#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/36/2103648.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103648_Fobs
loop_
_publ_author_name
'Saraswathi, N. T.'
'Manoj, N.'
'Vijayan, M.'
_publ_section_title
;
X-ray studies on crystalline complexes involving amino acids and
peptides. XXXVII. Novel aggregation patterns and effect of chirality
in the complexes of DL- and L-lysine
with glutaric acid
;
_journal_issue 3
_journal_name_full 'Acta Crystallographica Section B'
_journal_page_first 366
_journal_page_last 371
_journal_volume 57
_journal_year 2001
_space_group_IT_number 144
_symmetry_space_group_name_Hall 'P 31'
_symmetry_space_group_name_H-M 'P 31'
_cell_angle_alpha 90.000
_cell_angle_beta 90.000
_cell_angle_gamma 120.000
_cell_length_a 9.0440
_cell_length_b 9.0440
_cell_length_c 14.9430
_exptl_crystal_F_000 450.00
_reflns_d_resolution_high .7959
_[local]_cod_data_source_file de0009IIsup3.hkl
_[local]_cod_data_source_block II
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' L Lysine and Glutaric acid'
_shelx_refln_list_code 4
_shelx_F_calc_maximum 74.72
_shelx_F_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z+1/3'
'-x+y, -x, z+2/3'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 1 0 1059.60 996.88 21.22 o
-1 2 0 1441.36 1268.00 10.80 o
0 2 0 1448.71 1444.51 16.34 o
-2 3 0 440.97 387.26 2.02 o
-1 3 0 446.72 390.63 2.02 o
0 3 0 373.98 372.36 2.72 o
-3 4 0 500.60 484.92 2.76 o
-2 4 0 559.83 519.71 2.76 o
-1 4 0 131.68 146.80 1.55 o
0 4 0 943.31 950.52 15.18 o
-4 5 0 284.51 299.52 2.62 o
-3 5 0 52.56 45.56 1.01 o
-2 5 0 158.01 157.25 1.83 o
-1 5 0 238.89 250.26 2.39 o
0 5 0 144.14 151.10 2.72 o
-5 6 0 320.95 313.42 3.08 o
-4 6 0 84.68 90.58 1.60 o
-3 6 0 102.61 98.67 1.67 o
-2 6 0 131.69 127.84 1.91 o
-1 6 0 54.78 55.09 1.35 o
0 6 0 9.91 11.59 .35 o
-6 7 0 164.48 165.80 2.52 o
-5 7 0 99.88 105.61 1.96 o
-4 7 0 49.71 45.05 1.16 o
-3 7 0 130.44 117.81 2.03 o
-2 7 0 29.00 26.89 .78 o
-1 7 0 140.90 144.91 2.41 o
0 7 0 8.62 9.76 .35 o
-7 8 0 5.17 5.59 .42 o
-6 8 0 30.37 32.39 .96 o
-5 8 0 135.55 132.84 2.36 o
-4 8 0 21.08 27.32 .78 o
-3 8 0 14.82 17.22 .62 o
-2 8 0 185.20 210.51 2.98 o
-1 8 0 78.27 94.64 1.99 o
0 8 0 7.16 6.49 .30 o
-8 9 0 9.42 8.83 .42 o
-7 9 0 8.95 7.36 .44 o
-6 9 0 49.19 60.72 1.63 o
-5 9 0 15.87 17.65 .59 o
-4 9 0 9.74 16.17 .58 o
-3 9 0 56.87 37.66 1.14 o
-2 9 0 1.02 .79 .29 o
-1 9 0 12.74 17.78 .54 o
0 9 0 1.49 1.25 .20 o
-9 10 0 4.39 2.67 .31 o
-8 10 0 19.24 16.21 .49 o
-7 10 0 14.35 19.81 .61 o
-6 10 0 5.30 7.11 .42 o
-5 10 0 1.33 .45 .28 o
-4 10 0 41.89 17.16 .85 o
-3 10 0 40.03 12.81 .75 o
-2 10 0 14.27 21.84 .61 o
-1 10 0 4.79 5.36 .27 o
-7 11 0 11.65 15.60 .47 o
-6 11 0 10.49 .14 .49 o
-5 11 0 6.72 .13 .31 o
-4 11 0 15.16 22.21 .64 o
-1 1 1 75.43 66.91 1.20 o
0 1 1 1095.89 1011.41 41.21 o
1 1 1 4529.99 4679.46 24.53 o
-3 2 1 1270.57 1179.52 13.17 o
-2 2 1 4350.34 4583.69 167.61 o
-1 2 1 2665.40 2531.40 16.75 o
0 2 1 5411.85 5226.09 150.64 o
1 2 1 1202.99 1180.90 12.97 o
2 2 1 499.34 492.68 2.78 o
-5 3 1 676.27 649.98 3.80 o
-4 3 1 423.74 417.81 2.64 o
-3 3 1 1414.56 1354.57 18.67 o
-2 3 1 463.04 413.41 2.08 o
-1 3 1 274.04 249.16 1.67 o
0 3 1 655.77 668.38 5.03 o
1 3 1 1178.33 1186.85 4.44 o
2 3 1 139.25 139.42 1.72 o
3 3 1 109.86 102.92 1.71 o
-7 4 1 41.66 41.48 1.11 o
-6 4 1 124.27 110.83 1.82 o
-5 4 1 53.98 63.50 1.23 o
-4 4 1 354.59 329.30 4.63 o
-3 4 1 149.58 160.43 1.62 o
-2 4 1 676.45 650.48 3.22 o
-1 4 1 697.92 700.20 3.34 o
0 4 1 74.93 75.12 1.10 o
1 4 1 31.78 34.08 .93 o
2 4 1 11.55 13.62 .45 o
3 4 1 139.51 135.82 2.18 o
4 4 1 202.81 224.20 3.01 o
-9 5 1 70.53 63.06 1.73 o
-8 5 1 103.69 115.95 2.20 o
-7 5 1 14.08 15.58 .55 o
-6 5 1 147.40 163.69 2.27 o
-5 5 1 241.05 271.80 7.50 o
-4 5 1 7.88 9.38 .35 o
-3 5 1 127.40 118.76 1.59 o
-2 5 1 345.81 322.84 2.64 o
-1 5 1 53.37 51.14 1.10 o
0 5 1 19.49 23.34 .49 o
1 5 1 50.69 55.85 1.36 o
2 5 1 51.60 58.14 1.52 o
3 5 1 18.52 24.50 .74 o
4 5 1 38.90 41.41 1.17 o
5 5 1 6.27 4.84 .44 o
-11 6 1 22.94 25.72 15.52 o
-10 6 1 14.91 8.49 .53 o
-9 6 1 104.75 77.72 2.00 o
-8 6 1 138.22 177.30 2.73 o
-7 6 1 241.13 279.45 3.28 o
-6 6 1 156.77 151.94 5.95 o
-5 6 1 109.01 128.23 2.01 o
-4 6 1 236.12 240.68 2.62 o
-3 6 1 155.42 147.75 2.05 o
-2 6 1 133.13 148.06 2.05 o
-1 6 1 87.49 76.62 1.55 o
0 6 1 388.37 392.78 4.91 o
1 6 1 10.22 11.07 .51 o
2 6 1 26.01 21.30 .65 o
3 6 1 39.28 50.06 1.48 o
4 6 1 5.11 4.39 .40 o
5 6 1 4.37 4.44 2.48 o
-11 7 1 4.54 7.99 .28 o
-10 7 1 18.70 4.40 .56 o
-9 7 1 1.69 2.33 .35 o
-8 7 1 2.32 4.01 .40 o
-7 7 1 38.71 42.63 2.24 o
-6 7 1 7.53 7.50 .45 o
-5 7 1 71.56 54.17 1.44 o
-4 7 1 34.53 36.78 1.07 o
-3 7 1 29.71 41.56 1.11 o
-2 7 1 282.16 283.39 3.23 o
-1 7 1 112.24 126.65 2.25 o
0 7 1 14.22 14.97 1.66 o
1 7 1 19.86 23.75 .71 o
2 7 1 5.99 8.60 .45 o
3 7 1 22.20 27.28 .85 o
4 7 1 3.60 5.74 .24 o
-10 8 1 .36 .41 .22 o
-9 8 1 46.16 55.77 1.39 o
-8 8 1 52.94 57.58 1.08 o
-7 8 1 33.33 39.49 1.20 o
-6 8 1 55.05 56.43 1.60 o
-5 8 1 94.05 100.80 2.05 o
-4 8 1 251.19 304.79 3.51 o
-3 8 1 161.43 198.86 2.83 o
-2 8 1 121.27 135.19 2.43 o
-1 8 1 65.62 70.76 1.76 o
0 8 1 67.69 76.19 2.04 o
1 8 1 64.57 72.16 1.58 o
2 8 1 10.04 11.17 .45 o
-10 9 1 14.56 19.38 .56 o
-9 9 1 10.78 16.00 1.24 o
-8 9 1 9.86 7.20 .39 o
-7 9 1 5.53 6.35 .41 o
-6 9 1 40.20 41.36 1.17 o
-5 9 1 57.26 49.79 1.47 o
-4 9 1 14.81 13.84 .57 o
-3 9 1 10.33 4.70 .42 o
-2 9 1 27.49 12.73 .53 o
-1 9 1 1.13 1.55 .29 o
0 9 1 .18 .11 .20 o
1 9 1 5.81 5.83 2.44 o
-9 10 1 2.62 3.74 1.69 o
-8 10 1 8.85 9.01 .38 o
-7 10 1 5.98 7.18 .39 o
-6 10 1 2.98 2.84 .34 o
-5 10 1 69.46 32.28 1.01 o
-4 10 1 6.51 2.75 .41 o
-3 10 1 21.59 6.58 .51 o
-2 10 1 2.15 3.80 .30 o
-1 10 1 11.24 12.50 .37 o
-7 11 1 4.62 5.69 .25 o
-6 11 1 4.09 7.60 4.25 o
-5 11 1 1.67 .77 .48 o
-4 11 1 17.38 17.86 .50 o
-1 1 2 340.99 347.10 9.23 o
0 1 2 166.34 152.80 5.79 o
1 1 2 3479.16 3722.62 22.07 o
-3 2 2 265.27 231.70 1.61 o
-2 2 2 1773.73 1817.85 52.82 o
-1 2 2 2802.57 2555.28 17.79 o
0 2 2 1524.41 1458.30 50.88 o
1 2 2 3036.99 3252.83 23.99 o
2 2 2 158.94 142.98 1.53 o
-5 3 2 1205.19 1241.80 5.34 o
-4 3 2 385.04 399.63 2.58 o
-3 3 2 1425.03 1425.40 41.36 o
-2 3 2 390.03 350.75 2.00 o
-1 3 2 104.00 86.20 1.02 o
0 3 2 894.68 890.52 9.33 o
1 3 2 60.48 60.83 1.03 o
2 3 2 65.69 65.87 1.22 o
3 3 2 85.32 90.15 1.64 o
-7 4 2 105.85 134.62 2.22 o
-6 4 2 37.78 35.46 .92 o
-5 4 2 398.19 418.38 3.20 o
-4 4 2 208.72 214.66 7.20 o
-3 4 2 57.36 46.44 .90 o
-2 4 2 568.11 564.91 2.98 o
-1 4 2 172.85 164.15 1.64 o
0 4 2 15.55 11.52 .29 o
1 4 2 149.77 155.79 1.93 o
2 4 2 75.06 83.60 1.58 o
3 4 2 46.50 42.25 1.12 o
4 4 2 27.01 30.53 .88 o
-9 5 2 15.14 14.37 .57 o
-8 5 2 162.90 170.90 2.68 o
-7 5 2 9.30 10.80 .51 o
-6 5 2 23.59 25.74 .76 o
-5 5 2 406.96 433.64 11.21 o
-4 5 2 80.40 88.40 1.45 o
-3 5 2 153.74 151.21 1.79 o
-2 5 2 367.91 342.80 2.72 o
-1 5 2 345.72 348.99 2.83 o
0 5 2 377.94 404.96 3.10 o
1 5 2 4.72 2.27 .31 o
2 5 2 188.12 186.53 2.62 o
3 5 2 86.26 95.30 2.00 o
4 5 2 133.06 163.14 2.56 o
5 5 2 8.15 4.98 .44 o
-11 6 2 .39 .59 .18 o
-10 6 2 10.19 3.92 .47 o
-9 6 2 6.68 4.68 .41 o
-8 6 2 29.46 35.05 1.02 o
-7 6 2 185.17 188.89 2.76 o
-6 6 2 139.35 147.16 6.80 o
-5 6 2 24.70 17.21 .53 o
-4 6 2 9.44 12.00 .46 o
-3 6 2 636.50 597.73 4.19 o
-2 6 2 304.86 314.18 3.00 o
-1 6 2 369.06 391.11 3.54 o
0 6 2 101.45 100.10 4.28 o
1 6 2 162.36 158.06 2.52 o
2 6 2 4.15 2.33 .39 o
3 6 2 16.90 20.92 .62 o
4 6 2 34.46 34.89 1.05 o
5 6 2 2.91 4.41 .25 o
-11 7 2 2.87 3.38 .22 o
-10 7 2 24.75 10.54 .68 o
-9 7 2 5.16 6.68 .42 o
-8 7 2 8.93 11.07 .48 o
-7 7 2 4.96 7.12 .66 o
-6 7 2 98.65 104.05 2.04 o
-5 7 2 25.74 22.49 .67 o
-4 7 2 50.14 46.28 1.33 o
-3 7 2 72.54 78.29 1.69 o
-2 7 2 14.57 11.26 .49 o
-1 7 2 25.53 23.96 .71 o
0 7 2 10.51 16.40 .42 o
1 7 2 101.57 103.15 2.08 o
2 7 2 15.95 27.43 .78 o
3 7 2 .69 .45 .23 o
4 7 2 17.77 21.33 .61 o
-10 8 2 34.90 46.76 1.06 o
-9 8 2 54.98 70.35 1.52 o
-8 8 2 39.75 52.14 2.59 o
-7 8 2 7.84 8.70 .48 o
-6 8 2 25.11 23.21 .68 o
-5 8 2 3.25 4.98 .43 o
-4 8 2 277.98 304.81 3.51 o
-3 8 2 23.66 20.80 .66 o
-2 8 2 161.21 171.90 2.63 o
-1 8 2 112.01 122.88 2.22 o
0 8 2 25.61 18.15 11.16 o
1 8 2 6.82 7.49 .40 o
2 8 2 4.03 4.94 .36 o
-10 9 2 4.45 6.25 .26 o
-9 9 2 8.40 11.05 .83 o
-8 9 2 12.32 14.44 .52 o
-7 9 2 27.10 33.01 .99 o
-6 9 2 .09 .45 .44 o
-5 9 2 48.44 45.05 1.22 o
-4 9 2 15.87 12.38 .56 o
-3 9 2 43.33 17.44 .64 o
-2 9 2 14.48 5.35 .42 o
-1 9 2 29.83 32.76 .93 o
0 9 2 .86 1.68 .18 o
1 9 2 26.61 35.74 18.26 o
-9 10 2 .29 .68 .40 o
-8 10 2 6.14 3.59 .29 o
-7 10 2 9.01 11.01 .42 o
-6 10 2 11.35 13.37 .53 o
-5 10 2 2.35 .24 .35 o
-4 10 2 12.15 3.23 .46 o
-3 10 2 3.33 .42 .41 o
-2 10 2 27.08 36.34 .96 o
-1 10 2 3.91 7.03 .28 o
-7 11 2 5.54 6.34 .26 o
-6 11 2 3.51 5.65 .26 o
-5 11 2 12.49 13.75 .42 o
-4 11 2 9.79 12.35 .37 o
0 0 3 2191.70 2155.84 15.35 o
-1 1 3 1231.09 1235.59 61.49 o
0 1 3 5583.47 6158.42 424.05 o
1 1 3 322.63 318.03 1.74 o
-3 2 3 991.63 971.35 3.71 o
-2 2 3 320.78 268.84 12.28 o
-1 2 3 414.01 380.35 1.91 o
0 2 3 4062.14 3967.04 253.01 o
1 2 3 964.39 971.31 3.56 o
2 2 3 1524.25 1599.74 5.40 o
-5 3 3 363.42 372.95 2.93 o
-4 3 3 224.76 217.17 1.96 o
-3 3 3 577.50 580.00 20.81 o
-2 3 3 1974.26 1923.13 18.50 o
-1 3 3 1844.49 1730.43 17.46 o
0 3 3 270.57 265.92 1.38 o
1 3 3 176.38 206.76 1.90 o
2 3 3 358.39 356.23 2.86 o
3 3 3 350.42 341.21 3.22 o
-7 4 3 36.14 46.70 1.40 o
-6 4 3 145.54 164.55 2.22 o
-5 4 3 109.51 126.47 1.79 o
-4 4 3 236.96 245.83 8.25 o
-3 4 3 36.45 30.93 .81 o
-2 4 3 618.49 600.65 3.20 o
-1 4 3 20.88 20.95 .58 o
0 4 3 111.45 118.08 1.10 o
1 4 3 421.43 409.82 3.17 o
2 4 3 107.95 108.82 1.85 o
3 4 3 110.35 100.60 1.92 o
4 4 3 41.78 40.60 1.19 o
-9 5 3 27.21 31.08 .89 o
-8 5 3 50.11 69.89 1.71 o
-7 5 3 26.77 24.07 .73 o
-6 5 3 20.03 30.67 .95 o
-5 5 3 12.27 12.90 1.88 o
-4 5 3 90.51 94.59 1.55 o
-3 5 3 724.79 737.75 4.17 o
-2 5 3 241.17 227.16 2.28 o
-1 5 3 90.01 89.53 1.51 o
0 5 3 98.03 102.99 1.21 o
1 5 3 272.40 280.86 2.99 o
2 5 3 33.80 32.32 .93 o
3 5 3 148.69 157.45 2.57 o
4 5 3 5.82 8.27 .47 o
5 5 3 .50 .17 .28 o
-11 6 3 2.11 3.17 .23 o
-10 6 3 37.73 17.36 .87 o
-9 6 3 62.54 66.50 1.70 o
-8 6 3 78.14 94.77 2.03 o
-7 6 3 .38 .82 .34 o
-6 6 3 174.30 178.31 4.35 o
-5 6 3 145.77 126.93 2.05 o
-4 6 3 109.63 112.04 1.83 o
-3 6 3 162.94 156.11 2.16 o
-2 6 3 185.19 186.83 2.37 o
-1 6 3 130.70 127.98 2.06 o
0 6 3 199.75 185.45 2.73 o
1 6 3 222.69 252.97 3.19 o
2 6 3 28.58 29.56 .86 o
3 6 3 31.66 37.05 1.10 o
4 6 3 .88 .26 .23 o
5 6 3 6.47 6.16 .25 o
-11 7 3 1.72 1.45 .17 o
-10 7 3 15.52 6.59 .57 o
-9 7 3 5.32 5.75 .41 o
-8 7 3 7.77 8.84 .47 o
-7 7 3 21.37 32.60 3.27 o
-6 7 3 55.47 57.56 1.55 o
-5 7 3 49.42 56.04 1.50 o
-4 7 3 2.99 4.25 .38 o
-3 7 3 110.77 121.63 2.11 o
-2 7 3 3.15 2.24 .35 o
-1 7 3 216.88 210.88 2.92 o
0 7 3 51.14 65.80 1.20 o
1 7 3 119.25 126.60 2.25 o
2 7 3 11.03 16.10 .55 o
3 7 3 20.69 20.99 .62 o
4 7 3 10.72 11.04 .32 o
-10 8 3 1.74 3.23 .28 o
-9 8 3 4.79 3.37 .32 o
-8 8 3 14.57 16.96 .82 o
-7 8 3 93.96 100.76 2.05 o
-6 8 3 180.40 184.46 2.72 o
-5 8 3 84.76 95.12 1.99 o
-4 8 3 119.53 124.60 2.29 o
-3 8 3 115.74 116.14 2.21 o
-2 8 3 91.77 93.48 2.02 o
-1 8 3 4.46 6.25 .45 o
0 8 3 57.38 37.09 32.81 o
1 8 3 21.15 31.53 .92 o
2 8 3 4.48 2.81 .33 o
-10 9 3 11.44 13.71 .40 o
-9 9 3 23.70 22.91 1.18 o
-8 9 3 11.75 15.89 .52 o
-7 9 3 18.63 21.78 .59 o
-6 9 3 .54 1.33 .31 o
-5 9 3 7.06 8.44 .47 o
-4 9 3 1.30 1.11 .32 o
-3 9 3 13.44 4.27 .40 o
-2 9 3 33.74 6.16 .45 o
-1 9 3 48.27 66.27 1.44 o
0 9 3 25.33 25.83 .86 o
1 9 3 .88 1.90 .19 o
-9 10 3 6.60 6.32 .26 o
-8 10 3 35.20 33.08 .94 o
-7 10 3 5.60 3.97 .33 o
-6 10 3 21.59 16.59 .57 o
-5 10 3 3.87 1.64 .34 o
-4 10 3 12.60 3.10 .42 o
-3 10 3 .09 .48 .11 o
-2 10 3 4.44 7.39 .33 o
-1 10 3 21.63 29.95 .70 o
-7 11 3 17.05 20.40 .57 o
-6 11 3 1.40 2.95 .23 o
-5 11 3 .38 .67 .19 o
-4 11 3 5.13 7.71 .28 o
-1 1 4 310.16 340.29 11.96 o
0 1 4 66.68 53.23 2.01 o
1 1 4 2335.19 2664.92 20.72 o
-3 2 4 283.68 284.11 2.01 o
-2 2 4 626.48 594.45 17.22 o
-1 2 4 984.07 933.02 3.22 o
0 2 4 154.58 139.36 4.78 o
1 2 4 604.55 572.87 2.90 o
2 2 4 719.34 757.57 3.86 o
-5 3 4 71.15 61.35 1.28 o
-4 3 4 268.99 286.06 2.40 o
-3 3 4 98.96 100.36 5.27 o
-2 3 4 38.90 35.77 .73 o
-1 3 4 1041.36 981.12 3.87 o
0 3 4 4056.22 4264.91 278.06 o
1 3 4 379.67 395.51 2.75 o
2 3 4 29.50 31.00 .91 o
3 3 4 242.54 269.63 2.93 o
-7 4 4 26.49 38.23 1.09 o
-6 4 4 190.80 206.04 2.55 o
-5 4 4 78.06 88.06 1.58 o
-4 4 4 86.03 84.66 2.18 o
-3 4 4 251.43 230.19 2.08 o
-2 4 4 217.85 212.32 2.00 o
-1 4 4 892.97 838.04 4.08 o
0 4 4 683.82 697.70 23.53 o
1 4 4 216.84 207.75 2.37 o
2 4 4 355.01 348.68 3.34 o
3 4 4 66.85 67.56 1.64 o
4 4 4 36.78 39.81 1.20 o
-9 5 4 1.38 2.24 .35 o
-8 5 4 193.14 202.62 2.92 o
-7 5 4 29.93 35.27 1.00 o
-6 5 4 97.72 118.01 2.03 o
-5 5 4 47.27 49.99 2.65 o
-4 5 4 18.76 19.74 .54 o
-3 5 4 227.96 204.33 2.22 o
-2 5 4 184.51 171.33 2.03 o
-1 5 4 62.34 62.99 1.30 o
0 5 4 92.90 98.15 1.21 o
1 5 4 134.93 151.78 2.24 o
2 5 4 56.68 49.95 1.44 o
3 5 4 106.28 111.37 2.16 o
4 5 4 42.54 48.48 1.42 o
5 5 4 1.46 .05 .50 o
-11 6 4 1.16 1.11 .18 o
-10 6 4 13.88 5.32 .56 o
-9 6 4 80.68 89.48 1.93 o
-8 6 4 45.31 61.62 1.64 o
-7 6 4 82.49 94.26 1.99 o
-6 6 4 39.83 47.28 2.15 o
-5 6 4 .50 .90 .29 o
-4 6 4 57.55 61.65 1.43 o
-3 6 4 285.76 263.31 2.90 o
-2 6 4 15.32 15.48 .50 o
-1 6 4 384.56 387.28 3.61 o
0 6 4 41.46 41.26 .81 o
1 6 4 290.85 298.39 3.48 o
2 6 4 7.24 7.58 .46 o
3 6 4 46.32 57.40 1.51 o
4 6 4 1.64 .33 .36 o
5 6 4 6.92 7.66 .28 o
-10 7 4 15.74 9.14 .58 o
-9 7 4 44.41 45.07 1.19 o
-8 7 4 5.30 3.26 .38 o
-7 7 4 60.70 68.87 3.79 o
-6 7 4 27.17 23.06 .70 o
-5 7 4 78.81 80.95 1.80 o
-4 7 4 45.36 44.40 1.18 o
-3 7 4 91.29 92.87 1.93 o
-2 7 4 108.76 109.39 2.09 o
-1 7 4 31.25 28.52 .85 o
0 7 4 13.76 13.42 .49 o
1 7 4 39.43 43.96 1.20 o
2 7 4 10.18 13.55 .50 o
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1 5 7 19.58 17.09 .60 o
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1 3 8 56.19 62.40 1.43 o
2 3 8 176.62 197.87 2.63 o
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1 8 8 1.81 1.06 .26 o
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0 2 9 12.60 11.92 .99 o
1 2 9 94.20 90.24 1.64 o
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0 3 9 166.25 174.72 11.46 o
1 3 9 72.77 88.07 1.75 o
2 3 9 20.22 23.09 .65 o
3 3 9 167.91 183.39 2.72 o
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3 4 9 41.58 51.29 1.50 o
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1 5 9 110.17 125.19 2.29 o
2 5 9 16.48 25.52 .78 o
3 5 9 44.16 53.94 1.37 o
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1 6 9 11.00 11.69 .50 o
2 6 9 48.30 63.20 1.44 o
3 6 9 3.47 2.54 .27 o
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1 7 9 10.41 18.61 .57 o
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0 8 9 50.25 37.98 27.22 o
1 8 9 15.24 19.28 .56 o
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0 1 10 438.37 431.91 29.44 o
1 1 10 15.29 23.15 .68 o
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0 2 10 396.29 406.50 27.26 o
1 2 10 143.94 149.65 2.23 o
2 2 10 103.14 105.17 2.01 o
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-2 3 10 308.62 274.54 3.03 o
-1 3 10 51.68 43.04 1.22 o
0 3 10 16.62 16.55 1.29 o
1 3 10 286.85 301.44 3.34 o
2 3 10 289.59 283.56 3.39 o
3 3 10 56.13 55.28 1.55 o
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0 4 10 12.20 16.91 .42 o
1 4 10 47.79 45.59 1.26 o
2 4 10 17.54 20.03 .65 o
3 4 10 9.82 10.36 .48 o
4 4 10 19.28 22.87 .65 o
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-8 5 10 27.60 32.96 .91 o
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-1 5 10 64.21 65.13 1.69 o
0 5 10 54.40 50.49 1.52 o
1 5 10 138.61 167.69 2.59 o
2 5 10 5.59 8.03 .46 o
3 5 10 19.57 30.74 .88 o
4 5 10 .72 .54 .20 o
-9 6 10 10.77 12.35 .38 o
-8 6 10 29.55 35.14 1.02 o
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-6 6 10 62.18 63.14 3.65 o
-5 6 10 17.56 19.47 .62 o
-4 6 10 223.20 245.40 3.15 o
-3 6 10 157.36 168.94 2.61 o
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-1 6 10 31.32 26.70 .80 o
0 6 10 22.09 22.39 12.23 o
1 6 10 26.36 25.13 .73 o
2 6 10 1.98 3.29 .32 o
3 6 10 2.45 1.87 .25 o
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-8 7 10 11.56 14.61 .45 o
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-1 7 10 28.09 2.46 .38 o
0 7 10 14.53 14.75 8.36 o
1 7 10 4.75 7.79 .38 o
2 7 10 13.77 19.88 .57 o
-8 8 10 7.26 8.10 .39 o
-7 8 10 5.26 4.61 .30 o
-6 8 10 34.92 34.62 1.04 o
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-3 8 10 3.69 1.29 .31 o
-2 8 10 37.40 3.49 .36 o
-1 8 10 8.83 .26 .32 o
0 8 10 14.91 16.77 2.72 o
-7 9 10 6.01 8.02 .28 o
-6 9 10 12.48 10.35 .34 o
-5 9 10 27.17 18.20 .54 o
-4 9 10 .53 .20 .24 o
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-1 1 11 58.09 65.20 4.03 o
0 1 11 57.20 55.79 3.77 o
1 1 11 65.07 71.45 1.69 o
-3 2 11 10.58 12.57 .53 o
-2 2 11 36.26 30.00 2.95 o
-1 2 11 33.08 26.73 .80 o
0 2 11 91.25 92.51 7.65 o
1 2 11 137.18 128.82 2.22 o
2 2 11 156.36 158.97 2.53 o
-5 3 11 75.00 90.55 1.99 o
-4 3 11 712.49 801.11 5.64 o
-3 3 11 119.40 116.22 6.37 o
-2 3 11 245.26 230.04 2.91 o
-1 3 11 163.00 142.13 2.28 o
0 3 11 337.59 307.20 27.35 o
1 3 11 3.24 3.47 .41 o
2 3 11 18.85 18.41 .62 o
3 3 11 32.12 36.63 1.13 o
-7 4 11 2.52 2.97 .34 o
-6 4 11 13.86 18.32 .60 o
-5 4 11 62.90 62.70 1.65 o
-4 4 11 174.70 183.87 10.38 o
-3 4 11 25.42 25.12 .73 o
-2 4 11 39.31 38.48 1.13 o
-1 4 11 39.21 33.35 .97 o
0 4 11 26.18 23.95 1.88 o
1 4 11 17.38 22.31 .69 o
2 4 11 51.62 69.55 1.70 o
3 4 11 29.17 32.73 .99 o
4 4 11 1.08 .00 .91 o
-9 5 11 7.07 9.84 .31 o
-8 5 11 9.60 10.97 .41 o
-7 5 11 102.61 128.94 2.07 o
-6 5 11 53.55 65.28 1.61 o
-5 5 11 81.29 88.87 4.77 o
-4 5 11 29.76 28.76 .83 o
-3 5 11 39.43 38.01 1.12 o
-2 5 11 15.62 20.81 .64 o
-1 5 11 2.93 2.93 .39 o
0 5 11 31.33 39.84 2.37 o
1 5 11 1.09 .67 .32 o
2 5 11 3.85 3.59 .34 o
3 5 11 16.66 28.01 .77 o
4 5 11 15.15 16.72 .46 o
-9 6 11 1.00 .85 .16 o
-8 6 11 15.67 20.78 .58 o
-7 6 11 11.49 15.58 .52 o
-6 6 11 12.88 10.21 .59 o
-5 6 11 8.02 10.20 .48 o
-4 6 11 65.71 81.33 1.80 o
-3 6 11 130.44 131.08 2.24 o
-2 6 11 30.29 28.83 .90 o
-1 6 11 49.91 6.19 .45 o
0 6 11 66.85 42.34 37.13 o
1 6 11 7.13 10.22 .46 o
2 6 11 6.64 8.71 .37 o
3 6 11 4.77 5.88 .24 o
-8 7 11 .36 .92 .20 o
-7 7 11 31.34 33.69 3.41 o
-6 7 11 150.09 142.38 2.07 o
-5 7 11 60.32 71.29 1.57 o
-4 7 11 18.93 17.15 .54 o
-3 7 11 17.38 13.90 .52 o
-2 7 11 16.30 1.98 .33 o
-1 7 11 10.85 1.14 .30 o
0 7 11 7.44 4.66 2.75 o
1 7 11 5.41 4.42 .31 o
-7 8 11 24.80 23.75 .69 o
-6 8 11 6.65 7.11 .35 o
-5 8 11 5.81 5.77 .36 o
-4 8 11 72.50 53.85 1.27 o
-3 8 11 20.58 2.31 .31 o
-2 8 11 3.93 .38 .14 o
-1 8 11 19.16 .02 .52 o
-6 9 11 2.72 3.53 .21 o
-5 9 11 .39 .28 .18 o
-4 9 11 6.05 8.03 .30 o
-3 9 11 6.34 6.90 .26 o
0 0 12 304.61 316.94 19.18 o
-1 1 12 186.89 183.57 10.87 o
0 1 12 72.60 68.17 3.90 o
1 1 12 196.24 201.85 2.85 o
-3 2 12 233.67 246.28 3.15 o
-2 2 12 172.00 173.78 12.98 o
-1 2 12 82.55 83.02 1.82 o
0 2 12 98.79 95.39 8.30 o
1 2 12 501.80 526.90 4.65 o
2 2 12 171.92 176.89 2.73 o
-5 3 12 27.19 28.92 .85 o
-4 3 12 68.11 82.44 1.86 o
-3 3 12 48.58 46.85 1.71 o
-2 3 12 102.09 97.46 1.98 o
-1 3 12 106.09 91.82 1.92 o
0 3 12 22.72 19.38 1.50 o
1 3 12 78.46 92.31 1.96 o
2 3 12 20.09 17.71 .61 o
3 3 12 147.25 177.35 2.55 o
-7 4 12 18.00 23.90 .67 o
-6 4 12 119.50 143.61 2.29 o
-4 4 12 84.52 91.06 7.41 o
-3 4 12 107.13 104.71 2.09 o
-2 4 12 216.37 190.94 2.77 o
-1 4 12 176.03 145.71 2.42 o
0 4 12 51.66 51.34 3.41 o
1 4 12 22.72 21.34 .65 o
2 4 12 15.72 16.82 .58 o
3 4 12 6.72 5.48 .36 o
4 4 12 4.43 5.87 .30 o
-8 5 12 25.20 31.51 .84 o
-7 5 12 7.92 12.89 .47 o
-6 5 12 61.65 80.39 1.71 o
-5 5 12 .75 .91 .22 o
-3 5 12 25.68 24.65 .72 o
-2 5 12 15.74 15.14 .56 o
-1 5 12 1.89 2.45 .37 o
0 5 12 8.06 12.11 6.65 o
1 5 12 65.18 72.62 1.63 o
2 5 12 10.69 14.70 .50 o
3 5 12 7.78 9.16 .34 o
-8 6 12 1.23 2.45 .23 o
-7 6 12 21.30 26.39 .77 o
-6 6 12 94.19 103.76 7.12 o
-5 6 12 9.44 6.49 .43 o
-4 6 12 29.08 28.93 .83 o
-3 6 12 6.95 7.13 .45 o
-2 6 12 74.78 64.90 1.57 o
-1 6 12 .88 .37 .26 o
0 6 12 5.51 6.59 3.67 o
1 6 12 27.72 36.47 1.01 o
2 6 12 .11 .38 .15 o
-8 7 12 2.12 4.12 .22 o
-7 7 12 8.66 10.59 1.87 o
-6 7 12 21.67 21.49 .63 o
-5 7 12 20.17 22.15 .68 o
-4 7 12 2.98 4.05 .36 o
-3 7 12 15.29 13.86 .51 o
-2 7 12 26.48 2.79 .33 o
-1 7 12 .41 .13 .13 o
0 7 12 26.50 23.51 16.10 o
1 7 12 13.10 13.74 .39 o
-7 8 12 10.25 8.93 .27 o
-6 8 12 7.17 8.46 .30 o
-5 8 12 6.73 5.53 .30 o
-4 8 12 23.70 15.53 .43 o
-3 8 12 16.16 1.35 .25 o
-2 8 12 4.10 2.98 .24 o
-1 8 12 7.57 11.55 .34 o
-1 1 13 211.75 211.73 11.19 o
0 1 13 70.51 65.93 7.43 o
1 1 13 186.93 186.33 2.80 o
-3 2 13 129.82 137.12 2.40 o
-2 2 13 95.69 92.02 7.52 o
-1 2 13 377.59 339.56 3.72 o
0 2 13 45.76 47.56 6.11 o
1 2 13 156.99 160.17 2.59 o
2 2 13 253.23 269.12 3.30 o
-5 3 13 42.29 44.61 1.21 o
-4 3 13 108.58 121.65 2.21 o
-3 3 13 47.85 44.49 4.59 o
-2 3 13 23.07 20.55 .66 o
-1 3 13 1.02 1.47 .36 o
0 3 13 231.74 203.61 23.67 o
1 3 13 39.11 44.05 1.20 o
2 3 13 113.20 124.53 2.18 o
3 3 13 78.10 88.29 1.71 o
-7 4 13 8.40 11.92 .42 o
-6 4 13 51.61 55.83 1.36 o
-5 4 13 26.18 29.81 .89 o
-4 4 13 84.32 86.66 7.27 o
-3 4 13 53.83 51.46 1.47 o
-2 4 13 173.75 153.45 2.48 o
-1 4 13 134.56 121.15 2.20 o
0 4 13 15.01 11.59 1.39 o
1 4 13 15.26 17.31 .55 o
2 4 13 8.51 7.45 .46 o
3 4 13 20.45 25.58 .73 o
4 4 13 27.17 37.25 .75 o
-8 5 13 4.58 4.67 .24 o
-7 5 13 .05 .65 .22 o
-6 5 13 41.74 50.63 1.23 o
-5 5 13 47.70 52.69 4.82 o
-4 5 13 9.84 10.04 .45 o
-3 5 13 22.16 19.06 .57 o
-2 5 13 10.05 12.47 .50 o
-1 5 13 11.29 10.51 .49 o
0 5 13 4.19 2.94 1.88 o
1 5 13 67.91 76.82 1.51 o
2 5 13 96.24 127.11 1.69 o
3 5 13 .71 .96 .18 o
-7 6 13 13.18 18.66 .55 o
-6 6 13 17.87 21.65 1.26 o
-5 6 13 1.84 .43 .41 o
-4 6 13 44.21 43.81 1.23 o
-3 6 13 28.73 27.65 .88 o
-2 6 13 17.39 15.59 .54 o
-1 6 13 17.74 .96 .31 o
0 6 13 20.57 19.88 12.58 o
1 6 13 5.19 6.58 .31 o
-7 7 13 2.93 3.54 .16 o
-6 7 13 26.53 26.81 .78 o
-5 7 13 4.22 4.27 .28 o
-4 7 13 1.29 1.59 .27 o
-3 7 13 27.22 18.68 .55 o
-2 7 13 26.21 1.75 .29 o
-1 7 13 4.17 .65 .20 o
0 7 13 21.83 20.54 1.08 o
-5 8 13 29.28 29.83 .67 o
-4 8 13 5.09 9.70 .31 o
-3 8 13 4.32 6.00 .27 o
-1 1 14 27.71 29.75 2.21 o
0 1 14 163.92 170.73 15.94 o
1 1 14 65.32 91.10 1.99 o
-3 2 14 23.35 22.79 .67 o
-2 2 14 57.65 60.33 7.45 o
-1 2 14 516.96 455.45 4.23 o
0 2 14 33.96 31.21 4.34 o
1 2 14 93.97 104.07 2.04 o
2 2 14 20.90 20.63 .62 o
-5 3 14 28.32 29.25 .83 o
-4 3 14 5.89 5.57 .43 o
-3 3 14 19.21 17.66 1.93 o
-2 3 14 336.71 296.31 3.39 o
-1 3 14 11.37 10.87 .49 o
0 3 14 67.54 62.39 6.08 o
1 3 14 5.54 8.18 .45 o
2 3 14 49.22 53.86 1.37 o
3 3 14 40.02 43.77 1.14 o
-7 4 14 22.50 26.29 .72 o
-6 4 14 10.94 14.61 .47 o
-5 4 14 15.95 20.73 .60 o
-4 4 14 32.24 30.22 2.15 o
-3 4 14 7.95 10.57 .49 o
-2 4 14 25.69 22.97 .65 o
-1 4 14 16.03 10.09 .48 o
0 4 14 13.21 14.71 2.00 o
1 4 14 39.16 43.16 1.22 o
2 4 14 7.73 11.36 .41 o
3 4 14 26.39 29.81 .79 o
-7 5 14 17.28 18.28 .52 o
-6 5 14 1.93 2.61 .27 o
-5 5 14 4.37 5.53 .84 o
-4 5 14 1.65 2.85 .32 o
-3 5 14 18.43 16.64 .52 o
-2 5 14 24.30 21.37 .65 o
-1 5 14 44.56 43.72 1.20 o
0 5 14 45.93 32.85 24.43 o
1 5 14 15.90 22.10 .68 o
2 5 14 25.18 24.47 .67 o
-6 6 14 22.41 19.14 1.03 o
-5 6 14 12.31 8.24 .36 o
-4 6 14 8.14 9.12 .38 o
-3 6 14 27.42 26.36 .77 o
-2 6 14 39.02 37.78 1.03 o
-1 6 14 29.83 1.97 .30 o
0 6 14 16.54 18.26 11.34 o
1 6 14 35.87 41.09 .73 o
-5 7 14 .05 .90 .17 o
-4 7 14 3.30 1.82 .22 o
-3 7 14 9.45 4.79 .28 o
-2 7 14 14.86 17.83 .50 o
-1 7 14 .48 .33 .16 o
0 0 15 479.49 439.42 46.53 o
-1 1 15 36.20 34.14 3.86 o
0 1 15 97.13 103.55 13.89 o
1 1 15 49.81 53.56 1.50 o
-3 2 15 167.17 187.65 2.56 o
-2 2 15 75.96 74.66 7.92 o
-1 2 15 58.08 49.54 1.41 o
0 2 15 1.52 2.16 .40 o
1 2 15 2.55 3.62 .39 o
2 2 15 8.51 11.97 .52 o
-5 3 15 4.63 5.40 .35 o
-4 3 15 7.54 13.67 .52 o
-3 3 15 12.93 10.83 1.00 o
-2 3 15 10.01 6.99 .42 o
-1 3 15 62.82 55.15 1.42 o
0 3 15 68.67 69.73 1.59 o
1 3 15 3.33 3.21 .37 o
2 3 15 67.81 75.22 1.42 o
3 3 15 5.65 7.17 .33 o
-6 4 15 20.23 24.34 .63 o
-5 4 15 6.28 8.30 .38 o
-4 4 15 11.03 7.55 .69 o
-3 4 15 78.02 67.30 1.49 o
-2 4 15 9.46 9.21 .44 o
-1 4 15 22.18 16.68 .52 o
0 4 15 20.04 15.07 2.84 o
1 4 15 24.92 24.88 .75 o
2 4 15 1.46 1.12 .23 o
-6 5 15 37.77 46.22 .90 o
-5 5 15 14.57 16.04 1.29 o
-4 5 15 40.30 39.05 1.02 o
-3 5 15 6.90 9.46 .39 o
-2 5 15 21.26 16.56 .48 o
-1 5 15 13.82 15.09 .46 o
0 5 15 7.91 9.15 4.83 o
1 5 15 7.11 7.46 .28 o
-5 6 15 1.92 2.11 .21 o
-4 6 15 8.14 6.94 .30 o
-3 6 15 24.55 19.81 .59 o
-2 6 15 2.35 .82 .22 o
-1 6 15 2.36 1.96 .22 o
-1 1 16 13.34 11.71 2.01 o
0 1 16 17.68 16.90 .58 o
1 1 16 78.02 87.70 1.70 o
-3 2 16 97.47 99.55 1.72 o
-2 2 16 5.19 5.99 1.20 o
-1 2 16 .13 .34 .36 o
0 2 16 29.70 27.80 .79 o
1 2 16 30.53 31.38 .92 o
2 2 16 6.98 7.00 .38 o
-5 3 16 45.94 50.95 1.01 o
-4 3 16 47.21 51.58 1.14 o
-3 3 16 25.70 24.54 3.79 o
-2 3 16 24.56 19.66 .58 o
0 3 16 17.48 16.18 .51 o
1 3 16 46.89 53.82 1.17 o
2 3 16 20.48 26.30 .65 o
-5 4 16 34.54 36.03 .82 o
-4 4 16 42.64 42.48 5.38 o
-3 4 16 23.18 17.86 .52 o
-2 4 16 9.60 8.16 .35 o
-1 4 16 19.79 18.59 .53 o
0 4 16 2.17 3.03 .30 o
1 4 16 .85 2.28 .16 o
-5 5 16 4.44 5.08 .28 o
-4 5 16 47.26 35.88 .82 o
-3 5 16 15.04 12.20 .36 o
-2 5 16 14.16 11.46 .35 o
-1 5 16 6.30 5.08 .27 o
0 5 16 56.18 51.09 7.93 o
-1 1 17 13.61 12.40 .48 o
0 1 17 36.62 42.93 1.16 o
1 1 17 15.41 12.16 .46 o
-3 2 17 11.56 11.81 .41 o
-2 2 17 11.42 9.38 1.93 o
0 2 17 13.86 16.03 .49 o
1 2 17 22.34 28.95 .85 o
2 2 17 9.92 11.63 .34 o
-4 3 17 30.25 29.53 .74 o
-3 3 17 5.94 3.85 .66 o
0 3 17 15.97 16.37 .46 o
1 3 17 1.13 1.69 .21 o
-4 4 17 2.98 3.77 .64 o
-3 4 17 22.69 16.94 .49 o
-2 4 17 7.81 5.31 .26 o
0 4 17 37.75 45.29 .79 o
0 0 18 142.35 141.23 1.68 o
-1 1 18 3.30 2.02 .26 o
0 1 18 33.16 30.92 .83 o
1 1 18 7.91 5.92 .30 o
-3 2 18 14.54 14.42 .41 o
-2 2 18 .93 1.08 .21 o
0 2 18 13.13 15.41 .43 o
1 2 18 17.44 16.99 .45 o