#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/36/2103661.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103661_Fobs loop_ _publ_author_name 'Low, John N.' 'Moreno S\'anchez, Jose M.' 'Arranz Mascar\'os, Paloma' 'Godino Salido, M. Luz' 'L\'opez Garzon, Rafael' 'Cobo Domingo, Justo' 'Glidewell, Christopher' _publ_section_title ; Hydrated metal complexes of N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl)glycinate: interplay of molecular, molecular--electronic and supramolecular structures ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 317 _journal_page_last 328 _journal_volume 57 _journal_year 2001 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.375 _cell_angle_gamma 90.000 _cell_length_a 24.7736 _cell_length_b 7.6525 _cell_length_c 14.0096 _exptl_crystal_F_000 1200.00 _reflns_d_resolution_high 0.7707 _[local]_cod_data_source_file na01161sup2.hkl _[local]_cod_data_source_block 1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' aLI2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 394.26 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 3809.41 3449.38 135.23 o 6 0 0 3945.52 4088.12 149.91 o 8 0 0 65.71 86.52 8.03 o 10 0 0 7444.63 6941.52 274.75 o 12 0 0 9804.13 9964.67 360.29 o 14 0 0 5808.24 5820.31 230.73 o 16 0 0 252.68 206.72 24.13 o 18 0 0 835.30 959.82 65.88 o 20 0 0 45.01 59.65 17.95 o 22 0 0 1653.30 1514.80 94.50 o 24 0 0 8.76 -7.76 13.90 o 26 0 0 240.25 197.14 37.36 o 28 0 0 252.00 161.47 44.92 o 3 1 0 6962.68 6508.83 146.69 o 5 1 0 9359.97 9115.91 205.84 o 7 1 0 4413.48 4097.39 93.53 o 9 1 0 7160.81 6972.67 149.23 o 11 1 0 2713.56 2796.32 65.83 o 13 1 0 8208.59 8449.69 181.72 o 15 1 0 1087.12 1129.24 30.89 o 17 1 0 2681.32 2787.07 85.16 o 19 1 0 7.49 4.29 8.60 o 21 1 0 288.78 296.79 17.69 o 23 1 0 3551.59 3844.56 147.99 o 25 1 0 2.49 0.82 14.54 o 27 1 0 65.82 46.55 23.85 o 29 1 0 491.72 548.38 66.94 o 0 2 0 670.49 697.15 28.65 o 2 2 0 11609.54 10667.41 322.17 o 4 2 0 14.46 12.45 6.31 o 6 2 0 9716.94 9589.99 208.73 o 8 2 0 825.37 738.43 22.73 o 10 2 0 9.38 12.84 4.89 o 12 2 0 710.35 770.84 22.74 o 14 2 0 3124.40 3208.10 79.96 o 16 2 0 708.45 653.42 23.83 o 18 2 0 673.17 712.47 27.32 o 20 2 0 599.46 583.48 31.05 o 22 2 0 293.17 271.82 21.09 o 24 2 0 192.74 145.41 19.10 o 26 2 0 0.25 0.08 17.38 o 28 2 0 219.27 206.23 65.88 o 1 3 0 1236.27 1188.40 38.43 o 3 3 0 489.34 307.11 22.06 o 5 3 0 222.36 169.80 11.54 o 7 3 0 1423.15 1272.13 35.11 o 9 3 0 2869.14 3263.10 82.99 o 11 3 0 167.13 200.41 13.57 o 13 3 0 5.03 15.12 8.58 o 15 3 0 2577.69 2641.97 93.58 o 17 3 0 3440.13 3835.69 142.53 o 19 3 0 3503.41 3810.18 173.01 o 21 3 0 165.11 162.26 24.65 o 23 3 0 79.26 67.12 17.15 o 25 3 0 390.72 350.11 47.03 o 27 3 0 195.31 83.05 77.23 o 0 4 0 136.87 130.94 17.44 o 2 4 0 266.40 220.49 28.81 o 4 4 0 1652.62 1744.31 43.77 o 6 4 0 259.86 272.69 16.32 o 8 4 0 1576.97 1556.25 115.68 o 10 4 0 1529.29 1453.46 55.85 o 12 4 0 1826.80 1864.22 73.56 o 14 4 0 439.18 394.29 25.06 o 16 4 0 3145.81 3256.75 267.69 o 18 4 0 8.87 32.08 19.79 o 20 4 0 708.95 645.49 55.56 o 22 4 0 151.30 138.48 32.16 o 24 4 0 0.02 8.48 27.35 o 26 4 0 67.50 137.58 51.49 o 1 5 0 4.41 19.29 9.04 o 3 5 0 31.27 67.27 9.70 o 5 5 0 592.68 589.10 22.83 o 7 5 0 230.17 241.74 15.54 o 9 5 0 51.92 37.40 15.43 o 11 5 0 605.38 635.45 34.10 o 13 5 0 675.48 699.01 40.84 o 15 5 0 2372.61 2393.73 130.66 o 17 5 0 53.26 58.29 54.53 o 19 5 0 24.47 10.20 43.05 o 21 5 0 83.15 87.24 32.20 o 23 5 0 368.30 312.05 53.85 o 25 5 0 225.77 -25.74 112.11 o 0 6 0 775.38 771.50 81.39 o 2 6 0 6745.55 6701.63 204.95 o 4 6 0 696.02 666.09 35.58 o 6 6 0 513.56 545.09 24.91 o 8 6 0 160.46 159.99 21.22 o 10 6 0 2838.53 2727.90 130.54 o 12 6 0 1062.41 1040.82 42.84 o 14 6 0 494.27 407.05 42.77 o 16 6 0 30.22 22.87 26.33 o 18 6 0 65.30 68.44 29.20 o 20 6 0 474.07 416.31 110.17 o 22 6 0 20.01 -86.09 86.09 o 1 7 0 1595.34 1672.40 124.39 o 3 7 0 1175.71 1133.54 66.87 o 5 7 0 11.84 14.77 15.10 o 7 7 0 0.35 -1.91 14.07 o 9 7 0 2611.40 2549.09 104.44 o 11 7 0 106.48 74.61 18.03 o 13 7 0 600.47 703.02 46.95 o 15 7 0 494.27 394.02 42.22 o 17 7 0 22.95 37.94 34.29 o 19 7 0 5.93 94.40 80.00 o 0 8 0 4857.68 5042.23 314.15 o 2 8 0 170.93 159.29 21.20 o 4 8 0 353.88 360.94 43.20 o 6 8 0 103.51 104.41 24.68 o 8 8 0 86.21 146.98 30.77 o 10 8 0 246.88 242.19 32.35 o 12 8 0 1.85 -17.35 17.35 o 14 8 0 100.35 8.12 82.91 o 16 8 0 990.54 757.66 131.77 o 1 9 0 28.13 6.89 18.43 o 3 9 0 606.96 603.06 48.34 o 5 9 0 2.34 11.07 25.38 o 7 9 0 37.22 73.79 62.42 o 9 9 0 32.46 170.80 82.49 o -29 1 1 13.04 -22.53 37.54 o -27 1 1 458.62 345.58 33.77 o -25 1 1 819.17 836.91 50.86 o -23 1 1 790.92 727.92 39.91 o -21 1 1 7.04 18.26 10.09 o -19 1 1 517.36 450.12 22.61 o -17 1 1 6060.47 6284.21 147.31 o -15 1 1 388.47 423.17 14.73 o -13 1 1 956.16 1179.94 29.96 o -11 1 1 1174.35 1307.02 36.50 o -9 1 1 4604.45 4554.31 99.31 o -7 1 1 30113.18 28314.85 609.12 o -5 1 1 17472.87 16016.23 399.61 o -3 1 1 131.76 113.68 10.66 o -1 1 1 5840.84 5102.44 171.80 o 1 1 1 613.04 591.43 24.80 o 3 1 1 2521.66 2336.30 63.20 o 5 1 1 212.28 111.89 10.47 o 7 1 1 4248.38 4270.02 111.72 o 9 1 1 1754.95 1734.51 44.88 o 11 1 1 70.92 122.76 13.50 o 13 1 1 941.52 871.33 26.13 o 15 1 1 61.18 63.18 9.43 o 17 1 1 120.96 140.02 12.39 o 19 1 1 360.86 380.32 22.11 o 21 1 1 246.58 231.18 18.79 o 23 1 1 38.44 50.50 14.37 o 25 1 1 1921.77 2126.44 107.07 o 27 1 1 44.29 26.85 23.65 o -28 2 1 655.87 589.39 79.27 o -26 2 1 147.99 139.80 21.65 o -24 2 1 19.01 13.50 11.54 o -22 2 1 847.44 902.69 43.47 o -20 2 1 11.43 10.57 9.28 o -18 2 1 4448.13 4744.48 133.11 o -16 2 1 1900.96 2045.42 59.87 o -14 2 1 1553.21 1520.57 39.85 o -12 2 1 1498.97 1431.56 37.27 o -10 2 1 39.01 50.33 8.99 o -8 2 1 4232.23 4125.87 107.34 o -6 2 1 0.02 6.13 6.25 o -4 2 1 7200.50 6232.91 179.57 o -2 2 1 5397.89 5009.86 122.66 o 0 2 1 4119.69 4102.01 112.28 o 2 2 1 3367.90 3158.57 77.18 o 4 2 1 48838.46 42857.00 1140.12 o 6 2 1 1820.61 2200.35 58.54 o 8 2 1 354.41 356.49 16.90 o 10 2 1 11.40 3.90 6.50 o 12 2 1 58.46 74.12 9.48 o 14 2 1 121.04 116.27 10.46 o 16 2 1 0.01 0.77 8.63 o 18 2 1 826.34 763.12 35.41 o 20 2 1 88.41 84.94 13.82 o 22 2 1 352.81 317.63 34.24 o 24 2 1 373.44 321.65 27.58 o 26 2 1 194.41 156.29 52.32 o -27 3 1 209.05 214.26 54.26 o -25 3 1 135.33 134.86 24.55 o -23 3 1 159.29 182.51 26.31 o -21 3 1 3348.39 3671.14 125.48 o -19 3 1 6502.44 7212.05 278.09 o -17 3 1 68.42 88.79 17.30 o -15 3 1 716.84 637.22 31.70 o -13 3 1 1675.54 1824.65 62.33 o -11 3 1 307.00 333.66 19.26 o -9 3 1 27.06 22.78 12.91 o -7 3 1 12468.63 13644.26 360.83 o -5 3 1 24467.91 23304.03 590.31 o -3 3 1 2347.97 2179.67 67.69 o -1 3 1 539.18 618.11 22.92 o 1 3 1 1790.45 1755.31 45.51 o 3 3 1 879.01 776.21 32.23 o 5 3 1 1397.92 1604.53 49.36 o 7 3 1 8728.52 9837.51 230.43 o 9 3 1 1691.92 1883.24 60.78 o 11 3 1 4395.52 4237.95 122.78 o 13 3 1 3066.34 3335.70 109.15 o 15 3 1 2600.52 2856.01 96.32 o 17 3 1 3896.23 4188.09 135.47 o 19 3 1 3381.61 3783.44 193.11 o 21 3 1 21.42 11.48 24.87 o 23 3 1 347.76 339.76 37.16 o 25 3 1 36.60 56.35 26.33 o 27 3 1 13.10 -19.93 54.53 o -26 4 1 49.67 143.39 71.70 o -24 4 1 3.87 46.66 25.53 o -22 4 1 97.11 116.50 34.18 o -20 4 1 542.49 568.59 65.61 o -18 4 1 501.00 545.95 33.98 o -16 4 1 55.85 48.51 14.25 o -14 4 1 10.05 15.42 14.70 o -12 4 1 865.92 899.46 37.92 o -10 4 1 54.25 55.89 11.32 o -8 4 1 1738.29 1780.70 59.41 o -6 4 1 557.01 746.57 23.43 o -4 4 1 12854.06 13345.88 375.42 o -2 4 1 574.36 451.55 52.73 o 0 4 1 81.26 96.87 8.97 o 2 4 1 3802.39 4003.26 103.78 o 4 4 1 1883.08 1914.40 62.86 o 6 4 1 2.87 33.09 12.13 o 8 4 1 2239.71 2260.24 95.21 o 10 4 1 681.21 700.92 34.17 o 12 4 1 1079.89 1152.25 43.45 o 14 4 1 454.87 464.81 42.56 o 16 4 1 5190.10 5851.54 244.93 o 18 4 1 4387.30 4910.40 254.14 o 20 4 1 263.95 224.99 29.46 o 22 4 1 50.54 63.93 46.09 o 24 4 1 117.29 124.19 40.15 o 26 4 1 132.07 -22.98 74.74 o -25 5 1 80.09 31.56 48.72 o -23 5 1 0.10 8.58 23.75 o -21 5 1 111.79 76.73 15.87 o -19 5 1 2493.71 2934.90 212.48 o -17 5 1 339.63 326.03 35.78 o -15 5 1 596.19 700.90 49.15 o -13 5 1 582.33 570.14 34.95 o -11 5 1 20.04 0.66 10.92 o -9 5 1 1896.73 1918.22 58.26 o -7 5 1 487.36 519.83 21.41 o -5 5 1 1068.15 981.98 31.07 o -3 5 1 11.65 22.48 11.78 o -1 5 1 80.05 48.76 11.66 o 1 5 1 187.48 162.13 11.68 o 3 5 1 962.13 1009.24 32.70 o 5 5 1 37.43 33.57 9.65 o 7 5 1 251.62 243.71 28.25 o 9 5 1 4244.06 4557.25 178.22 o 11 5 1 83.27 67.16 18.13 o 13 5 1 2973.24 3357.03 152.16 o 15 5 1 96.93 150.79 36.06 o 17 5 1 20.20 6.12 21.32 o 19 5 1 166.09 182.09 35.07 o 21 5 1 215.16 282.11 48.24 o 23 5 1 1501.47 1428.73 182.29 o -22 6 1 378.67 424.64 94.67 o -20 6 1 131.40 124.50 28.86 o -18 6 1 174.28 162.66 35.91 o -16 6 1 414.04 337.10 38.32 o -14 6 1 926.74 754.58 45.75 o -12 6 1 506.53 474.51 23.88 o -10 6 1 93.51 131.93 14.57 o -8 6 1 1168.25 1209.50 39.95 o -6 6 1 5.91 1.07 8.85 o -4 6 1 1368.30 1395.67 50.51 o -2 6 1 1921.86 2020.90 73.96 o 0 6 1 2978.64 3081.49 105.64 o 2 6 1 1176.18 1175.13 38.86 o 4 6 1 5943.05 5900.28 204.89 o 6 6 1 100.76 66.48 13.21 o 8 6 1 1.50 -2.54 12.49 o 10 6 1 755.37 642.75 42.04 o 12 6 1 1120.59 1075.96 64.32 o 14 6 1 204.62 158.94 28.67 o 16 6 1 100.52 69.40 33.91 o 18 6 1 4.72 57.55 47.06 o 20 6 1 31.13 39.40 43.05 o -19 7 1 1.80 -48.72 48.72 o -17 7 1 447.91 361.18 45.54 o -15 7 1 135.07 116.28 20.69 o -13 7 1 0.00 -6.98 14.66 o -11 7 1 9.14 -5.11 13.67 o -9 7 1 34.80 7.41 15.18 o -7 7 1 30.61 13.02 17.35 o -5 7 1 74.05 77.69 18.27 o -3 7 1 9.96 5.73 11.36 o -1 7 1 585.73 646.04 33.35 o 1 7 1 2913.31 2920.75 132.84 o 3 7 1 1202.85 1202.86 58.71 o 5 7 1 157.57 119.27 18.05 o 7 7 1 486.56 502.04 49.56 o 9 7 1 2327.42 2170.79 113.98 o 11 7 1 109.77 66.55 19.34 o 13 7 1 57.33 61.74 20.73 o 15 7 1 118.27 110.50 21.37 o 17 7 1 0.86 19.40 17.61 o -16 8 1 225.90 168.86 57.30 o -14 8 1 250.21 251.77 121.66 o -12 8 1 216.53 160.03 28.32 o -10 8 1 41.23 52.24 15.57 o -8 8 1 5.89 -9.86 12.78 o -6 8 1 0.59 0.18 14.50 o -4 8 1 345.39 353.76 26.91 o -2 8 1 39.03 42.78 15.88 o 0 8 1 395.75 413.53 28.22 o 2 8 1 313.43 257.11 29.90 o 4 8 1 21.00 7.34 37.23 o 6 8 1 963.24 906.15 68.46 o 8 8 1 264.51 221.47 33.44 o 10 8 1 169.09 135.67 24.48 o 12 8 1 0.01 14.37 17.14 o 14 8 1 361.77 192.39 71.70 o -11 9 1 750.15 702.29 123.74 o -9 9 1 155.19 133.56 36.92 o -7 9 1 481.85 545.90 43.51 o -5 9 1 81.95 51.04 18.85 o -3 9 1 105.42 117.26 23.77 o -1 9 1 367.66 378.43 32.69 o 1 9 1 933.37 985.99 77.53 o 3 9 1 35.03 37.36 27.54 o 5 9 1 4.16 30.52 38.48 o 7 9 1 130.78 142.74 34.04 o -28 0 2 31.39 63.97 26.41 o -26 0 2 222.77 132.72 26.09 o -24 0 2 1593.66 1405.31 100.91 o -22 0 2 1055.81 1056.52 84.19 o -20 0 2 0.89 22.49 11.70 o -18 0 2 7.89 -2.41 8.79 o -16 0 2 7220.90 7995.89 232.52 o -14 0 2 721.27 870.14 36.69 o -12 0 2 21251.90 23195.26 590.88 o -10 0 2 55263.99 54885.87 1508.19 o -8 0 2 1621.63 1312.55 39.40 o -6 0 2 2434.69 1744.98 59.34 o -4 0 2 3597.19 3246.00 174.12 o -2 0 2 6005.01 5206.79 239.90 o 0 0 2 2114.58 2003.73 97.42 o 2 0 2 546.28 394.55 20.45 o 4 0 2 214.13 152.64 11.03 o 6 0 2 1549.63 1644.46 61.36 o 8 0 2 31869.49 33510.49 1173.18 o 10 0 2 3420.85 3402.60 163.10 o 12 0 2 13565.25 15958.97 566.51 o 14 0 2 8377.83 8623.97 326.76 o 16 0 2 760.92 803.50 47.37 o 18 0 2 3406.15 3703.31 234.88 o 20 0 2 2272.95 2141.48 134.85 o 22 0 2 132.25 124.23 22.80 o 24 0 2 996.38 1015.61 103.24 o 26 0 2 945.00 947.60 115.18 o -29 1 2 215.22 138.57 55.64 o -27 1 2 226.30 257.48 24.89 o -25 1 2 83.54 56.14 12.92 o -23 1 2 302.11 294.53 22.18 o -21 1 2 1.12 11.28 8.82 o -19 1 2 1.60 9.06 6.15 o -17 1 2 907.79 986.57 32.48 o -15 1 2 5.37 14.95 4.37 o -13 1 2 6578.55 7445.65 145.82 o -11 1 2 2500.98 2332.15 41.02 o -9 1 2 14950.77 13884.27 291.11 o -7 1 2 5508.38 5122.24 113.94 o -5 1 2 10425.14 9246.34 304.60 o -3 1 2 402.72 298.88 11.47 o -1 1 2 41.70 31.24 6.92 o 1 1 2 57.01 62.47 10.87 o 3 1 2 15407.31 13620.25 339.20 o 5 1 2 12627.71 12045.97 294.43 o 7 1 2 14978.92 13764.96 331.83 o 9 1 2 535.56 589.80 19.21 o 11 1 2 7379.00 8208.23 217.33 o 13 1 2 227.43 267.04 19.92 o 15 1 2 0.25 2.51 13.39 o 17 1 2 328.10 346.23 18.54 o 19 1 2 20.23 27.26 12.96 o 21 1 2 3.40 1.41 13.30 o 23 1 2 504.25 487.29 36.13 o 25 1 2 15.72 35.88 24.06 o 27 1 2 473.77 486.34 58.89 o -28 2 2 109.24 68.37 60.07 o -26 2 2 72.00 84.16 18.24 o -24 2 2 1609.02 1663.20 73.48 o -22 2 2 1391.00 1452.50 63.53 o -20 2 2 231.94 230.37 20.98 o -18 2 2 4654.68 5079.28 138.54 o -16 2 2 2991.25 3136.22 72.31 o -14 2 2 3596.55 3888.77 103.46 o -12 2 2 5930.60 5863.33 122.37 o -10 2 2 293.34 302.83 10.51 o -8 2 2 2958.89 2691.99 65.80 o -6 2 2 74.75 38.33 14.26 o -4 2 2 829.68 1052.30 30.32 o -2 2 2 4949.44 4381.22 128.93 o 0 2 2 1127.57 1086.42 32.06 o 2 2 2 1037.65 1069.23 36.07 o 4 2 2 969.94 945.61 35.40 o 6 2 2 202.29 183.52 11.63 o 8 2 2 1144.08 1060.03 28.27 o 10 2 2 684.96 697.47 21.10 o 12 2 2 2234.98 2194.39 61.31 o 14 2 2 2507.63 2640.31 76.56 o 16 2 2 3410.36 3796.94 103.18 o 18 2 2 2143.39 2364.30 79.69 o 20 2 2 675.41 724.78 37.57 o 22 2 2 105.46 85.82 20.92 o 24 2 2 104.45 106.66 23.13 o 26 2 2 0.64 17.77 34.66 o -29 3 2 699.81 699.80 114.33 o -27 3 2 0.36 -25.74 34.33 o -25 3 2 138.86 112.84 18.65 o -23 3 2 110.08 115.00 16.64 o -21 3 2 610.80 581.53 36.17 o -19 3 2 2710.56 2822.73 92.84 o -17 3 2 135.63 118.92 11.32 o -15 3 2 2592.29 2471.56 76.15 o -13 3 2 1559.92 1603.19 45.86 o -11 3 2 4330.72 4939.16 120.93 o -9 3 2 2504.29 2214.72 73.24 o -7 3 2 5336.53 5461.09 148.24 o -5 3 2 14107.34 13385.67 396.98 o -3 3 2 816.90 777.58 22.58 o -1 3 2 11137.39 10214.40 287.81 o 1 3 2 14811.26 14353.10 474.15 o 3 3 2 1215.78 1243.32 37.46 o 5 3 2 11273.34 11680.95 271.05 o 7 3 2 1561.04 1735.37 59.77 o 9 3 2 134.97 191.43 15.46 o 11 3 2 50.12 63.85 11.75 o 13 3 2 82.30 87.80 13.05 o 15 3 2 2094.54 2144.02 103.17 o 17 3 2 1985.05 2168.81 98.66 o 19 3 2 127.73 120.27 24.39 o 21 3 2 1075.42 1133.40 80.11 o 23 3 2 279.14 270.65 44.29 o 25 3 2 37.44 40.51 50.80 o -28 4 2 48.96 42.91 51.49 o -26 4 2 635.82 618.69 106.02 o -24 4 2 2159.19 2363.73 134.15 o -22 4 2 930.78 1047.21 79.99 o -20 4 2 1051.98 1038.98 97.67 o -18 4 2 525.04 575.22 24.77 o -16 4 2 590.18 563.74 31.31 o -14 4 2 4305.30 4614.32 145.04 o -12 4 2 1435.70 1505.83 47.66 o -10 4 2 1509.11 1618.30 54.17 o -8 4 2 4008.01 3860.21 96.50 o -6 4 2 9397.93 8943.40 233.57 o -4 4 2 895.85 699.71 29.53 o -2 4 2 1154.91 1164.71 32.06 o 0 4 2 605.77 645.37 27.92 o 2 4 2 92.78 76.37 11.76 o 4 4 2 155.71 199.33 20.35 o 6 4 2 3882.43 4128.67 105.99 o 8 4 2 3971.31 3968.61 128.44 o 10 4 2 431.00 431.59 22.77 o 12 4 2 157.16 123.61 16.11 o 14 4 2 172.48 176.28 22.43 o 16 4 2 698.84 786.23 49.94 o 18 4 2 2001.41 2272.14 103.10 o 20 4 2 365.40 351.96 36.34 o 22 4 2 0.06 -18.63 28.48 o 24 4 2 341.55 188.79 66.71 o -25 5 2 8.18 -11.63 48.72 o -23 5 2 178.39 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