#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:20 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180896 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/36/2103663.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103663_Fobs loop_ _publ_author_name 'Low, John N.' 'Moreno S\'anchez, Jose M.' 'Arranz Mascar\'os, Paloma' 'Godino Salido, M. Luz' 'L\'opez Garzon, Rafael' 'Cobo Domingo, Justo' 'Glidewell, Christopher' _publ_section_title ; Hydrated metal complexes of N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl)glycinate: interplay of molecular, molecular--electronic and supramolecular structures ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 317 _journal_page_last 328 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.408 _cell_angle_gamma 90.000 _cell_length_a 7.8114 _cell_length_b 16.4811 _cell_length_c 8.5560 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.6998 _cod_data_source_file na01163sup4.hkl _cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 189' _shelx_refln_list_code 4 _shelx_f_calc_maximum 129.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 211.57 194.07 10.66 o 3 0 0 32.26 45.49 2.19 o 4 0 0 1750.15 1657.61 53.81 o 5 0 0 64.81 86.43 10.35 o 6 0 0 1088.79 1135.47 51.52 o 7 0 0 1.09 2.96 4.78 o 8 0 0 365.29 380.74 42.69 o 9 0 0 202.40 211.81 36.10 o 10 0 0 462.01 437.17 65.00 o 1 1 0 1318.71 1263.89 29.90 o 2 1 0 3827.63 3761.49 78.55 o 3 1 0 43.02 26.88 2.30 o 4 1 0 1383.90 1405.99 29.73 o 5 1 0 3761.29 3819.80 73.68 o 6 1 0 624.04 635.46 22.77 o 7 1 0 144.61 152.66 10.47 o 8 1 0 133.65 122.31 13.65 o 9 1 0 128.74 159.28 23.97 o 10 1 0 224.34 178.64 27.88 o 1 2 0 18.11 21.22 1.06 o 2 2 0 12714.50 11319.31 242.58 o 3 2 0 1.98 9.76 1.19 o 4 2 0 1363.42 1411.31 32.00 o 5 2 0 21.61 13.98 2.54 o 6 2 0 296.93 320.28 10.20 o 7 2 0 117.15 130.16 8.64 o 8 2 0 49.04 52.49 7.18 o 9 2 0 334.63 374.35 31.43 o 10 2 0 190.35 207.81 38.07 o 1 3 0 80.21 99.37 2.70 o 2 3 0 8060.23 7624.58 158.39 o 3 3 0 3346.48 3059.69 64.17 o 4 3 0 2691.46 2618.34 48.16 o 5 3 0 2932.23 3145.98 71.51 o 6 3 0 1049.75 1096.46 26.41 o 7 3 0 99.94 93.78 7.37 o 8 3 0 1992.47 2192.47 150.92 o 9 3 0 173.00 179.68 23.03 o 10 3 0 46.68 38.01 17.68 o 0 4 0 6356.58 5577.14 290.51 o 1 4 0 1722.85 1649.90 32.56 o 2 4 0 428.83 484.13 10.23 o 3 4 0 2580.72 2408.40 50.91 o 4 4 0 1375.80 1419.62 29.68 o 5 4 0 365.25 327.05 10.17 o 6 4 0 42.94 44.38 5.64 o 7 4 0 21.85 22.40 4.73 o 8 4 0 21.46 19.62 9.05 o 9 4 0 326.65 353.87 37.41 o 10 4 0 29.64 24.27 8.80 o 1 5 0 3031.78 2884.22 62.96 o 2 5 0 71.58 66.36 2.94 o 3 5 0 84.08 130.00 4.31 o 4 5 0 1058.95 1095.94 24.12 o 5 5 0 557.34 582.29 15.73 o 6 5 0 840.83 839.53 27.88 o 7 5 0 0.41 -0.67 4.43 o 8 5 0 341.39 332.17 28.00 o 9 5 0 139.33 129.90 16.55 o 0 6 0 9864.98 8709.43 379.88 o 1 6 0 11245.29 10608.09 200.18 o 2 6 0 909.19 863.42 18.07 o 3 6 0 4228.61 4266.56 105.31 o 4 6 0 121.49 101.20 4.72 o 5 6 0 1045.46 1103.08 31.23 o 6 6 0 139.14 123.22 6.09 o 7 6 0 82.01 78.08 6.65 o 8 6 0 94.51 95.97 10.87 o 9 6 0 16.41 21.17 10.89 o 1 7 0 1703.40 1695.17 43.97 o 2 7 0 115.35 117.64 4.17 o 3 7 0 575.28 598.78 14.16 o 4 7 0 120.82 104.71 4.96 o 5 7 0 287.90 266.89 9.17 o 6 7 0 422.81 421.33 16.55 o 7 7 0 1093.89 1070.22 47.37 o 8 7 0 471.06 493.38 41.34 o 9 7 0 104.02 94.76 22.70 o 0 8 0 120.01 106.43 9.76 o 1 8 0 141.40 125.99 4.73 o 2 8 0 376.32 356.14 8.72 o 3 8 0 2886.37 3099.43 61.97 o 4 8 0 6.24 8.86 3.57 o 5 8 0 105.92 109.47 8.97 o 6 8 0 266.89 244.06 10.82 o 7 8 0 453.13 467.33 21.82 o 8 8 0 44.73 61.85 28.19 o 9 8 0 19.81 12.95 11.67 o 1 9 0 450.47 466.76 10.75 o 2 9 0 1040.44 971.91 21.51 o 3 9 0 1513.79 1646.02 41.58 o 4 9 0 357.38 322.61 11.52 o 5 9 0 3685.27 4017.35 139.25 o 6 9 0 107.01 103.78 7.31 o 7 9 0 279.88 267.26 18.08 o 8 9 0 474.66 574.92 50.86 o 9 9 0 192.66 195.98 36.84 o 0 10 0 1.52 6.86 3.61 o 1 10 0 1418.56 1418.81 30.47 o 2 10 0 453.20 442.24 11.32 o 3 10 0 43.37 33.36 2.97 o 4 10 0 1177.61 1210.02 32.11 o 5 10 0 1388.59 1430.80 50.28 o 6 10 0 224.74 201.54 11.20 o 7 10 0 105.29 95.43 9.57 o 8 10 0 10.07 -1.97 11.89 o 9 10 0 13.41 22.36 15.09 o 1 11 0 1129.63 1186.79 30.22 o 2 11 0 838.50 827.10 20.46 o 3 11 0 461.35 449.54 13.95 o 4 11 0 100.04 87.74 6.64 o 5 11 0 37.07 23.32 4.33 o 6 11 0 188.60 162.88 15.41 o 7 11 0 492.12 488.36 42.11 o 8 11 0 93.47 94.77 15.53 o 9 11 0 346.84 335.15 62.47 o 0 12 0 1120.59 1089.19 34.14 o 1 12 0 494.74 488.34 20.83 o 2 12 0 1228.67 1324.42 36.09 o 3 12 0 3847.64 4020.12 112.14 o 4 12 0 128.38 129.85 7.43 o 5 12 0 172.67 179.70 11.28 o 6 12 0 50.66 59.11 8.75 o 7 12 0 157.07 187.87 19.29 o 8 12 0 8.55 9.96 8.26 o 1 13 0 7.81 3.83 3.32 o 2 13 0 14.02 9.29 3.54 o 3 13 0 28.82 26.22 3.98 o 4 13 0 650.49 673.60 24.29 o 5 13 0 182.13 187.05 11.87 o 6 13 0 91.84 83.39 11.15 o 7 13 0 446.72 453.62 48.53 o 8 13 0 104.26 110.46 24.34 o 0 14 0 310.04 307.24 15.30 o 1 14 0 436.32 443.31 16.65 o 2 14 0 207.27 214.17 9.61 o 3 14 0 297.90 279.39 20.54 o 4 14 0 41.35 41.38 6.68 o 5 14 0 1.65 2.87 6.74 o 6 14 0 42.55 58.68 11.84 o 7 14 0 0.01 -10.09 10.09 o 8 14 0 1.79 34.19 16.45 o 1 15 0 79.80 87.56 6.45 o 2 15 0 143.01 143.59 7.97 o 3 15 0 351.41 366.07 15.56 o 4 15 0 233.85 254.55 15.74 o 5 15 0 872.43 984.68 67.93 o 6 15 0 317.34 326.95 32.47 o 7 15 0 113.18 58.43 29.33 o 0 16 0 564.85 566.90 32.68 o 1 16 0 59.94 53.82 7.57 o 2 16 0 320.66 314.62 14.59 o 3 16 0 6.33 6.32 7.53 o 4 16 0 228.42 215.08 15.62 o 5 16 0 59.36 57.64 12.41 o 6 16 0 75.95 83.37 12.07 o 7 16 0 0.02 0.68 15.77 o 1 17 0 2.82 3.04 5.81 o 2 17 0 74.91 85.20 8.80 o 3 17 0 85.29 102.84 9.81 o 4 17 0 22.08 7.95 7.74 o 5 17 0 0.49 -6.76 7.90 o 6 17 0 36.59 21.68 9.44 o 0 18 0 94.97 114.53 18.85 o 1 18 0 296.49 306.89 21.93 o 2 18 0 552.01 556.75 37.14 o 3 18 0 88.85 106.92 14.55 o 4 18 0 2.54 4.55 8.93 o 5 18 0 12.65 6.12 10.13 o 6 18 0 38.47 37.52 22.36 o 1 19 0 101.73 147.27 18.61 o 2 19 0 0.02 -1.36 12.14 o 3 19 0 8.23 1.58 7.94 o 4 19 0 415.76 446.91 58.59 o 5 19 0 2.03 12.57 14.54 o 0 20 0 26.85 48.42 15.46 o 1 20 0 197.14 218.28 23.04 o 2 20 0 45.07 34.11 12.66 o 3 20 0 10.55 6.31 11.41 o 4 20 0 4.64 -9.30 16.63 o 1 21 0 42.51 45.63 12.03 o 2 21 0 191.43 251.23 41.55 o 3 21 0 13.37 10.72 16.70 o 0 22 0 19.04 47.01 20.15 o 1 22 0 220.99 246.13 35.67 o -10 1 1 20.50 18.02 12.50 o -9 1 1 21.83 19.48 8.11 o -8 1 1 79.80 61.17 10.49 o -7 1 1 0.97 -1.79 3.75 o -6 1 1 500.61 454.05 12.88 o -5 1 1 615.49 656.13 14.72 o -4 1 1 374.88 386.86 9.81 o -3 1 1 0.11 -0.49 0.92 o -2 1 1 12701.55 10969.21 301.14 o -1 1 1 124.32 110.01 2.64 o 1 1 1 0.10 6.41 4.68 o 2 1 1 301.53 251.69 7.11 o 3 1 1 0.74 0.53 2.00 o 4 1 1 526.44 559.17 13.60 o 5 1 1 236.43 252.40 8.73 o 6 1 1 904.69 978.18 34.49 o 7 1 1 7.03 11.95 4.67 o 8 1 1 36.44 16.13 7.58 o 9 1 1 9.12 15.77 14.42 o -10 2 1 209.10 173.90 24.35 o -9 2 1 2.09 4.02 7.24 o -8 2 1 28.99 19.86 10.10 o -7 2 1 47.95 34.77 3.02 o -6 2 1 269.52 260.44 8.70 o -5 2 1 0.69 1.97 2.36 o -4 2 1 592.83 589.12 13.76 o -3 2 1 457.90 484.57 10.39 o -2 2 1 12172.62 11314.02 224.83 o -1 2 1 608.85 524.58 11.27 o 0 2 1 159.01 136.71 3.27 o 1 2 1 198.49 178.55 4.74 o 2 2 1 1551.31 1444.93 33.75 o 3 2 1 284.78 306.54 7.90 o 4 2 1 1344.58 1315.08 27.56 o 5 2 1 245.96 275.54 9.18 o 6 2 1 3.96 3.01 3.00 o 7 2 1 29.38 23.35 4.99 o 8 2 1 19.30 15.13 10.50 o 9 2 1 2.41 -8.87 9.70 o -10 3 1 6.91 13.12 10.19 o -9 3 1 191.11 190.04 25.72 o -8 3 1 11.69 9.70 7.54 o -7 3 1 31.56 29.88 3.72 o -6 3 1 42.99 49.76 4.67 o -5 3 1 7.49 10.50 3.07 o -4 3 1 2712.29 2683.64 47.41 o -3 3 1 1992.46 2138.77 38.28 o -2 3 1 5600.98 5356.63 118.59 o -1 3 1 153.33 110.78 3.03 o 0 3 1 3283.52 3032.03 64.70 o 1 3 1 178.50 197.75 5.01 o 2 3 1 193.89 196.19 5.17 o 3 3 1 827.03 876.86 18.32 o 4 3 1 516.20 576.52 12.83 o 5 3 1 39.08 31.60 3.55 o 6 3 1 96.00 93.33 7.03 o 7 3 1 4.07 -4.18 4.18 o 8 3 1 4.78 -1.79 6.85 o 9 3 1 136.77 133.59 17.77 o -10 4 1 118.40 87.15 28.86 o -9 4 1 599.11 653.93 60.59 o -8 4 1 220.54 219.79 13.57 o -7 4 1 100.90 79.53 5.42 o -6 4 1 8.91 14.08 3.26 o -5 4 1 1153.76 1221.64 28.36 o -4 4 1 862.83 922.82 19.30 o -3 4 1 1337.09 1346.13 28.63 o -2 4 1 16656.71 15326.86 300.13 o -1 4 1 2846.00 2711.15 54.72 o 0 4 1 76.09 78.09 2.51 o 1 4 1 1273.85 1317.09 28.29 o 2 4 1 1667.12 1759.62 35.70 o 3 4 1 2543.23 2566.28 54.44 o 4 4 1 734.10 793.83 17.87 o 5 4 1 462.83 456.75 11.54 o 6 4 1 99.19 93.62 6.00 o 7 4 1 6.89 5.94 4.46 o 8 4 1 168.86 165.63 16.05 o 9 4 1 1.36 -3.38 8.32 o -10 5 1 33.87 7.89 14.42 o -9 5 1 234.41 226.83 22.51 o -8 5 1 48.77 44.87 5.13 o -7 5 1 6.49 8.98 4.21 o -6 5 1 19.50 17.49 2.77 o -5 5 1 21.98 22.89 2.57 o -4 5 1 3792.45 3793.80 73.48 o -3 5 1 0.29 0.66 1.72 o -2 5 1 250.33 234.46 6.35 o -1 5 1 1153.37 1074.94 21.61 o 0 5 1 5381.06 5393.06 109.46 o 1 5 1 184.68 180.39 5.85 o 2 5 1 492.46 494.75 13.13 o 3 5 1 962.98 951.63 19.91 o 4 5 1 93.73 109.00 4.61 o 5 5 1 325.83 334.48 10.68 o 6 5 1 363.28 346.29 15.26 o 7 5 1 3.27 3.68 5.81 o 8 5 1 3.11 7.52 8.13 o 9 5 1 192.00 215.65 20.15 o -10 6 1 12.53 1.97 16.39 o -9 6 1 134.89 126.48 16.50 o -8 6 1 2.20 -4.55 8.09 o -7 6 1 113.26 120.04 9.34 o -6 6 1 96.12 90.94 6.35 o -5 6 1 3.78 8.46 2.59 o -4 6 1 1434.90 1515.43 34.97 o -3 6 1 2.88 8.00 2.17 o -2 6 1 812.51 846.46 19.11 o -1 6 1 162.51 164.01 4.82 o 0 6 1 1148.67 1082.57 26.46 o 1 6 1 64.46 70.98 3.84 o 2 6 1 972.59 1106.65 21.99 o 3 6 1 18.44 18.55 4.15 o 4 6 1 15.65 16.97 2.64 o 5 6 1 855.76 888.50 28.57 o 6 6 1 426.30 434.08 17.76 o 7 6 1 32.15 25.55 5.72 o 8 6 1 161.55 152.75 17.57 o 9 6 1 3.46 8.31 9.96 o -10 7 1 25.57 26.92 15.09 o -9 7 1 39.41 16.99 14.14 o -8 7 1 16.79 29.87 8.99 o -7 7 1 1771.48 1926.06 69.76 o -6 7 1 22.23 23.35 3.54 o -5 7 1 1897.53 2048.03 49.83 o -4 7 1 564.67 554.17 14.50 o -3 7 1 41.60 36.38 2.60 o -2 7 1 299.22 329.89 11.48 o -1 7 1 5565.48 5946.07 124.90 o 0 7 1 360.20 353.95 9.01 o 1 7 1 1435.96 1384.63 27.98 o 2 7 1 180.04 150.60 6.95 o 3 7 1 706.79 709.01 16.17 o 4 7 1 26.17 30.29 3.20 o 5 7 1 558.42 611.21 21.62 o 6 7 1 221.49 225.37 8.03 o 7 7 1 18.59 16.02 6.67 o 8 7 1 21.09 11.21 12.85 o 9 7 1 127.36 98.67 16.87 o -9 8 1 37.46 34.79 10.56 o -8 8 1 15.81 8.56 12.78 o -7 8 1 1818.68 2046.88 98.63 o -6 8 1 256.36 269.94 12.11 o -5 8 1 386.45 398.87 13.93 o -4 8 1 18.81 12.54 2.77 o -3 8 1 37.56 39.61 3.04 o -2 8 1 66.65 62.51 5.22 o -1 8 1 69.71 75.09 3.32 o 0 8 1 263.56 273.83 13.56 o 1 8 1 5.67 1.58 1.97 o 2 8 1 244.80 246.01 8.29 o 3 8 1 33.33 31.65 3.17 o 4 8 1 42.83 40.45 3.81 o 5 8 1 286.70 276.10 11.29 o 6 8 1 32.53 21.41 4.74 o 7 8 1 10.31 19.20 4.60 o 8 8 1 0.15 1.69 9.07 o 9 8 1 98.18 89.39 23.04 o -9 9 1 38.20 27.13 23.66 o -8 9 1 80.00 79.24 13.39 o -7 9 1 3.86 9.26 4.22 o -6 9 1 61.72 56.36 4.77 o -5 9 1 1159.39 1199.07 40.88 o -4 9 1 114.92 102.92 5.07 o -3 9 1 171.83 211.86 6.80 o -2 9 1 1137.78 1184.98 38.57 o -1 9 1 560.13 574.46 21.49 o 0 9 1 450.34 479.81 12.98 o 1 9 1 142.45 178.72 7.39 o 2 9 1 629.18 638.64 14.54 o 3 9 1 16.64 16.67 3.24 o 4 9 1 441.49 444.52 13.13 o 5 9 1 29.19 31.39 4.36 o 6 9 1 754.33 745.23 32.18 o 7 9 1 0.19 5.25 11.86 o 8 9 1 50.12 59.51 11.83 o 9 9 1 0.09 9.18 14.48 o -9 10 1 47.06 36.84 16.45 o -8 10 1 23.64 30.59 8.84 o -7 10 1 0.10 3.32 4.12 o -6 10 1 68.80 58.67 5.34 o -5 10 1 356.25 337.20 14.23 o -4 10 1 63.16 63.05 4.68 o -3 10 1 1235.70 1246.73 30.84 o -2 10 1 360.24 353.01 11.85 o -1 10 1 98.14 82.75 3.70 o 0 10 1 897.78 823.41 17.58 o 1 10 1 3333.84 3544.91 82.00 o 2 10 1 459.42 418.98 10.48 o 3 10 1 795.22 839.19 26.84 o 4 10 1 55.58 62.83 5.42 o 5 10 1 105.56 113.57 7.51 o 6 10 1 11.76 11.62 5.61 o 7 10 1 225.60 219.38 21.90 o 8 10 1 238.78 243.54 38.94 o -9 11 1 141.59 139.54 30.93 o -8 11 1 171.42 165.90 19.79 o -7 11 1 55.80 40.41 5.98 o -6 11 1 20.28 16.02 5.63 o -5 11 1 107.92 110.28 7.59 o -4 11 1 0.64 5.78 3.22 o -3 11 1 240.69 242.51 9.62 o -2 11 1 299.67 279.88 10.38 o -1 11 1 151.69 153.41 12.90 o 0 11 1 3.60 5.10 2.68 o 1 11 1 1492.97 1650.22 36.82 o 2 11 1 370.45 375.22 11.58 o 3 11 1 1571.78 1655.56 50.79 o 4 11 1 387.12 442.69 17.46 o 5 11 1 125.32 107.76 7.70 o 6 11 1 624.48 642.67 42.09 o 7 11 1 91.22 66.22 11.63 o 8 11 1 85.29 102.47 24.80 o -9 12 1 11.49 10.54 13.18 o -8 12 1 92.19 87.10 28.46 o -7 12 1 29.04 24.08 5.94 o -6 12 1 28.91 18.31 5.67 o -5 12 1 131.47 131.26 8.46 o -4 12 1 546.81 556.35 20.91 o -3 12 1 431.67 483.89 25.46 o -2 12 1 175.99 169.75 6.86 o -1 12 1 57.48 49.08 3.68 o 0 12 1 621.82 615.35 15.99 o 1 12 1 836.01 890.99 29.91 o 2 12 1 183.77 176.05 9.23 o 3 12 1 410.58 376.38 14.34 o 4 12 1 201.25 201.61 9.60 o 5 12 1 7.78 16.64 4.54 o 6 12 1 68.54 58.15 16.17 o 7 12 1 56.07 75.78 18.48 o 8 12 1 13.75 5.24 13.12 o -8 13 1 306.75 362.57 42.26 o -7 13 1 199.21 217.60 21.05 o -6 13 1 33.13 40.26 6.36 o -5 13 1 779.13 781.15 38.46 o -4 13 1 216.83 186.17 10.03 o -3 13 1 32.07 34.29 4.76 o -2 13 1 375.07 375.12 14.45 o -1 13 1 0.03 -2.73 2.98 o 0 13 1 329.47 330.33 11.51 o 1 13 1 77.34 74.07 5.39 o 2 13 1 643.59 689.58 27.87 o 3 13 1 1126.39 1119.86 34.06 o 4 13 1 0.26 5.54 4.47 o 5 13 1 140.65 137.07 12.40 o 6 13 1 401.21 458.86 40.00 o 7 13 1 2.30 10.73 10.87 o 8 13 1 211.11 170.78 28.96 o -8 14 1 68.21 73.75 21.07 o -7 14 1 377.91 422.88 38.57 o -6 14 1 65.10 30.21 11.74 o -5 14 1 29.85 19.26 6.76 o -4 14 1 550.65 537.51 21.84 o -3 14 1 108.52 140.29 7.76 o -2 14 1 368.45 361.89 13.72 o -1 14 1 108.39 91.77 6.01 o 0 14 1 153.02 134.11 7.43 o 1 14 1 90.46 82.38 5.38 o 2 14 1 910.70 932.43 31.94 o 3 14 1 132.28 109.23 10.31 o 4 14 1 24.12 20.96 5.03 o 5 14 1 13.81 24.28 8.16 o 6 14 1 54.83 54.08 17.62 o 7 14 1 58.67 59.24 15.34 o -8 15 1 225.29 213.90 40.17 o -7 15 1 54.94 35.61 12.17 o -6 15 1 93.71 102.33 12.92 o -5 15 1 2.83 3.80 6.47 o -4 15 1 759.83 806.32 43.52 o -3 15 1 27.90 35.95 7.40 o -2 15 1 1.02 -4.12 4.12 o -1 15 1 244.27 257.43 11.09 o 0 15 1 82.56 82.24 6.22 o 1 15 1 2664.48 2727.75 100.10 o 2 15 1 225.97 228.03 12.27 o 3 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