.16 o 2 6 1 10.49 9.47 6.80 o 3 6 1 11.69 13.45 6.95 o 4 6 1 0.50 0.00 6.82 o 5 6 1 33.43 35.99 8.35 o 6 6 1 5.02 20.46 7.41 o 7 6 1 12.56 0.00 7.78 o 8 6 1 16.42 12.12 8.07 o 9 6 1 12.46 21.21 8.33 o 10 6 1 4.98 9.66 8.37 o 11 6 1 0.42 0.00 8.56 o 12 6 1 15.02 32.01 8.58 o 0 7 1 70.23 71.03 9.87 o 1 7 1 33.51 40.34 8.83 o 2 7 1 26.98 29.55 8.62 o 3 7 1 8.21 14.96 8.35 o 4 7 1 2.78 0.00 8.13 o 5 7 1 0.39 9.85 7.54 o 6 7 1 12.12 17.24 8.66 o 7 7 1 10.61 7.39 8.92 o 8 7 1 15.49 32.20 9.00 o 0 0 2 5836.12 6425.81 257.83 o 1 0 2 9.47 17.61 3.73 o 2 0 2 129.16 164.21 9.85 o 3 0 2 33.43 36.36 5.81 o 4 0 2 1109.73 1098.53 45.25 o 5 0 2 29.53 32.01 4.43 o 6 0 2 118.82 128.98 7.69 o 7 0 2 202.56 221.41 11.27 o 8 0 2 1988.70 2076.59 85.97 o 9 0 2 224.92 208.15 11.59 o 10 0 2 6.90 8.52 5.38 o 11 0 2 392.09 401.34 19.60 o 12 0 2 1515.80 1508.96 63.94 o 13 0 2 224.27 224.06 14.00 o 14 0 2 7.46 1.14 7.41 o 15 0 2 168.86 162.51 14.03 o 16 0 2 71.53 80.31 10.87 o 17 0 2 0.06 0.38 9.07 o 18 0 2 37.35 4.36 10.87 o 1 1 2 834.09 911.02 37.50 o 2 1 2 725.70 744.16 30.93 o 3 1 2 4476.19 4841.28 194.99 o 4 1 2 100.18 102.28 6.21 o 5 1 2 1435.52 1393.61 57.31 o 6 1 2 176.72 164.40 8.88 o 7 1 2 81.52 67.24 5.93 o 8 1 2 6.26 7.58 4.45 o 9 1 2 62.74 53.03 6.17 o 10 1 2 95.73 103.41 8.13 o 11 1 2 324.93 334.48 17.08 o 12 1 2 217.62 216.30 13.16 o 13 1 2 139.39 142.05 10.87 o 14 1 2 12.94 4.92 7.54 o 15 1 2 14.16 16.10 7.65 o 16 1 2 125.71 124.25 12.06 o 17 1 2 25.65 27.08 10.02 o 18 1 2 98.51 111.18 12.52 o 0 2 2 3214.75 3177.39 128.64 o 1 2 2 5.30 6.06 3.50 o 2 2 2 132.30 137.13 7.54 o 3 2 2 22.35 24.05 4.81 o 4 2 2 882.37 817.64 34.47 o 5 2 2 6.19 5.68 3.77 o 6 2 2 91.59 96.03 6.48 o 7 2 2 77.23 74.62 6.50 o 8 2 2 1324.02 1271.07 53.39 o 9 2 2 155.36 156.07 9.64 o 10 2 2 4.64 0.00 5.76 o 11 2 2 276.47 253.99 14.28 o 12 2 2 1076.20 1011.02 44.45 o 13 2 2 172.83 139.40 11.29 o 14 2 2 3.67 0.00 7.75 o 15 2 2 121.97 98.11 10.61 o 16 2 2 46.93 38.07 9.92 o 17 2 2 0.07 16.86 8.26 o 1 3 2 341.79 311.06 6.54 o 2 3 2 69.69 68.46 2.63 o 3 3 2 1307.52 1236.92 23.12 o 4 3 2 26.49 20.64 4.85 o 5 3 2 507.66 473.50 21.42 o 6 3 2 42.42 32.01 5.36 o 7 3 2 48.42 39.02 5.72 o 8 3 2 2.67 3.22 5.08 o 9 3 2 58.60 63.07 6.99 o 10 3 2 61.14 65.91 7.31 o 11 3 2 188.06 172.17 11.80 o 12 3 2 100.50 86.37 9.64 o 13 3 2 84.54 99.81 9.62 o 14 3 2 13.17 0.00 8.71 o 15 3 2 9.56 8.33 8.35 o 16 3 2 70.60 62.69 10.72 o 0 4 2 818.09 805.52 34.87 o 1 4 2 10.42 8.52 4.75 o 2 4 2 41.28 39.02 5.47 o 3 4 2 13.56 12.69 4.92 o 4 4 2 306.22 273.31 14.11 o 5 4 2 0.58 13.45 4.96 o 6 4 2 17.21 17.05 5.57 o 7 4 2 8.04 21.21 5.57 o 8 4 2 438.03 448.69 22.71 o 9 4 2 45.60 37.69 7.25 o 10 4 2 3.65 0.38 6.69 o 11 4 2 110.86 94.89 9.75 o 12 4 2 400.41 373.31 20.47 o 13 4 2 82.54 71.97 9.72 o 14 4 2 0.02 0.00 8.49 o 15 4 2 47.52 49.24 9.85 o 1 5 2 57.16 57.39 6.76 o 2 5 2 9.08 3.22 6.12 o 3 5 2 246.07 248.68 13.79 o 4 5 2 0.98 0.00 5.44 o 5 5 2 118.34 129.17 9.62 o 6 5 2 17.86 21.59 6.91 o 7 5 2 12.39 17.24 6.88 o 8 5 2 0.33 0.00 6.82 o 9 5 2 25.01 27.27 9.60 o 10 5 2 16.11 23.49 7.75 o 11 5 2 69.09 52.84 9.36 o 12 5 2 21.81 24.81 8.64 o 13 5 2 30.49 22.35 9.41 o 14 5 2 8.91 0.00 9.15 o 0 6 2 133.15 159.85 11.31 o 1 6 2 1.69 10.04 6.38 o 2 6 2 3.45 0.00 6.86 o 3 6 2 4.81 0.57 7.08 o 4 6 2 47.64 59.09 8.22 o 5 6 2 2.17 15.72 6.88 o 6 6 2 0.01 0.00 7.25 o 7 6 2 0.64 0.00 7.65 o 8 6 2 85.96 89.78 10.78 o 9 6 2 6.58 11.74 8.09 o 10 6 2 3.02 8.52 8.31 o 11 6 2 29.25 28.22 9.92 o 1 7 2 3.32 17.24 7.86 o 2 7 2 1.66 4.74 7.50 o 3 7 2 32.46 35.61 9.17 o 4 7 2 0.39 0.00 8.30 o 5 7 2 16.79 19.13 8.88 o 6 7 2 6.49 16.67 8.69 o 7 7 2 0.89 0.00 8.71 o 8 7 2 0.00 1.33 8.20 o 1 0 3 1808.93 2064.09 83.87 o 2 0 3 1342.22 1547.97 63.35 o 3 0 3 16.56 16.86 4.09 o 4 0 3 643.56 705.52 29.94 o 5 0 3 776.17 941.32 39.47 o 6 0 3 7.88 11.55 4.64 o 7 0 3 202.10 193.00 10.66 o 8 0 3 214.29 192.81 10.78 o 9 0 3 32.88 25.76 5.93 o 10 0 3 252.73 262.70 14.66 o 11 0 3 344.68 355.51 18.24 o 12 0 3 126.83 155.31 11.16 o 13 0 3 182.46 189.78 12.88 o 14 0 3 76.20 87.69 9.22 o 15 0 3 234.54 259.67 16.33 o 16 0 3 46.79 56.25 9.72 o 17 0 3 42.89 24.62 9.94 o 0 1 3 1640.74 1624.87 66.42 o 1 1 3 473.80 477.29 20.64 o 2 1 3 0.26 8.52 3.56 o 3 1 3 395.85 388.84 17.41 o 4 1 3 3349.93 3573.81 144.95 o 5 1 3 1168.04 1325.24 54.89 o 6 1 3 1065.83 1165.57 48.77 o 7 1 3 15.94 14.58 4.74 o 8 1 3 1497.22 1487.56 62.07 o 9 1 3 622.56 619.72 27.73 o 10 1 3 21.99 23.68 6.02 o 11 1 3 224.94 218.00 12.78 o 12 1 3 583.12 540.36 25.74 o 13 1 3 266.26 282.59 16.14 o 14 1 3 110.15 132.96 11.36 o 15 1 3 56.32 44.70 9.34 o 16 1 3 119.55 123.68 12.16 o 17 1 3 26.51 38.26 9.75 o 1 2 3 734.43 720.67 30.65 o 2 2 3 765.14 761.20 32.33 o 3 2 3 1.66 0.00 3.94 o 4 2 3 388.51 401.72 18.28 o 5 2 3 366.15 412.52 18.81 o 6 2 3 5.57 1.14 4.51 o 7 2 3 176.68 179.55 11.08 o 8 2 3 129.73 122.92 8.52 o 9 2 3 17.96 17.61 5.53 o 10 2 3 184.85 166.29 11.27 o 11 2 3 218.27 202.28 12.82 o 12 2 3 98.55 110.23 9.58 o 13 2 3 126.69 118.19 10.93 o 14 2 3 52.38 46.97 8.81 o 15 2 3 167.38 170.46 13.71 o 16 2 3 33.23 36.36 9.94 o 17 2 3 30.88 40.91 10.02 o 0 3 3 552.17 493.49 16.50 o 1 3 3 239.78 232.13 5.35 o 2 3 3 21.34 22.47 2.44 o 3 3 3 216.98 208.24 4.99 o 4 3 3 1202.17 1183.60 102.75 o 5 3 3 410.79 416.68 19.51 o 6 3 3 507.97 500.21 23.07 o 7 3 3 18.05 8.90 6.27 o 8 3 3 677.14 602.86 27.61 o 9 3 3 272.94 267.62 14.75 o 10 3 3 17.50 23.30 6.53 o 11 3 3 114.19 114.59 10.08 o 12 3 3 293.12 251.52 16.16 o 13 3 3 134.39 134.66 12.84 o 14 3 3 66.13 100.38 10.59 o 15 3 3 17.69 25.95 9.91 o 16 3 3 59.80 65.72 10.49 o 1 4 3 109.61 121.78 8.37 o 2 4 3 190.84 189.97 11.21 o 3 4 3 1.21 0.00 4.87 o 4 4 3 126.62 134.66 9.26 o 5 4 3 90.94 91.86 8.20 o 6 4 3 5.63 12.50 5.57 o 7 4 3 72.88 81.63 8.13 o 8 4 3 33.18 28.60 6.89 o 9 4 3 6.45 0.00 6.69 o 10 4 3 78.21 76.71 8.92 o 11 4 3 68.58 81.06 9.20 o 12 4 3 50.90 47.16 9.00 o 13 4 3 52.72 51.90 10.10 o 14 4 3 18.80 32.96 8.92 o 15 4 3 59.86 67.99 11.14 o 0 5 3 126.16 133.53 9.79 o 1 5 3 52.94 63.07 7.20 o 2 5 3 9.35 5.30 6.23 o 3 5 3 57.22 67.81 7.88 o 4 5 3 253.41 279.75 15.74 o 5 5 3 56.40 64.78 7.67 o 6 5 3 136.24 164.02 11.31 o 7 5 3 7.39 15.34 6.86 o 8 5 3 173.38 193.38 13.14 o 9 5 3 55.86 24.62 8.50 o 10 5 3 6.24 6.25 7.63 o 11 5 3 27.87 31.82 8.69 o 12 5 3 82.81 86.94 10.83 o 13 5 3 36.61 34.66 9.79 o 1 6 3 14.87 16.10 7.54 o 2 6 3 32.21 43.37 8.26 o 3 6 3 1.20 0.76 7.33 o 4 6 3 36.73 35.99 8.49 o 5 6 3 21.24 28.22 7.95 o 6 6 3 5.05 8.14 7.58 o 7 6 3 14.93 21.02 8.30 o 8 6 3 3.45 9.66 7.86 o 9 6 3 1.87 1.89 8.75 o 10 6 3 22.10 32.39 9.15 o 11 6 3 13.49 14.02 9.60 o 0 7 3 14.59 28.60 8.79 o 1 7 3 5.97 4.74 8.14 o 2 7 3 0.74 0.00 8.66 o 3 7 3 7.81 6.82 8.88 o 4 7 3 29.74 55.12 9.15 o 5 7 3 2.57 9.47 8.75 o 6 7 3 25.38 13.07 10.10 o 7 7 3 1.03 0.00 8.94 o 0 0 4 29.88 31.06 5.21 o 1 0 4 284.33 327.10 15.28 o 2 0 4 4997.71 5819.54 235.71 o 3 0 4 3319.36 3827.60 155.52 o 4 0 4 101.17 119.32 7.84 o 5 0 4 5.24 8.52 4.98 o 6 0 4 1885.97 1979.05 81.58 o 7 0 4 735.05 767.26 33.43 o 8 0 4 1.87 3.03 5.53 o 9 0 4 5.80 0.95 6.12 o 10 0 4 1226.06 1251.18 53.52 o 11 0 4 864.30 811.39 36.50 o 12 0 4 14.42 6.44 7.52 o 13 0 4 7.35 4.36 7.50 o 14 0 4 170.74 168.00 13.43 o 15 0 4 21.58 37.31 8.43 o 16 0 4 7.91 13.64 9.09 o 17 0 4 0.07 0.00 9.13 o 1 1 4 1417.99 1532.63 63.32 o 2 1 4 806.16 922.38 38.90 o 3 1 4 96.58 90.53 6.86 o 4 1 4 599.34 612.14 26.78 o 5 1 4 104.79 98.87 7.24 o 6 1 4 3.03 12.69 4.87 o 7 1 4 34.51 31.82 5.42 o 8 1 4 290.59 303.61 15.68 o 9 1 4 1272.79 1210.27 51.93 o 10 1 4 26.94 25.19 7.10 o 11 1 4 45.70 45.65 7.67 o 12 1 4 177.26 173.30 12.12 o 13 1 4 97.88 90.15 9.92 o 14 1 4 45.07 45.27 8.96 o 15 1 4 1.81 0.00 8.47 o 16 1 4 23.19 30.49 8.96 o 17 1 4 158.19 167.05 14.17 o 0 2 4 49.91 48.11 5.44 o 1 2 4 113.12 113.64 7.44 o 2 2 4 2896.66 2987.23 121.61 o 3 2 4 1964.74 2001.97 82.35 o 4 2 4 63.95 53.03 5.91 o 5 2 4 5.50 14.58 5.09 o 6 2 4 1220.09 1194.55 50.55 o 7 2 4 432.43 409.67 19.66 o 8 2 4 0.34 0.19 5.38 o 9 2 4 5.84 9.66 6.19 o 10 2 4 874.23 838.48 37.44 o 11 2 4 623.38 588.09 27.86 o 12 2 4 6.29 0.00 7.12 o 13 2 4 7.30 4.74 7.82 o 14 2 4 120.63 139.78 12.33 o 15 2 4 14.48 20.83 8.43 o 16 2 4 4.39 0.00 8.83 o 1 3 4 593.15 589.98 26.33 o 2 3 4 257.25 250.96 13.18 o 3 3 4 97.47 95.65 7.71 o 4 3 4 234.17 216.49 12.18 o 5 3 4 66.28 72.54 9.89 o 6 3 4 2.19 0.00 5.59 o 7 3 4 15.93 16.48 5.99 o 8 3 4 135.40 131.44 9.85 o 9 3 4 588.92 561.76 26.63 o 10 3 4 13.13 17.24 6.89 o 11 3 4 26.68 37.12 7.84 o 12 3 4 89.62 73.68 9.64 o 13 3 4 37.53 46.97 8.62 o 14 3 4 17.83 12.12 8.30 o 15 3 4 0.98 6.06 8.81 o 0 4 4 21.79 12.50 6.29 o 1 4 4 19.93 9.09 6.04 o 2 4 4 777.36 746.05 33.37 o 3 4 4 527.86 529.19 24.74 o 4 4 4 22.25 19.70 6.19 o 5 4 4 6.03 15.15 5.99 o 6 4 4 391.00 360.62 18.62 o 7 4 4 122.96 111.94 9.70 o 8 4 4 5.10 0.00 6.84 o 9 4 4 3.66 2.46 6.80 o 10 4 4 342.46 326.34 18.69 o 11 4 4 247.34 231.26 15.53 o 12 4 4 0.05 9.85 7.50 o 13 4 4 6.35 9.28 8.31 o 14 4 4 42.50 64.96 9.96 o 1 5 4 178.53 187.70 12.24 o 2 5 4 64.04 61.74 7.95 o 3 5 4 49.22 54.17 7.95 o 4 5 4 50.91 41.67 7.44 o 5 5 4 19.88 13.26 7.46 o 6 5 4 0.30 0.57 6.84 o 7 5 4 5.17 12.69 6.63 o 8 5 4 39.13 34.85 8.16 o 9 5 4 153.78 139.97 12.29 o 10 5 4 6.64 0.76 9.68 o 11 5 4 8.40 6.63 8.79 o 12 5 4 23.79 33.71 9.26 o 0 6 4 2.42 0.00 7.46 o 1 6 4 2.58 0.00 7.59 o 2 6 4 123.25 134.85 11.82 o 3 6 4 90.62 103.22 10.23 o 4 6 4 6.60 7.95 7.75 o 5 6 4 6.01 9.85 7.73 o 6 6 4 68.01 83.34 10.06 o 7 6 4 22.45 24.81 9.20 o 8 6 4 4.15 3.79 8.35 o 9 6 4 1.93 0.00 8.69 o 10 6 4 80.24 103.41 12.31 o 1 7 4 38.10 42.05 9.75 o 2 7 4 13.32 15.15 8.66 o 3 7 4 14.25 29.93 9.13 o 4 7 4 8.13 15.91 8.85 o 5 7 4 2.71 17.05 9.03 o 1 0 5 359.25 363.65 17.44 o 2 0 5 23.77 26.33 6.78 o 3 0 5 723.08 730.71 31.90 o 4 0 5 61.22 73.49 7.22 o 5 0 5 415.31 389.79 18.86 o 6 0 5 231.33 216.86 12.54 o 7 0 5 1099.14 1005.91 43.49 o 8 0 5 119.09 135.80 9.96 o 9 0 5 8.00 7.95 6.99 o 10 0 5 65.54 71.03 8.77 o 11 0 5 51.38 56.82 8.86 o 12 0 5 5.16 0.00 7.90 o 13 0 5 7.54 0.00 7.84 o 14 0 5 31.65 33.71 9.02 o 15 0 5 362.40 382.78 21.72 o 16 0 5 53.22 42.24 10.40 o 0 1 5 459.39 498.12 22.58 o 1 1 5 923.89 998.33 42.43 o 2 1 5 296.21 306.45 15.17 o 3 1 5 465.88 431.08 20.15 o 4 1 5 691.37 664.04 29.43 o 5 1 5 518.65 562.33 25.53 o 6 1 5 21.85 18.18 5.63 o 7 1 5 39.23 28.79 6.46 o 8 1 5 2.11 14.02 5.93 o 9 1 5 978.87 976.93 42.80 o 10 1 5 891.47 910.45 40.55 o 11 1 5 18.83 17.99 7.69 o 12 1 5 0.14 1.70 7.46 o 13 1 5 29.76 28.79 8.71 o 14 1 5 8.16 0.00 8.75 o 15 1 5 34.43 32.77 10.32 o 16 1 5 2.51 6.82 9.45 o 1 2 5 262.05 248.68 13.26 o 2 2 5 13.29 7.77 5.02 o 3 2 5 470.59 474.83 22.50 o 4 2 5 33.48 47.16 6.17 o 5 2 5 291.30 289.03 15.08 o 6 2 5 130.97 114.97 8.94 o 7 2 5 757.23 693.40 31.38 o 8 2 5 90.15 78.98 8.41 o 9 2 5 4.84 10.61 6.33 o 10 2 5 42.68 42.43 7.73 o 11 2 5 31.03 32.58 8.47 o 12 2 5 2.23 0.00 7.33 o 13 2 5 4.79 12.50 7.67 o 14 2 5 23.03 22.35 8.79 o 15 2 5 258.99 283.15 18.18 o 0 3 5 183.32 177.47 10.99 o 1 3 5 404.11 415.92 19.94 o 2 3 5 160.02 166.29 10.42 o 3 3 5 129.93 111.56 8.90 o 4 3 5 276.55 263.27 14.43 o 5 3 5 202.74 204.93 12.46 o 6 3 5 10.80 13.45 5.76 o 7 3 5 12.70 7.77 6.57 o 8 3 5 0.89 5.49 6.46 o 9 3 5 513.77 490.93 24.34 o 10 3 5 455.27 442.25 22.67 o 11 3 5 3.59 0.00 7.50 o 12 3 5 0.13 0.00 7.84 o 13 3 5 12.46 24.43 8.33 o 14 3 5 2.43 0.00 8.92 o 1 4 5 104.73 100.19 8.92 o 2 4 5 0.55 0.00 5.78 o 3 4 5 153.33 162.70 11.17 o 4 4 5 7.13 3.22 6.59 o 5 4 5 107.21 101.71 9.53 o 6 4 5 31.23 28.03 7.25 o 7 4 5 259.75 294.71 16.46 o 8 4 5 41.03 44.51 8.58 o 9 4 5 1.66 0.00 7.71 o 10 4 5 11.55 14.21 7.73 o 11 4 5 5.45 0.00 8.43 o 12 4 5 0.01 0.00 8.54 o 13 4 5 1.60 3.41 8.43 o 0 5 5 27.86 23.30 7.58 o 1 5 5 91.45 97.54 9.41 o 2 5 5 45.92 50.19 8.28 o 3 5 5 16.14 16.86 7.56 o 4 5 5 46.27 46.40 8.62 o 5 5 5 50.31 61.74 8.71 o 6 5 5 1.44 6.82 7.35 o 7 5 5 0.23 3.41 8.07 o 8 5 5 0.07 0.00 8.62 o 9 5 5 152.47 154.93 12.86 o 10 5 5 134.97 141.10 13.11 o 11 5 5 0.02 1.14 8.96 o 1 6 5 24.32 13.83 8.73 o 2 6 5 0.65 0.57 8.24 o 3 6 5 26.24 54.36 9.34 o 4 6 5 1.07 0.00 8.26 o 5 6 5 20.58 25.38 9.02 o 6 6 5 4.35 0.00 8.94 o 7 6 5 46.39 64.59 10.49 o 8 6 5 11.87 11.55 9.49 o 0 7 5 2.07 9.28 8.83 o 1 7 5 12.69 9.28 10.11 o 0 0 6 0.02 0.38 6.46 o 1 0 6 636.96 622.18 28.16 o 2 0 6 1770.10 1795.90 74.87 o 3 0 6 1.29 0.00 6.61 o 4 0 6 99.97 107.01 9.22 o 5 0 6 4.46 0.00 6.27 o 6 0 6 1245.05 1181.29 50.84 o 7 0 6 274.15 272.55 15.59 o 8 0 6 22.84 28.22 7.75 o 9 0 6 223.16 206.64 13.45 o 10 0 6 698.12 656.65 31.19 o 11 0 6 31.59 31.63 8.83 o 12 0 6 95.49 86.37 10.59 o 13 0 6 10.64 15.72 8.60 o 14 0 6 191.62 199.82 15.44 o 15 0 6 45.94 33.71 10.64 o 1 1 6 238.41 210.42 12.52 o 2 1 6 55.65 59.09 7.25 o 3 1 6 0.07 0.00 6.00 o 4 1 6 25.79 31.82 6.95 o 5 1 6 0.32 3.60 5.91 o 6 1 6 252.58 269.14 14.98 o 7 1 6 117.44 108.53 9.43 o 8 1 6 10.59 14.96 6.67 o 9 1 6 52.63 37.12 8.18 o 10 1 6 72.24 59.85 8.98 o 11 1 6 16.77 9.09 7.99 o 12 1 6 11.03 0.00 8.03 o 13 1 6 5.14 4.17 8.60 o 14 1 6 66.82 67.43 11.08 o 15 1 6 52.13 52.84 11.04 o 0 2 6 5.50 0.00 5.99 o 1 2 6 481.50 475.78 22.65 o 2 2 6 1273.56 1252.70 53.41 o 3 2 6 0.35 1.89 5.80 o 4 2 6 71.82 71.40 8.13 o 5 2 6 3.43 1.33 8.28 o 6 2 6 883.04 861.59 38.60 o 7 2 6 187.03 166.67 11.84 o 8 2 6 20.60 15.91 7.08 o 9 2 6 170.48 158.72 11.93 o 10 2 6 489.58 458.54 23.50 o 11 2 6 21.82 25.00 8.50 o 12 2 6 68.35 65.34 9.72 o 13 2 6 5.72 11.93 7.97 o 14 2 6 134.01 136.37 13.16 o 1 3 6 110.60 101.14 9.02 o 2 3 6 24.21 26.14 6.67 o 3 3 6 0.27 0.00 6.27 o 4 3 6 10.90 7.58 6.99 o 5 3 6 0.24 0.00 6.50 o 6 3 6 104.65 109.85 10.21 o 7 3 6 59.98 49.05 8.49 o 8 3 6 6.31 4.74 7.05 o 9 3 6 31.66 25.76 8.09 o 10 3 6 29.09 35.99 8.56 o 11 3 6 14.13 0.00 9.58 o 12 3 6 4.75 0.00 8.73 o 13 3 6 2.58 4.55 8.98 o 0 4 6 17.97 24.81 7.06 o 1 4 6 193.17 203.80 13.01 o 2 4 6 490.46 471.04 23.83 o 3 4 6 0.91 4.17 6.65 o 4 4 6 42.59 60.04 8.26 o 5 4 6 0.75 7.58 7.20 o 6 4 6 320.89 319.71 17.84 o 7 4 6 55.59 53.79 9.17 o 8 4 6 11.23 7.20 8.09 o 9 4 6 74.91 75.00 10.17 o 10 4 6 174.02 164.02 13.58 o 11 4 6 6.81 18.56 8.86 o 12 4 6 28.35 21.21 9.47 o 1 5 6 29.57 36.36 8.24 o 2 5 6 5.48 5.49 7.94 o 3 5 6 1.26 7.58 7.88 o 4 5 6 2.83 0.00 11.57 o 5 5 6 0.43 0.00 7.94 o 6 5 6 21.07 40.53 9.07 o 7 5 6 15.86 23.11 9.19 o 8 5 6 2.32 0.00 8.79 o 9 5 6 13.04 32.01 9.11 o 0 6 6 13.25 0.00 9.17 o 1 6 6 44.00 73.30 9.39 o 2 6 6 108.82 133.15 12.52 o 3 6 6 2.91 3.98 8.58 o 4 6 6 18.61 8.33 9.75 o 5 6 6 0.00 0.00 8.90 o 6 6 6 62.80 79.74 11.67 o 1 0 7 30.09 33.15 7.88 o 2 0 7 116.28 123.68 10.38 o 3 0 7 163.02 169.32 12.10 o 4 0 7 1.65 0.00 8.54 o 5 0 7 125.90 147.35 11.38 o 6 0 7 20.89 16.48 7.75 o 7 0 7 35.23 46.59 8.54 o 8 0 7 72.18 65.15 9.24 o 9 0 7 20.34 2.46 8.69 o 10 0 7 23.25 14.58 9.13 o 11 0 7 16.09 0.00 46.65 o 12 0 7 9.20 0.00 9.43 o 13 0 7 0.74 0.00 9.49 o 0 1 7 161.58 140.35 11.08 o 1 1 7 33.21 43.56 7.75 o 2 1 7 1688.50 1673.17 70.65 o 3 1 7 856.37 782.23 35.42 o 4 1 7 495.23 471.42 23.22 o 5 1 7 27.07 22.73 7.52 o 6 1 7 698.75 716.31 33.11 o 7 1 7 0.01 0.00 7.06 o 8 1 7 11.62 0.00 7.65 o 9 1 7 30.46 35.04 8.45 o 10 1 7 567.12 575.21 28.52 o 11 1 7 64.04 52.09 9.83 o 12 1 7 11.28 8.71 8.66 o 13 1 7 11.34 24.81 9.22 o 1 2 7 25.85 20.64 7.10 o 2 2 7 86.65 87.31 9.19 o 3 2 7 102.65 113.07 10.27 o 4 2 7 0.75 0.00 7.12 o 5 2 7 83.43 77.65 9.26 o 6 2 7 19.33 19.89 7.88 o 7 2 7 25.06 13.26 8.09 o 8 2 7 51.75 35.61 8.83 o 9 2 7 12.04 4.74 8.43 o 10 2 7 17.93 8.71 9.07 o 11 2 7 13.08 0.00 9.58 o 12 2 7 6.16 11.55 8.45 o 0 3 7 91.57 91.10 9.60 o 1 3 7 16.07 25.95 7.39 o 2 3 7 861.80 839.24 38.24 o 3 3 7 426.39 411.95 21.40 o 4 3 7 280.72 259.86 16.04 o 5 3 7 14.44 6.06 7.88 o 6 3 7 356.69 351.53 19.64 o 7 3 7 0.05 17.80 7.46 o 8 3 7 9.71 2.27 8.13 o 9 3 7 13.97 32.77 8.75 o 10 3 7 307.20 346.79 20.25 o 11 3 7 34.03 20.83 9.55 o 1 4 7 19.31 12.12 7.71 o 2 4 7 37.43 38.64 8.07 o 3 4 7 27.31 29.93 8.81 o 4 4 7 0.01 0.00 7.77 o 5 4 7 26.97 15.91 8.81 o 6 4 7 12.17 7.39 8.71 o 7 4 7 7.92 13.64 8.43 o 8 4 7 20.50 25.00 11.55 o 9 4 7 2.71 0.00 9.45 o 10 4 7 8.53 0.00 11.74 o 0 5 7 27.88 34.28 8.49 o 1 5 7 7.90 9.66 8.31 o 2 5 7 248.13 248.49 16.88 o 3 5 7 119.72 120.84 12.41 o 4 5 7 105.75 96.22 11.59 o 5 5 7 3.24 0.00 9.13 o 6 5 7 97.51 92.05 11.93 o 7 5 7 0.18 6.25 8.86 o 0 0 8 1.18 0.00 8.39 o 1 0 8 270.46 275.20 16.76 o 2 0 8 3.08 11.74 7.99 o 3 0 8 21.95 27.84 8.60 o 4 0 8 71.22 69.32 9.49 o 5 0 8 164.07 174.06 12.63 o 6 0 8 31.56 25.19 8.66 o 7 0 8 57.38 48.87 9.85 o 8 0 8 0.03 0.00 8.33 o 9 0 8 133.45 162.13 13.39 o 10 0 8 0.31 1.33 8.85 o 11 0 8 26.06 51.71 10.06 o 1 1 8 53.86 55.68 9.22 o 2 1 8 118.38 111.94 10.28 o 3 1 8 1.57 15.53 7.63 o 4 1 8 12.21 40.15 8.13 o 5 1 8 0.04 0.00 7.78 o 6 1 8 5.97 0.00 8.18 o 7 1 8 143.89 151.33 12.52 o 8 1 8 17.79 22.54 9.45 o 9 1 8 95.60 110.42 11.82 o 10 1 8 75.53 77.28 10.87 o 11 1 8 265.21 290.92 19.19 o 0 2 8 1.80 9.28 7.84 o 1 2 8 184.43 182.01 13.22 o 2 2 8 2.34 0.19 7.65 o 3 2 8 15.10 23.68 8.03 o 4 2 8 52.52 59.47 8.69 o 5 2 8 99.51 97.92 10.74 o 6 2 8 22.76 21.59 8.30 o 7 2 8 41.84 45.27 8.88 o 8 2 8 0.02 6.44 8.85 o 9 2 8 90.45 91.86 11.06 o 10 2 8 0.14 0.00 9.17 o 1 3 8 27.98 25.95 8.90 o 2 3 8 74.06 73.68 9.96 o 3 3 8 0.22 0.00 8.73 o 4 3 8 6.59 13.83 8.47 o 5 3 8 0.03 0.00 7.84 o 6 3 8 4.24 0.95 8.24 o 7 3 8 73.48 93.37 11.04 o 8 3 8 10.77 21.97 8.79 o 9 3 8 48.59 49.62 10.87 o 0 4 8 2.92 14.21 8.35 o 1 4 8 61.74 72.54 10.13 o 2 4 8 1.09 16.86 8.45 o 3 4 8 5.56 22.35 8.73 o 4 4 8 21.76 18.18 8.92 o 5 4 8 22.12 46.21 8.67 o 6 4 8 9.00 31.44 8.41 o 7 4 8 16.62 19.89 9.34 o 1 5 8 5.89 15.53 8.83 o 2 5 8 28.54 39.96 8.94 o 1 0 9 176.56 167.05 14.09 o 2 0 9 12.23 15.53 9.81 o 3 0 9 30.83 37.50 9.74 o 4 0 9 3.33 0.00 8.71 o 5 0 9 21.79 27.84 9.83 o 6 0 9 0.68 0.00 9.39 o 7 0 9 77.06 92.43 12.29 o 8 0 9 15.85 26.89 9.89 o 9 0 9 55.93 50.00 11.67 o 0 1 9 7.00 14.96 8.18 o 1 1 9 2.52 4.36 9.32 o 2 1 9 602.68 604.38 30.04 o 3 1 9 16.78 29.55 9.15 o 4 1 9 5.00 6.06 8.98 o 5 1 9 61.08 41.48 10.44 o 6 1 9 370.15 350.58 21.08 o 7 1 9 11.45 1.89 9.32 o 8 1 9 0.00 0.00 9.36 o 9 1 9 10.71 24.43 9.72 o 1 2 9 121.92 109.28 11.82 o 2 2 9 8.96 27.46 9.09 o 3 2 9 19.91 20.83 9.32 o 4 2 9 1.82 2.65 8.43 o 5 2 9 15.77 25.19 9.53 o 6 2 9 0.49 6.63 8.88 o 7 2 9 58.15 82.01 11.19 o 8 2 9 10.39 21.97 9.60 o 0 3 9 5.64 9.47 8.94 o 1 3 9 2.15 0.00 9.11 o 2 3 9 305.25 324.63 19.45 o 3 3 9 8.87 9.47 10.11 o 4 3 9 5.56 4.92 8.62 o 5 3 9 32.40 14.58 10.38 o 6 3 9 191.87 188.26 15.59 o 0 0 10 193.78 185.23 14.92 o 1 0 10 148.16 145.27 14.03 o 2 0 10 73.44 79.36 12.14 o 3 0 10 8.20 0.00 10.13 o 4 0 10 84.96 72.54 12.16 o 5 0 10 125.56 132.01 14.45 o 1 1 10 93.45 112.13 12.96 o 2 1 10 18.45 17.80 11.76 o 3 1 10 18.93 2.84 10.32 o 4 1 10 21.40 25.95 10.17 o 0 2 10 143.52 134.47 14.15 o 1 2 10 105.03 110.80 13.24 o